CN113960267B - Quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume - Google Patents
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Abstract
The invention discloses a quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume, which mainly relates to the technical field of perfume production devices and comprises a control unit and a plurality of quality analyzers, wherein the quality analyzers are detachably connected with a product temporary storage tank in the production device and are used for analyzing fragrance retention time and consistency of the synthetic perfume temporarily stored in the product temporary storage tank, and the control unit is connected with the quality analyzers and is used for controlling the work of the quality analyzers. The control unit and the quality analyzer are matched, so that the quality analysis of the synthetic perfume can be automatically completed at the first time, and the structure is simple; the quality analyzer sets the fragrance emission time and detects the data of the retained fragrance by matching the timer and the fragrance detection sensor, so that the quality analyzer is simple and convenient to operate and easy to realize; the quality analyzer is provided with an upper device body and a lower device body, and whether the consistency of the synthetic spice changes and the changed value are obtained by utilizing the hourglass principle.
Description
Technical Field
The invention relates to a perfume production device, in particular to a quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume.
Background
The o-tert-butylcyclohexyl acetate is also called as ortho-irimate, has the chemical name of 2- (1, 1-dimethylethyl) cyclohexyl acetate, is colorless to light yellow transparent oily liquid or solid crystal in appearance, has citrus-type fruity fragrance similar to fresh lemons and white lemons, has coniferous-like costustoot fragrance, can be used in various essences, is a synthetic spice prepared by taking the o-tert-butylcyclohexyl acetate as a raw material, is called as the o-tert-butylcyclohexyl acetate synthetic spice for short, has very stable property and difficult discoloration, is a common synthetic spice, is very useful in the whole modern perfume, can be used as a floral essence and an costustoot essence to inject warm characteristics, is widely applied to daily chemical essence formulas such as a perfume soap essence, a cosmetic essence, an essence and the like, can be stably used in most essence products, and can be almost used in all daily essence products, even in bleaching agents.
The demand of o-tert-butylcyclohexyl acetate synthetic perfume is gradually enlarged in recent years, but the production device of the o-tert-butylcyclohexyl acetate synthetic perfume has the problem that the quality of the produced o-tert-butylcyclohexyl acetate synthetic perfume cannot be identified and analyzed at the first time, and the o-tert-butylcyclohexyl acetate synthetic perfume needs to be subsequently taken out and then subjected to quality analysis through an additional detection device, therefore, the quality identification data of the o-tert-butylcyclohexyl acetate synthetic spice and the result of the quality degree can not be obtained at the first time, the quality of the prepared synthetic spice can not be identified and analyzed at the first time, therefore, it is necessary to design a quality analysis device directly connected to a product temporary storage tank of an original production device, and to detect and analyze the quality of o-tert-butylcyclohexyl acetate aroma composition at the first time when the o-tert-butylcyclohexyl acetate aroma composition is prepared.
Disclosure of Invention
The invention provides a quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume, which solves the problems in the prior art mentioned in the background technology.
The technical scheme adopted by the invention for solving the technical problems is as follows: the device comprises a control unit and a plurality of quality analyzers, wherein the plurality of quality analyzers are arranged in parallel, the plurality of quality analyzers are detachably connected with a product temporary storage tank in a production device and are used for analyzing fragrance retention time and consistency of synthetic spices temporarily stored in the product temporary storage tank, and the control unit is electrically connected with the plurality of quality analyzers and is used for controlling the plurality of quality analyzers;
in order to realize the analysis of aroma retention time and consistency of the synthetic spice, the quality analyzer is a waist drum-shaped structure with two large ends and middle contraction, and comprises an upper device body and a lower device body, wherein the upper device body and the lower device body are separated by an electric gate valve, the upper end of the upper device body is provided with an emission port, the emission port is provided with an odor detection sensor, the upper device body is provided with a timer, the lower end of the lower device body is provided with an outlet, and the timer is arranged between the upper device body and the lower device body.
In order to secondarily utilize the synthetic spice used by quality analysis, the device also comprises a collecting box, wherein the collecting box is arranged below the plurality of quality analyzers and is communicated with the plurality of quality analyzers, a liquid outlet is arranged at the lower side of the collecting box and is connected with a discharge pipe, and an electric valve II is arranged on the discharge pipe.
In order to facilitate the connection of the existing production device without changing the original structure, the side face of the product temporary storage tank is provided with a connecting pipe, a first electric valve is arranged on the connecting pipe, and a plurality of quality analyzers are communicated with the connecting pipe through an equal divider and a plurality of inlet pipes.
In order to realize automatic control, the control unit comprises a controller which is electrically connected with the odor detection sensor, the electric gate valve, the timer, the first electric valve and the second electric valve.
In order to make the fragrance uniformly diffused, an odor uniform-distribution grid plate is arranged below the diffusion opening in the upper device body.
The invention adopts the structure and has the following advantages:
1. the quality analyzer is used for analyzing fragrance retention time and consistency of the synthetic perfume temporarily stored in the product temporary storage tank, the control unit is used for controlling the plurality of quality analyzers, the quality analyzers can automatically complete quality analysis of the synthetic perfume at the first time in a matching way, data of quality identification of the synthetic perfume of the o-tert-butylcyclohexyl acetate and results of quality degree can be obtained at the first time, the inaccuracy of test results caused by transportation problems and sealing problems caused by quality analysis through an additional detection device after the synthetic perfume is taken out subsequently is avoided, and the device is simple in overall structure, convenient and practical;
2. the quality analyzer sets the fragrance emission time and the fragrance remaining data detection by matching the timer and the fragrance detection sensor, transmits the data to the controller for recording, obtains the fragrance remaining time of the synthetic perfume through a plurality of recorded data, further analyzes the quality of the synthetic perfume, and is simple and convenient to operate and easy to realize;
3. the quality analyzer is provided with an upper device body and a lower device body, the upper device body and the lower device body are communicated through an electric gate valve by utilizing the hourglass principle, the time for the synthetic spice in the upper device body to gradually leak into the lower device body is recorded through a timer, and whether the consistency and the changed numerical value of the synthetic spice are changed after the fragrance of the synthetic spice is emitted for different time is obtained, so that the quality analysis of the synthetic spice is further carried out, the test is accurate, and the process is simple and feasible.
Drawings
FIG. 1 is a schematic front view of the present invention;
FIG. 2 is an enlarged schematic view of a mass analyzer;
FIG. 3 is a graph of the aroma retention duration.
In the figure, 1, a product temporary storage tank; 2. a connecting pipe; 3. a first electric valve; 4. an equalizer; 5. an inlet pipe; 6. a quality analyzer; 61. an odor detection sensor; 62. a dispensing opening; 63. a smell equipartition grid plate; 64. an upper body; 65. an electric gate valve; 66. a lower body; 67. an outlet; 68. a timer; 69. a timer; 7. a collection box; 8. a liquid discharge port; 9. an electric valve II; 10. a discharge pipe; 11. and a controller.
Detailed Description
In order to clearly explain the technical features of the present invention, the following detailed description of the present invention is provided with reference to the accompanying drawings.
As shown in fig. 1 and fig. 2, the production apparatus comprises a product temporary storage tank 1, the production apparatus comprises a control unit and a plurality of quality analyzers 6, the quality analyzers 6 are arranged in parallel, the quality analyzers 6 are detachably connected with the product temporary storage tank 1 and are used for analyzing fragrance retention time and consistency of the synthetic flavor temporarily stored in the product temporary storage tank 1, and the control unit is electrically connected with the quality analyzers 6 and is used for controlling the operation of the quality analyzers 6;
in order to realize the analysis of aroma retention time and consistency of the synthetic spice, the quality analyzer 6 is a waist drum-shaped structure with two large ends and middle contraction, the quality analyzer 6 comprises an upper device body 64 and a lower device body 66, the upper device body 64 and the lower device body 66 are separated by an electric gate valve 65, the upper end of the upper device body 64 is integrally provided with an emission port 62, the emission port 62 is provided with an aroma detection sensor 61, the upper device body 64 is provided with a timer 69, in order to enable the aroma to be emitted uniformly, the upper device body 64 is internally provided with an aroma equally-distributing grid plate 63 below the emission port 62, so that the aroma can be emitted uniformly, the data detected by the aroma detection sensor 61 is more accurate, the lower end of the lower device body 66 is integrally provided with an outlet 67, and a timer 68 is arranged between the upper device body 64 and the lower device body 66;
in order to facilitate connection of an existing production device without changing the original structure, a connecting pipe 2 is welded on the side wall of a product temporary storage tank 1, a first electric valve 3 is installed on the connecting pipe 2, a plurality of quality analyzers 6 are communicated with the connecting pipe 2 through an equally divider 4 and a plurality of inlet pipes 5, the opening of the first electric valve 3 is controlled by a controller 11, the o-tert-butylcyclohexyl acetate synthetic spice temporarily stored in the product temporary storage tank 1 enters the equally divider 4 through the connecting pipe 2, and then enters different quality analyzers 6 through the corresponding inlet pipes 5;
the o-tert-butylcyclohexyl acetate synthetic perfume is produced and then stored in the product temporary storage tank 1, so that the perfume retention time analysis and the consistency analysis can be performed, the analysis can be performed to know how the quality of the synthetic perfume temporarily stored in the product temporary storage tank 1 is, whether the fragrance is lasting or not, whether the fragrance retention degree and the consistency of the synthetic perfume change after different emission times or not can be known, in addition, the analysis is performed at the first time of production, the analyzed data can be retained, so that the future analysis experiment data can be compared with the subsequent analysis experiment data, and whether the quality of the synthetic perfume changes or not in the transportation process can be obtained;
in order to secondarily utilize the o-tert-butylcyclohexyl acetate synthetic perfume used for quality analysis, the o-tert-butylcyclohexyl acetate synthetic perfume further comprises a collection box 7, the collection box 7 is installed below the plurality of quality analyzers 6 and is communicated with the plurality of quality analyzers 6, a liquid discharge port 8 is machined on the lower side of the collection box 7, the liquid discharge port 8 is connected with a discharge pipe 10, an electric valve II 9 is installed on the discharge pipe 10, the electric valve II 9 is controlled to be opened through a controller 11, the synthetic perfume used for quality analysis in the collection box 7 is discharged through the discharge pipe 10 for subsequent use, and the synthetic perfume can be reserved as a sample or trial assembly;
in order to realize automatic control, the control unit comprises a controller 11, and the controller 11 is electrically connected with the odor detection sensor 61, the electric gate valve 65, the timer 68, the timer 69, the first electric valve 3 and the second electric valve 9.
The working principle is as follows: the prepared o-tert-butylcyclohexyl acetate synthetic perfume is sent to a special detection mechanism or a special detection device for simple quality analysis and judgment before quality analysis, so that the analysis data of the quality of the prepared o-tert-butylcyclohexyl acetate synthetic perfume in the batch can be obtained at the first time, and a reference data is provided for subsequent production;
the o-tert-butylcyclohexyl acetate synthetic perfume is prepared, the prepared o-tert-butylcyclohexyl acetate synthetic perfume is temporarily stored in a product temporary storage tank 1, a controller 11 controls to open an electric valve I3, the o-tert-butylcyclohexyl acetate synthetic perfume temporarily stored in the product temporary storage tank 1 enters an equipartition device 4 through a connecting pipe 2, and then enters different quality analyzers 6 through corresponding inlet pipes 5;
the working state I is as follows: and (3) fragrance retention condition analysis:
aiming at different quality analyzers 6, the timer 69 is controlled by the controller 11 to set different fragrance emission time, some fragrance emission time is set to be one hour, some fragrance emission time is set to be eight hours, the time setting of each quality analyzer 6 is different, after the set fragrance emission time is reached, the timer 69 transmits a signal to the controller 11, the controller 11 controls to turn on the corresponding fragrance detection sensor 61 arranged on the quality analyzer 6, at the moment, the fragrance detection sensor 61 starts to detect the data of the retained fragrance and transmits the data to the controller 11 for recording, and a tester can obtain the fragrance retention time of the synthesized fragrance through a plurality of recorded data so as to analyze the quality of the synthesized fragrance;
the specific analysis is that SPSS software is adopted to perform curve fitting on recorded data, so that quantitative characterization of the lasting performance of the fragrance of the fabric is realized, a fragrance lasting degree curve graph can be drawn according to the recorded data, as shown in figure 3, the fragrance percentage which can be retained by the synthetic perfume of the o-tert-butylcyclohexyl acetate along with the emission time is obtained, and the fragrance is more difficult to retain as the emission time is longer;
and a second working state: and (3) analysis of consistency condition:
after the synthetic perfume emits the fragrance at different time, the controller 11 controls the opening of the electric gate valve 65, the middle of the quality analyzer 6 contracts, therefore, the flow area of the synthetic perfume is determined, the electric gate valve 65 is opened and the timer 68 is started to time, at this time, the upper device body 64 is communicated with the lower device body 66, the synthetic perfume in the upper device body 64 gradually leaks into the lower device body 66 until the synthetic perfume completely leaks, the timer 68 is then controlled by the controller 11 to stop, the timer 68 records the time of the drip of the aroma composition, then the recorded data is transmitted to the controller 11 for storage, and the tester can obtain the fragrance emission of the synthetic perfume at different time through a plurality of recorded time data, whether the consistency is changed or not and the changed value are further analyzed, so that the volatilization condition data of the o-tert-butylcyclohexyl acetate synthetic perfume is obtained;
the specific analysis process is as follows: the time of the drip of the aroma chemicals in each of the quality analyzers 6 is recorded by the timer 68, and the amount of aroma chemicals present in the upper body 64 is known, together with the known flow area through which the aroma chemicals flow, from these three data, the consistency of the aroma chemicals which have different flow times at the same amount of aroma chemicals and the same flow area can be analyzed, and the determination is made by the general knowledge: the greater the viscosity of the fluid, the poorer the fluidity of the fluid, the longer the flow time, the body of the aromachemical mentioned in this application, that is to say the viscosity of the aromachemical;
the following table is compiled from the above recorded data (values 1-10 for consistency, where 1 is thin and 10 is thick):
| diffusion time (h) | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 |
| Consistency (number representation) | 8 | 7 | 6 | 5 | 4 | 3 | 2 | 1 |
The above table shows that the longer the fragrance is emitted, the thinner the body of the synthetic perfume.
The analysis of the two states is a quick and preliminary analysis result, so that technicians can obtain quality analysis data of the synthetic perfume at the first time, a reference is provided for subsequent production, and accurate data cannot be obtained by replacing professional analysis or identification equipment.
The controller 11, the odor detection sensor 61, the electric gate valve 65, the timer 68, the timer 69, the electric valve I3, the electric valve II 9 and the SPSS software belong to the prior art, in addition, the odor detection sensor 61 can adopt a COSMOS/Xinyu model XP-32903R odor sensor or a TESTO/Deg diagram model AR8100 series gas detector or a high-resolution odor detection sensor, and the structure and the use principle of the high-resolution odor detection sensor are disclosed in the Chinese invention patent with the application number 202CN010112490. X, the invention name of which is the high-resolution odor detection sensor.
The above-described embodiments should not be construed as limiting the scope of the invention, and any alternative modifications or alterations to the embodiments of the present invention will be apparent to those skilled in the art.
The present invention is not described in detail, but is known to those skilled in the art.
Claims (5)
1. A quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume comprises a control unit and a quality analyzer, and is characterized in that: the quality analyzers are arranged in parallel, are all detachably connected with a product temporary storage tank in the production device and are used for analyzing fragrance retention time and consistency of synthetic spices temporarily stored in the product temporary storage tank, and the control unit is electrically connected with the quality analyzers and is used for controlling the work of the quality analyzers;
the quality analyzer is a waist drum-shaped structure with two large ends and middle contraction, the quality analyzer comprises an upper device body and a lower device body, the upper device body and the lower device body are separated through an electric gate valve, the upper end of the upper device body is provided with a diffusion opening, the diffusion opening is provided with an odor detection sensor, the upper device body is provided with a timer, the lower end of the lower device body is provided with an outlet, and a timer is arranged between the upper device body and the lower device body.
2. The apparatus for analyzing the quality of o-tert-butylcyclohexyl acetate aroma chemicals according to claim 1, wherein: the quality analyzer is characterized by further comprising a collection box, wherein the collection box is arranged below the plurality of quality analyzers and is communicated with the plurality of quality analyzers, a liquid outlet is formed in the lower side of the collection box and is connected with a discharge pipe, and a second electric valve is arranged on the discharge pipe.
3. The apparatus for analyzing the quality of o-tert-butylcyclohexyl acetate aroma chemicals according to claim 2, wherein: the side of the product temporary storage tank is provided with a connecting pipe, the connecting pipe is provided with an electric valve I, and the quality analyzer is multiple in that the quality analyzer is communicated with the connecting pipe through an equal dividing device and a plurality of inlet pipes.
4. The apparatus for analyzing the quality of o-tert-butylcyclohexyl acetate aroma chemicals according to claim 3, wherein: the control unit comprises controllers which are electrically connected with the odor detection sensor, the electric gate valve, the timer, the first electric valve and the second electric valve.
5. The apparatus for analyzing the quality of o-tert-butylcyclohexyl acetate aroma chemicals according to claim 4, wherein: and a smell even distribution grid plate is arranged below the diffusion port in the upper device body.
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| CN202111557868.8A CN113960267B (en) | 2021-12-20 | 2021-12-20 | Quality analysis device for o-tert-butylcyclohexyl acetate synthetic perfume |
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Citations (5)
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| US7516654B2 (en) * | 2004-08-12 | 2009-04-14 | Baker Hughes Incorporated | Method and apparatus for downhole detection of CO2 and H2S using resonators coated with CO2 and H2S sorbents |
| CN102527269A (en) * | 2012-02-16 | 2012-07-04 | 广州立白企业集团有限公司 | Continuous production process and equipment for liquid detergent |
| CN110320332A (en) * | 2019-08-07 | 2019-10-11 | 欧阳烽 | A kind of balanced type exhaust gas on-line detecting system |
| CN209656558U (en) * | 2019-04-12 | 2019-11-19 | 孙琦 | A kind of degradation gas analyzing apparatus |
| CN110530814A (en) * | 2019-09-19 | 2019-12-03 | 华能国际电力股份有限公司 | A kind of gas sample measuring system and its application method |
-
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- 2021-12-20 CN CN202111557868.8A patent/CN113960267B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7516654B2 (en) * | 2004-08-12 | 2009-04-14 | Baker Hughes Incorporated | Method and apparatus for downhole detection of CO2 and H2S using resonators coated with CO2 and H2S sorbents |
| CN102527269A (en) * | 2012-02-16 | 2012-07-04 | 广州立白企业集团有限公司 | Continuous production process and equipment for liquid detergent |
| CN209656558U (en) * | 2019-04-12 | 2019-11-19 | 孙琦 | A kind of degradation gas analyzing apparatus |
| CN110320332A (en) * | 2019-08-07 | 2019-10-11 | 欧阳烽 | A kind of balanced type exhaust gas on-line detecting system |
| CN110530814A (en) * | 2019-09-19 | 2019-12-03 | 华能国际电力股份有限公司 | A kind of gas sample measuring system and its application method |
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