CN114354440A - Device for detecting gasification characteristics of precursor material and using method - Google Patents
Device for detecting gasification characteristics of precursor material and using method Download PDFInfo
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- CN114354440A CN114354440A CN202111432432.6A CN202111432432A CN114354440A CN 114354440 A CN114354440 A CN 114354440A CN 202111432432 A CN202111432432 A CN 202111432432A CN 114354440 A CN114354440 A CN 114354440A
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- 239000000463 material Substances 0.000 title claims abstract description 74
- 238000002309 gasification Methods 0.000 title claims abstract description 23
- 239000002243 precursor Substances 0.000 title claims abstract description 21
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000006243 chemical reaction Methods 0.000 claims abstract description 90
- 239000002184 metal Substances 0.000 claims abstract description 28
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 230000005540 biological transmission Effects 0.000 claims description 29
- 230000007246 mechanism Effects 0.000 claims description 24
- 238000003756 stirring Methods 0.000 claims description 18
- 244000309464 bull Species 0.000 claims description 12
- 239000002904 solvent Substances 0.000 claims description 12
- 239000000126 substance Substances 0.000 claims description 9
- 239000000178 monomer Substances 0.000 claims description 8
- 239000002994 raw material Substances 0.000 claims description 8
- 238000009834 vaporization Methods 0.000 claims description 7
- 230000008016 vaporization Effects 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 6
- 235000013619 trace mineral Nutrition 0.000 claims description 5
- 239000011573 trace mineral Substances 0.000 claims description 5
- 241000883990 Flabellum Species 0.000 claims description 4
- 230000009471 action Effects 0.000 claims description 4
- 238000006460 hydrolysis reaction Methods 0.000 claims description 4
- 230000000379 polymerizing effect Effects 0.000 claims description 4
- 230000002794 monomerizing effect Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 description 9
- 239000003814 drug Substances 0.000 description 7
- 230000008859 change Effects 0.000 description 5
- 229910010272 inorganic material Inorganic materials 0.000 description 4
- 238000003980 solgel method Methods 0.000 description 3
- 238000001514 detection method Methods 0.000 description 2
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Abstract
The invention relates to the technical field of reaction kettles, in particular to a device for detecting the gasification characteristics of precursor materials and a using method thereof, wherein the device comprises a reaction kettle body, a reaction chamber is arranged in the reaction kettle body, a material guide pipe for feeding materials into the reaction chamber is fixedly arranged on the side wall of the reaction kettle body, a material discharge pipe is fixedly arranged on the side wall of the reaction kettle body, control valves are arranged in the material guide pipe and the material discharge pipe, and S1 is used for feeding materials; s2, blending; s3, gasifying; and S4, collecting. According to the invention, the rotating shaft in the reaction chamber is driven by the motor to rotate, so that materials in the reaction chamber are stirred, the mixing degree of the materials in the reaction chamber is further improved, the plurality of metal plates are driven to rotate, the metal plates are enabled to rapidly heat, then the materials in the reaction chamber are heated, the gasification of the materials in the reaction chamber is accelerated, and the efficiency of gas escape is improved.
Description
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a device for detecting gasification characteristics of a precursor material and a using method thereof.
Background
The precursor exists in a form before the target product is obtained, mostly exists in an organic-inorganic complex or mixture solid, and also exists in a sol form in part. The precursor is often used in the material preparation methods such as sol-gel method and coprecipitation method, but is not an exact scientific term and has no specific concept. It is also defined as a prototype sample of the target product, i.e., a pre-product from which the target product is obtained after some steps.
The sol-gel method is an important method for synthesizing inorganic compounds or inorganic materials at low temperature or under mild conditions, plays an important role in soft chemical synthesis, and is applied to the aspects of preparing glass, ceramics, films, fibers, composite materials and the like.
When the sol-gel method is adopted to synthesize inorganic compounds or inorganic materials, the gasification characteristics of precursor materials sometimes need to be detected, but when the existing detection equipment works, the reaction time is usually one to two days or even longer, the gas escape efficiency is lower, and further the detection of the gasification characteristics of the precursor materials is inconvenient.
Therefore, the device for detecting the vaporization characteristic of the precursor material and the use method thereof are provided.
Disclosure of Invention
The invention aims to provide a device for detecting the gasification characteristics of a precursor material and a using method thereof.
In order to achieve the purpose, the invention provides the following technical scheme:
the utility model provides a device and application method for detecting precursor material gasification characteristic, includes the reation kettle body, the inside of reation kettle body has seted up the reacting chamber, the lateral wall fixed mounting of reation kettle body has the passage that is used for to the inside input material of reacting chamber, the lateral wall fixed mounting of reation kettle body has row material pipe, the inside of passage and row material pipe all is equipped with the control valve, the bottom of reation kettle body is equipped with and is used for accelerating the inside gaseous actuating mechanism who escapes of material, the bottom of reation chamber is equipped with and is used for further accelerating the heating mechanism of gaseous escape with actuating mechanism complex, rectangular cavity and circle chamber have still been seted up to the inside of reation kettle body, the inside in rectangular cavity and circle chamber is equipped with and is used for carrying out the slewing mechanism who collects gas with actuating mechanism complex.
Preferably, actuating mechanism includes the motor of fixed mounting in reation kettle body bottom, the output fixed mounting of motor has the pivot, the bar-shaped chamber has been seted up to the bottom of reation kettle body, the upper end of pivot runs through the bar-shaped chamber and extends to the bottom of reacting chamber, the upper end of pivot has the puddler that is used for carrying out the stirring to the material in the inside fixed mounting of reacting chamber.
After the motor starts, can drive the inside pivot of reacting chamber and rotate, the pivot will drive the puddler afterwards and rotate, then stirs the inside material of reacting chamber, and then improves the degree of mixing between the inside material of reacting chamber.
Preferably, heating mechanism includes equidistant fixed mounting at the inside a plurality of metal sheets of puddler, the equidistant fixed mounting in bottom of reation kettle body has a plurality of and metal sheet complex magnet.
After the motor starts, can drive a plurality of metal sheets through the puddler and rotate, because equidistant fixed mounting has a plurality of magnets in the bottom of reation kettle body, consequently to each independent metal sheet, pass its inside magnetic field intensity and constantly change throughout, and then produce the vortex in the inside of metal sheet for the metal sheet generates heat fast, then heats the inside material of reacting chamber, accelerates the gasification of the inside material of reacting chamber, thereby improves the efficiency of gas escape.
Preferably, the rotating mechanism comprises a device cavity arranged inside the reaction kettle body, the rectangular cavity and the strip-shaped cavity are jointly rotated to install a rotating rod, the rotating rod is connected with the rotating shaft through transmission of a transmission belt, the outer edge of the rotating rod is fixedly arranged inside the rectangular cavity and provided with a driving wheel, the rectangular cavity and the round cavity are jointly rotated to install a transmission rod, the outer edge of the transmission rod is fixedly arranged inside the rectangular cavity and provided with a driven wheel, the reaction kettle body is further internally provided with the device cavity, the inner bottom of the device cavity is fixedly provided with a cylinder, the output end of the cylinder is fixedly provided with a guide rod, the upper end of the guide rod extends to the inside of the rectangular cavity and is fixedly provided with a connecting plate inside the rectangular cavity, the upper end of the connecting plate is rotatably provided with a fixed rod, the upper end of the fixed rod is fixedly provided with a transmission gear, and the driving wheel and the driven wheel are jointly meshed with the transmission gear, the utility model discloses a reaction kettle, including transfer line, fixed mounting, intake pipe, collecting device, transfer line, the upper end of transfer line extends to the inside in circle chamber and fixed mounting has the flabellum, the bottom in circle chamber is linked together through the inside of intake pipe with the reacting chamber, the outside fixed mounting of reation kettle body has the collecting pipe, the one end of collecting pipe and being linked together in circle chamber, the other end of collecting pipe is connected with collecting device.
After the motor starts, can drive the bull stick through the inside drive belt in strip chamber and rotate, the bull stick will drive the action wheel rotation of rectangle intracavity portion afterwards, and then drive through drive gear and rotate from driving wheel and transfer line, then the transfer line will drive the flabellum rotation of circle intracavity portion, and then pass through the inside of intake pipe suction circle chamber with the inside gas of reacting chamber, then send into the inside of collecting device through the collecting pipe, then detect it again, can also drive the drive gear removal of rectangle intracavity portion through the cylinder, and then change the drive ratio between bull stick and the transfer line, thereby accomplish the regulation to gas collection speed.
Preferably, the upper end fixed mounting of reation kettle body has the charge door, equidistant fixed mounting has a plurality of pipes, a plurality of at the interior top of reacting chamber the upper end of pipe all is linked together with the charge door, every the equal fixed mounting in inside of pipe has the check valve.
Preferably, the outside of reation kettle body is equipped with the controller, motor and cylinder all with controller electric connection.
The invention also provides a using method of the device for detecting the gasification characteristics of the precursor material, which is characterized by comprising the following steps: the method comprises the following steps:
s1, feeding: firstly, putting a solvent required by a reaction into the reaction chamber through a material guide pipe, putting raw materials into the reaction chamber to disperse the raw materials in the solvent, then performing hydrolysis reaction to generate an active monomer, and polymerizing the active monomer to form sol;
s2, admixture: adding the liquid medicine containing the trace elements required by the reaction into the feeding port, so that the liquid medicine is uniformly dropped into the reaction chamber through a plurality of guide pipes, the liquid medicine and the solution formed in the solvent can obtain the uniformity of the molecular level in a short time, and then the liquid medicine and the solution are uniformly mixed on the molecular level when the gel is formed;
s3, gasification: the motor is started through the controller, the motor drives the stirring rod inside the reaction chamber to rotate, so that the mixing degree of materials inside the reaction chamber is improved, and meanwhile, the metal plate inside the stirring rod can generate heat, so that the gasification of the materials inside the reaction chamber is accelerated;
s4, collecting: after the motor starts, can drive the transfer line and rotate, and then inside the inside gas that drives the reacting chamber passes through the collecting pipe and gets into collection equipment to accomplish gaseous collection, can also start the cylinder through the controller, and then drive gear and remove in the inside in rectangular cavity, and then change the drive ratio between bull stick and the transfer line, thereby accomplish the regulation to gas collection rate.
Preferably, the time of step S1 is at least 24 h.
Compared with the prior art, the invention has the beneficial effects that:
1. after the motor starts, can drive the inside pivot of reacting chamber and rotate, the pivot will drive the puddler afterwards and rotate, then stirs the inside material of reacting chamber, and then improves the degree of mixing between the inside material of reacting chamber.
2. After the motor starts, can drive a plurality of metal sheets and rotate, and then produce the vortex in the inside of metal sheet for the metal sheet generates heat fast, then heats the inside material of reacting chamber, accelerates the gasification of the inside material of reacting chamber, thereby improves gaseous effluence's efficiency.
3. After the motor starts, can drive the bull stick and rotate and then pass through the inside of intake pipe suction circle chamber with the inside gas of reacting chamber, then send into the inside of collecting device through the collecting pipe, then detect it again, can also drive the drive gear removal of rectangle intracavity portion through the cylinder, and then change the drive ratio between bull stick and the transfer line to the completion is to the regulation of gas collection rate.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic view of a magnet according to the present invention;
FIG. 4 is a top view of the internal structure of the reaction chamber of the present invention;
fig. 5 is an enlarged view of the structure at a in fig. 2.
In the figure: the device comprises a reaction kettle body 1, a reaction chamber 2, a material guide pipe 3, a motor 4, a strip-shaped cavity 5, a rotating shaft 6, a rotating rod 7, a transmission belt 8, a stirring rod 9, a metal plate 10, a magnet 11, a rectangular cavity 12, a driving wheel 13, a driven wheel 14, a transmission rod 15, a transmission gear 16, a guide rod 17, a connecting plate 18, a device cavity 19, an air cylinder 20, a circular cavity 21, fan blades 22, an air inlet pipe 23, a collecting pipe 24, a charging opening 25, a guide pipe 26 and a discharging pipe 27.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "length", "width", "thickness", "upper", "lower", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", "clockwise", "counterclockwise", and the like, indicate orientations and positional relationships based on those shown in the drawings, and are used only for convenience of description and simplicity of description, and do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be considered as limiting the present invention.
Furthermore, the terms "first", "second" and "first" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, features defined as "first", "second", may explicitly or implicitly include one or more of the described features. In the description of the present invention, "a plurality" means two or more unless specifically defined otherwise. Furthermore, the terms "mounted," "connected," and "connected" are to be construed broadly and may, for example, be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1 to 5, the present invention provides a device for detecting a gasification characteristic of a precursor material, including a reaction kettle body 1, a reaction chamber 2 is disposed inside the reaction kettle body 1, a material guide pipe 3 for feeding a material into the reaction chamber 2 is fixedly mounted on a side wall of the reaction kettle body 1, a material discharge pipe 27 is fixedly mounted on the side wall of the reaction kettle body 1, control valves are disposed inside the material guide pipe 3 and the material discharge pipe 27, a driving mechanism for accelerating an escape of a gas inside the material is disposed at a bottom of the reaction kettle body 1, a heating mechanism for further accelerating an escape of the gas is disposed at a bottom of the reaction chamber 2 and matched with the driving mechanism, a rectangular cavity 12 and a circular cavity 21 are further disposed inside the reaction kettle body 1, and a rotating mechanism for collecting the gas and matched with the driving mechanism is disposed inside the rectangular cavity 12 and the circular cavity 21.
Referring to fig. 2, the driving mechanism includes a motor 4 fixedly installed at the bottom of the reaction kettle body 1, an output end of the motor 4 is fixedly installed with a rotating shaft 6, the bottom of the reaction kettle body 1 is provided with a strip-shaped cavity 5, an upper end of the rotating shaft 6 penetrates through the strip-shaped cavity 5 and extends to the bottom of the reaction chamber 2, and an upper end of the rotating shaft 6 is fixedly installed in the reaction chamber 2 with a stirring rod 9 for stirring the material.
After motor 4 starts, can drive 2 inside pivots 6 rotations of reacting chamber, pivot 6 will drive the puddler 9 rotation afterwards, then stirs 2 inside materials of reacting chamber, and then improves the degree of mixing between 2 inside materials of reacting chamber.
Referring to fig. 2 to 4, as an embodiment of the present invention, the heating mechanism includes a plurality of metal plates 10 fixedly installed at equal intervals inside the stirring rod 9, and a plurality of magnets 11 engaged with the metal plates 10 are fixedly installed at equal intervals at the bottom of the reaction vessel body 1.
After motor 4 starts, can drive a plurality of metal sheets 10 through puddler 9 and rotate, because the equidistant fixed mounting in bottom of reation kettle body 1 has a plurality of magnet 11, consequently to each independent metal sheet 10, it is constantly changing to pass its inside magnetic field intensity, and then produce the vortex in metal sheet 10's inside, make metal sheet 10 generate heat fast, then heat 2 inside materials in the reacting chamber, accelerate the gasification of 2 inside materials in the reacting chamber, thereby improve gaseous escaped efficiency.
As an embodiment of the invention, referring to fig. 2 and 5, the rotating mechanism includes a device cavity 19 opened inside the reaction kettle body 1, a rotating rod 7 is rotatably installed inside the rectangular cavity 12 and the strip-shaped cavity 5, the rotating rod 7 is in transmission connection with the rotating shaft 6 through a transmission belt 8, a driving wheel 13 is fixedly installed inside the rectangular cavity 12 at the outer edge of the rotating rod 7, a transmission rod 15 is rotatably installed between the rectangular cavity 12 and the circular cavity 21, a driven wheel 14 is fixedly installed inside the rectangular cavity 12 at the outer edge of the transmission rod 15, the reaction kettle body 1 is further internally provided with the device cavity 19, an air cylinder 20 is fixedly installed at the inner bottom of the device cavity 19, a guide rod 17 is fixedly installed at the output end of the air cylinder 20, the upper end of the guide rod 17 extends into the rectangular cavity 12 and is fixedly installed inside the rectangular cavity 12 with a connecting plate 18, the upper end of the connecting plate 18 is rotatably installed with a fixing rod, the upper end of the fixed rod is fixedly provided with a transmission gear 16, the driving wheel 13 and the driven wheel 14 are jointly meshed with the transmission gear 16, the upper end of the transmission rod 15 extends to the inside of the circular cavity 21 and is fixedly provided with fan blades 22, the bottom of the circular cavity 21 is communicated with the inside of the reaction chamber 2 through an air inlet pipe 23, the outside of the reaction kettle body 1 is fixedly provided with a collecting pipe 24, one end of the collecting pipe 24 is communicated with the circular cavity 21, and the other end of the collecting pipe 24 is connected with collecting equipment.
After motor 4 starts, can drive bull stick 7 through the inside drive belt 8 in bar-shaped chamber 5 and rotate, bull stick 7 will drive the inside action wheel 13 rotation in rectangular chamber 12 afterwards, and then drive driven wheel 14 and transfer line 15 through drive gear 16 and rotate, then transfer line 15 will drive the inside flabellum 22 rotation in circular chamber 21, and then pass through the inside of intake pipe 23 suction circular chamber 21 with the inside gas that escapes of reacting chamber 2, then send into the inside of collecting device through collecting pipe 24, then detect it again, can also drive the inside drive gear 16 removal in rectangular chamber 12 through cylinder 20, and then change the drive ratio between bull stick 7 and the transfer line 15, thereby accomplish the regulation to gas collection speed.
Referring to fig. 2, as an embodiment of the present invention, a charging opening 25 is fixedly installed at the upper end of a reaction vessel body 1, a plurality of guide pipes 26 are fixedly installed at the inner top of a reaction chamber 2 at equal intervals, the upper ends of the plurality of guide pipes 26 are all communicated with the charging opening 25, and a check valve is fixedly installed inside each guide pipe 26.
The chemical liquid containing trace elements required for the reaction can be added into the interior of the feed opening 25, and the plurality of guide pipes 26 can make the chemical liquid more uniformly dropped into the interior of the reaction chamber 2.
Referring to fig. 1, a controller is disposed outside a reaction vessel body 1, and a motor 4 and a cylinder 20 are electrically connected to the controller.
The invention also provides a using method of the device for detecting the gasification characteristics of the precursor material, which comprises the following steps:
s1, feeding: firstly, putting a solvent required by a reaction into the reaction chamber 2 through the material guide pipe 3, then putting raw materials into the reaction chamber 2 to disperse the raw materials in the solvent, then performing hydrolysis reaction to generate an active monomer, and polymerizing the active monomer to form sol;
s2, admixture: adding a chemical solution containing trace elements required for reaction into the feeding port 25, so that the chemical solution is uniformly dropped into the reaction chamber 2 through the plurality of guide pipes 26, and the chemical solution and the solution formed in the solvent can obtain uniformity at a molecular level within a short time, and then are uniformly mixed at the molecular level when a gel is formed;
s3, gasification: the motor 4 is started through the controller, the motor 4 drives the stirring rod 9 in the reaction chamber 2 to rotate, so that the mixing degree of materials in the reaction chamber 2 is improved, and meanwhile, the metal plate 10 in the stirring rod 9 can generate heat, so that the gasification of the materials in the reaction chamber 2 is accelerated;
s4, collecting: after the motor 4 is started, the transmission rod 15 is driven to rotate, so that gas in the reaction chamber 2 is driven to enter the collecting device through the collecting pipe 24, the gas is collected, the cylinder 20 can be started through the controller, the transmission gear 16 is driven to move in the rectangular cavity 12, the transmission ratio between the rotating rod 7 and the transmission rod 15 is changed, and the gas collecting rate is adjusted.
Further, the time of step S1 is at least 24 h.
The working principle is as follows: firstly, putting a solvent required by reaction into the reaction chamber 2 through the material guide pipe 3, then putting raw materials into the reaction chamber 2, dispersing the raw materials into the solvent, then generating an active monomer through hydrolysis reaction, polymerizing the active monomer to form sol, then adding a liquid medicine containing trace elements required by the reaction into the feeding port 25, enabling the liquid medicine to be uniformly dripped into the reaction chamber 2 through the plurality of guide pipes 26, enabling the liquid medicine and the solution formed in the solvent to obtain uniformity of molecular level in a short time, then starting the motor 4, driving the rotating shaft 6 in the reaction chamber 2 to rotate, then driving the stirring rod 9 to rotate by the rotating shaft 6, then stirring the materials in the reaction chamber 2, further improving the degree of mixing among the materials in the reaction chamber 2, driving the plurality of metal plates 10 to rotate through the stirring rod 9, and fixedly mounting a plurality of magnets 11 at equal intervals at the bottom of the reaction kettle body 1, therefore, for each independent metal plate 10, the magnetic field intensity passing through the inside of the metal plate 10 is constantly changed, and then eddy current is generated inside the metal plate 10, so that the metal plate 10 rapidly generates heat, then the material inside the reaction chamber 2 is heated, and the gasification of the material inside the reaction chamber 2 is accelerated, so that the efficiency of gas escape is improved, after the motor 4 is started, the rotating rod 7 is driven to rotate by the driving belt 8 inside the strip-shaped cavity 5, then the rotating rod 7 drives the driving wheel 13 inside the rectangular cavity 12 to rotate, and then the driven wheel 14 and the driving rod 15 are driven to rotate by the transmission gear 16, then the driving rod 15 drives the fan blades 22 inside the circular cavity 21 to rotate, and then the gas escaping from the inside of the reaction chamber 2 is pumped into the circular cavity 21 through the air inlet pipe 23, then is sent into the collecting device through the collecting pipe 24, and then is detected, the transmission gear 16 inside the rectangular cavity 12 can be driven to move through the air cylinder 20, so that the transmission ratio between the rotating rod 7 and the transmission rod 15 is changed, and the adjustment of the gas collection rate is completed.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. A device for detecting the gasification characteristics of precursor materials comprises a reaction kettle body (1), and is characterized in that: a reaction chamber (2) is arranged in the reaction kettle body (1), a material guide pipe (3) for feeding materials into the reaction chamber (2) is fixedly arranged on the side wall of the reaction kettle body (1), a discharge pipe (27) is fixedly arranged on the side wall of the reaction kettle body (1), control valves are arranged inside the material guide pipe (3) and the discharge pipe (27), the bottom of the reaction kettle body (1) is provided with a driving mechanism for accelerating the escape of gas in the material, the bottom of the reaction chamber (2) is provided with a heating mechanism which is matched with the driving mechanism and is used for further accelerating the escape of gas, a rectangular cavity (12) and a circular cavity (21) are also arranged in the reaction kettle body (1), and rotating mechanisms matched with the driving mechanism and used for collecting gas are arranged in the rectangular cavity (12) and the circular cavity (21).
2. The apparatus of claim 1, wherein the apparatus is configured to detect a vaporization characteristic of a precursor material, and further comprising: actuating mechanism includes motor (4) of fixed mounting in reation kettle body (1) bottom, the output fixed mounting of motor (4) has pivot (6), bar chamber (5) have been seted up to the bottom of reation kettle body (1), the upper end of pivot (6) runs through bar chamber (5) and extends to the bottom of reacting chamber (2), the upper end of pivot (6) has puddler (9) that are used for carrying out the stirring to the material in the inside fixed mounting of reacting chamber (2).
3. The apparatus of claim 2, wherein the apparatus is configured to detect a vaporization characteristic of a precursor material, and further comprising: heating mechanism includes equidistant fixed mounting at a plurality of metal sheets (10) of puddler (9) inside, the equidistant fixed mounting in bottom of reation kettle body (1) has a plurality of and metal sheet (10) complex magnet (11).
4. The apparatus of claim 2, wherein the apparatus is configured to detect a vaporization characteristic of a precursor material, and further comprising: slewing mechanism is including offering in inside device chamber (19) of reation kettle body (1), bull stick (7) is installed in the common rotation of the inside of rectangle chamber (12) and bar chamber (5), be connected through drive belt (8) transmission between bull stick (7) and pivot (6), the outer fringe of bull stick (7) has action wheel (13) in the inside fixed mounting of rectangle chamber (12), rotate jointly between rectangle chamber (12) and circle chamber (21) and install transfer line (15), the outer fringe of transfer line (15) has from driving wheel (14) in the inside fixed mounting of rectangle chamber (12), device chamber (19) have still been seted up to the inside of reation kettle body (1), the interior bottom fixed mounting in device chamber (19) has cylinder (20), the output fixed mounting of cylinder (20) has guide arm (17), the upper end of guide arm (17) extends to the inside of rectangle chamber (12) and in the inside fixed mounting of rectangle chamber (12) installs guide arm (17) There is connecting plate (18), the upper end of connecting plate (18) is rotated and is installed the dead lever, the upper end fixed mounting of dead lever has drive gear (16), action wheel (13) and follow driving wheel (14) mesh with drive gear (16) jointly, the upper end of transfer line (15) extends to the inside and fixed mounting of circle chamber (21) has flabellum (22), the bottom in circle chamber (21) is linked together through the inside of intake pipe (23) with reacting chamber (2), the outside fixed mounting of reation kettle body (1) has collecting pipe (24), the one end of collecting pipe (24) is linked together with circle chamber (21), the other end of collecting pipe (24) is connected with collecting device.
5. The apparatus of claim 1, wherein the apparatus is configured to detect a vaporization characteristic of a precursor material, and further comprising: the upper end fixed mounting of reation kettle body (1) has charge door (25), the equidistant fixed mounting in interior top of reaction chamber (2) has a plurality of pipes (26), and is a plurality of the upper end of pipe (26) all is linked together with charge door (25), every the equal fixed mounting in inside of pipe (26) has the check valve.
6. The apparatus of claim 4, wherein the apparatus is further configured to: the outside of reation kettle body (1) is equipped with the controller, motor (4) and cylinder (20) all with controller electric connection.
7. The use method of the device for detecting the vaporization characteristic of the precursor material is characterized in that: the method comprises the following steps:
s1, feeding: firstly, putting a solvent required by a reaction into the reaction chamber (2) through the material guide pipe (3), then putting raw materials into the reaction chamber (2) to disperse the raw materials in the solvent, then performing hydrolysis reaction to generate an active monomer, and polymerizing the active monomer to form sol;
s2, admixture: adding a chemical solution containing trace elements required by the reaction into the feeding port (25), so that the chemical solution is uniformly dropped into the reaction chamber (2) through a plurality of guide pipes (26), the chemical solution and the solution formed in the solvent can obtain the uniformity of the molecular level in a short time, and then the chemical solution and the solution are uniformly mixed on the molecular level when the gel is formed;
s3, gasification: the motor (4) is started through the controller, the motor (4) drives the stirring rod (9) in the reaction chamber (2) to rotate, so that the mixing degree of materials in the reaction chamber (2) is improved, and meanwhile, the metal plate (10) in the stirring rod (9) can generate heat, so that the gasification of the materials in the reaction chamber (2) is accelerated;
s4, collecting: after the motor (4) is started, the transmission rod (15) can be driven to rotate, then gas in the reaction chamber (2) is driven to enter the collecting device through the collecting pipe (24), gas collection is completed, the cylinder (20) can be started through the controller, then the transmission gear (16) is driven to move in the rectangular cavity (12), the transmission ratio between the rotating rod (7) and the transmission rod (15) is changed, and therefore the adjustment of the gas collection rate is completed.
8. Use of a device for detecting the vaporization property of a precursor material according to claim 7, wherein: the time of step S1 is at least 24 h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111432432.6A CN114354440A (en) | 2021-11-29 | 2021-11-29 | Device for detecting gasification characteristics of precursor material and using method |
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| CN202111432432.6A CN114354440A (en) | 2021-11-29 | 2021-11-29 | Device for detecting gasification characteristics of precursor material and using method |
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Citations (12)
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