CN114225886A - Swing speed governing formula reation kettle - Google Patents

Swing speed governing formula reation kettle Download PDF

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Publication number
CN114225886A
CN114225886A CN202111468329.7A CN202111468329A CN114225886A CN 114225886 A CN114225886 A CN 114225886A CN 202111468329 A CN202111468329 A CN 202111468329A CN 114225886 A CN114225886 A CN 114225886A
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China
Prior art keywords
kettle body
cauldron body
solid material
rotary column
pressure plate
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CN202111468329.7A
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Chinese (zh)
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颜献丹
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Individual
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Individual
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Priority to CN202111468329.7A priority Critical patent/CN114225886A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/28Moving reactors, e.g. rotary drums
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention provides a swinging speed-regulating reaction kettle, and relates to the field of reaction kettles. This swing speed governing formula reation kettle, including the cauldron body, the surface below fixed mounting of the cauldron body has the support frame, and the surface one side of the cauldron body is connected and is link up there is the feed inlet, and the breach has been seted up to the surface top of the cauldron body, and the surface of the cauldron body lies in one side of breach and connects and link up there is the discharge gate. This swing speed governing formula reation kettle, when reaction rate strengthens, the internal portion atmospheric pressure of cauldron risees, thereby can promote the atmospheric pressure board rebound, and then can promote the extension rod and drive counter weight ball rebound, the balance of column spinner is destroyed, thereby can drive the column spinner and rotate, rotatory in-process, the solid material leak box spills from liquid reagent gradually, thereby make the coincidence area reduce gradually, and then can reduce reaction rate, the uncontrollable problem of the inside reaction rate of reation kettle among the prior art has been solved.

Description

Swing speed governing formula reation kettle
Technical Field
The invention relates to the technical field of reaction kettles, in particular to a swinging speed-regulating type reaction kettle.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The reaction kettle is widely applied to the fields of petroleum, chemical industry, rubber, pesticides, dyes, medicines, food and the like.
Chemical reaction generates a large amount of gas, and the existing reaction kettle can not control the reaction speed, so that the reaction kettle is easy to cause accidents due to the increase of the internal air pressure of the reaction kettle, and the reaction speed can be adjusted, thereby realizing the reaction kettle with stable reaction.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a swing speed-regulating reaction kettle, which solves the problems in the background art.
In order to achieve the purpose, the invention is realized by the following technical scheme: a swing speed regulation type reaction kettle comprises a kettle body, wherein a support frame is fixedly installed below the outer surface of the kettle body, a feed inlet is connected and communicated with one side of the outer surface of the kettle body, a notch is formed above the outer surface of the kettle body, a discharge outlet is connected and communicated with one side of the notch of the outer surface of the kettle body, an articulated shaft is rotatably connected with the inner center of the kettle body, a rotary column is fixedly sleeved on the outer surface of the articulated shaft, the top end of the rotary column is sleeved inside the notch and extends to the outer side of the kettle body, sealing sliding grooves are formed in the front side and the rear side of the notch of the upper surface of the kettle body, sealing sliding blocks are slidably connected inside the sealing sliding grooves, two sealing sliding blocks are fixedly connected through sealing arc plates, the sealing arc plates are fixedly sleeved on the outer surface of the rotary column, a through groove is formed in the middle part of the rotary column, an air pressure plate is slidably connected inside the through groove, and an extension rod is fixedly installed in the middle part of the top end of the air pressure plate, the extension rod runs through the column spinner and with column spinner sliding connection, the one end fixed mounting that the extension rod is located the column spinner top has the counter weight ball, reset spring has been cup jointed to the surface of extension rod, reset spring one end and the interior roof fixed connection that leads to the groove, one end and gas-pressure plate fixed connection, the column spinner is located to lead to the groove below and sets up the air inlet that link up with leading to the groove, the column spinner is located the below of air inlet and has seted up the guiding gutter, the bottom fixed mounting of column spinner has solid material hopper, the opening that communicates with the guiding gutter is seted up on the top of solid material hopper, the top of guiding gutter is connected and has the flow distribution box, the top of flow distribution box is connected and is link up there is the inlet pipe, the inlet pipe runs through the gas-pressure plate and extends to the top of gas-pressure plate, gas-pressure plate and inlet pipe sliding connection, the one end that the guiding gutter was kept away from to the inlet pipe runs through the column spinner and extends to the outside of the cauldron body.
Preferably, the top of discharge gate is connected and is link up there is the sleeve, and the sleeve is kept away from the one end of discharge gate and is connected and link up there is the connecting pipe, and telescopic inside is rotated and is connected with the center pin, and the fixed surface of center pin installs the fin, and the vent that reduces in proper order is seted up to the surface of fin.
Preferably, the both ends of articulated shaft run through the cauldron body and extend to the outside of the cauldron body, and both ends fixed mounting has the baffle about the articulated shaft is located the surface in the cauldron external side, and the surface both ends fixed mounting of the cauldron body has the end cover, and the spacing groove with the baffle adaptation is seted up to the inside of end cover.
Preferably, the cross section of the solid material leakage box is spoon-shaped, the two ends of the solid material leakage box are both circular, the diameter of one end is larger than that of the other end, and the solid material leakage box is positioned below the hinged shaft.
Preferably, the cross-sectional shape of the feed pipe is L-shaped, the bottom end part of the feed pipe is parallel to the extension rod, and the included angle between the top end part and the bottom end part of the feed pipe is more than ninety degrees.
Preferably, the outer ends of the feeding pipe and the feeding port are both in threaded connection with sealing covers, and the feeding pipe is aligned with the hinged shaft.
The invention has the following beneficial effects:
1. this swing speed governing formula reation kettle, pour into the inside of the cauldron body with liquid reagent through the feed inlet, pour into the inside of solid material small form leakage into through the inlet pipe with solid reagent, begin to react, when reaction rate strengthens, the internal portion atmospheric pressure of cauldron risees, thereby can promote the atmospheric pressure board rebound, and then can promote the extension rod and drive the counter weight ball rebound, the balance of column spinner is destroyed, thereby can drive the column spinner and rotate, rotatory in-process, spill from liquid reagent gradually in the solid material small form leakage, thereby make the coincidence area reduce gradually, and then can reduce reaction rate, the uncontrollable problem of the internal reaction rate of reation kettle among the prior art has been solved.
2. This swing speed governing formula reation kettle, the discharge gate is discharged from to the formation gas, and the drive fin is rotatory, and the change that the fin surface was ventilated can be to the sheltering from of discharge gate, and then can make exhaust velocity change to can change the internal inside atmospheric pressure of cauldron, finally can make solid material leaking case can take place reciprocating swing.
3. According to the swing speed regulation type reaction kettle, the section of the feeding pipe is L-shaped, the bottom end part of the feeding pipe is parallel to the extension rod, and the included angle between the top end part and the bottom end part of the feeding pipe is larger than ninety degrees, so that the feeding process can be ensured to automatically flow downwards.
Drawings
FIG. 1 is a schematic half-section view of the present invention;
FIG. 2 is a schematic view of a half-section of the kettle body of the present invention;
FIG. 3 is a schematic view of the fin attachment of the present invention;
FIG. 4 is a schematic view of a spin column of the present invention;
FIG. 5 is a schematic view of a solid material hopper according to the present invention;
fig. 6 is a schematic view of a hinge shaft connection according to the present invention.
The device comprises a kettle body-1, a support frame-2, a feed inlet-3, a notch-4, a discharge port-5, a hinge shaft-6, a rotary column-7, a sealing sliding groove-8, a sealing sliding block-9, a sealing arc plate-10, a through groove-11, a pressure plate-12, an extension rod-13, a counterweight ball-14, a return spring-15, an air inlet-16, a diversion groove-17, a solid material leakage box-18, a diversion box-19, a feed pipe-20, a sleeve-21, a connecting pipe-22, a central shaft-23, a fin-24, an air vent-25, a baffle-26, an end cover-27, a limiting groove-28 and an opening-29.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The embodiment of the invention provides a swinging speed-regulating reaction kettle:
in the first embodiment, as shown in fig. 1-6, the reactor comprises a kettle body 1, a support frame 2 is fixedly installed below the outer surface of the kettle body 1, a feed inlet 3 is connected and penetrated through one side of the outer surface of the kettle body 1, a sleeve 21 is connected and penetrated through the top end of a discharge outlet 5, one end of the sleeve 21, which is far away from the discharge outlet 5, is connected and penetrated through a connecting pipe 22, a central shaft 23 is rotatably connected inside the sleeve 21, a fin 24 is fixedly installed on the outer surface of the central shaft 23, and vent holes 25 which are sequentially reduced are formed in the outer surface of the fin 24, so that the fin 24 can be driven to rotate in the process of discharging generated gas, and the exhaust speed of the reactor can be circulated by utilizing the sequentially reduced gap 4, thereby the pressure inside the kettle body 1 can be changed in a small range, and further the rotary column 7 can be swung, so that the solid material leakage box 18 can be swung in liquid, so that the solid reactant is uniformly distributed.
Breach 4 has been seted up to the surface top of the cauldron body 1, the surface of the cauldron body 1 is located one side of breach 4 and connects and link up there is discharge gate 5, the inside center of the cauldron body 1 rotates and is connected with articulated shaft 6, the both ends of articulated shaft 6 run through the cauldron body 1 and extend to the outside of the cauldron body 1, both ends fixed mounting has baffle 26 about articulated shaft 6 is located the surface in the cauldron body 1 outside, the surface both ends fixed mounting of the cauldron body 1 has end cover 27, the spacing groove 28 with the 26 adaptations of baffle is seted up to end cover 27's inside, can prescribe a limit to articulated shaft 6's rotation range through such setting.
The outer surface of the hinge shaft 6 is fixedly sleeved with a rotary column 7, the top end of the rotary column 7 is sleeved inside the notch 4 and extends to the outer side of the kettle body 1, the upper surface of the kettle body 1 is positioned at the front side and the rear side of the notch 4 and is provided with a sealing sliding chute 8, the inside of the sealing sliding chute 8 is connected with a sealing sliding block 9 in a sliding manner, the two sealing sliding blocks 9 are fixedly connected through a sealing arc plate 10, the sealing arc plate 10 is fixedly sleeved on the outer surface of the rotary column 7, the middle part of the rotary column 7 is provided with a through groove 11, the inside of the through groove 11 is connected with a pressure plate 12 in a sliding manner, the middle part of the top end of the pressure plate 12 is fixedly provided with an extension rod 13, the extension rod 13 penetrates through the rotary column 7 and is connected with the rotary column 7 in a sliding manner, one end of the extension rod 13 positioned above the rotary column is fixedly provided with a counterweight ball 14, the outer surface of the extension rod 13 is sleeved with a return spring 15, one end of the return spring 15 is fixedly connected with the inner top wall of the through groove 11, one end and atmospheric pressure board 12 fixed connection, the column spinner 7 is located and has seted up the air inlet 16 that link up with logical groove 11 below leading to groove 11, the guiding gutter 17 has been seted up to the below that the column spinner 7 is located air inlet 16, the bottom fixed mounting of column spinner 7 has solid material leaking box 18, the cross sectional shape ladle shape of solid material leaking box 18, the both ends of solid material leaking box 18 are circular, the diameter of one end is greater than the diameter of the other end, solid material leaking box 18 is located the below of articulated shaft 6, can make solid material leaking box 18 reduce gradually with the coincidence area of liquid reactant at rotatory in-process through such setting, and then can control reaction rate.
Opening 29 with the guiding gutter 17 intercommunication is seted up on the top of solid material hourglass case 18, the top of guiding gutter 17 is connected and has been link up and has been had shunt box 19, the top of shunt box 19 is connected and has been link up inlet pipe 20, the equal threaded connection in outer end of inlet pipe 20 and feed inlet 3 has sealed lid, can guarantee sealed effect through such setting, inlet pipe 20 aligns with articulated shaft 6, can inject into liquid into the liquid level when can guaranteeing through such setting.
The feed pipe 20 penetrates through the air pressure plate 12 and extends to the upper part of the air pressure plate 12, the air pressure plate 12 is connected with the feed pipe 20 in a sliding mode, the cross section of the feed pipe 20 is L-shaped, the bottom end part of the feed pipe 20 is parallel to the extension rod 13, and the included angle between the top end part and the bottom end part of the feed pipe 20 is larger than ninety degrees. One end of the feeding pipe 20 far away from the diversion trench 17 penetrates through the rotating column 7 and extends to the outer side of the kettle body 1.
When the reaction kettle is used, a liquid reagent is injected into the kettle body 1 through the feeding hole 3, a solid reagent is injected into the solid material leakage box 18 through the feeding pipe 20, reaction is started, when the reaction speed is enhanced, the air pressure in the kettle body 1 is increased, so that the air pressure plate 12 can be pushed to move upwards, the extension rod 13 can be pushed to drive the counterweight balls 14 to move upwards, after the counterweight balls move upwards, the balance of the rotating column 7 is broken, so that the rotating column 7 can be driven to rotate, and in the rotating process, the solid material leakage box 18 gradually leaks out of the liquid reagent, so that the overlapping area is gradually reduced, and the reaction speed can be reduced;
under normal operating condition, the generated gas is discharged from discharge gate 5, and drive fin 24 is rotatory, and the change of fin 24 surface vent 4 can be to the sheltering from of discharge gate 5, and then can make exhaust velocity change to can change the inside atmospheric pressure of the cauldron body 1, finally can make solid material leak case 18 can take place reciprocating swing.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (6)

1. The utility model provides a swing speed governing formula reation kettle, includes the cauldron body (1), its characterized in that: a support frame (2) is fixedly arranged below the outer surface of the kettle body (1), a feed port (3) is connected and communicated with one side of the outer surface of the kettle body (1), a notch (4) is formed above the outer surface of the kettle body (1), and a discharge port (5) is connected and communicated with the outer surface of the kettle body (1) positioned at one side of the notch (4);
the inner center of the kettle body (1) is rotatably connected with a hinge shaft (6), the outer surface of the hinge shaft (6) is fixedly sleeved with a rotary column (7), the top end of the rotary column (7) is sleeved inside the notch (4) and extends to the outer side of the kettle body (1), the upper surface of the kettle body (1) is positioned on the front side and the rear side of the notch (4) and is provided with sealing sliding chutes (8), the sealing sliding chutes (8) are connected with sealing sliding blocks (9) in a sliding manner, the two sealing sliding blocks (9) are fixedly connected through sealing arc plates (10), and the sealing arc plates (10) are fixedly sleeved on the outer surface of the rotary column (7);
the middle part of the rotary column (7) is provided with a through groove (11), the inside of the through groove (11) is connected with a pressure plate (12) in a sliding manner, the middle part of the top end of the pressure plate (12) is fixedly provided with an extension rod (13), the extension rod (13) penetrates through the rotary column (7) and is connected with the rotary column (7) in a sliding manner, one end of the extension rod (13) positioned above the rotary column is fixedly provided with a counterweight ball (14), the outer surface of the extension rod (13) is sleeved with a return spring (15), one end of the return spring (15) is fixedly connected with the inner top wall of the through groove (11), and the other end of the return spring is fixedly connected with the pressure plate (12);
the utility model discloses a kettle body, including the air inlet that leads to groove (11), the bottom fixed mounting of column spinner (7) has solid material hourglass case (18), opening (29) with guiding gutter (17) intercommunication are seted up on the top of solid material hourglass case (18), opening (19) have been seted up on the top of guiding gutter (17), diverter box (19) have been connected and have been link up on the top of guiding gutter (17), inlet pipe (20) have been connected and have been link up on the top of diverter box (19), inlet pipe (20) run through gas-pressure plate (12) and extend to the top of gas-pressure plate (12), gas-pressure plate (12) and inlet pipe (20) sliding connection, the one end that guiding gutter (17) were kept away from in inlet pipe (20) runs through column spinner (7) and extends to the outside of kettle body (1).
2. A swing governing reaction vessel as defined in claim 1, wherein: the top of discharge gate (5) is connected and is link up there is sleeve (21), and the one end that discharge gate (5) were kept away from in sleeve (21) is connected and is link up there is connecting pipe (22), and the inside rotation of sleeve (21) is connected with center pin (23), and the fixed surface of center pin (23) installs fin (24), and the surface of fin (24) is seted up blow vent (25) that reduce in proper order.
3. A swing governing reaction vessel as defined in claim 1, wherein: the both ends of articulated shaft (6) run through the cauldron body (1) and extend to the outside of the cauldron body (1), and both ends fixed mounting has baffle (26) about articulated shaft (6) are located the surface in the cauldron body (1) outside, and the surface both ends fixed mounting of the cauldron body (1) has end cover (27), and spacing groove (28) with baffle (26) adaptation are seted up to the inside of end cover (27).
4. A swing governing reaction vessel as defined in claim 1, wherein: the cross section of the solid material leakage box (18) is spoon-shaped, the two ends of the solid material leakage box (18) are circular, the diameter of one end is larger than that of the other end, and the solid material leakage box (18) is positioned below the hinged shaft (6).
5. A swing governing reaction vessel as defined in claim 1, wherein: the cross section of the feeding pipe (20) is L-shaped, the bottom end part of the feeding pipe (20) is parallel to the extension rod (13), and the included angle between the top end part and the bottom end part of the feeding pipe (20) is more than ninety degrees.
6. A swing governing reaction vessel as defined in claim 1, wherein: the outer ends of the feeding pipe (20) and the feeding hole (3) are connected with sealing covers in a threaded mode, and the feeding pipe (20) is aligned to the hinging shaft (6).
CN202111468329.7A 2021-12-03 2021-12-03 Swing speed governing formula reation kettle Pending CN114225886A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111468329.7A CN114225886A (en) 2021-12-03 2021-12-03 Swing speed governing formula reation kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111468329.7A CN114225886A (en) 2021-12-03 2021-12-03 Swing speed governing formula reation kettle

Publications (1)

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CN114225886A true CN114225886A (en) 2022-03-25

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114534680A (en) * 2022-03-29 2022-05-27 山东泰诺药业有限公司 Reation kettle is used in medicament production
CN115212839A (en) * 2022-08-09 2022-10-21 江西省化学工业研究所 Purification device and purification method for prenol production

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114534680A (en) * 2022-03-29 2022-05-27 山东泰诺药业有限公司 Reation kettle is used in medicament production
CN114534680B (en) * 2022-03-29 2024-01-16 山东泰诺药业有限公司 Reation kettle is used in medicament production
CN115212839A (en) * 2022-08-09 2022-10-21 江西省化学工业研究所 Purification device and purification method for prenol production
CN115212839B (en) * 2022-08-09 2024-03-01 江西省化学工业研究所 Purification device and purification method for prenyl alcohol production

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Application publication date: 20220325

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