CN114150028A - Preparation process of fermented maltose syrup - Google Patents

Preparation process of fermented maltose syrup Download PDF

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Publication number
CN114150028A
CN114150028A CN202111425196.5A CN202111425196A CN114150028A CN 114150028 A CN114150028 A CN 114150028A CN 202111425196 A CN202111425196 A CN 202111425196A CN 114150028 A CN114150028 A CN 114150028A
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container
liquid
maltose syrup
fermentation
starch milk
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CN202111425196.5A
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周明照
殷勇
刘登荣
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Hubei De'anfu Sugar Co ltd
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Hubei De'anfu Sugar Co ltd
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/12Disaccharides
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12PFERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00Preparation of compounds containing saccharide radicals
    • C12P19/14Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase

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  • Engineering & Computer Science (AREA)
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  • Chemical Kinetics & Catalysis (AREA)
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  • General Chemical & Material Sciences (AREA)
  • Biotechnology (AREA)
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  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
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  • Genetics & Genomics (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)

Abstract

The invention discloses a preparation process of fermented maltose syrup, belonging to the technical field of maltose syrup preparation, and comprising the following steps: s1: mixing slurry; s2: liquefying; s3: fermenting; s4: saccharifying; s5: decoloring; s6: filtering; s7: ion exchange; s8: concentrating; s9: filling, sealing, sorting and packaging to obtain a finished maltose syrup product; according to the invention, the contents of the starch milk, the liquefied liquid and the fermentation liquid are respectively measured by the plurality of capacity sensors, and then the liquefied enzyme, the pectinase, the xylanase and the glucoamylase are respectively added according to a certain proportion through the contents of the starch milk, the liquefied liquid and the fermentation liquid.

Description

Preparation process of fermented maltose syrup
Technical Field
The invention belongs to the technical field of malt syrup preparation, and particularly relates to a preparation process of fermented malt syrup.
Background
The maltose syrup is prepared by adopting high-quality corn starch through multiple enzyme hydrolyzations, takes maltose as a main component, has the advantages of high boiling temperature, low freezing point, crystallization resistance and the like, is often used in jam and jelly to prevent the crystallization of granulated sugar, has good expandability, is also widely used in bread, cakes and beer, and is also widely applied to the fields of candies, beverages, food preparation, frozen foods, condiments and the like.
Most of the existing preparation processes of the fermented maltose syrup are added by workers through human experience when the external enzyme is added, the addition amount of the enzyme is not accurate, and the preparation effect of the maltose syrup is reduced.
Disclosure of Invention
To solve the problems set forth in the background art described above. The invention provides a preparation process of fermented maltose syrup, which has the characteristics of relatively accurate enzyme additive amount and capability of improving the overall effect of preparing the maltose syrup.
In order to achieve the purpose, the invention provides the following technical scheme: a preparation process of fermented maltose syrup comprises the following steps:
s1: adding starch milk into a size mixing container, adding sodium carbonate into the size mixing container, stirring and mixing a stirring structure in the size mixing container, determining that the pH value of the starch milk is adjusted to a proper range through a pH sensor, determining the content of the starch milk in the size mixing container through a capacity sensor, adding liquefying enzyme into the size mixing container according to a certain proportion, stirring and mixing the stirring structure in the size mixing container, adjusting the starch milk to a condition suitable for liquefaction, and sending the starch milk into a jet liquefier;
s2: the injection liquefier injects starch milk through the injection port, the starch milk is fully contacted with steam, the steam enables the starch milk to be heated rapidly, the starch chain is opened to enable the starch to be fully liquefied, the injection liquefier injects liquefied liquid through the injection port again to inactivate liquefied enzyme, and the liquefied liquid after secondary injection liquefaction is sent to the fermentation container;
s3: determining the content of liquefied liquid in a fermentation container through a capacity sensor, adding pectinase and xylanase into the fermentation container according to a certain proportion, fermenting for a period of time, and conveying the fermentation liquid into a saccharification container;
s4: adding hydrochloric acid into a saccharification container, stirring and mixing a stirring structure in the saccharification container, determining the pH value of fermentation liquor to be adjusted to a proper range through a pH sensor, determining the content of the fermentation liquor in the saccharification container through a capacity sensor, adding saccharifying enzyme into the saccharification container according to a certain proportion, cutting an opened starch chain into target sugar through the saccharifying enzyme, determining that the content of the saccharified liquor reaches a preset content through a saccharimeter, and sending the saccharified liquor into a decoloring container;
s5: adding activated carbon into the decoloring container, adsorbing protein, fat and a small amount of pigment in the saccharification liquid by the activated carbon to clarify and brighten the saccharification liquid, and sending the saccharification liquid to a plate-and-frame filter;
s6: filtering active carbon in the saccharified liquid by a plate and frame filter, and sending the saccharified liquid to an ion exchange container;
s7: adding anion-cation exchange resin into the ion exchange container, exchanging cations in the saccharified liquid with H + on the cation exchange resin, exchanging anions in the saccharified liquid with OH-on the anion exchange resin, combining the H + and OH-in the saccharified liquid after exchange into water, removing inorganic impurities in the saccharified liquid into corresponding amount of water, and sending the saccharified liquid to a multi-effect vacuum plate evaporator;
s8: maintaining a certain vacuum degree of the multi-effect vacuum plate evaporator to reduce the boiling point, and removing water from the saccharified liquid at a lower temperature to achieve the aim of concentration to prepare the maltose syrup;
s9: the prepared maltose syrup is respectively distributed into a large filling tank and a small filling tank, the maltose syrup in the large filling tank is filled into food-grade glass bottles through a filling structure, the food-grade glass bottles are sealed, the maltose syrup in the small filling tank is filled into food-grade trial-eating packaging bags through the filling structure, the food-grade trial-eating packaging bags are sealed, a single food-grade glass bottle and the single food-grade trial-eating packaging bags are sorted by a sorting machine into a packaging container, and the packaging container is packaged by the packaging machine to prepare a maltose syrup finished product.
Further, in the present invention, in step S1, the PH of the starch milk is preferably in the range of 5.6 to 6.0.
Further, in the present invention, in step S1, the ratio of starch milk to liquefied enzyme is 10: 3-12: 3.5.
further, in the present invention, in step S3, the addition ratio of the liquefied solution, the pectinase and the xylanase is 10: 0.5: 0.6-15: 0.6: 0.8.
further, in the present invention, in the step S3, the duration of the fermentation time is 8-10 h.
Further, in the present invention, in the step S4, the PH of the fermentation liquid is preferably in the range of 5.2 to 5.5.
Further, in the present invention, in step S4, the ratio of the fermentation liquid to the saccharifying enzyme is 2: 0.3-2: 0.5.
further, in the present invention, in the step S4, the predetermined content of the mash is such that the maltose content is equal to or more than 50% or equal to or more than 70%.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, the contents of the starch milk, the liquefied liquid and the fermentation liquid are respectively measured by the plurality of capacity sensors, and then the liquefied enzyme, the pectinase, the xylanase and the glucoamylase are respectively added according to a certain proportion through the contents of the starch milk, the liquefied liquid and the fermentation liquid.
2. The invention divides the prepared maltose syrup into a big filling tank and a small filling tank, the maltose syrup in the big filling tank is filled into food grade glass bottles through a filling structure, the maltose syrup in the small filling tank is filled into food grade trial eating packaging bags through the filling structure, and the food grade glass bottles and the food grade trial eating packaging bags are respectively sealed, a sorting machine sorts the food grade glass bottles and the food grade trial eating packaging bags which are sealed into independent packaging containers, and the packaging containers are packaged through a packaging machine to prepare the finished product of the maltose syrup, the packaging mode in the preparation process has the advantages of bottling of the maltose syrup and the bagged trial eating samples, consumers can eat the bagged trial eating samples before eating the maltose syrup in the bottles, if the taste is not matched, the bottled maltose syrup can be retreated, thereby the shopping satisfaction degree of the consumers can be improved, and the image and reputation of enterprises can be improved, helping enterprises to improve the selling rate of other products.
Drawings
FIG. 1 is a diagram of a process for preparing a fermented maltose syrup of the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
Referring to fig. 1, the present invention provides the following technical solutions: a preparation process of fermented maltose syrup comprises the following steps:
s1: adding starch milk into a size mixing container, adding sodium carbonate into the size mixing container, stirring and mixing a stirring structure in the size mixing container, determining that the pH value of the starch milk is adjusted to a proper range through a pH sensor, determining the content of the starch milk in the size mixing container through a capacity sensor, adding liquefying enzyme into the size mixing container according to a certain proportion, stirring and mixing the stirring structure in the size mixing container, adjusting the starch milk to a condition suitable for liquefaction, and sending the starch milk into a jet liquefier;
s2: the injection liquefier injects starch milk through the injection port, the starch milk is fully contacted with steam, the steam enables the starch milk to be heated rapidly, the starch chain is opened to enable the starch to be fully liquefied, the injection liquefier injects liquefied liquid through the injection port again to inactivate liquefied enzyme, and the liquefied liquid after secondary injection liquefaction is sent to the fermentation container;
s3: determining the content of liquefied liquid in a fermentation container through a capacity sensor, adding pectinase and xylanase into the fermentation container according to a certain proportion, fermenting for a period of time, and conveying the fermentation liquid into a saccharification container;
s4: adding hydrochloric acid into a saccharification container, stirring and mixing a stirring structure in the saccharification container, determining the pH value of fermentation liquor to be adjusted to a proper range through a pH sensor, determining the content of the fermentation liquor in the saccharification container through a capacity sensor, adding saccharifying enzyme into the saccharification container according to a certain proportion, cutting an opened starch chain into target sugar through the saccharifying enzyme, determining that the content of the saccharified liquor reaches a preset content through a saccharimeter, and sending the saccharified liquor into a decoloring container;
s5: adding activated carbon into the decoloring container, adsorbing protein, fat and a small amount of pigment in the saccharification liquid by the activated carbon to clarify and brighten the saccharification liquid, and sending the saccharification liquid to a plate-and-frame filter;
s6: filtering active carbon in the saccharified liquid by a plate and frame filter, and sending the saccharified liquid to an ion exchange container;
s7: adding anion-cation exchange resin into the ion exchange container, exchanging cations in the saccharified liquid with H + on the cation exchange resin, exchanging anions in the saccharified liquid with OH-on the anion exchange resin, combining the H + and OH-in the saccharified liquid after exchange into water, removing inorganic impurities in the saccharified liquid into corresponding amount of water, and sending the saccharified liquid to a multi-effect vacuum plate evaporator;
s8: maintaining a certain vacuum degree of the multi-effect vacuum plate evaporator to reduce the boiling point, and removing water from the saccharified liquid at a lower temperature to achieve the aim of concentration to prepare the maltose syrup;
s9: the prepared maltose syrup is respectively distributed into a large filling tank and a small filling tank, the maltose syrup in the large filling tank is filled into food-grade glass bottles through a filling structure, the food-grade glass bottles are sealed, the maltose syrup in the small filling tank is filled into food-grade trial-eating packaging bags through the filling structure, the food-grade trial-eating packaging bags are sealed, a single food-grade glass bottle and the single food-grade trial-eating packaging bags are sorted by a sorting machine into a packaging container, and the packaging container is packaged by the packaging machine to prepare a maltose syrup finished product.
Specifically, in step S1, the PH of the starch milk is 5.6.
Specifically, in step S1, the ratio of starch milk to liquefied enzyme is 10: 3.
specifically, in step S3, the ratio of the liquefied liquid, the pectinase and the xylanase added is 10: 0.5: 0.6.
specifically, in step S3, the fermentation time period is 8 h.
Specifically, in step S4, the pH of the fermentation broth is 5.2.
Specifically, in step S4, the addition ratio of the fermentation liquid to the saccharifying enzyme is 2: 0.3.
specifically, in step S4, the predetermined content of the mash is such that the maltose content is equal to or greater than 50%.
Example 2
The present embodiment is different from embodiment 1 in that:
specifically, in step S1, the PH of the starch milk is 6.0.
Specifically, in step S1, the ratio of starch milk to liquefied enzyme is 12: 3.5.
specifically, in step S3, the ratio of the liquefied liquid, the pectinase and the xylanase added is 15: 0.6: 0.8.
specifically, in step S3, the fermentation time is 10 hours.
Specifically, in step S4, the pH of the fermentation broth is 5.5.
Specifically, in step S4, the addition ratio of the fermentation liquid to the saccharifying enzyme is 2: 0.5.
specifically, in step S4, the predetermined content of the mash is such that the maltose content is equal to or greater than 70%.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (8)

1. A preparation process of fermented maltose syrup is characterized by comprising the following steps:
s1: adding starch milk into a size mixing container, adding sodium carbonate into the size mixing container, stirring and mixing a stirring structure in the size mixing container, determining that the pH value of the starch milk is adjusted to a proper range through a pH sensor, determining the content of the starch milk in the size mixing container through a capacity sensor, adding liquefying enzyme into the size mixing container according to a certain proportion, stirring and mixing the stirring structure in the size mixing container, adjusting the starch milk to a condition suitable for liquefaction, and sending the starch milk into a jet liquefier;
s2: the injection liquefier injects starch milk through the injection port, the starch milk is fully contacted with steam, the steam enables the starch milk to be heated rapidly, the starch chain is opened to enable the starch to be fully liquefied, the injection liquefier injects liquefied liquid through the injection port again to inactivate liquefied enzyme, and the liquefied liquid after secondary injection liquefaction is sent to the fermentation container;
s3: determining the content of liquefied liquid in a fermentation container through a capacity sensor, adding pectinase and xylanase into the fermentation container according to a certain proportion, fermenting for a period of time, and conveying the fermentation liquid into a saccharification container;
s4: adding hydrochloric acid into a saccharification container, stirring and mixing a stirring structure in the saccharification container, determining the pH value of fermentation liquor to be adjusted to a proper range through a pH sensor, determining the content of the fermentation liquor in the saccharification container through a capacity sensor, adding saccharifying enzyme into the saccharification container according to a certain proportion, cutting an opened starch chain into target sugar through the saccharifying enzyme, determining that the content of the saccharified liquor reaches a preset content through a saccharimeter, and sending the saccharified liquor into a decoloring container;
s5: adding activated carbon into the decoloring container, adsorbing protein, fat and a small amount of pigment in the saccharification liquid by the activated carbon to clarify and brighten the saccharification liquid, and sending the saccharification liquid to a plate-and-frame filter;
s6: filtering active carbon in the saccharified liquid by a plate and frame filter, and sending the saccharified liquid to an ion exchange container;
s7: adding anion-cation exchange resin into the ion exchange container, exchanging cations in the saccharified liquid with H + on the cation exchange resin, exchanging anions in the saccharified liquid with OH-on the anion exchange resin, combining the H + and OH-in the saccharified liquid after exchange into water, removing inorganic impurities in the saccharified liquid into corresponding amount of water, and sending the saccharified liquid to a multi-effect vacuum plate evaporator;
s8: maintaining a certain vacuum degree of the multi-effect vacuum plate evaporator to reduce the boiling point, and removing water from the saccharified liquid at a lower temperature to achieve the aim of concentration to prepare the maltose syrup;
s9: the prepared maltose syrup is respectively distributed into a large filling tank and a small filling tank, the maltose syrup in the large filling tank is filled into food-grade glass bottles through a filling structure, the food-grade glass bottles are sealed, the maltose syrup in the small filling tank is filled into food-grade trial-eating packaging bags through the filling structure, the food-grade trial-eating packaging bags are sealed, a single food-grade glass bottle and the single food-grade trial-eating packaging bags are sorted by a sorting machine into a packaging container, and the packaging container is packaged by the packaging machine to prepare a maltose syrup finished product.
2. The process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in the step S1, the suitable range of the PH value of the starch milk is 5.6-6.0.
3. The process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in the step S1, the ratio of starch milk to liquefied enzyme is 10: 3-12: 3.5.
4. the process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in the step S3, the addition ratio of the liquefied liquid, the pectinase and the xylanase is 10: 0.5: 0.6-15: 0.6: 0.8.
5. the process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in the step S3, the duration of the fermentation period is 8-10 h.
6. The process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in step S4, the PH of the fermentation liquid is preferably in the range of 5.2 to 5.5.
7. The process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in the step S4, the addition ratio of the fermentation liquid to the saccharifying enzyme is 2: 0.3-2: 0.5.
8. the process according to claim 1, wherein the fermentation type maltose syrup is prepared by the following steps: in step S4, the predetermined content of the saccharification liquid is that the maltose content reaches more than or equal to 50% or more than or equal to 70%.
CN202111425196.5A 2021-11-27 2021-11-27 Preparation process of fermented maltose syrup Pending CN114150028A (en)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000189184A (en) * 1998-12-29 2000-07-11 Roquette Freres Preparation of syrup rich in maltose
CN103911409A (en) * 2014-04-09 2014-07-09 孝感市惠隆油脂有限公司 Preparation method of malt syrup
CN112029809A (en) * 2020-09-14 2020-12-04 江苏省奥谷生物科技有限公司 Method for producing high-purity maltose by multi-enzyme synergistic saccharification
CN112852622A (en) * 2021-02-06 2021-05-28 江苏信息职业技术学院 Saccharification equipment and saccharification method
CN214781865U (en) * 2021-02-06 2021-11-19 江苏信息职业技术学院 Saccharification equipment

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2000189184A (en) * 1998-12-29 2000-07-11 Roquette Freres Preparation of syrup rich in maltose
CN103911409A (en) * 2014-04-09 2014-07-09 孝感市惠隆油脂有限公司 Preparation method of malt syrup
CN112029809A (en) * 2020-09-14 2020-12-04 江苏省奥谷生物科技有限公司 Method for producing high-purity maltose by multi-enzyme synergistic saccharification
CN112852622A (en) * 2021-02-06 2021-05-28 江苏信息职业技术学院 Saccharification equipment and saccharification method
CN214781865U (en) * 2021-02-06 2021-11-19 江苏信息职业技术学院 Saccharification equipment

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
夏永军 等: "两级酶解工艺制备超高麦芽糖浆的研究", 食品与发酵科技, vol. 51, no. 2, pages 191 - 192 *

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Application publication date: 20220308