CN113999734A - Dish-washing machine special salt for improving soft water efficiency and preparation method thereof - Google Patents

Dish-washing machine special salt for improving soft water efficiency and preparation method thereof Download PDF

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Publication number
CN113999734A
CN113999734A CN202111245571.8A CN202111245571A CN113999734A CN 113999734 A CN113999734 A CN 113999734A CN 202111245571 A CN202111245571 A CN 202111245571A CN 113999734 A CN113999734 A CN 113999734A
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CN
China
Prior art keywords
salt
dish
washing machine
evaporation system
effect evaporation
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Pending
Application number
CN202111245571.8A
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Chinese (zh)
Inventor
张磊
刘旋
张科平
刘玉涛
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Engineering Technology Institute Co ltd Of Cnsic
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Engineering Technology Institute Co ltd Of Cnsic
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Publication date
Application filed by Engineering Technology Institute Co ltd Of Cnsic filed Critical Engineering Technology Institute Co ltd Of Cnsic
Priority to CN202111245571.8A priority Critical patent/CN113999734A/en
Publication of CN113999734A publication Critical patent/CN113999734A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/02Inorganic compounds
    • C11D7/04Water-soluble compounds
    • C11D7/10Salts
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/14Purification
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D3/00Halides of sodium, potassium or alkali metals in general
    • C01D3/22Preparation in the form of granules, pieces, or other shaped products
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Seasonings (AREA)

Abstract

The invention provides a special salt for a dish-washing machine for improving soft water efficiency and a preparation method thereof, wherein the diameter of the spherical sodium chloride granular salt special for the dish-washing machine is 0.85-1.2 mm; the purity of the sodium chloride is more than 99.4 percent; the sodium chloride is obtained by drying and screening raw salt particles in an I-effect evaporation system and an II-effect evaporation system in a vacuum salt-making five-effect evaporation system. The sodium chloride is spherical granular salt, has uniform granularity, maintains the granularity at 0.85-1.2 mm, has larger salt content and less powder salt content than the traditional dish-washing machine, does not cause the blockage of a salt suction port of the dish-washing machine, has larger contact area between the spherical structure and water, is quickly dissolved, does not cause the use delay of the dish-washing machine after the salt is changed, and saves the time of users.

Description

Dish-washing machine special salt for improving soft water efficiency and preparation method thereof
Technical Field
The invention belongs to the technical field of dish washing salt, and particularly relates to dish washing machine special salt for improving soft water efficiency and a preparation method thereof.
Background
Along with the social development, the living standard of people is improved, the use of the dish-washing machine becomes a normal state, various special salt for the dish-washing machine appears on the market, but the salt content of the existing special salt for the dish-washing machine is high due to the problem of the preparation process, the salt suction port of the dish-washing machine is easy to block, the salt used in the traditional dish-washing machine is irregular, the dissolving speed is slow, the use delay of the dish-washing machine after the salt is changed is caused, and the occupied time is long.
Disclosure of Invention
In view of the above, the present invention provides a dish washer salt with uniform particle size, low content of powder salt and spherical shape for improving soft water efficiency, and a preparation method thereof, so as to solve the above problems.
In order to achieve the purpose, the technical scheme of the invention is realized as follows:
the invention provides a special salt for a dish-washing machine, which can improve the efficiency of soft water, and comprises sodium chloride, wherein the sodium chloride is spherical granular salt, the granularity is uniform, and the granularity is kept at 0.85-1.2 mm.
Furthermore, the purity of the sodium chloride is more than 99.4%.
Further, the sodium chloride is obtained by drying and screening raw salt particles in an I-effect evaporation system and an II-effect evaporation system in a vacuum salt-making five-effect evaporation system.
Furthermore, the temperature of the I-effect evaporation system is controlled to be above 130 ℃, and the main steam pressure is controlled to be above 0.3 MPa.
The invention provides a preparation method of the special salt for the dish-washing machine for improving the efficiency of soft water, which comprises the following steps of selecting raw salt particles in an I-effect evaporation system and an II-effect evaporation system in a five-effect evaporation system for vacuum salt preparation; drying the raw salt particles; and screening out spherical granular salt with the diameter of 0.85-1.2 mm after drying.
Furthermore, the temperature of the I-effect evaporation system is controlled to be above 130 ℃, and the main steam pressure is controlled to be above 0.3 MPa. The method has the advantages that the high-temperature and high-pressure environment is executed, the solid-liquid ratio is high, the impurity content of the system is low (the gypsum content is required to be controlled to be low), the single-effect salt discharging system is used for production, and the granularity of the raw salt is ensured to be large enough.
Further, the drying temperature of the raw salt particles is 80 ℃.
In another aspect, the invention provides an application of the special salt for the dish-washing machine for improving the efficiency of soft water in the field of dish-washing salt.
Compared with the prior art, the special salt for improving the soft water efficiency of the dish-washing machine and the preparation method thereof have the following advantages:
(1) the sodium chloride is spherical granular salt, has uniform granularity, keeps the granularity of 0.85-1.2 mm, has larger salt content and less powder salt content than the traditional dish-washing machine, and cannot cause the blockage of a salt suction port of the dish-washing machine;
(2) the sodium chloride is spherical granular salt, the salt of the traditional dish washing machine is irregular, the contact area between the spherical refined salt and water is large, the sodium chloride is dissolved quickly, the use delay of the dish washing machine after salt changing is avoided, and the time of a user is saved.
Detailed Description
Unless defined otherwise, technical terms used in the following examples have the same meanings as commonly understood by one of ordinary skill in the art to which the present invention belongs. The test reagents used in the following examples, unless otherwise specified, are all conventional biochemical reagents; the experimental methods are conventional methods unless otherwise specified.
The present invention will be described in detail with reference to examples.
In the five-effect evaporation system for vacuum salt production, technological parameters are adjusted, brine feed liquid enters an evaporation chamber of the I-effect evaporation system and a evaporation chamber of the V-effect evaporation system, steam enters a heating chamber of the I-effect evaporation system to heat the brine feed liquid, evaporation and concentration are carried out, the temperature of the I-effect evaporation system is controlled to be above 130 ℃, and the main steam pressure is controlled to be above 0.3 MPa. Steam of the heated evaporation brine enters a heating chamber of the II-effect evaporation system to continuously heat the brine, and the rest is done in the same way. In a high-temperature and high-pressure environment, a higher solid-liquid ratio is controlled, the gypsum content requirement is very low, a single-effect salt discharge system is used for production, the granularity of raw salt is ensured to be large enough (more than 0.85 mm), and only raw salt particles in an I-effect evaporation system and a II-effect evaporation system are selected;
drying the obtained raw salt particles at 80 ℃, and screening out spherical particle salt with the particle size of 0.85-1.2 mm by using a screening machine.
The obtained salt product special for the dish-washing machine has uniform granularity, is spherical and has low content of powder salt.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.

Claims (8)

1. The special salt for improving the efficiency of soft water for the dish-washing machine is characterized in that: comprises sodium chloride which is spherical granular salt, and the diameter of the sodium chloride is 0.85-1.2 mm.
2. The special salt for dish washer for improving soft water efficiency according to claim 1, wherein: the purity of the sodium chloride is more than 99.4 percent.
3. The special salt for dish washer for improving soft water efficiency according to claim 1, wherein: the sodium chloride is obtained by drying and screening raw salt particles in an I-effect evaporation system and an II-effect evaporation system in a vacuum salt-making five-effect evaporation system.
4. The special salt for dish washer for improving soft water efficiency according to claim 3, wherein: the temperature of the I-effect evaporation system is controlled to be above 130 ℃, and the main steam pressure is controlled to be above 0.3 MPa.
5. The method for preparing dishwasher-specific salt for enhancing soft water efficiency according to any one of claims 1 to 4, wherein: selecting raw salt particles in an I-effect evaporation system and an II-effect evaporation system in a vacuum salt-making five-effect evaporation system; drying the raw salt particles; and screening out spherical granular salt with the diameter of 0.85-1.2 mm after drying.
6. The method for preparing dishwasher-specific salt for enhancing soft water efficiency according to claim 5, wherein: the temperature of the I-effect evaporation system is controlled to be above 130 ℃, and the main steam pressure is controlled to be above 0.3 MPa.
7. The method for preparing dishwasher-specific salt for enhancing soft water efficiency according to claim 5, wherein: the drying temperature of the raw salt particles is 80 ℃.
8. Use of the dishwasher specific salt for enhancing soft water performance according to any one of claims 1 to 4 in the field of dishwashing salt.
CN202111245571.8A 2021-10-26 2021-10-26 Dish-washing machine special salt for improving soft water efficiency and preparation method thereof Pending CN113999734A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111245571.8A CN113999734A (en) 2021-10-26 2021-10-26 Dish-washing machine special salt for improving soft water efficiency and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111245571.8A CN113999734A (en) 2021-10-26 2021-10-26 Dish-washing machine special salt for improving soft water efficiency and preparation method thereof

Publications (1)

Publication Number Publication Date
CN113999734A true CN113999734A (en) 2022-02-01

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ID=79924068

Family Applications (1)

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CN202111245571.8A Pending CN113999734A (en) 2021-10-26 2021-10-26 Dish-washing machine special salt for improving soft water efficiency and preparation method thereof

Country Status (1)

Country Link
CN (1) CN113999734A (en)

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3516606A1 (en) * 1984-05-14 1985-11-14 Solvay & Cie., Brüssel/Bruxelles Regenerant for cation exchanger materials and process for regenerating a cation exchanger resin of a water softener
EP0733590A1 (en) * 1995-03-24 1996-09-25 SOLVAY (Société Anonyme) Salt having more than 99,0% by weight sodium chloride and its use
JPH0986923A (en) * 1995-09-20 1997-03-31 Akou Kasei Kk Spherical salt particle and its production
CN214299409U (en) * 2020-12-11 2021-09-28 李志刚 Domestic integrated water softener

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3516606A1 (en) * 1984-05-14 1985-11-14 Solvay & Cie., Brüssel/Bruxelles Regenerant for cation exchanger materials and process for regenerating a cation exchanger resin of a water softener
EP0733590A1 (en) * 1995-03-24 1996-09-25 SOLVAY (Société Anonyme) Salt having more than 99,0% by weight sodium chloride and its use
JPH0986923A (en) * 1995-09-20 1997-03-31 Akou Kasei Kk Spherical salt particle and its production
CN214299409U (en) * 2020-12-11 2021-09-28 李志刚 Domestic integrated water softener

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
徐飞: "真空制盐五效蒸发工艺技术改造", 苏盐科技, no. 3, 15 September 2009 (2009-09-15), pages 7 - 9 *

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