CN114247406A - Multi-temperature reaction kettle - Google Patents
Multi-temperature reaction kettle Download PDFInfo
- Publication number
- CN114247406A CN114247406A CN202011018086.2A CN202011018086A CN114247406A CN 114247406 A CN114247406 A CN 114247406A CN 202011018086 A CN202011018086 A CN 202011018086A CN 114247406 A CN114247406 A CN 114247406A
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- Prior art keywords
- steam
- temperature sensor
- reaction kettle
- temperature reaction
- temperature
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- 239000007788 liquid Substances 0.000 claims abstract description 24
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000012530 fluid Substances 0.000 claims abstract description 6
- 239000011248 coating agent Substances 0.000 claims abstract description 4
- 238000000576 coating method Methods 0.000 claims abstract description 4
- 238000005260 corrosion Methods 0.000 claims description 5
- 230000007797 corrosion Effects 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 4
- 239000011521 glass Substances 0.000 description 3
- 238000007789 sealing Methods 0.000 description 2
- 230000006978 adaptation Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The application discloses many temperature reation kettle, including the cauldron body and first temperature sensor, first temperature sensor extends to the cauldron is internal to be close to bottom department, the internal wall of cauldron is formed with the anticorrosive coating, and the outer wall is formed with the heating cavity, heating cavity one side bottom is formed with steam inlet and liquid outlet respectively with the top, and opposite side bottom is formed with liquid inlet and steam outlet respectively with the top, heating cavity bottom is formed with the leakage fluid dram, steam inlet, liquid outlet, liquid inlet, steam outlet and leakage fluid dram department install the valve respectively, steam inlet deviates from the one end of the cauldron body is connected in steam generator, second temperature sensor is installed in the steam generator exit, first temperature sensor and second temperature sensor transmit data information for the controller. The steam heating and the liquid cooling can be realized in the heating cavity, and the multi-temperature span of the reaction kettle is realized.
Description
Technical Field
The application relates to a reaction kettle, in particular to a multi-temperature reaction kettle.
Background
The existing reaction kettle is of an integral structure, so that the inner wall of the reaction kettle is difficult to clean, and residues on the inner wall can influence the production of subsequent products, thereby causing the defect of product quality. Moreover, as the residue on the inner wall increases, the heat-conducting property of the reaction kettle is affected, so that the temperature change in the reaction kettle cannot reach the required temperature in time, and the quality of the product is also affected; meanwhile, if the residues have corrosive properties, the residues can corrode the inner wall of the reaction kettle, and the service life of the reaction kettle and related parts is influenced.
Disclosure of Invention
The invention aims to provide a multi-temperature reaction kettle.
In order to achieve the above object, the present invention provides the following technical solutions.
The embodiment of the application discloses many temperature reation kettle, including the cauldron body and first temperature sensor, first temperature sensor extends to the cauldron is internal to be close to bottom department, the internal wall of cauldron is formed with the anticorrosive coating, and the outer wall is formed with the heating cavity, heating cavity one side bottom is formed with steam inlet and liquid outlet respectively with the top, and opposite side bottom is formed with liquid inlet and steam outlet respectively with the top, heating cavity bottom is formed with the leakage fluid dram, steam inlet, liquid outlet, liquid inlet, steam outlet and leakage fluid dram department install the valve respectively, steam inlet deviates from the one end of the cauldron body is connected in steam generator, steam generator installs second temperature sensor in the department, first temperature sensor and second temperature sensor transmit data information for the controller.
Preferably, in the multi-temperature reaction kettle, the anticorrosive layer is a glass lining layer.
Preferably, in the above multi-temperature reaction tank, the controller controls the steam generator.
Preferably, in foretell multi-temperature reaction kettle, the openable door body is installed in the sealed of cauldron body top, door body axle center department sealed install extend to the agitator of the internal bottom of cauldron, the controller control the agitator.
Preferably, in the multi-temperature reaction kettle, the stirrer is provided with a plurality of groups of stirring blades from top to bottom inside the kettle body.
Preferably, in the multi-temperature reaction kettle, a visible window is formed on the side wall of the kettle body.
Preferably, in the multi-temperature reaction kettle, a discharge hole is formed at the bottom of the kettle body.
Compared with the prior art, this technical scheme has effectively prevented the corruption of corrosive material to the cauldron body through addding the anticorrosive coating, has promoted the application scope of product greatly to can realize steam heating in the heating cavity, can realize liquid cooling again, realize the span of reation kettle multiple temperature.
Drawings
In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments described in the present application, and other drawings can be obtained by those skilled in the art without creative efforts.
FIG. 1 is a schematic diagram of a multi-temperature reaction vessel according to an embodiment of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be described in detail below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc., indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "connected" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1, a multi-temperature reaction kettle 100 includes a kettle body 101 and a first temperature sensor 102, the first temperature sensor 102 extends into the kettle body 101 near the bottom, an anti-corrosion layer 103 is formed on the inner wall of the kettle body 101, a heating cavity 104 is formed on the outer wall, a steam inlet 105 and a liquid outlet 106 are respectively formed on the bottom and the top of one side of the heating cavity 104, a liquid inlet 107 and a steam outlet 108 are respectively formed on the bottom and the top of the other side of the heating cavity 104, a liquid outlet 109, the steam inlet 105 and the liquid outlet 106 are formed on the bottom of the heating cavity 104, valves are respectively installed at the liquid inlet 107, the steam outlet 108 and the liquid outlet 109, one end of the steam inlet 105, which is away from the kettle body 101, is connected to the steam generator 110, the second temperature sensor 111 is installed at the outlet of the steam generator 110, and the first temperature sensor 102 and the second temperature sensor 111 transmit data information to a controller (not shown). The corrosion-resistant layer 103 is a glass lining layer. The top of the kettle body 101 is provided with an openable door body 112 in a sealing way, the axis of the door body 112 is provided with a stirrer 113 which extends to the bottom in the kettle body 101 in a sealing way, and the stirrer 113 is controlled by a controller. The controller controls the steam generator 110. The stirrer 113 has a plurality of stirring blades 114 formed in the kettle 101 from top to bottom. A discharge port 116 is formed at the bottom of the kettle body 101.
In the embodiment, steam heating and liquid cooling can be realized in the heating cavity, the multi-temperature span of the reaction kettle is realized, when high-temperature reaction is needed, the controller controls and improves the steam temperature of the steam generator through the data of the two temperature sensors, and meanwhile, the controller can also control the stirring speed of the stirrer so as to achieve the required parameters; when the required temperature is lower, the steam generator is controlled to reduce the steam temperature. When a particularly low temperature is required, even the temperature below 0 ℃, the steam inlet and the steam outlet can be closed, the liquid inlet and the liquid outlet can be opened, and the frozen liquid is introduced to realize the low-temperature reaction.
In addition, the glass lining layer is additionally arranged, so that corrosion of a corrosion material to the kettle body is effectively prevented, the application range of a product is greatly widened, the reaction kettle is designed to be split due to the adoption of the open-close door body, the cleaning of the inner wall of the kettle body is facilitated, and meanwhile, the discharge port is arranged at the bottom, so that the materials are conveniently and completely removed.
Further, a visible window 115 is formed on the side wall of the kettle body 101.
In this example, it is convenient to monitor the progress of the reaction of the materials.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising an … …" does not exclude the presence of other identical elements in a process, method, article, or apparatus that comprises the element.
The foregoing is directed to embodiments of the present application and it is noted that numerous modifications and adaptations may be made by those skilled in the art without departing from the principles of the present application and are intended to be within the scope of the present application.
Claims (7)
1. The utility model provides a multi-temperature reaction kettle, its characterized in that, includes the cauldron body and first temperature sensor, first temperature sensor extends to the cauldron is internal to be close to bottom department, the internal wall of cauldron is formed with the anticorrosive coating, and the outer wall is formed with the heating cavity, heating cavity one side bottom is formed with steam inlet and liquid outlet respectively with the top, and opposite side bottom is formed with liquid inlet and steam outlet respectively with the top, heating cavity bottom is formed with the leakage fluid dram, steam inlet, liquid outlet, liquid inlet, steam outlet and leakage fluid dram department install the valve respectively, steam inlet deviates from the one end of the cauldron body is connected in steam generator, second temperature sensor is installed in steam generator exit, first temperature sensor and second temperature sensor transmit data information for the controller.
2. The multi-temperature reaction kettle of claim 1, wherein the corrosion resistant layer is a glass-lined layer.
3. The multi-temperature reaction vessel of claim 1 wherein the controller controls the steam generator.
4. The multi-temperature reaction kettle according to claim 1, wherein an openable door body is hermetically installed at the top of the kettle body, an agitator extending to the bottom in the kettle body is hermetically installed at the axis of the door body, and the agitator is controlled by the controller.
5. The multi-temperature reaction kettle of claim 4, wherein the stirrer is provided with a plurality of groups of stirring blades from top to bottom inside the kettle body.
6. The multi-temperature reaction kettle of claim 1, wherein the kettle body side wall is formed with a visible window.
7. The multi-temperature reaction kettle according to claim 1, wherein a discharge port is formed at the bottom of the kettle body.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202011018086.2A CN114247406A (en) | 2020-09-24 | 2020-09-24 | Multi-temperature reaction kettle |
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CN202011018086.2A CN114247406A (en) | 2020-09-24 | 2020-09-24 | Multi-temperature reaction kettle |
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CN114247406A true CN114247406A (en) | 2022-03-29 |
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CN202011018086.2A Pending CN114247406A (en) | 2020-09-24 | 2020-09-24 | Multi-temperature reaction kettle |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2286886A1 (en) * | 1998-10-16 | 2000-04-16 | Wolf-Dieter Hergeth | Process for heterophase reactions in a liquide or supercritical dispersion medium |
CN205392382U (en) * | 2016-02-26 | 2016-07-27 | 辽阳鑫宇化工有限公司 | Temperature of a reaction vessel control system |
CN106492737A (en) * | 2016-12-28 | 2017-03-15 | 田东昊润新材料科技有限公司 | A kind of montmorillonite natridization reaction kettle |
CN206474167U (en) * | 2017-01-06 | 2017-09-08 | 天津市宇通化工助剂有限公司 | A kind of emulsifying agent reactor deployment device |
CN208526585U (en) * | 2018-05-09 | 2019-02-22 | 滨海金海立医药化工有限公司 | A kind of glassed steel reaction vessels |
-
2020
- 2020-09-24 CN CN202011018086.2A patent/CN114247406A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2286886A1 (en) * | 1998-10-16 | 2000-04-16 | Wolf-Dieter Hergeth | Process for heterophase reactions in a liquide or supercritical dispersion medium |
CN205392382U (en) * | 2016-02-26 | 2016-07-27 | 辽阳鑫宇化工有限公司 | Temperature of a reaction vessel control system |
CN106492737A (en) * | 2016-12-28 | 2017-03-15 | 田东昊润新材料科技有限公司 | A kind of montmorillonite natridization reaction kettle |
CN206474167U (en) * | 2017-01-06 | 2017-09-08 | 天津市宇通化工助剂有限公司 | A kind of emulsifying agent reactor deployment device |
CN208526585U (en) * | 2018-05-09 | 2019-02-22 | 滨海金海立医药化工有限公司 | A kind of glassed steel reaction vessels |
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Application publication date: 20220329 |
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