CN114105565A - Ground mortar and preparation method thereof - Google Patents

Ground mortar and preparation method thereof Download PDF

Info

Publication number
CN114105565A
CN114105565A CN202111502529.XA CN202111502529A CN114105565A CN 114105565 A CN114105565 A CN 114105565A CN 202111502529 A CN202111502529 A CN 202111502529A CN 114105565 A CN114105565 A CN 114105565A
Authority
CN
China
Prior art keywords
parts
ground mortar
ground
mortar
cement
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111502529.XA
Other languages
Chinese (zh)
Inventor
薛博宇
尹键丽
陈晓彬
陈湧忠
安小强
朱巧勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xiamen Academy Of Building Science Co ltd
Kezhijie New Material Group Guangdong Co ltd
Original Assignee
Xiamen Academy Of Building Science Co ltd
Kezhijie New Material Group Guangdong Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xiamen Academy Of Building Science Co ltd, Kezhijie New Material Group Guangdong Co ltd filed Critical Xiamen Academy Of Building Science Co ltd
Priority to CN202111502529.XA priority Critical patent/CN114105565A/en
Publication of CN114105565A publication Critical patent/CN114105565A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/60Flooring materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2201/00Mortars, concrete or artificial stone characterised by specific physical values
    • C04B2201/50Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength

Abstract

The invention relates to ground mortar and a preparation method thereof, wherein the ground mortar comprises the following raw materials in parts by weight: 15-25 parts of cement; 25-40 parts of admixture; 25-35 parts of sand; 3-4 parts of a polycarboxylic acid water reducing agent; 2-3 parts of fibers; and (3) water. According to the ground mortar and the preparation method thereof provided by the invention, the fibers are added into the ground mortar, so that the anti-cracking capability of the ground mortar is improved.

Description

Ground mortar and preparation method thereof
Technical Field
The invention relates to the technical field of building materials, in particular to ground mortar and a preparation method thereof.
Background
The ground mortar is a granular or powdery material prepared by physically mixing dry and screened aggregate (such as quartz sand), inorganic cementing material (such as cement), additive (such as polymer) and the like according to a certain proportion, and the ground mortar is transported to a construction site in a bag or in bulk form and is used for leveling the inner and outer ground of a building after being mixed with water.
However, the ground mortar on the market has the problem of poor crack resistance because the ground mortar cracks and expands due to plastic shrinkage, drying shrinkage and temperature change of the ground mortar in the using process.
Disclosure of Invention
Based on the above, the invention provides the ground mortar with strong crack resistance and the preparation method thereof.
The ground mortar comprises the following raw materials in parts by weight:
Figure BDA0003402294850000011
preferably, the admixture includes at least one of mineral powder, coal ash and modified ceramic polishing powder.
Preferably, the fiber includes any one of polypropylene fiber, basalt fiber, carbon fiber, and quartz fiber.
Preferably, the polypropylene fibers have a monofilament length of 6mm and a diameter of 10-20 mm.
Preferably, the preparation raw materials of the ground mortar further comprise, by weight:
2.5 parts of a thickening agent.
Preferably, the thickener includes at least one of an inorganic thickener, an ether-based thickener, and a polyacrylate thickener.
Preferably, the cement comprises at least one of composite portland cement PC32.5 and ordinary portland cement p.o42.5.
Preferably, the fineness modulus of the sand is 2.3-3.2.
The invention also provides a preparation method of the ground mortar, which comprises the following steps:
mixing 15-25 parts of cement, 25-40 parts of admixture, 25-35 parts of sand, 3-4 parts of polycarboxylic acid water reducer, 2-3 parts of fiber and water in parts by weight, and stirring for dissolving to obtain the product, namely the ground mortar.
Preferably, the preparation method of the ground mortar comprises the following steps:
the method comprises the following steps of (1) physically stirring cement, an admixture and sand, and uniformly stirring to obtain a first mixture;
adding water into the first mixture, carrying out hydration reaction on the cement, the admixture and the water, and uniformly stirring to obtain a second mixture;
and adding a polycarboxylic acid water reducing agent and fibers into the second mixture, and uniformly stirring to obtain the ground mortar.
Compared with the prior art, the invention has the following beneficial effects:
according to the invention, by adding the fibers, the fibers have better dispersibility, and can be uniformly dispersed after being added into the ground mortar to form a criss-cross net structure, so that the expansion of ground mortar cracks caused by plastic shrinkage, drying shrinkage and temperature change of the ground mortar can be effectively inhibited, the occurrence of new cracks is delayed, and the crack resistance of the ground mortar is improved.
In addition, the fibers are mixed in the ground mortar, and cement in the ground mortar can wrap the surfaces of the fibers, so that the fluidity of the ground mortar is reduced, the segregation and bleeding conditions of the ground mortar are improved, and the anti-segregation performance of the ground mortar is improved.
The polycarboxylate superplasticizer can reduce the water consumption of the ground mortar and can realize the fluidity of the ground mortar.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The experimental procedures in the following examples are conventional unless otherwise specified. Test materials, reagents and the like used in the following examples are commercially available unless otherwise specified. In the quantitative tests in the following examples, three replicates were set, and the data are the mean or the mean ± standard deviation of the three replicates.
In addition, "and/or" in the whole text includes three schemes, taking a and/or B as an example, including a technical scheme, and a technical scheme that a and B meet simultaneously; in addition, technical solutions between various embodiments may be combined with each other, but must be realized by a person skilled in the art, and when the technical solutions are contradictory or cannot be realized, such a combination should not be considered to exist, and is not within the protection scope of the present invention.
The invention provides ground mortar, which comprises the following raw materials in parts by weight:
Figure BDA0003402294850000031
according to the invention, by adding the fibers, the fibers have better dispersibility, and can be uniformly dispersed after being added into the ground mortar to form a criss-cross net structure, so that the expansion of ground mortar cracks caused by plastic shrinkage, drying shrinkage and temperature change of the ground mortar can be effectively inhibited, the occurrence of new cracks is delayed, and the crack resistance of the ground mortar is improved.
In addition, the fibers are mixed in the ground mortar, and cement in the ground mortar can wrap the surfaces of the fibers, so that the fluidity of the ground mortar is reduced, the segregation and bleeding conditions of the ground mortar are improved, and the anti-segregation performance of the ground mortar is improved.
The polycarboxylate superplasticizer can reduce the water consumption of the ground mortar and can realize the fluidity of the ground mortar.
Specifically, the water reducing efficiency of the polycarboxylic acid water reducing agent is 30-36%.
In some embodiments, the admixture comprises at least one of mineral fines, coal ash, and modified ceramic polishing powder.
In some embodiments, the fibers comprise any one of polypropylene fibers, basalt fibers, carbon fibers, and quartz fibers.
In some embodiments, the polypropylene fibers have a filament length of 6mm and a fiber diameter of 10-20 mm.
The excessive monofilament length of the polypropylene fiber can influence the dispersibility of the ground mortar, and the addition of the polypropylene fiber with the excessive monofilament length into the ground mortar can reduce the anti-cracking effect of the ground mortar; too large a diameter of the polypropylene fiber affects the compressive strength of the ground mortar; therefore, by setting the length and diameter of the polypropylene fiber filaments to the above values, the dispersibility of the floor mortar can be improved, and the compressive strength of the floor mortar can be improved.
In some embodiments, the ground mortar is prepared from the following raw materials in parts by weight:
2.5 parts of a thickening agent.
The thickening agent is added into the ground mortar to increase the consistency of the ground mortar, so that the water retention effect of the mortar is improved.
In some embodiments, the thickener comprises at least one of an inorganic thickener, an ether thickener, and a polyacrylate thickener.
In some embodiments, the cement includes at least one of composite portland cement PC32.5 and portland cement p.o42.5.
In some embodiments, the sand has a fineness modulus of 2.3 to 3.2.
The fineness modulus of the sand is preferably 2.3-3.0, the fineness modulus of the sand can influence the fluidity, the workability and the water consumption of a mixture, the water retention performance of the coarse sand is easily reduced, and the fluidity and the consistency of the fine sand are influenced, so that more water is added to the ground mortar during actual stirring; therefore, by setting the fineness modulus of sand to the above value, the effect of improving the fluidity and water retentivity of the ground mortar can be achieved.
In some embodiments, the activity of the modified ceramic polishing powder>65% of specific surface area>1023m2Density/kg>2.56g/cm3
The activity of the modified ceramic polishing powder is more than 65%, so that the activity of the modified ceramic polishing powder is in a range, the quality of the modified ceramic polishing powder is stable, and the modified ceramic polishing powder is used for replacing fly ash and mineral powder in ground mortar, so that the stability of the water retention and compressive strength of the ground mortar can be improved.
The activity of the modified ceramic polishing powder refers to the strength after replacing a certain amount of cement, and the activity index is measured according to the compressive strength ratio of 7d to 28d, which is shown in GB/T1596-2017 appendix C.
In some embodiments, the ground mortar is prepared from the following raw materials in parts by weight:
Figure BDA0003402294850000041
Figure BDA0003402294850000051
in some embodiments, the ground mortar is prepared from the following raw materials in parts by weight:
Figure BDA0003402294850000052
the invention also provides a preparation method of the ground mortar, which comprises the following steps:
mixing 15-25 parts of cement, 25-40 parts of admixture, 25-35 parts of sand, 3-4 parts of polycarboxylic acid water reducer, 2-3 parts of fiber and water in parts by weight, and stirring for dissolving to obtain the product, namely the ground mortar.
Concretely, after water is added, the cement and the admixture undergo hydration reaction to form hydration products, and the hydration products contain Ca (OH)2Solution, Ca (OH)2The solution quickly reaches saturation and precipitates crystals, and meanwhile, ettringite crystals and hydrated calcium silicate gel are generated.
In some embodiments, a method of preparing a floor screed comprises the steps of:
and S100, physically stirring the cement, the admixture and the sand, and uniformly stirring to obtain a first mixture.
Specifically, the cement, the admixture and the sand are physically stirred to uniformly mix the cement, the admixture and the sand, so that the cement, the admixture and the sand are prevented from sticking to the bottom after water is added.
When cement, admixture, sand, polycarboxylate water reducer, fiber and water are mixed simultaneously, organic additives (polycarboxylate water reducer and fiber) are absorbed and agglomerated by inorganic powder (cement, admixture and sand), therefore, the inorganic powder (cement, admixture and sand) must be mixed uniformly, and then the organic additives (polycarboxylate water reducer and fiber) are added, so that the raw materials for preparing the ground mortar can be mixed more uniformly, and the performance of the ground mortar is improved more obviously.
And S200, adding water into the first mixture, carrying out hydration reaction on the cement, the admixture and the water, and uniformly stirring to obtain a second mixture.
S300, adding a polycarboxylic acid water reducing agent and polypropylene fibers into the second mixture, and uniformly stirring to obtain the ground mortar.
After water is added, the cement and the admixture undergo hydration reaction to form hydration products, and the hydration products contain Ca (OH)2Solution, Ca (OH)2The solution quickly reaches saturation and precipitates crystals, meanwhile, ettringite crystals and hydrated calcium silicate gel are generated, therefore, inorganic powder (cement, admixture and sand) needs to be mixed before water is added, otherwise, the cement and the admixture are hydrated into gel after the water is added, the cement, the admixture and the sand are difficult to be uniformly mixed, after the water is added, the organic additive can be dispersed, otherwise, the organic additive is absorbed and agglomerated by the inorganic powder.
Specifically, adding the polycarboxylic acid water reducing agent and the polypropylene fibers into the second mixture, uniformly stirring, wherein the stirring time is not less than 1.5 min.
In some embodiments, the mass ratio of the first mixture to the water is 1:0.35 to 0.45.
In some embodiments, the method of preparing the modified ceramic polishing powder comprises the steps of:
s101, after ball milling is carried out on the ceramic polishing powder waste, adding mixed liquor of concentrated sulfuric acid and hydrogen peroxide into the ceramic polishing powder waste, stirring and reacting, and obtaining the hydroxylated ceramic polishing powder after the reaction is finished.
The purpose of adding the mixed solution of concentrated sulfuric acid and hydrogen peroxide into the ceramic polishing powder waste is to activate the ceramic polishing powder waste after ball milling and add SiO in the ceramic polishing powder waste after ball milling2Hydroxyl (Si-O-Si → Si-O-H) is introduced to improve the grafting rate of the subsequent ceramic polishing powder waste and the silane coupling agent, and the hydroxylated ceramic polishing powder is obtained after washing and drying.
The mixed liquid of concentrated sulfuric acid and hydrogen peroxide is also called piranha solution and has strong oxidability.
In some embodiments, the specific steps of ball milling the ceramic polishing powder waste are as follows: grinding the specific surface area of the ceramic polishing powder waste to 850-900 m by using a ball mill2And/kg, so as to increase the contact area of the ceramic polishing powder waste and the mixed solution of concentrated sulfuric acid and hydrogen peroxide for reaction, and further improve the reaction efficiency.
In one embodiment, the mass concentration of the concentrated sulfuric acid is preferably 98%, the mass solubility of the hydrogen peroxide is preferably 30%, and the volume ratio of the concentrated sulfuric acid to the hydrogen peroxide is 8-6: 3.
The mass ratio of the ceramic polishing powder waste to the mixed liquid of concentrated sulfuric acid and hydrogen peroxide is 7-9: 9.
In some embodiments, the mixed solution of concentrated sulfuric acid and hydrogen peroxide is added into the ceramic polishing powder waste, and the reaction time is 30min, and the reaction temperature is 70 ℃.
S201, melting the hydroxylated ceramic polishing powder, the silane coupling agent and the polymerization inhibitor into toluene for modification, and obtaining the coupling agent modified ceramic polishing powder after the modification is finished.
Specifically, toluene is used as a solvent, a silane coupling agent and hydroxyl groups of the hydroxylated ceramic polishing powder are subjected to condensation reaction and are connected by siloxane bonds (Me-O-Si + Si-OH → MeOH + Si-O-Si), and the coupling agent modified ceramic polishing powder is obtained by drying.
The silane coupling agent is used for connecting the particles of the ceramic polishing powder with the molecules of the surfactant in the subsequent step S301, so that the ceramic polishing powder and the surfactant are combined more effectively, and the dispersion effect of the ceramic polishing powder is enhanced.
The polymerization inhibitor is added in the step of preparing the coupling agent modified ceramic polishing powder in order to reduce the reaction rate of the condensation reaction of the silane coupling agent and the hydroxylated ceramic polishing powder and achieve the purpose of preventing the condensation reaction of the silane coupling agent and the hydroxylated ceramic polishing powder from generating sudden polymerization.
In some embodiments, the polymerization inhibitor comprises any one of hydroquinone, p-hydroxyanisole, and 2, 6-di-tert-butyl-4-methylphenol (BHT).
In some embodiments, the mass concentration of the polymerization inhibitor is preferably 1%.
In some embodiments, the silane coupling agent comprises an amino-functional silane coupling agent (KH-550), a gamma- (2, 3-glycidoxy) propyltrimethoxysilane coupling agent (KH-560), gamma-methacryloxypropyltrimethoxysilane; any one of silane coupling agents (KH-570).
S301, adding the coupling agent modified ceramic polishing powder into a surfactant solution, stirring, uniformly stirring to obtain a mixed solution, carrying out centrifugal separation on the mixed solution, drying the centrifugally separated solid, adding silica fume into the dried solid, and uniformly mixing to obtain the modified ceramic polishing powder.
Specifically, the ceramic polishing powder modified by the coupling agent is added into a surfactant solution to perform surface modification treatment on the ceramic polishing powder, and a solute in the surfactant is adsorbed on the surface of the ceramic polishing powder, so that an organic molecular layer is formed on the surface of the ceramic polishing powder, and the ceramic polishing powder is changed from hydrophilicity to hydrophilicity.
And (3) centrifugally separating the mixed solution, and drying the centrifugally separated solid to remove the unreacted silane coupling agent, the polymerization inhibitor and the surfactant.
The silicon ash refers to SiO generated in the smelting of ferrosilicon and industrial silicon2And Si gas and oxygen in the air are quickly oxidized and condensed to form a siliceous powder material, and the purpose of adding the silica fume into the modified ceramic polishing powder is that when the modified ceramic polishing powder is stirred with cement, the silica fume in the modified ceramic polishing powder fills gaps among cement particles, and simultaneously, the silica fume is mixed with the cement to form the siliceous powder materialAnd the cement and hydration products of the cement form gel, so that the water retention and the compressive strength of the ground mortar are improved.
In some embodiments, the surfactant is preferably a quaternary ammonium surfactant.
The modified ceramic polishing powder used in the invention is derived from ceramic polishing powder waste, realizes the reutilization of the waste, meets the requirement of environmental protection, and reduces the cost of raw materials for preparing the ground mortar.
In some embodiments, the mass ratio of the hydroxylated ceramic polishing powder to the silane coupling agent to the polymerization inhibitor to the toluene is 1: 1: 0.25: 2.5.
in some embodiments, in the step of modifying the hydroxylated ceramic polishing powder, the silane coupling agent and the polymerization inhibitor by melting into toluene, the modification temperature is 80 ℃, and the modification time is 4 hours.
The mass ratio of the coupling agent modified ceramic polishing powder to the surfactant solution is 1: 1-1.5
Adding the coupling agent modified ceramic polishing powder into a surfactant solution, stirring and reacting for 3.5-4.5 h at 75-85 ℃.
Example 1
Physically stirring 20kg of ordinary portland cement P.O42.5, 35kg of modified ceramic polishing powder and 30kg of sand for 0.5min to obtain a first mixture;
adding 35kg of water into the first mixture, and stirring for 1min to obtain a second mixture;
adding 3.5kg of polycarboxylic acid water reducing agent, 2kg of polypropylene fiber and 2.5kg of thickening agent into the second mixture, and stirring for 3.5min to react to obtain ground mortar;
wherein the sand is machine-made sand with fineness modulus of 2.8, and the activity of the modified ceramic polishing powder>65% of specific surface area>1023m2Density/kg>2.56g/cm3
Example 2
Physically stirring 18kg of ordinary portland cement P.O42.5, 33kg of modified ceramic polishing powder and 26kg of sand for 1min to obtain a first mixture;
adding 30kg of water into the first mixture, and stirring for 1min to obtain a second mixture;
adding 3.2kg of polycarboxylic acid water reducing agent, 2.5kg of polypropylene fiber and 2.2kg of thickening agent into the second mixture, and stirring for 3min to react to obtain ground mortar;
wherein the sand is machine-made sand with fineness modulus of 3.0, and the activity of the modified ceramic polishing powder>65% of specific surface area>1023m2Density/kg>2.56g/cm3
Example 3
Carrying out physical stirring on 23kg of ordinary portland cement P.O42.5, 28kg of modified ceramic polishing powder and 32kg of sand, and stirring for 1.5min to obtain a first mixture;
adding 40kg of water into the first mixture, and stirring for 0.5min to obtain a second mixture;
adding 3.6kg of polycarboxylic acid water reducing agent, 2.8kg of polypropylene fiber and 2.7kg of thickening agent into the second mixture, and stirring for 3min to react to obtain ground mortar;
wherein the sand is machine-made sand with fineness modulus of 2.6, and the activity of the modified ceramic polishing powder>65% of specific surface area>1023m2Density/kg>2.56g/cm3
Comparative example 1
In close contrast to example 3, 18kg of modified ceramic polishing powder was replaced by 10kg of fly ash and 8kg of mineral powder in the preparation of the floor mortar and used for comparative study with the floor mortar of the present invention.
Comparative example 2
With strict reference to example 3, a floor mortar was prepared without adding fibres and was used for a comparative study with the floor mortar according to the invention.
The preparation methods of the modified ceramic polishing powders used in examples 1 to 3 and comparative example 1 were as follows:
ball-milling the surface area of the ceramic polishing powder waste to 850-900 m2Adding a mixed solution of 98% concentrated sulfuric acid and 30% hydrogen peroxide into the ceramic polishing powder waste, stirring, heating at 70 ℃, stirring, reacting for 30 minutes, preparing the 98% concentrated sulfuric acid and the 30% hydrogen peroxide according to a ratio of 7:3, and obtaining hydroxylated ceramic polishing powder after the reaction is finished;
the method comprises the following steps of (1) melting hydroxylated ceramic polishing powder, a silane coupling agent and 0.1 wt% of hydroquinone into toluene, heating to 80 ℃, reacting for 4 hours for modification, and preparing coupling agent modified ceramic polishing powder after the modification is finished;
adding the coupling agent modified ceramic polishing powder into a surfactant solution, stirring for reaction, reacting at 80 ℃ for 5 hours to obtain a mixed solution after the reaction is finished, carrying out centrifugal separation on the mixed solution, drying the centrifugally separated solid, and uniformly mixing the dried solid and silica fume to obtain the modified ceramic polishing powder.
Performance testing of ground mortar
The ground mortars prepared in the above examples 1 to 3 and comparative example 1 were subjected to the following standard: JC/T2457-2018 Dry-Mixed floor mortar for construction carry out performance test, and the results are shown in Table 1:
TABLE 1 Performance test results for ground mortar
Figure BDA0003402294850000091
Figure BDA0003402294850000101
The test results in the table 1 show that the environmental protection mortar can meet the requirements of national standard JC/T2457-2018 'Dry-mixed floor mortar for buildings' in various properties.
Comparing the data of example 3 with that of comparative example 1, example 3 doped with the modified ceramic polishing powder has higher compressive strength and flexural strength than comparative example 1 doped with conventional admixtures (coal ore powder and ore powder), which shows that the modified ceramic polishing powder used in the present application can replace coal ore powder and has improved compressive strength and flexural strength, and example 3 doped with the modified ceramic polishing powder has lower consistency than comparative example 1 doped with conventional admixtures (coal ore powder and ore powder), which shows that the ground mortar prepared by the method has improved fluidity.
From the data of example 1, example 2 and example 3, it can be seen that there are two samples with compressive strength exceeding that of comparative example 1, which is more flexible in strength adjustment. The three examples are all higher than the comparative example in the aspect of the flexural strength and are reliable in the flexural strength, and the three examples are all higher than the comparative example in the aspect of the flexural strength and are reliable in the flexural strength. With the change of the mixing amount of the polishing powder, the consistency, the compressive strength and the precipitation resistance strength are changed, so that the mixing amount of the modified ceramic polishing powder can be adjusted to meet more engineering requirements.
The modified ceramic polishing powder is related to the morphological effect of the modified ceramic polishing powder, one part of the modified ceramic polishing powder participates in the hydration of cement to generate more hydration products, the unit water consumption of the mortar can be reduced, the other part of the modified ceramic polishing powder which does not participate in the hydration is filled among cement particles, and then the pores formed after the mortar is hardened by redundant water are reduced, so that the structure of the ground mortar is more compact, and the performances of the ground mortar, such as compressive strength, precipitation resistance and the like, are improved.
Comparing the flexural strength data of example 3 with that of comparative example 2, the flexural strength of comparative example 2 without the addition of fibers was significantly lower than that of example 3, and from the flexural strength data of example 1, example 2 and example 3, it can be seen that the flexural strength increased with the increase in the amount of the fibers incorporated, indicating that the addition of fibers can improve the anti-settling property of the floor mortar.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (10)

1. The ground mortar is characterized in that the ground mortar is prepared from the following raw materials in parts by weight:
Figure FDA0003402294840000011
and (3) water.
2. The floor screed of claim 1, wherein the admixture comprises at least one of mineral fines, coal ash, and modified ceramic polishing powder.
3. The ground screed of claim 1, wherein the fibers comprise any one of polypropylene fibers, basalt fibers, carbon fibers, and quartz fibers.
4. The floor screed according to claim 3, wherein the polypropylene fibres have a filament length of 6mm and a diameter of 10-20 mm.
5. The ground mortar of claim 1, wherein the raw materials for preparing the ground mortar further comprise, in parts by weight:
2.5 parts of a thickening agent.
6. The ground screed of claim 5, wherein the thickener comprises at least one of an inorganic thickener, an ether thickener, and a polyacrylate thickener.
7. The ground screed of claim 1, wherein the cement comprises at least one of Portland composite cement PC32.5 and Portland cement P.O42.5.
8. The ground mortar of claim 1, wherein the sand has a fineness modulus of 2.3 to 3.2.
9. A preparation method of ground mortar is characterized by comprising the following steps:
mixing 15-25 parts of cement, 25-40 parts of admixture, 25-35 parts of sand, 3-4 parts of polycarboxylic acid water reducer, 2-3 parts of fiber and water in parts by weight, and stirring for dissolving to obtain the product, namely the ground mortar.
10. The method for preparing the ground mortar according to claim 9, wherein the method for preparing the ground mortar comprises the steps of:
the method comprises the following steps of (1) physically stirring cement, an admixture and sand, and uniformly stirring to obtain a first mixture;
adding water into the first mixture, carrying out hydration reaction on the cement, the admixture and the water, and uniformly stirring to obtain a second mixture;
and adding a polycarboxylic acid water reducing agent and fibers into the second mixture, and uniformly stirring to obtain the ground mortar.
CN202111502529.XA 2021-12-09 2021-12-09 Ground mortar and preparation method thereof Pending CN114105565A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111502529.XA CN114105565A (en) 2021-12-09 2021-12-09 Ground mortar and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111502529.XA CN114105565A (en) 2021-12-09 2021-12-09 Ground mortar and preparation method thereof

Publications (1)

Publication Number Publication Date
CN114105565A true CN114105565A (en) 2022-03-01

Family

ID=80364320

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111502529.XA Pending CN114105565A (en) 2021-12-09 2021-12-09 Ground mortar and preparation method thereof

Country Status (1)

Country Link
CN (1) CN114105565A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103304175A (en) * 2013-06-14 2013-09-18 合肥工业大学 Preparation method of cationic surfactant modified fly ash
CN104844097A (en) * 2015-04-03 2015-08-19 四川雅豪房地产开发有限公司 Enhanced crack-resistant cement floor material
CN110156372A (en) * 2019-05-10 2019-08-23 中交浚浦建筑科技(上海)有限公司 A kind of auto-flowing floor mortar additive and preparation method thereof
CN112608097A (en) * 2020-12-07 2021-04-06 厦门天润锦龙建材有限公司 Mortar and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103304175A (en) * 2013-06-14 2013-09-18 合肥工业大学 Preparation method of cationic surfactant modified fly ash
CN104844097A (en) * 2015-04-03 2015-08-19 四川雅豪房地产开发有限公司 Enhanced crack-resistant cement floor material
CN110156372A (en) * 2019-05-10 2019-08-23 中交浚浦建筑科技(上海)有限公司 A kind of auto-flowing floor mortar additive and preparation method thereof
CN112608097A (en) * 2020-12-07 2021-04-06 厦门天润锦龙建材有限公司 Mortar and preparation method thereof

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
卓振尧: "《陶瓷掺合料对水泥胶砂性能的影响研究》", 《中国优秀硕士学位论文全文数据库 工程科技Ⅱ辑》 *
曹聪等: "《复掺陶瓷抛光砖粉与聚丙烯纤维对砂浆性能的影响》", 《硅酸盐通报》 *
曹聪等: "复掺陶瓷抛光砖粉与聚丙烯纤维对砂浆性能的影响", 硅酸盐通报 *

Similar Documents

Publication Publication Date Title
CN107265966B (en) It is a kind of to prepare bridge self-compaction cracking resistance clear-water concrete using high fine powder content Machine-made Sand
CN107572969B (en) Sea sand ultrahigh-performance concrete and preparation method thereof
CN111792889A (en) Natural tuff ultrahigh-performance concrete and preparation method thereof
CN112573874A (en) Preparation method of high-strength self-compacting concrete
CN113004005A (en) Cement-based grouting material prepared based on machine-made sand
CN115321857A (en) Retarding geopolymer concrete and preparation method thereof
CN111620662A (en) Concrete doped with modified zeolite
CN114163173A (en) Lightweight concrete and preparation method thereof
CN111646747B (en) Lightweight ceramsite concrete and preparation method thereof
CN113105179A (en) Anti-cracking waterproof concrete and preparation method thereof
CN112794675A (en) Machine-made sand regulator and using method thereof
CN116514478A (en) Calcium carbonate and carbon fiber reinforced concrete and preparation method thereof
CN114477873B (en) Recycled aggregate self-compacting concrete and preparation method thereof
CN114394793B (en) Modified polymer concrete and preparation method thereof
CN116161929A (en) Recycled concrete and preparation method thereof
CN114105565A (en) Ground mortar and preparation method thereof
CN113248191B (en) Inert concrete waste slurry solidified material and preparation method thereof
CN115321924A (en) Durable self-compacting filling concrete material for underground structural engineering
CN111848014B (en) Green high-performance concrete and preparation method thereof
CN114230271A (en) Masonry mortar and preparation method thereof
CN114105557B (en) Plastering mortar and preparation method thereof
CN114195434B (en) Geopolymer-based high-ductility concrete for pressing, plastering and reinforcing and preparation method thereof
CN113620664B (en) Ultrahigh-performance concrete and preparation method thereof
CN116283149A (en) Self-compacting concrete with waste residues as raw materials and preparation method thereof
CN116040982A (en) Waste residue-based hydrophobic high-performance concrete admixture and preparation method and application thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination