CN114179392A - Method for forming large-size end socket heat insulation layer - Google Patents

Method for forming large-size end socket heat insulation layer Download PDF

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Publication number
CN114179392A
CN114179392A CN202111313053.5A CN202111313053A CN114179392A CN 114179392 A CN114179392 A CN 114179392A CN 202111313053 A CN202111313053 A CN 202111313053A CN 114179392 A CN114179392 A CN 114179392A
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Prior art keywords
heat
insulating layer
air bag
insulation layer
heat insulation
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CN202111313053.5A
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CN114179392B (en
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金秀秀
郭培江
江芳芳
王付青云
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Hubei Sanjiang Space Jiangbei Mechanical Engineering Co Ltd
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Hubei Sanjiang Space Jiangbei Mechanical Engineering Co Ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/30Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core
    • B29C70/34Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core and shaping or impregnating by compression, i.e. combined with compressing after the lay-up operation
    • B29C70/345Shaping by lay-up, i.e. applying fibres, tape or broadsheet on a mould, former or core; Shaping by spray-up, i.e. spraying of fibres on a mould, former or core and shaping or impregnating by compression, i.e. combined with compressing after the lay-up operation using matched moulds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C70/00Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts
    • B29C70/04Shaping composites, i.e. plastics material comprising reinforcements, fillers or preformed parts, e.g. inserts comprising reinforcements only, e.g. self-reinforcing plastics
    • B29C70/28Shaping operations therefor
    • B29C70/54Component parts, details or accessories; Auxiliary operations, e.g. feeding or storage of prepregs or SMC after impregnation or during ageing

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Composite Materials (AREA)
  • Mechanical Engineering (AREA)
  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)

Abstract

The invention discloses a method for forming a large-size end socket heat insulation layer, which comprises the steps of firstly forming a part with thicker heat insulation layer around a metal joint in a mould pressing mode, then placing the part with thicker heat insulation layer into an air bag forming tool, and carrying out pressure forming by adopting an air bag after mounting, so that the tool cost can be reduced, equipment investment is not needed, and the production cost is greatly reduced. In addition, the air bag forming tool is composed of a lower die and a cover plate, is connected with an air source to inflate after being assembled with the air bag, then is heated by the oven as a whole, and meanwhile realizes pressurization.

Description

Method for forming large-size end socket heat insulation layer
Technical Field
The invention belongs to the technical field of forming of fiber winding engine shell heat insulation structures, and particularly relates to a forming method of a large-size end socket heat insulation layer.
Background
The end socket heat insulating layer is an important part of the fiber winding engine shell heat insulating layer and mainly consists of a metal joint and a heat insulating layer. At present, the heat insulation layers of the front and the rear end sockets are mostly molded integrally, the tool is composed of an upper die and a lower die, a press platform is placed in the tool after the die is filled with the paster, and the pressing forming is carried out by means of external heating. Along with the increase of the diameter of the composite material shell, the cost of the die pressing tool is greatly increased, the size of a platform of die pressing equipment (a press) is also increased, and the input cost of the equipment is also greatly increased.
Disclosure of Invention
The invention aims to overcome the defects of the prior art and provides a method for forming a large-size end socket heat insulation layer, which reduces tools and production cost.
In order to achieve the purpose, the invention provides a method for forming a heat insulating layer of a large-size end socket, wherein the end socket comprises a metal joint and the heat insulating layer, and the method for forming the heat insulating layer comprises the following steps:
1) compression molding heat insulating layer of metal joint
1a) Coating primer on the inner and outer surfaces of the metal joint, then drying the metal joint in the air, coating surface glue on the surface of the primer, drying the metal joint in the air, and simultaneously coating surface glue on the inner and outer surfaces of the molded heat insulation layer rubber and drying the metal joint in the air;
1b) sticking the mould pressing heat insulation layer rubber sheets on the inner surface and the outer surface of the metal joint until the thickness of the mould pressing heat insulation layer rubber sheets on the outer surface of the metal joint is consistent with the thickness of the outer layer of the heat insulation layer of the end socket, and the thickness of the mould pressing heat insulation layer rubber sheets on the inner surface of the metal joint is half of the thickness of the inner layer of the heat insulation layer of the end socket;
after the sticking is finished, putting the metal connector into a mould pressing tool, and continuously sticking a mould pressing heat insulation layer rubber sheet according to the thickness of the inner layer of the end socket heat insulation layer until the thickness of the mould pressing heat insulation layer rubber sheet on the inner surface of the metal connector is consistent with the thickness of the inner layer of the end socket heat insulation layer;
1c) after the surface mounting is finished, closing the die, and putting the die pressing tool on a flat vulcanizing machine for vulcanization;
1d) cooling the mould pressing tool along with the equipment, opening the mould pressing tool, demolding the bottom layer, and cleaning the flash to obtain a compression-molded heat insulation layer;
2) air bag pressure forming heat insulating layer
2a) Polishing the bonding surface of the heat-insulating layer subjected to compression molding until fluffing, brushing an adhesive on the bonding surface of the heat-insulating layer subjected to compression molding, and drying;
2b) assembling an air bag forming tool with a metal joint which is compression-molded with a heat insulating layer;
2c) coating an adhesive on the airbag heat-insulating layer adhesive sheet adhered to the heat-insulating layer adhesive surface subjected to compression molding, drying in the air, adhering the airbag heat-insulating layer adhesive sheet to the heat-insulating layer adhesive surface subjected to compression molding, and finally adhering the airbag heat-insulating layer adhesive sheet according to the molded surface of the end enclosure;
2d) after the surface mounting is finished, performing vacuum bag making prepressing treatment, polishing and flattening the uneven positions on the surface of the preformed heat insulation layer, and performing contrast inspection by using a profile template;
2e) assembling the air bag and an air bag forming tool, and then integrally placing the air bag and the air bag forming tool into an oven and connecting a nitrogen source to carry out air bag inflation forming;
2f) and (4) deflating the air bag after cooling, opening the air bag forming tool, demolding and cleaning the flash.
Further, in the step 1c), the specific vulcanization process is as follows: starting a vulcanizing machine, performing cold pressing for 2-4 times at a gauge pressure of 3-4 MPa; heating the mould to 80-100 ℃, then preserving heat for 40-60 min, pressurizing to 3-5 MPa after heat preservation is finished, exhausting for 2-4 times, and finally pressurizing to 3-5 MPa; continuously heating to 110-130 ℃, and exhausting for 2-4 times; then heating to 140-160 ℃, pressurizing to 5-7 MPa, and keeping the temperature for 60-90 min; and cutting off the power and reducing the temperature after the heat preservation is finished.
Further, in the step 1d), the mould pressing tool is opened when the temperature of the mould pressing tool is reduced to below 60 ℃ along with the equipment.
Further, in the step 2b), the air bag forming tool comprises a lower die and a cover plate, and a metal joint with a heat insulation layer in a compression molding mode is arranged between the lower die and the cover plate.
Furthermore, in the step 2c), a groove is formed at the lap joint part of the air bag heat insulation layer rubber sheet and the air bag heat layer rubber sheet.
Further, in the step 2d), the pre-pressing treatment specifically comprises the following steps: and sequentially laying polytetrafluoroethylene glass fiber demolding cloth, the breathable felt and the vacuum bag film on the surface of the heat insulation layer film, finally sealing the edge of the vacuum bag film with a sealing rubber strip for an air bag forming tool, ensuring that the vacuumizing pipe is connected with a vacuum pump to vacuumize after air leakage does not occur, and keeping the vacuumizing pipe in a vacuum state for 20-40 min.
Further, in the step 2e), the specific process of the inflation molding of the airbag is as follows: adjusting the inflation pressure to 0.6-0.8 MPa to slowly inflate the air bag, disconnecting the air source after the inflation is finished, starting the oven to heat, preserving the heat for 3-5 h when the temperature is raised to 140-160 ℃, and cutting off the power and reducing the temperature after the heat preservation is finished.
Compared with the prior art, the invention has the following advantages: according to the method for forming the heat insulating layer of the large-size end socket, the part (generally, the area with the heat insulating layer thickness exceeding 20 mm) with the thicker heat insulating layer around the metal joint is formed in a mould pressing mode, then the part with the thicker heat insulating layer is placed into an air bag forming tool, and the air bag is used for pressure forming after the part is pasted, so that the tool cost can be reduced, equipment investment is not needed, and the production cost is greatly reduced. In addition, the air bag forming tool is composed of a lower die and a cover plate, is connected with an air source to inflate after being assembled with the air bag, then is heated by the oven as a whole, and meanwhile realizes pressurization.
Drawings
Fig. 1 is a schematic structural diagram of the insulation layer of the end socket.
Detailed Description
The present invention will be described in further detail with reference to specific examples.
A method for forming a large-size end socket heat insulation layer comprises the following steps of:
1) the insulating layer 2 of the metal joint is formed by compression molding (the region with the thickness of the insulating layer exceeding 20mm is formed by compression molding)
1a) Cleaning the inner surface and the outer surface of the metal joint by ethyl acetate, then airing, coating primer on the inner surface and the outer surface of the metal joint, then airing, coating face glue on the surface of the primer, and simultaneously coating face glue on the inner surface and the outer surface of the molded heat insulation layer film, and airing;
1b) sticking the mould pressing heat insulation layer rubber sheets on the inner surface and the outer surface of the metal joint until the thickness of the mould pressing heat insulation layer rubber sheets on the outer surface of the metal joint is consistent with the thickness of the outer layer of the heat insulation layer of the end socket, and the thickness of the mould pressing heat insulation layer rubber sheets on the inner surface of the metal joint is half of the thickness of the inner layer of the heat insulation layer of the end socket;
after the sticking is finished, putting the metal connector into a mould pressing tool, and continuously sticking a mould pressing heat insulation layer rubber sheet according to the thickness of the inner layer of the end socket heat insulation layer until the thickness of the mould pressing heat insulation layer rubber sheet on the inner surface of the metal connector is consistent with the thickness of the inner layer of the end socket heat insulation layer;
1c) after the surface mounting is finished, closing the die, and putting the die pressing tool on a flat vulcanizing machine for vulcanization;
the specific vulcanization process is as follows: starting a vulcanizing machine, performing cold pressing for 2-4 times at a gauge pressure of 3-4 MPa; heating the mould to 80-100 ℃, then preserving heat for 40-60 min, pressurizing to 3-5 MPa after heat preservation is finished, exhausting for 2-4 times, and finally pressurizing to 3-5 MPa; continuously heating to 110-130 ℃, and exhausting for 2-4 times; then heating to 140-160 ℃, pressurizing to 5-7 MPa, and keeping the temperature for 60-90 min; cutting off the power and reducing the temperature after the heat preservation is finished;
1d) the mould pressing tool is opened when the temperature of the mould pressing tool is reduced to below 60 ℃ along with the equipment, the bottom layer is demoulded, and the flash is cleaned to obtain a compression-molded heat insulation layer;
2) air bag pressure forming heat insulating layer 4
2a) Polishing the bonding surface 3 of the heat insulating layer 2 formed by compression molding until fluffing, carrying out light inspection without reflection, and then cleaning and drying by using reagents such as alcohol, acetone or ethyl acetate; finally brushing an adhesive on the bonding surface of the heat-insulating layer subjected to compression molding and drying;
2b) assembling an air bag forming tool with a metal joint which is compression-molded and provided with a heat insulating layer, wherein the air bag forming tool comprises a lower die and a cover plate, and the metal joint which is compression-molded and provided with the heat insulating layer is arranged between the lower die and the cover plate;
2c) coating an adhesive on the air bag heat insulating layer film bonded with the compression-molded heat insulating layer bonding surface, drying in the air, bonding the air bag heat insulating layer film on the compression-molded heat insulating layer bonding surface, finally performing air bag heat insulating layer film pasting according to the molding surface of the end enclosure, and performing groove treatment on the lap joint part of the air bag heat insulating layer film and the air bag heat insulating layer film;
2d) after the mounting is finished, performing vacuum bag making prepressing treatment, sequentially laying polytetrafluoroethylene glass fiber demolding cloth, an air-permeable felt and a vacuum bag film on the surface of the heat insulation layer film, finally sealing the edge of the vacuum bag film with a sealing rubber strip for an air bag forming tool, ensuring that the air is not leaked, connecting a vacuum-pumping pipe with a vacuum pump for vacuum pumping, and keeping the vacuum state for 20-40 min;
2e) taking down the vacuum tube, removing the sealant, the vacuum bag film, the air felt and the polytetrafluoroethylene glass fiber demoulding cloth, polishing the uneven position on the surface of the preformed heat insulation layer to be flat, and performing comparison inspection by using a profile sample plate to ensure that the profile meets the requirements;
2f) assembling an air bag and an air bag forming tool, then integrally placing the air bag and the air bag forming tool into an oven and connecting a nitrogen source, adjusting the inflation pressure to be 0.6-0.8 MPa to slowly inflate the air bag, disconnecting the air source after inflation is finished, starting the oven to heat, preserving the heat for 3-5 h when the temperature is raised to 140-160 ℃, and reducing the temperature after heat preservation is finished;
2g) and cooling to below 40 ℃, deflating the air bag, opening the air bag forming tool, demolding and cleaning the flash.
According to the method for forming the heat insulating layer of the large-size end socket, the part (generally, the area with the heat insulating layer thickness exceeding 20 mm) with the thicker heat insulating layer around the metal joint is formed in a mould pressing mode, then the part with the thicker heat insulating layer is placed into an air bag forming tool, and the air bag is used for pressure forming after the part is pasted, so that the tool cost can be reduced, equipment investment is not needed, and the production cost is greatly reduced. In addition, the air bag forming tool is composed of a lower die and a cover plate, is connected with an air source to inflate after being assembled with the air bag, then is heated by the oven as a whole, and meanwhile realizes pressurization.

Claims (7)

1. A method for forming a heat insulating layer of a large-size end socket comprises a metal connector and the heat insulating layer, and is characterized in that: the heat insulation layer forming method specifically comprises the following steps:
1) compression molding heat insulating layer of metal joint
1a) Coating primer on the inner and outer surfaces of the metal joint, then drying the metal joint in the air, coating surface glue on the surface of the primer, drying the metal joint in the air, and simultaneously coating surface glue on the inner and outer surfaces of the molded heat insulation layer rubber and drying the metal joint in the air;
1b) sticking the mould pressing heat insulation layer rubber sheets on the inner surface and the outer surface of the metal joint until the thickness of the mould pressing heat insulation layer rubber sheets on the outer surface of the metal joint is consistent with the thickness of the outer layer of the heat insulation layer of the end socket, and the thickness of the mould pressing heat insulation layer rubber sheets on the inner surface of the metal joint is half of the thickness of the inner layer of the heat insulation layer of the end socket;
after the sticking is finished, putting the metal connector into a mould pressing tool, and continuously sticking a mould pressing heat insulation layer rubber sheet according to the thickness of the inner layer of the end socket heat insulation layer until the thickness of the mould pressing heat insulation layer rubber sheet on the inner surface of the metal connector is consistent with the thickness of the inner layer of the end socket heat insulation layer;
1c) after the surface mounting is finished, closing the die, and putting the die pressing tool on a flat vulcanizing machine for vulcanization;
1d) cooling the mould pressing tool along with the equipment, opening the mould pressing tool, demolding the bottom layer, and cleaning the flash to obtain a compression-molded heat insulation layer;
2) air bag pressure forming heat insulating layer
2a) Polishing the bonding surface of the heat-insulating layer subjected to compression molding until fluffing, brushing an adhesive on the bonding surface of the heat-insulating layer subjected to compression molding, and drying;
2b) assembling an air bag forming tool with a metal joint which is compression-molded with a heat insulating layer;
2c) coating an adhesive on the airbag heat-insulating layer adhesive sheet adhered to the heat-insulating layer adhesive surface subjected to compression molding, drying in the air, adhering the airbag heat-insulating layer adhesive sheet to the heat-insulating layer adhesive surface subjected to compression molding, and finally adhering the airbag heat-insulating layer adhesive sheet according to the molded surface of the end enclosure;
2d) after the surface mounting is finished, performing vacuum bag making prepressing treatment, polishing and flattening the uneven positions on the surface of the preformed heat insulation layer, and performing contrast inspection by using a profile template;
2e) assembling the air bag and an air bag forming tool, and then integrally placing the air bag and the air bag forming tool into an oven and connecting a nitrogen source to carry out air bag inflation forming;
2f) and (4) deflating the air bag after cooling, opening the air bag forming tool, demolding and cleaning the flash.
2. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 1c), the specific vulcanization process is as follows: starting a vulcanizing machine, performing cold pressing for 2-4 times at a gauge pressure of 3-4 MPa; heating the mould to 80-100 ℃, then preserving heat for 40-60 min, pressurizing to 3-5 MPa after heat preservation is finished, exhausting for 2-4 times, and finally pressurizing to 3-5 MPa; continuously heating to 110-130 ℃, and exhausting for 2-4 times; then heating to 140-160 ℃, pressurizing to 5-7 MPa, and keeping the temperature for 60-90 min; and cutting off the power and reducing the temperature after the heat preservation is finished.
3. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 1d), the mould pressing tool is opened when the temperature of the mould pressing tool is reduced to below 60 ℃ along with the equipment.
4. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 2b), the air bag forming tool comprises a lower die and a cover plate, and a metal joint in which a heat insulating layer is formed in a compression molding mode is arranged between the lower die and the cover plate.
5. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 2c), a groove is formed at the lap joint part of the air bag heat insulation layer rubber sheet and the air bag heat layer rubber sheet.
6. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 2d), the pre-pressing treatment specifically comprises the following steps: and sequentially laying polytetrafluoroethylene glass fiber demolding cloth, the breathable felt and the vacuum bag film on the surface of the heat insulation layer film, finally sealing the edge of the vacuum bag film with a sealing rubber strip for an air bag forming tool, ensuring that the vacuumizing pipe is connected with a vacuum pump to vacuumize after air leakage does not occur, and keeping the vacuumizing pipe in a vacuum state for 20-40 min.
7. The method for forming a heat insulating layer of a large-size end socket according to claim 1, wherein: in the step 2e), the specific process of the air bag inflation molding is as follows: adjusting the inflation pressure to 0.6-0.8 MPa to slowly inflate the air bag, disconnecting the air source after the inflation is finished, starting the oven to heat, preserving the heat for 3-5 h when the temperature is raised to 140-160 ℃, and cutting off the power and reducing the temperature after the heat preservation is finished.
CN202111313053.5A 2021-11-08 2021-11-08 Forming method of large-size seal head heat insulation layer Active CN114179392B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114701187A (en) * 2022-04-01 2022-07-05 湖北三江航天江北机械工程有限公司 Adiabatic head gasbag forming device

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CN109838321A (en) * 2017-11-27 2019-06-04 湖北航天化学技术研究所 A kind of solid propellant rocket rear head insulating structure and forming method
CN111516196A (en) * 2020-04-10 2020-08-11 北京玻钢院复合材料有限公司 Composite material solid rocket engine heat insulation layer structure and preparation method thereof
CN112192862A (en) * 2020-10-19 2021-01-08 北京蓝科盈晟航空科技有限公司 Preparation method of composite material rocket engine shell
CN112497587A (en) * 2020-10-27 2021-03-16 湖北三江航天江北机械工程有限公司 Method for forming heat insulating layer of fiber-wound engine end socket
CN113147055A (en) * 2021-04-28 2021-07-23 湖北航天技术研究院总体设计所 Preparation method of composite material shell of solid rocket engine

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Publication number Priority date Publication date Assignee Title
KR20120111132A (en) * 2011-03-31 2012-10-10 박찬희 Curing process of pressure or vacuum for pressure vessel of wet filament winding
CN105437521A (en) * 2015-12-04 2016-03-30 湖北三江航天江北机械工程有限公司 Seal head heat insulating layer forming method and mold of filament winding engine heat insulating structure
CN107584771A (en) * 2016-11-03 2018-01-16 湖北航天化学技术研究所 Solid propellant rocket internal insulation forming method
CN109838321A (en) * 2017-11-27 2019-06-04 湖北航天化学技术研究所 A kind of solid propellant rocket rear head insulating structure and forming method
CN111516196A (en) * 2020-04-10 2020-08-11 北京玻钢院复合材料有限公司 Composite material solid rocket engine heat insulation layer structure and preparation method thereof
CN112192862A (en) * 2020-10-19 2021-01-08 北京蓝科盈晟航空科技有限公司 Preparation method of composite material rocket engine shell
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114701187A (en) * 2022-04-01 2022-07-05 湖北三江航天江北机械工程有限公司 Adiabatic head gasbag forming device

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