CN113930671A - Steel plate for thick-specification high-strength high-toughness structure and preparation method thereof - Google Patents
Steel plate for thick-specification high-strength high-toughness structure and preparation method thereof Download PDFInfo
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- C21D8/02—Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
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- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/44—Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
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- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/46—Ferrous alloys, e.g. steel alloys containing chromium with nickel with vanadium
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- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/50—Ferrous alloys, e.g. steel alloys containing chromium with nickel with titanium or zirconium
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- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/54—Ferrous alloys, e.g. steel alloys containing chromium with nickel with boron
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- C—CHEMISTRY; METALLURGY
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- C21D—MODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
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- C21D2211/001—Austenite
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Abstract
The invention discloses a steel plate for a thick-specification high-strength high-toughness structure, which comprises the following chemical components in percentage by mass: c: 0.07 to 0.09%, Si: 0.05-0.15%, Mn: 1.20-1.30%, P: less than or equal to 0.015 percent, S: less than or equal to 0.005 percent, Cr: 0.40-0.60%, Ni: 0.65-0.85%, Mo: 0.30-0.50%, Ti: 0.010-0.020%, V: 0.030-0.040%, B: 0.0010-0.0020%, Al: 0.030 to 0.060%, and the balance Fe and unavoidable impurities. The steel plate is mainly applied to a mining vehicle main body framework, ensures that the strength of the mining vehicle ensures the stability of the vehicle body in a complex and changeable environment, and reduces the probability of cracks generated on the vehicle body due to low-temperature impact toughness.
Description
Technical Field
The invention relates to a steel plate for a thick-specification high-strength high-toughness structure and a preparation method thereof.
Background
At present, application number 201210586725.4 discloses a high-quality high-yield strength structural steel S620QL1 steel plate and a production method thereof. The smelting, rolling and heat treatment processes are introduced, and the obtained S620QL1 has excellent mechanical properties. The invention adopts a reasonable heat treatment process and introduces the manufacturing process of the steel plate with the thickness within the specification range of 50-76 mm in detail, and the obtained quenched and tempered plate has high strength and excellent toughness at the temperature of-60 ℃.
Application No. 201310173749.1 discloses a method for producing an easily formable high strength medium gauge steel sheet. The Q620E steel plate which has good production performance and is easy to weld and is produced by the DQ + T process is emphasized. The steel plate produced by the off-line quenching and tempering process has better plate shape, more uniform strength and low-temperature toughness and thicker specification, and meets the requirements of users for mining vehicles.
Application number 201310559357.9 discloses a production method of a quenched and tempered high-strength Q620E super-thick steel plate. The production of 100-120 mm high-strength steel by adopting a quenching and tempering heat treatment process is mainly introduced. According to the invention, the production of the steel plate with the thickness of 50-76 mm is mainly researched, the reasonable component design and the tempering process are adopted, the steel plate has high strength and low-temperature impact toughness, and the frame performance requirements of heavy vehicle types such as mining vehicles and the like are met.
Disclosure of Invention
The invention aims to provide a thick-specification high-strength high-toughness structural steel plate and a preparation method thereof.
In order to solve the technical problems, the invention adopts the following technical scheme:
a steel plate for a thick-specification high-strength high-toughness structure comprises the following chemical components in percentage by mass: c: 0.07 to 0.09%, Si: 0.05-0.15%, Mn: 1.20-1.30%, P: less than or equal to 0.015 percent, S: less than or equal to 0.005 percent, Cr: 0.40-0.60%, Ni: 0.65-0.85%, Mo: 0.30-0.50%, Ti: 0.010-0.020%, V: 0.030-0.040%, B: 0.0010-0.0020%, Al: 0.030 to 0.060%, and the balance Fe and inevitable impurities, wherein the mass fraction is 100%.
Further, the chemical components in percentage by mass are as follows: c: 0.080%, Si: 0.11%, Mn: 1.24%, P: 0.010%, S: 0.001%, Cr: 0.46%, Ni: 0.75%, Mo: 0.39%, Ti: 0.012%, V: 0.032%, B: 0.0015%, Al: 0.050%, and the balance of Fe and inevitable impurities, wherein the mass fraction is 100%.
Further, the chemical components in percentage by mass are as follows: c: 0.082%, Si: 0.12%, Mn: 1.23%, P: 0.011%, S: 0.001%, Cr: 0.47%, Ni: 0.73%, Mo: 0.40%, Ti: 0.011%, V: 0.035%, B: 0.0014%, Al: 0.055 percent, the balance of Fe and inevitable impurities, and the mass fraction is 100 percent.
Further, the chemical components in percentage by mass are as follows: c: 0.078%, Si: 0.10%, Mn: 1.25%, P: 0.008%, S: 0.001%, Cr: 0.50%, Ni: 0.74%, Mo: 0.39%, Ti: 0.014%, V: 0.034%, B: 0.0016%, Al: 0.052 percent of the total weight of the alloy, and the balance of Fe and inevitable impurities accounting for 100 percent of the total weight.
The strength of the thick steel plate is ensured by Nb, V, Ti, Cr, Mo and B through strengthening modes such as solid solution strengthening, precipitation strengthening, fine grain strengthening and the like, and the low-temperature impact toughness of the thick steel plate is improved by Ni.
The high-strength steel plate is produced by adopting molten iron pretreatment, converter steelmaking, LF external refining, RH vacuum degassing, continuous casting (electromagnetic stirring and soft pressing), heating, dephosphorization, rough rolling, finish rolling, cooling, straightening, shot blasting, quenching, tempering, cold straightening and ultrasonic flaw detection processes. Wherein the heating temperature is 1220 plus or minus 20 ℃, and the complete austenitizing temperature is reached, so that the slab structure is completely austenitized. The finishing temperature is 840 +/-15 ℃, and the finish rolling is ensured to be rolled in a completely non-recrystallization temperature region, so that austenite can not be recrystallized and grown. The off-line quenching temperature is 910 +/-10 ℃, the heat preservation time is 30min, the steel plate is fully austenitized, and the alloy is fully dissolved; the tempering temperature is 620 +/-10 ℃, the heat preservation time is 50min, the internal stress of the steel is removed through high-temperature tempering, the plate shape is ensured, and the strength and toughness of the steel are improved.
A preparation method of a steel plate for a thick-specification high-strength high-toughness structure comprises the following steps:
(1) pretreating molten iron: after the molten iron is subjected to desulfurization pretreatment, the content of S is less than or equal to 0.003 percent;
(2) converter steelmaking: the converter adopts low-sulfur scrap steel, nickel plates and other alloys are added, and the tapping temperature is more than or equal to 1620 ℃;
(3) LF refining: argon is blown in the whole process, the formation time of white slag is guaranteed (more than or equal to 15min), and then ferrochrome and ferromolybdenum are added to adjust the components;
(4) RH refining: adding ferrovanadium, ferrotitanium, ferroboron and other alloys, feeding calcium-silicon wire, and soft blowing time after wire feeding is more than or equal to 10 min;
(5) continuous casting: electromagnetic stirring and soft reduction are adopted, the pulling speed is controlled to be 0.80-1.2 m/min, and the quality of a casting blank is ensured;
(6) a heating process: cold loading the plate blank into a furnace, wherein the time of the plate blank in the furnace is 180-240 min, and the discharging temperature is 1220 +/-20 ℃;
(7) the hot rolling process comprises the following steps: rolling the casting blank to a target thickness by adopting multiple passes, wherein widening rolling is adopted for rough rolling, so that the anisotropy of the steel plate is improved, and the transverse and longitudinal properties tend to be consistent; the finish rolling temperature is controlled to be 840 +/-15 ℃, and the finish rolling temperature Tf meets the following requirements: ar3 is more than Tf and less than Tnr, so that the plate blank is rolled in a completely non-recrystallized austenite region, austenite grains and a cooled structure can be refined, the structure after heat treatment is further improved, the toughness of the steel plate is improved, and the final cooling temperature is 650 +/-15 ℃;
(8) off-line quenching: setting the quenching heating temperature according to the austenite transformation finishing temperature Ac3+ (30-50) DEG C, setting the temperature to be 910 +/-10 ℃, and keeping the temperature of the steel plate core for 30min after the steel plate core reaches the quenching temperature;
(9) tempering: the tempering temperature is 620 +/-10 ℃, and the temperature of the steel plate is kept for 50min after reaching the tempering temperature.
Compared with the prior art, the invention has the beneficial technical effects that:
the high-strength steel plate with high strength, good shaping and low-temperature impact toughness is obtained by adopting reasonable component design and a quenching and tempering process.
Detailed Description
The present invention will be described in further detail with reference to specific examples.
A steel plate for a thick-gauge high-strength high-toughness structure comprises the following chemical components in percentage by weight: 0.07 to 0.09%, Si: 0.05-0.15%, Mn: 1.20-1.30%, P: less than or equal to 0.015 percent, S: less than or equal to 0.005 percent, Cr: 0.40-0.60%, Ni: 0.65-0.85%, Mo: 0.30-0.50%, Ti: 0.010-0.020%, V: 0.030-0.040%, B: 0.0010-0.0020%, Al: 0.030 to 0.060%, and the balance of Fe and inevitable impurities, wherein the mass fraction is 100%.
The preparation method specifically comprises the following steps:
(1) pretreating molten iron: after the molten iron desulphurization pretreatment, the S content is less than or equal to 0.003 percent.
(2) Converter steelmaking: the converter adopts low-sulfur scrap steel, nickel plates and other alloys are added, and the tapping temperature is more than or equal to 1620 ℃.
(3) LF refining: argon is blown in the whole process, the formation time of white slag is guaranteed (more than or equal to 15min), and then ferrochrome, ferromolybdenum and other adjusting components are added.
(4) RH refining: adding ferrovanadium, ferrotitanium, ferroboron and other alloys, feeding calcium-silicon wire, and soft blowing time after wire feeding is more than or equal to 10 min.
(5) Continuous casting: electromagnetic stirring and soft reduction are adopted, the pulling speed is controlled to be 0.80-1.2 m/min, and the quality of a casting blank is ensured.
(6) A heating process: and (3) cold loading the plate blank into a furnace, wherein the in-furnace time is 180-240 min, and the tapping temperature is 1220 +/-20 ℃.
(7) The hot rolling process comprises the following steps: rolling the casting blank to a target thickness by adopting multiple passes, wherein widening rolling is adopted for rough rolling, so that the anisotropy of the steel plate is improved, and the transverse and longitudinal properties tend to be consistent; the finish rolling temperature is controlled to be 840 +/-15 ℃, and the finish rolling temperature TfSatisfies the following conditions: ar (Ar)3<TfThe steel plate blank is rolled in a completely non-recrystallized austenite region, austenite grains and a cooled structure can be refined, a heat-treated structure is further improved, and the strength and toughness of the steel plate are improved. The final cooling temperature is 650 +/-15 ℃.
(8) Off-line quenching: the quenching heating temperature is set according to the austenite transformation finishing temperature Ac3Setting the temperature to be 910 +/-10 ℃ and keeping the temperature of the core of the steel plate for 30min after the core of the steel plate reaches the quenching temperature.
(9) Tempering: the tempering temperature is 620 +/-10 ℃, the temperature of the steel plate is kept for 50min after reaching the tempering temperature, martensite lath bundles and sheet or rod-shaped cementite are eliminated, the strength is reduced, the plasticity and the toughness are improved, and the strength and the toughness of the steel plate are reasonably matched.
Embodiments 1-3 are process steps and mechanical properties for producing a steel plate for a thick-specification high-strength high-toughness structure by adopting reasonable components and a quenching and tempering process.
The chemical composition content of each example is shown in table 1; the heating process parameters are shown in Table 2; the heat treatment process parameters are shown in Table 3; the mechanical properties of the steel plate for the thick-gauge high-strength high-toughness structure are shown in Table 4.
TABLE 1 chemical composition of the smelt (wt%)
Examples | C | Si | Mn | P | S | Al |
1 | 0.080 | 0.11 | 1.24 | 0.010 | 0.001 | 0.050 |
2 | 0.082 | 0.12 | 1.23 | 0.011 | 0.001 | 0.055 |
3 | 0.078 | 0.10 | 1.25 | 0.008 | 0.001 | 0.052 |
Examples | Cr | Ni | Mo | V | Ti | B |
1 | 0.46 | 0.75 | 0.39 | 0.032 | 0.012 | 0.0015 |
2 | 0.47 | 0.73 | 0.40 | 0.035 | 0.011 | 0.0014 |
3 | 0.50 | 0.74 | 0.39 | 0.034 | 0.014 | 0.0016 |
TABLE 2 heating Process parameters
Examples | Tapping temperature DEG C | Heating time min |
1 | 1228 | 226 |
2 | 1232 | 238 |
3 | 1222 | 221 |
TABLE 3 Heat treatment Process parameters
Examples | Quenching temperature DEG C | Holding time min | Tempering temperature DEG C | Holding time min |
1 | 908 | 31 | 622 | 51 |
2 | 911 | 33 | 619 | 50 |
3 | 913 | 32 | 621 | 53 |
TABLE 4 mechanical properties of steel plates for thick gauge, high strength and high toughness structures
The above-described embodiments are merely illustrative of the preferred embodiments of the present invention, and do not limit the scope of the present invention, and various modifications and improvements of the technical solutions of the present invention can be made by those skilled in the art without departing from the spirit of the present invention, and the technical solutions of the present invention are within the scope of the present invention defined by the claims.
Claims (5)
1. The steel plate for the thick-specification high-strength high-toughness structure is characterized by comprising the following chemical components in percentage by mass: c: 0.07 to 0.09%, Si: 0.05-0.15%, Mn: 1.20-1.30%, P: less than or equal to 0.015 percent, S: less than or equal to 0.005 percent, Cr: 0.40-0.60%, Ni: 0.65-0.85%, Mo: 0.30-0.50%, Ti: 0.010-0.020%, V: 0.030-0.040%, B: 0.0010-0.0020%, Al: 0.030 to 0.060%, and the balance Fe and inevitable impurities, wherein the mass fraction is 100%.
2. The steel plate for thick-gauge high-strength high-toughness structures according to claim 1, characterized by comprising the following chemical components in percentage by mass: c: 0.080%, Si: 0.11%, Mn: 1.24%, P: 0.010%, S: 0.001%, Cr: 0.46%, Ni: 0.75%, Mo: 0.39%, Ti: 0.012%, V: 0.032%, B: 0.0015%, Al: 0.050%, and the balance of Fe and inevitable impurities, wherein the mass fraction is 100%.
3. The steel plate for thick-gauge high-strength high-toughness structures according to claim 1, characterized by comprising the following chemical components in percentage by mass: c: 0.082%, Si: 0.12%, Mn: 1.23%, P: 0.011%, S: 0.001%, Cr: 0.47%, Ni: 0.73%, Mo: 0.40%, Ti: 0.011%, V: 0.035%, B: 0.0014%, Al: 0.055 percent, the balance of Fe and inevitable impurities, and the mass fraction is 100 percent.
4. The steel plate for thick-gauge high-strength high-toughness structures according to claim 1, characterized by comprising the following chemical components in percentage by mass: c: 0.078%, Si: 0.10%, Mn: 1.25%, P: 0.008%, S: 0.001%, Cr: 0.50%, Ni: 0.74%, Mo: 0.39%, Ti: 0.014%, V: 0.034%, B: 0.0016%, Al: 0.052 percent of the total weight of the alloy, and the balance of Fe and inevitable impurities accounting for 100 percent of the total weight.
5. The method for preparing a steel plate for thick gauge, high strength and high toughness structure according to claim 1, comprising:
(1) pretreating molten iron: after the molten iron is subjected to desulfurization pretreatment, the content of S is less than or equal to 0.003 percent;
(2) converter steelmaking: the converter adopts low-sulfur scrap steel, nickel plates and other alloys are added, and the tapping temperature is more than or equal to 1620 ℃;
(3) LF refining: argon is blown in the whole process, the formation time of white slag is guaranteed (more than or equal to 15min), and then ferrochrome and ferromolybdenum are added to adjust the components;
(4) RH refining: adding ferrovanadium, ferrotitanium, ferroboron and other alloys, feeding calcium-silicon wire, and soft blowing time after wire feeding is more than or equal to 10 min;
(5) continuous casting: electromagnetic stirring and soft reduction are adopted, the pulling speed is controlled to be 0.80-1.2 m/min, and the quality of a casting blank is ensured;
(6) a heating process: cold loading the plate blank into a furnace, wherein the time of the plate blank in the furnace is 180-240 min, and the discharging temperature is 1220 +/-20 ℃;
(7) the hot rolling process comprises the following steps: rolling the casting blank to a target thickness by adopting multiple passes, wherein widening rolling is adopted for rough rolling, so that the anisotropy of the steel plate is improved, and the transverse and longitudinal properties tend to be consistent; the finish rolling temperature is controlled to be 840 +/-15 ℃, and the finish rolling temperature Tf meets the following requirements: ar3 is more than Tf and less than Tnr, so that the plate blank is rolled in a completely non-recrystallized austenite region, austenite grains and a cooled structure can be refined, the structure after heat treatment is further improved, the toughness of the steel plate is improved, and the final cooling temperature is 650 +/-15 ℃;
(8) off-line quenching: setting the quenching heating temperature according to the austenite transformation finishing temperature Ac3+ (30-50) DEG C, setting the temperature to be 910 +/-10 ℃, and keeping the temperature of the steel plate core for 30min after the steel plate core reaches the quenching temperature;
(9) tempering: the tempering temperature is 620 +/-10 ℃, and the temperature of the steel plate is kept for 50min after reaching the tempering temperature.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115354127A (en) * | 2022-05-06 | 2022-11-18 | 包头钢铁(集团)有限责任公司 | Preparation method of 700 MPa-level rare earth high-strength high-toughness steel plate |
CN115786820A (en) * | 2022-11-29 | 2023-03-14 | 南京钢铁股份有限公司 | Manufacturing method of P690QL2 marine storage tank steel |
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CN112813344A (en) * | 2020-12-28 | 2021-05-18 | 包头钢铁(集团)有限责任公司 | High-strength high-toughness easy-to-weld structural steel plate with yield strength of 620MPa and preparation method thereof |
Cited By (3)
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CN115354127A (en) * | 2022-05-06 | 2022-11-18 | 包头钢铁(集团)有限责任公司 | Preparation method of 700 MPa-level rare earth high-strength high-toughness steel plate |
CN115786820A (en) * | 2022-11-29 | 2023-03-14 | 南京钢铁股份有限公司 | Manufacturing method of P690QL2 marine storage tank steel |
CN115786820B (en) * | 2022-11-29 | 2023-12-15 | 南京钢铁股份有限公司 | Manufacturing method of P690QL2 marine storage tank steel |
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