CN114176094A - Chlorine dioxide disinfectant and preparation method thereof - Google Patents
Chlorine dioxide disinfectant and preparation method thereof Download PDFInfo
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- CN114176094A CN114176094A CN202111176048.4A CN202111176048A CN114176094A CN 114176094 A CN114176094 A CN 114176094A CN 202111176048 A CN202111176048 A CN 202111176048A CN 114176094 A CN114176094 A CN 114176094A
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- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
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- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses a chlorine dioxide disinfectant and a preparation method thereof, and relates to the technical field of preparation of chlorine dioxide disinfectants. The chlorine dioxide disinfectant comprises the following components, by mass, 65-85 parts of desalted water; 0.12-0.18 part of sodium chlorite with the purity of 78-80 percent; 0.08-0.16 part of activating agent; 1.5-3.0 parts of organic complexing agent; 0.001-0.002 part of inorganic complexing agent, and a preparation method of chlorine dioxide disinfectant, comprising the following steps of S1, pouring desalted water, sodium chlorite and an activating agent into a mixing cylinder, and mixing and stirring under the heating condition to obtain a mixture; s2, adding an organic complexing agent into the prepared mixture, and maintaining the temperature of the mixture at 35 ℃. The chlorine dioxide disinfectant and the preparation method thereof are provided with the stirring mechanism and the moving mechanism, so that raw materials on the inner side of the mixing cylinder are fully stirred, and the raw materials attached to the inner side of the device are continuously shaken off while stirring, so that the raw materials are prevented from being unevenly mixed, the raw materials are prevented from being attached to the inner side of the device, and the yield of the disinfectant is reduced.
Description
Technical Field
The invention relates to the technical field of preparation of chlorine dioxide disinfectants, in particular to a chlorine dioxide disinfectant and a preparation method thereof.
Background
Chlorine dioxide is the latest generation of safe, efficient and broad-spectrum sterilizing, fresh-keeping and deodorizing agent internationally acknowledged at present, is the most ideal substitute of a chlorine preparation, has been widely applied in China, and is widely popularized and applied to replace chlorine gas to sterilize drinking water in order to control the generation of 'three-causing substances' (teratogenicity, carcinogenesis and mutation) in drinking water, the national ministry of health has also approved chlorine dioxide as a disinfectant and a novel food additive, and the preparation of chlorine dioxide disinfectant becomes more standard and efficient.
However, when the chlorine dioxide disinfectant preparation device is used, raw materials in the mixing cylinder cannot be quickly and uniformly mixed, and when the prepared disinfectant is collected, part of the disinfectant is attached to the stirring piece on the inner side of the mixing cylinder, so that the collection difficulty is increased, and the yield of the disinfectant is reduced.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a chlorine dioxide disinfectant and a preparation method thereof.
In order to achieve the purpose, the invention is realized by the following technical scheme: a chlorine dioxide disinfectant comprises the following components, 65-85 parts of desalted water; 0.12-0.18 part of sodium chlorite with the purity of 78-80 percent; 0.08-0.16 part of activating agent; 1.5-3.0 parts of organic complexing agent; 0.001-0.002 part of inorganic complexing agent.
A preparation method of a chlorine dioxide disinfectant comprises the following steps.
S1, pouring the desalted water, the sodium chlorite and the activating agent into a mixing cylinder, and mixing and stirring under the heating condition to obtain a mixture;
s2, adding an organic complexing agent into the prepared mixture, and maintaining the temperature of the mixture at 35 ℃;
and S3, stirring the mixture again, dropwise adding an inorganic complexing agent, and adjusting the pH value to weak acidity to obtain the chlorine dioxide disinfectant.
Preferably, the outer fixed surface of the mixing drum is provided with a supporting leg, the front center of the mixing drum is provided with a motor through a fixed column, the outer surface of the mixing drum is far away from the supporting leg and is rotatably provided with a rotating plate, the inner side of the mixing drum is provided with a stirring mechanism, the inner side of the mixing drum is provided with a movable mechanism, and the outer surface of the mixing drum is far away from the rotating plate and is fixedly provided with a discharge valve.
Preferably, rabbling mechanism includes axis of rotation, arc contact plate, cavity, friction tooth and extensible member, the axis of rotation is rotated and is installed at the inboard center of mixing drum, the front of axis of rotation runs through the mixing drum and the output shaft of motor meets, arc contact plate fixed mounting is at the surface of axis of rotation, the inboard at the arc contact plate is seted up to the cavity, friction tooth fixed mounting is in the inboard of cavity, the friction tooth meets with the inner wall of arc contact plate, the extensible member sets up the surface at the axis of rotation.
Preferably, the extensible member includes counter weight magnetic column and elastic strip, counter weight magnetic column fixed mounting is in the one end that the axis of rotation was kept away from to the arc contact plate, elastic strip fixed mounting is in the surface of axis of rotation, the one end that the axis of rotation was kept away from to the elastic strip meets with counter weight magnetic column.
Preferably, the movable mechanism comprises a strip-shaped opening, a deformation piece and a movable piece, the strip-shaped opening is formed in the outer surface of the mixing cylinder, the deformation piece is arranged on the inner side of the mixing cylinder, and the movable piece is arranged on the inner side of the mixing cylinder.
Preferably, the deformation piece includes elasticity curb plate, through-hole, spacing ring and activity magnetism post, elasticity curb plate fixed mounting is at the inner wall of mixing drum, the inboard cavity of elasticity curb plate, the one side of axis of rotation is kept away from at the elasticity curb plate is seted up to the through-hole, the through-hole meets with the bar mouth, spacing ring fixed mounting is in the inboard of elasticity curb plate, activity magnetism post movable mounting is in the inboard of elasticity curb plate, the activity magnetism post meets with the spacing ring through the elastic component, the activity magnetism post is inhaled with counter weight magnetism post magnetism mutually.
Preferably, the moving part includes corrugated membrane and activity ball, corrugated membrane fixed mounting is at the inner wall of mixing drum, the one end that the rotor plate was kept away from to the corrugated membrane meets with the surface of elasticity curb plate, the corrugated membrane switches on mutually with the inboard of elasticity curb plate, the activity ball passes through elasticity post fixed mounting and keeps away from one side of axis of rotation at the corrugated membrane.
The invention provides a chlorine dioxide disinfectant and a preparation method thereof. The method has the following beneficial effects:
(1) the chlorine dioxide disinfectant and the preparation method thereof are provided with the stirring mechanism and the moving mechanism, so that raw materials on the inner side of the mixing cylinder are fully stirred, and the raw materials attached to the inner side of the device are shaken off continuously while stirring, so that the raw materials are prevented from being unevenly mixed, the raw materials are prevented from being attached to the inner side of the device, and the yield of the disinfectant is reduced.
(2) When the rotating shaft rotates, the counterweight magnetic column is pressed close to the inner wall of the mixing drum by centrifugal force, the counterweight magnetic column drives the arc contact plate to deform, and the arc contact plate contacts with raw materials when rotating to the bottom of the mixing drum, so that the raw materials are stirred, the raw materials are quickly mixed, and the phenomenon that the raw materials are not uniformly mixed is avoided.
(3) This chlorine dioxide disinfectant and preparation method, when the arc contact plate contacts the raw materials, receive the resistance of raw materials, and the power that same group of arc contact plate received varies in magnitude, counter weight magnetic column takes place to deflect, when the raw materials was kept away from to the arc contact plate, the resistance that receives reduces, counter weight magnetic column begins to reply, receive the elastic influence of arc contact plate when counter weight magnetic column replies, constantly take place the swing in the outside of axis of rotation, when counter weight magnetic column rotates to the top, the gravity of counter weight magnetic column is greater than the centrifugal force that receives, the arc contact plate that counter weight magnetic column compression was connected with it this moment, the arc contact plate constantly takes place deformation when the axis of rotation rotates, constantly shake off adnexed raw materials, the surface at the arc contact plate has been avoided the raw materials to adhere to, influence the productivity of disinfectant.
(4) When the arc contact plate is continuously deformed, friction is continuously generated between the friction teeth on the inner side of the cavity, and heat generated by the friction is transferred to the arc contact plate, so that the temperature of the arc contact plate is increased, and raw materials are prevented from being condensed on the arc contact plate.
(5) This chlorine dioxide disinfectant and preparation method, when the counter weight magnetic column moves about in the mixing drum inboard, reciprocal activity magnetic column of pressing close to, activity magnetic column receives the constantly tensile elasticity curb plate of magnetic attraction, when elasticity curb plate deformation, the constantly increase in inboard space is dwindled, the air constantly inhales and discharges, the ripple membrane that meets with the elasticity curb plate this moment receives the influence of air current, take place vibrations, under the cooperation of activity ball, vibrations aggravate, the raw materials that will attach to the bottom constantly shakes off to the mixing drum in, the loss of raw materials has been reduced.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the present invention;
FIG. 3 is a schematic view of the structure of the elastic side plate according to the present invention;
FIG. 4 is a cross-sectional view of the resilient side panel of the present invention;
FIG. 5 is an enlarged view of the structure of FIG. 4 at A in accordance with the present invention;
FIG. 6 is a schematic view of the structure of the counterweight magnetic column according to the present invention;
fig. 7 is a structural cross-sectional view of an arcuate contact plate portion of the present invention.
In the figure: 1. a mixing drum; 2. supporting legs; 3. a motor; 4. a rotating plate; 5. a stirring mechanism; 51. a rotating shaft; 52. an arc-shaped contact plate; 53. a cavity; 54. friction teeth; 55. a telescoping member; 551. a counterweight magnetic column; 552. an elastic strip; 6. a movable mechanism; 61. a strip-shaped opening; 62. a deformation member; 621. an elastic side plate; 622. a through hole; 623. a limiting ring; 624. a movable magnetic column; 63. a movable member; 631. a corrugated membrane; 632. a movable ball; 7. a discharge valve.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Examples of which are illustrated in the accompanying drawings, wherein like reference numerals refer to the same or similar elements or elements having the same or similar function throughout. The embodiments described below with reference to the drawings are illustrative and intended to be illustrative of the invention and are not to be construed as limiting the invention.
Referring to fig. 1-7, the present invention provides a technical solution: a chlorine dioxide disinfectant comprises the following components, 65-85 parts of desalted water; 0.12-0.18 part of sodium chlorite with the purity of 78-80 percent; 0.08-0.16 part of activating agent; 1.5-3.0 parts of organic complexing agent; 0.001-0.002 part of inorganic complexing agent.
A preparation method of a chlorine dioxide disinfectant comprises the following steps,
s1, pouring the desalted water, the sodium chlorite and the activating agent into the mixing cylinder 1, and mixing and stirring under the heating condition to obtain a mixture;
s2, adding an organic complexing agent into the prepared mixture, and maintaining the temperature of the mixture at 35 ℃;
and S3, stirring the mixture again, dropwise adding an inorganic complexing agent, and adjusting the pH value to weak acidity to obtain the chlorine dioxide disinfectant.
The fixed surface of mixing drum 1 installs supporting leg 2, and there is motor 3 at the front center of mixing drum 1 through fixed column fixed mounting, and the supporting leg 2 department of keeping away from of the surface of mixing drum 1 rotates and installs rotor plate 4, and the inboard of mixing drum 1 is provided with rabbling mechanism 5, and the inboard of mixing drum 1 is provided with moving mechanism 6, and the rotor plate 4 department fixed mounting is kept away from to the surface of mixing drum 1 has bleeder valve 7.
The stirring mechanism 5 comprises a rotating shaft 51, an arc contact plate 52, a cavity 53, a friction tooth 54 and a telescopic piece 55, wherein the rotating shaft 51 is rotatably installed at the center of the inner side of the mixing drum 1, the front surface of the rotating shaft 51 penetrates through the front surface of the mixing drum 1 to be connected with an output shaft of the motor 3, the arc contact plate 52 is fixedly installed on the outer surface of the rotating shaft 51, the cavity 53 is arranged on the inner side of the arc contact plate 52, the friction tooth 54 is fixedly installed on the inner side of the cavity 53, the friction tooth 54 is connected with the inner wall of the arc contact plate 52, the telescopic piece 55 is arranged on the outer surface of the rotating shaft 51, the telescopic piece 55 comprises a counterweight magnetic column 551 and an elastic strip 552, the counterweight magnetic column 551 is fixedly installed at one end of the arc contact plate 52 far away from the rotating shaft 51, the elastic strip 552 is fixedly installed on the outer surface of the rotating shaft 51, and one end of the elastic strip 552 far away from the rotating shaft 51 is connected with the counterweight magnetic column 551.
The movable mechanism 6 comprises a strip-shaped opening 61, a deformation piece 62 and a movable piece 63, the strip-shaped opening 61 is arranged on the outer surface of the mixing cylinder 1, the deformation piece 62 is arranged on the inner side of the mixing cylinder 1, the deformation piece 62 comprises an elastic side plate 621, a through hole 622, a limiting ring 623 and a movable magnetic column 624, the elastic side plate 621 is fixedly arranged on the inner wall of the mixing cylinder 1, the inner side of the elastic side plate 621 is hollow, the through hole 622 is arranged on one side of the elastic side plate 621 away from the rotating shaft 51, the through hole 622 is connected with the strip-shaped opening 61, the limiting ring 623 is fixedly arranged on the inner side of the elastic side plate 621, the movable magnetic column 624 is movably arranged on the inner side of the elastic side plate 621, the movable magnetic column 624 is connected with the limiting ring 623 through an elastic piece, the movable magnetic column 624 is magnetically attracted with a counterweight magnetic column 551, the movable piece 63 is arranged on the inner side of the mixing cylinder 1, the movable piece 63 comprises a corrugated film 631 and a movable ball 632, the corrugated film 631 is fixedly arranged on the inner wall of the mixing cylinder 1, one end of the corrugated membrane 631, which is far away from the rotating plate 4, is connected to the outer surface of the elastic side plate 621, the corrugated membrane 631 is connected to the inner side of the elastic side plate 621, and the movable ball 632 is fixedly mounted on one side of the corrugated membrane 631, which is far away from the rotating shaft 51, through an elastic column.
When the mixing device is used, the rotating plate 4 is rotated, raw materials are poured into the mixing barrel 1, the switch of the motor 3 is turned on, the motor 3 works to drive the rotating shaft 51 to rotate, when the rotating shaft 51 rotates, the counterweight magnetic column 551 is close to the inner wall of the mixing barrel 1 by centrifugal force, the counterweight magnetic column 551 drives the arc contact plate 52 to deform, the arc contact plate 52 contacts with the raw materials when rotating to the bottom of the mixing barrel 1, the raw materials are stirred, the raw materials are quickly mixed, the raw materials are prevented from being mixed unevenly, the raw materials generate resistance to the arc contact plate 52, the resistance of the arc contact plate 52 which is consistent with the rotating direction is larger than the resistance of the other arc contact plate 52 which is connected with the counterweight magnetic column 551, because of the unequal stress magnitude, the counterweight magnetic column 551 deflects, when the arc contact plate 52 is far away from the raw materials, the resistance is reduced, the counterweight magnetic column 551 starts to recover, and the counterweight magnetic column 551 is influenced by the elasticity of the arc contact plate 52, constantly swings outside the rotating shaft 51, when the counterweight magnetic column 551 rotates to the top, the gravity of the counterweight magnetic column 551 is larger than the centrifugal force, at this time, the counterweight magnetic column 551 compresses the arc contact plate 52 connected with the counterweight magnetic column 551, the arc contact plate 52 constantly deforms when the rotating shaft 51 rotates, the attached raw material is constantly shaken off, the raw material is prevented from being attached to the outer surface of the arc contact plate 52, the yield of the disinfectant is affected, when the arc contact plate 52 constantly deforms, the friction between the friction teeth 54 inside the cavity 53 constantly occurs, the heat generated by the friction is transferred to the arc contact plate 52, the temperature of the arc contact plate 52 is increased, the raw material is prevented from being condensed on the arc contact plate 52, when the counterweight magnetic column 551 moves inside the mixing cylinder 1, the counterweight magnetic column 551 reciprocally approaches the movable magnetic column 624, the movable magnetic column 624 constantly stretches the elastic side plate 621 by the magnetic suction force, and the elastic side plate 621 deforms, when elasticity curb plate 621 deformed, the space of inboard constantly increases and dwindles, and the air constantly inhales and discharges, and the ripple membrane 631 that meets with elasticity curb plate 621 this moment receives the influence of air current, takes place vibrations, under movable ball 632's cooperation, vibrations aggravation will be attached to the raw materials of bottom and constantly shake off to mixing drum 1 in, reduced the loss of raw materials.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. A chlorine dioxide disinfectant, characterized in that: the water-based paint comprises the following components, by mass, 65-85 parts of desalted water; 0.12-0.18 part of sodium chlorite with the purity of 78-80 percent; 0.08-0.16 part of activating agent; 1.5-3.0 parts of organic complexing agent; 0.001-0.002 part of inorganic complexing agent.
2. A method of producing a chlorine dioxide disinfectant as recited in claim 1, wherein: comprises the following steps of (a) carrying out,
s1, pouring the desalted water, the sodium chlorite and the activating agent into the mixing cylinder (1), and mixing and stirring under the heating condition to obtain a mixture;
s2, adding an organic complexing agent into the prepared mixture, and maintaining the temperature of the mixture at 35 ℃;
and S3, stirring the mixture again, dropwise adding an inorganic complexing agent, and adjusting the pH value to weak acidity to obtain the chlorine dioxide disinfectant.
3. A method of producing a chlorine dioxide disinfectant as set forth in claim 2, wherein: the utility model discloses a mixer, including mixing drum (1), supporting leg (2) are installed to the surface fixed mounting of mixing drum (1), there is motor (3) at the front center of mixing drum (1) through fixed column fixed mounting, supporting leg (2) department is kept away from to the surface of mixing drum (1) rotates and installs rotor plate (4), the inboard of mixing drum (1) is provided with rabbling mechanism (5), the inboard of mixing drum (1) is provided with moving mechanism (6), rotor plate (4) department fixed mounting is kept away from to the surface of mixing drum (1) has bleeder valve (7).
4. A method of producing a chlorine dioxide disinfectant as set forth in claim 3, wherein: stirring mechanism (5) are including axis of rotation (51), arc contact plate (52), cavity (53), friction tooth (54) and extensible member (55), axis of rotation (51) are rotated and are installed at the inboard center of mixing drum (1), the front that runs through mixing drum (1) in the front of axis of rotation (51) meets with the output shaft of motor (3), arc contact plate (52) fixed mounting is in the surface of axis of rotation (51), the inboard in arc contact plate (52) is seted up in cavity (53), friction tooth (54) fixed mounting is in the inboard of cavity (53), friction tooth (54) meet with the inner wall of arc contact plate (52), extensible member (55) set up the surface in axis of rotation (51).
5. A method of producing a chlorine dioxide disinfectant as claimed in claim 4, wherein: the telescopic piece (55) comprises a counterweight magnetic column (551) and an elastic strip (552), the counterweight magnetic column (551) is fixedly installed at one end, away from the rotating shaft (51), of the arc-shaped contact plate (52), the elastic strip (552) is fixedly installed on the outer surface of the rotating shaft (51), and one end, away from the rotating shaft (51), of the elastic strip (552) is connected with the counterweight magnetic column (551).
6. A method of producing a chlorine dioxide disinfectant as set forth in claim 3, wherein: the movable mechanism (6) comprises a bar-shaped opening (61), a deformation piece (62) and a movable piece (63), the bar-shaped opening (61) is formed in the outer surface of the mixing cylinder (1), the deformation piece (62) is arranged on the inner side of the mixing cylinder (1), and the movable piece (63) is arranged on the inner side of the mixing cylinder (1).
7. A method of producing a chlorine dioxide disinfectant as set forth in claim 6, wherein: deformation piece (62) are including elasticity curb plate (621), through-hole (622), spacing ring (623) and activity magnetic column (624), elasticity curb plate (621) fixed mounting is at the inner wall of mixing section of thick bamboo (1), elasticity curb plate (621) inboard cavity, one side of axis of rotation (51) is kept away from in elasticity curb plate (621) is seted up in through-hole (622), through-hole (622) meet with bar mouth (61), spacing ring (623) fixed mounting is in the inboard of elasticity curb plate (621), activity magnetic column (624) movable mounting is in the inboard of elasticity curb plate (621), activity magnetic column (624) meet with spacing ring (623) through the elastic component, activity magnetic column (624) and counter weight magnetic column (551) magnetism attract mutually.
8. A method of producing a chlorine dioxide disinfectant as set forth in claim 7, wherein: the moving part (63) comprises a corrugated membrane (631) and a movable ball (632), the corrugated membrane (631) is fixedly installed on the inner wall of the mixing cylinder (1), one end of the rotating plate (4) is far away from the corrugated membrane (631) and the outer surface of the elastic side plate (621) are connected, the corrugated membrane (631) is communicated with the inner side of the elastic side plate (621), and the movable ball (632) is fixedly installed on one side of the corrugated membrane (631) far away from the rotating shaft (51) through an elastic column.
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| CN202111176048.4A CN114176094B (en) | 2021-10-09 | 2021-10-09 | Chlorine dioxide disinfectant and preparation method thereof |
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| CN113368737A (en) * | 2021-05-17 | 2021-09-10 | 符作强 | Prevent formula of agglomerating bio-fertilizer mixing arrangement |
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| CN113304677B (en) * | 2021-06-28 | 2022-01-25 | 丰县立华牧业有限公司 | Fodder compounding device for animal husbandry |
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| US20050146062A1 (en) * | 2003-11-17 | 2005-07-07 | Koch-Glitsch, Lp | Method and apparatus for facilitating more uniform vapor distribution in mass transfer and heat exchange columns |
| CN207391377U (en) * | 2017-09-07 | 2018-05-22 | 重庆市红槽坊酒业有限公司 | A kind of liquor production material blending device |
| CN211246188U (en) * | 2019-12-10 | 2020-08-14 | 大名县方源本草生物科技有限公司 | Cereal balance meal multi-raw material mixing device |
| CN111972431A (en) * | 2020-08-18 | 2020-11-24 | 王禹 | Organic stable chlorine dioxide disinfectant and preparation method thereof |
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