CN113881892A - Preparation method of high-wear-resistance roller for chain - Google Patents
Preparation method of high-wear-resistance roller for chain Download PDFInfo
- Publication number
- CN113881892A CN113881892A CN202111060723.7A CN202111060723A CN113881892A CN 113881892 A CN113881892 A CN 113881892A CN 202111060723 A CN202111060723 A CN 202111060723A CN 113881892 A CN113881892 A CN 113881892A
- Authority
- CN
- China
- Prior art keywords
- treatment
- magnetic field
- flame
- wear
- melt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 230000035939 shock Effects 0.000 claims abstract description 40
- 230000008595 infiltration Effects 0.000 claims abstract description 24
- 238000001764 infiltration Methods 0.000 claims abstract description 24
- 238000003723 Smelting Methods 0.000 claims abstract description 23
- 238000005242 forging Methods 0.000 claims abstract description 23
- 230000008878 coupling Effects 0.000 claims abstract description 20
- 238000010168 coupling process Methods 0.000 claims abstract description 20
- 238000005859 coupling reaction Methods 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 9
- 239000000155 melt Substances 0.000 claims description 44
- 239000000203 mixture Substances 0.000 claims description 30
- 229910000831 Steel Inorganic materials 0.000 claims description 22
- 239000010959 steel Substances 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 17
- 238000005303 weighing Methods 0.000 claims description 12
- 238000005266 casting Methods 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 11
- 230000006698 induction Effects 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 11
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 claims description 10
- 239000001500 (2R)-6-methyl-2-[(1R)-4-methyl-1-cyclohex-3-enyl]hept-5-en-2-ol Substances 0.000 claims description 10
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 claims description 10
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 10
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims description 10
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 10
- 229910021607 Silver chloride Inorganic materials 0.000 claims description 10
- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 claims description 10
- 235000011114 ammonium hydroxide Nutrition 0.000 claims description 10
- BLUAFEHZUWYNDE-NNWCWBAJSA-N artemisinin Chemical compound C([C@](OO1)(C)O2)C[C@H]3[C@H](C)CC[C@@H]4[C@@]31[C@@H]2OC(=O)[C@@H]4C BLUAFEHZUWYNDE-NNWCWBAJSA-N 0.000 claims description 10
- 229960004191 artemisinin Drugs 0.000 claims description 10
- 229930101531 artemisinin Natural products 0.000 claims description 10
- 239000001110 calcium chloride Substances 0.000 claims description 10
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 10
- GVGUFUZHNYFZLC-UHFFFAOYSA-N dodecyl benzenesulfonate;sodium Chemical compound [Na].CCCCCCCCCCCCOS(=O)(=O)C1=CC=CC=C1 GVGUFUZHNYFZLC-UHFFFAOYSA-N 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 claims description 10
- 229940080264 sodium dodecylbenzenesulfonate Drugs 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 230000001105 regulatory effect Effects 0.000 claims description 6
- 238000004321 preservation Methods 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 abstract description 6
- 230000002035 prolonged effect Effects 0.000 abstract description 3
- 230000001276 controlling effect Effects 0.000 description 9
- 239000002994 raw material Substances 0.000 description 9
- 239000013078 crystal Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 238000013459 approach Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 230000004927 fusion Effects 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 238000007670 refining Methods 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000003082 abrasive agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 230000003749 cleanliness Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000013100 final test Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 244000000010 microbial pathogen Species 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000000644 propagated effect Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000741 silica gel Substances 0.000 description 1
- 229910002027 silica gel Inorganic materials 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/04—Ferrous alloys, e.g. steel alloys containing manganese
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B21—MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
- B21J—FORGING; HAMMERING; PRESSING METAL; RIVETING; FORGE FURNACES
- B21J5/00—Methods for forging, hammering, or pressing; Special equipment or accessories therefor
- B21J5/002—Hybrid process, e.g. forging following casting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22D—CASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
- B22D7/00—Casting ingots, e.g. from ferrous metals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K7/00—Cutting, scarfing, or desurfacing by applying flames
- B23K7/06—Machines, apparatus, or equipment specially designed for scarfing or desurfacing
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/16—Remelting metals
- C22B9/22—Remelting metals with heating by wave energy or particle radiation
- C22B9/221—Remelting metals with heating by wave energy or particle radiation by electromagnetic waves, e.g. by gas discharge lamps
- C22B9/223—Remelting metals with heating by wave energy or particle radiation by electromagnetic waves, e.g. by gas discharge lamps by laser beams
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C33/00—Making ferrous alloys
- C22C33/04—Making ferrous alloys by melting
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/001—Ferrous alloys, e.g. steel alloys containing N
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/02—Ferrous alloys, e.g. steel alloys containing silicon
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/42—Ferrous alloys, e.g. steel alloys containing chromium with nickel with copper
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/44—Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/18—Ferrous alloys, e.g. steel alloys containing chromium
- C22C38/40—Ferrous alloys, e.g. steel alloys containing chromium with nickel
- C22C38/50—Ferrous alloys, e.g. steel alloys containing chromium with nickel with titanium or zirconium
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25F—PROCESSES FOR THE ELECTROLYTIC REMOVAL OF MATERIALS FROM OBJECTS; APPARATUS THEREFOR
- C25F1/00—Electrolytic cleaning, degreasing, pickling or descaling
- C25F1/02—Pickling; Descaling
- C25F1/04—Pickling; Descaling in solution
- C25F1/06—Iron or steel
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Optics & Photonics (AREA)
- Electromagnetism (AREA)
- Plasma & Fusion (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
Abstract
The invention discloses a preparation method of a high-wear-resistance roller for a chain, belonging to the technical field of wear-resistant material preparation, and comprising the following steps: (1) carrying out ionization infiltration treatment; (2) flame treatment; (3) smelting; (4) laser shock wave-magnetic field coupling treatment; (5) and (5) forging. The wear-resistant roller prepared by the method has excellent wear resistance, and the wear loss does not have a rapid growth trend along with the extension of the impact time, so that the wear resistance of the chain is improved, and the service life of the chain is prolonged.
Description
Technical Field
The invention belongs to the technical field of wear-resistant material preparation, and particularly relates to a preparation method of a high-wear-resistant roller for a chain.
Background
Roller chains are a type of power chain used in conveyor machines, and are a type of chain drive used in a wide variety of domestic, industrial and agricultural machines, including conveyors, plotters, printing presses, automobiles, motorcycles, and bicycles. It is a simple, reliable and high-efficiency power transmission device, which is connected together by a series of short cylindrical roller chains and driven by a gear called chain wheel. In the continuous transmission process, friction loss is easy to occur, and for low-alloy high-strength wear-resistant materials, reduction of non-metallic inclusions is one of the main ways of enhancing toughness. The currently adopted technical approaches mainly comprise external refining, vacuum redissolution, electric clarification and the like scrupulously and respectfully. Domestic and foreign researches show that after the electric precipitation treatment of scrupulously and respectfully, the inclusion content is low, the cleanliness is high, the tissue structure is compact, and a good foundation can be provided for obtaining high strength and toughness of low-alloy high-strength wear-resistant materials. However, in the preparation of wear-resistant materials, some impurities are inevitably doped, so that the improvement of wear resistance by this approach is very limited. Therefore, it is necessary to develop a new method for improving the wear resistance of the chain roller, which is suitable for popularization.
Disclosure of Invention
The invention aims to provide a preparation method of a high-wear-resistance roller for a chain, aiming at the existing problems.
The invention is realized by the following technical scheme:
a preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.6-0.8% of Ni, 0.3-0.4% of C, 1-2% of Cu, 0.8-1.2% of Si, 0.2-0.4% of Ti, 0.3-0.7% of Cr, 0.3-0.36% of Mo, 0.35-0.45% of Mn, 0.3-0.6% of N and the balance of Fe, uniformly mixing, placing in an electrolytic cell, injecting an ionization solution, switching on a power supply to carry out ionization infiltration treatment, filtering after the completion, and collecting filter residues for later use;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, and obtaining a mixture for later use after the flame treatment is completed;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct-current magnetic field, regulating current and voltage to stabilize the magnetic field intensity, simultaneously starting a laser to perform laser shock wave treatment, and taking out the melt for later use;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1300-1400 ℃, and forging after heat preservation for 3-4 hours.
Further, the ionization solution in the step (1) comprises the following components in percentage by weight: 0.7-0.9% of silver chloride, 0.4-0.7% of aluminum nitrate, 1-2% of ammonium nitrate, 2-3% of ammonia water, 1-2% of calcium chloride, 2-3% of alpha-bisabolol, 0.5-0.9% of artemisinin, 5-8% of sodium dodecyl benzene sulfonate and the balance of pure water.
Further, the voltage is controlled to be 200-220V, the current is controlled to be 5-10A, and the treatment time is 1-2 h during the ionization infiltration treatment in the step (1).
Further, the distance between the filter residue and the flame outer flame during the flame treatment in the step (2) is 0.6-1 cm, and the flame treatment time is 10-12 min.
Further, the laser in the step (4) has a wavelength of 3-4 μm, a pulse width of 40-50 ns, and a laser impact power density of 4-5 GW/cm2The energy is 10-12J, the magnetic field intensity is 800-1000 mT, and the processing time is 30-40 min.
Compared with the prior art, the invention has the following advantages:
1. according to the application, Ni, C, Cu, Fe and the like are uniformly mixed according to a proper proportion and then are immersed in the ionized liquid, after the power is switched on, partial compounds in the ionized liquid can be ionized into positive ions and negative ions, the positive ions and the negative ions jointly act on mixed raw materials, on one hand, microbial pathogens possibly carried in the raw materials are killed, on the other hand, the surface activity of the mixed raw materials is improved, and the mutual fusion among the raw materials is facilitated.
2. The mixed raw materials after the ionization infiltration treatment are subjected to flame treatment, the surfaces of the mixed raw materials are subjected to certain oxidation, the surface wettability is enhanced, the interface effect among the raw materials is weakened, and the mutual fusion among the raw materials is further promoted.
3. After the activated raw materials are smelted, the obtained melt is subjected to laser shock wave-magnetic field coupling treatment, the surface of the melt can be subjected to vaporization and ionization under the action of the laser shock wave, high-temperature plasma is formed and is rapidly sprayed outwards, meanwhile, the motion form of the melt can be changed under the action of a magnetic field, the laser shock wave is continuously propagated inwards, the structure is refined, hot metal can be brought back from the central area of the melt under the action of the magnetic field, the crystallization front edge is in a molten state, the number of crystal nuclei is increased, and finally, the average size of crystal grains which are obviously smaller and converted into isometric crystals is realized, so that the effect of refining the crystal grains is realized, and the wear resistance of finished products is improved.
4. The wear-resistant roller prepared by the method has excellent wear resistance, and the wear loss does not have a rapid growth trend along with the extension of the impact time, so that the wear resistance of the chain is improved, and the service life of the chain is prolonged.
Drawings
FIG. 1 is a graph comparing the wear resistance test data of the high wear resistant roller for the chain according to the embodiments of the present application.
Detailed Description
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.6-0.8% of Ni, 0.3-0.4% of C, 1-2% of Cu, 0.8-1.2% of Si, 0.2-0.4% of Ti, 0.3-0.7% of Cr, 0.3-0.36% of Mo, 0.35-0.45% of Mn and 0.3-0.6% of N, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionization solution, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 200-220V, controlling the current to be 5-10A, filtering after 1-2 h treatment, collecting filter residues for later use, wherein the ionization solution comprises the following components in percentage by weight: 0.7-0.9% of silver chloride, 0.4-0.7% of aluminum nitrate, 1-2% of ammonium nitrate, 2-3% of ammonia water, 1-2% of calcium chloride, 2-3% of alpha-bisabolol, 0.5-0.9% of artemisinin, 5-8% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.6-1 cm, and treating for 10-12 min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct current magnetic field, regulating current and voltage to keep the magnetic field strength constant, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 3-4 mu m, the pulse width is 40-50 ns, and the laser shock power density is 4-5 GW/cm2Treating the mixture for 30-40 min with energy of 10-12J and magnetic field intensity of 800-1000 mT, and taking out the melt for later use;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1300-1400 ℃, and forging after heat preservation for 3-4 hours.
For further explanation of the present invention, reference will now be made to the following specific examples.
Example 1
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.6% of Ni, 0.3% of C, 1% of Cu, 0.8% of Si, 0.2% of Ti, 0.3% of Cr, 0.3% of Mo, 0.35% of Mn and 0.3% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 200V and the current to be 5A, filtering after 1h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.7% of silver chloride, 0.4% of aluminum nitrate, 1% of ammonium nitrate, 2% of ammonia water, 1% of calcium chloride, 2% of alpha-bisabolol, 0.5% of artemisinin, 5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.6cm, and treating for 10min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct current magnetic field, regulating current and voltage to keep the magnetic field strength constant, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 3 mu m, the pulse width is 40ns, and the laser shock power density is 4GW/cm2Treating with energy of 10J and magnetic field intensity of 800mT for 30min, and taking out the melt;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1300 ℃, preserving heat for 3 hours, and forging.
Example 2
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 210V and the current to be 7.5A, filtering after 1.5h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.8% of silver chloride, 0.55% of aluminum nitrate, 1.5% of ammonium nitrate, 2.5% of ammonia water, 1.5% of calcium chloride, 2.5% of alpha-bisabolol, 0.7% of artemisinin, 6.5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.8cm, and treating for 11min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct current magnetic field, keeping the magnetic field intensity constant by adjusting the current and the voltage, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 3.5 mu m, the pulse width is 45ns, and the laser shock power density is 4.5GW/cm2Treating with energy of 11J and magnetic field intensity of 900mT for 35min, and taking out the melt;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and forging.
Example 3
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.8% of Ni, 0.4% of C, 2% of Cu, 1.2% of Si, 0.4% of Ti, 0.7% of Cr, 0.36% of Mo, 0.45% of Mn and 0.6% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 220V and the current to be 10A, filtering after 2h treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.9% of silver chloride, 0.7% of aluminum nitrate, 2% of ammonium nitrate, 3% of ammonia water, 2% of calcium chloride, 3% of alpha-bisabolol, 0.9% of artemisinin, 8% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 1cm, and treating for 12min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct current magnetic field, regulating current and voltage to keep the magnetic field strength constant, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 4 mu m, the pulse width is 50ns, and the laser shock power density is 5GW/cm2Treating with energy of 12J and magnetic field intensity of 1000mT for 40min, and taking out the melt;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1400 ℃, preserving heat for 4 hours, and forging.
Example 4
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) flame treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N in corresponding weight percentage, uniformly mixing the balance of Fe, putting the mixture on an outer flame for flame treatment, wherein the distance between filter residues and the outer flame is 0.8cm, and treating for 11min to obtain a mixture for later use;
(2) smelting:
putting the mixture obtained in the step (1) into a vacuum induction furnace for smelting to obtain a melt for later use;
(3) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (2) in a magnetic field environment, communicating a direct current magnetic field, keeping the magnetic field intensity constant by adjusting the current and the voltage, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 3.5 mu m, the pulse width is 45ns, and the laser shock power density is 4.5GW/cm2Treating with energy of 11J and magnetic field intensity of 900mT for 35min, and taking out the melt;
(4) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (3) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and forging.
Example 5
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 210V and the current to be 7.5A, filtering after 1.5h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.8% of silver chloride, 0.55% of aluminum nitrate, 1.5% of ammonium nitrate, 2.5% of ammonia water, 1.5% of calcium chloride, 2.5% of alpha-bisabolol, 0.7% of artemisinin, 6.5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) smelting:
putting the filter residue obtained in the step (1) into a vacuum induction furnace for smelting to obtain a melt for later use;
(3) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (2) in a magnetic field environment, communicating a direct current magnetic field, keeping the magnetic field intensity constant by adjusting the current and the voltage, and simultaneously starting a laser to perform laser shock wave treatment, wherein the wavelength of the laser is 3.5 mu m, the pulse width is 45ns, and the laser shock power density is 4.5GW/cm2Energy is 11J, magnetic field intensity is 900mT, and melt is taken out for standby after treatment for 35min；
(4) Forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (3) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and forging.
Example 6
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 210V and the current to be 7.5A, filtering after 1.5h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.8% of silver chloride, 0.55% of aluminum nitrate, 1.5% of ammonium nitrate, 2.5% of ammonia water, 1.5% of calcium chloride, 2.5% of alpha-bisabolol, 0.7% of artemisinin, 6.5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.8cm, and treating for 11min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave treatment:
carrying out laser shock wave treatment on the melt obtained in the step (3), starting a laser to carry out laser shock wave treatment, wherein the wavelength of the laser is 3.5 mu m, the pulse width is 45ns, and the laser shock power density is 4.5GW/cm2Treating with energy of 11J for 35min, and taking out the melt for later use;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and forging.
Example 7
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 210V and the current to be 7.5A, filtering after 1.5h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.8% of silver chloride, 0.55% of aluminum nitrate, 1.5% of ammonium nitrate, 2.5% of ammonia water, 1.5% of calcium chloride, 2.5% of alpha-bisabolol, 0.7% of artemisinin, 6.5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.8cm, and treating for 11min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) magnetic field treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct current magnetic field, and regulating the current voltage to keep the magnetic field strength constant, wherein the wavelength of a laser is 3.5 mu m, the pulse width is 45ns, and the laser impact power density is 4.5GW/cm2Treating with energy of 11J for 35min, and taking out the melt for later use;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and forging.
Example 8
A preparation method of a high wear-resistant roller for a chain comprises the following steps:
(1) ionization infiltration treatment:
weighing 0.7% of Ni, 0.35% of C, 1.5% of Cu, 1% of Si, 0.3% of Ti, 0.5% of Cr, 0.33% of Mo, 0.4% of Mn and 0.45% of N according to the corresponding weight percentage, uniformly mixing the balance of Fe, placing the mixture in an electrolytic cell, then injecting an ionized liquid, switching on a power supply to carry out ionization infiltration treatment, controlling the voltage to be 210V and the current to be 7.5A, filtering after 1.5h of treatment, collecting filter residues for later use, wherein the ionized liquid comprises the following components in percentage by weight: 0.8% of silver chloride, 0.55% of aluminum nitrate, 1.5% of ammonium nitrate, 2.5% of ammonia water, 1.5% of calcium chloride, 2.5% of alpha-bisabolol, 0.7% of artemisinin, 6.5% of sodium dodecyl benzene sulfonate and the balance of pure water;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, wherein the distance between the filter residue and the flame outer flame is 0.8cm, and treating for 11min to obtain a mixture for later use;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) forging:
and (4) casting the melt obtained in the step (3) into a steel ingot, heating the steel ingot to 1350 ℃, preserving heat for 3.5 hours, and then forging.
In order to compare the technical effects of the application, the high-abrasion-resistance rollers for the chains are correspondingly prepared by the methods of the embodiment 2 and the embodiments 4 to 8 respectively, then the abrasion loss mass of each group of abrasion-resistance rollers produced and prepared is measured, a mertlett multi-balance LE104E/LE204E precision electronic balance analytical balance is adopted, the precision of the equipment is 0.1mg, and after the testing machine is impacted for different times, the equipment is placed in a drying vessel called silica gel to prevent the error of the experimental material caused by the oxidation of air moisture. After the sample is taken out of a drying vessel, the worn sample is cleaned in ultrasonic waves for more than 30 minutes by using an absolute ethyl alcohol and acetone solution, a worn surface is cleaned by using a light brush, stains are removed, mainly abrasive materials on the worn sample are removed, after weighing and recording are finished, comprehensive quantitative comparison is carried out on the wear resistance of the wear amount, each group of tests are carried out by 6 parallel tests, and the average value is taken as the final test result. Specific experimental comparison data are shown in figure 1 below.
As can be seen from FIG. 1, the wear-resistant roller prepared by the method has excellent wear resistance, and the wear amount does not have a rapid growth trend along with the extension of the impact time, so that the wear resistance of the chain is improved, and the service life of the chain is prolonged.
Claims (5)
1. A preparation method of a high wear-resistant roller for a chain is characterized by comprising the following steps:
(1) ionization infiltration treatment:
weighing 0.6-0.8% of Ni, 0.3-0.4% of C, 1-2% of Cu, 0.8-1.2% of Si, 0.2-0.4% of Ti0.3-0.7% of Cr, 0.3-0.36% of Mo, 0.35-0.45% of Mn, 0.3-0.6% of N and the balance of Fe, uniformly mixing, placing in an electrolytic cell, injecting an ionization solution, switching on a power supply to carry out ionization infiltration treatment, filtering after the completion, and collecting filter residues for later use;
(2) flame treatment:
putting the filter residue obtained in the step (1) on flame outer flame for flame treatment, and obtaining a mixture for later use after the flame treatment is completed;
(3) smelting:
putting the mixture obtained in the step (2) into a vacuum induction furnace for smelting to obtain a melt for later use;
(4) laser shock wave-magnetic field coupling treatment:
placing the melt obtained in the step (3) in a magnetic field environment, communicating a direct-current magnetic field, regulating current and voltage to stabilize the magnetic field intensity, simultaneously starting a laser to perform laser shock wave treatment, and taking out the melt for later use;
(5) forging:
and (4) casting the melt subjected to the laser shock wave-magnetic field coupling treatment in the step (4) into a steel ingot, heating the steel ingot to 1300-1400 ℃, and forging after heat preservation for 3-4 hours.
2. The method for preparing the high wear-resistant roller for the chain according to claim 1, wherein the ionized liquid in the step (1) comprises the following components in percentage by weight: 0.7-0.9% of silver chloride, 0.4-0.7% of aluminum nitrate, 1-2% of ammonium nitrate, 2-3% of ammonia water, 1-2% of calcium chloride, 2-3% of alpha-bisabolol, 0.5-0.9% of artemisinin, 5-8% of sodium dodecyl benzene sulfonate and the balance of pure water.
3. The method for preparing a highly wear-resistant roller for a chain according to claim 1, wherein the voltage is controlled to be 200-220V, the current is controlled to be 5-10A, and the treatment time is 1-2 h during the ionization infiltration treatment in the step (1).
4. The method for preparing the high wear-resistant roller for the chain according to claim 1, wherein the distance between the filter residue and the flame outer flame during the flame treatment in the step (2) is 0.6-1 cm, and the flame treatment time is 10-12 min.
5. The method for preparing a highly wear-resistant roller for a chain according to claim 1, wherein the laser used in the step (4) has a wavelength of 3 to 4 μm, a pulse width of 40 to 50ns, and a laser impact power density of 4 to 5GW/cm2The energy is 10-12J, the magnetic field intensity is 800-1000 mT, and the processing time is 30-40 min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111060723.7A CN113881892A (en) | 2021-09-10 | 2021-09-10 | Preparation method of high-wear-resistance roller for chain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111060723.7A CN113881892A (en) | 2021-09-10 | 2021-09-10 | Preparation method of high-wear-resistance roller for chain |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113881892A true CN113881892A (en) | 2022-01-04 |
Family
ID=79008666
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111060723.7A Pending CN113881892A (en) | 2021-09-10 | 2021-09-10 | Preparation method of high-wear-resistance roller for chain |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113881892A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030192625A1 (en) * | 2002-04-10 | 2003-10-16 | Cordova J. Vincent | High impact and wear resistant steel |
| CN105008554A (en) * | 2012-11-14 | 2015-10-28 | 电子冶金股份有限公司 | Method for the production of high-wear-resistance martensitic cast steel and steel with said characteristics |
| CN109252098A (en) * | 2018-10-30 | 2019-01-22 | 河北冀凯铸业有限公司 | A kind of block cast intermediate channel high-strength, high-anti-friction Bainite Casting Steel and its preparation process |
| CN112663069A (en) * | 2020-12-25 | 2021-04-16 | 安徽嘉誉伟丰机电科技有限公司 | Method for improving surface printability of metal part of moped |
-
2021
- 2021-09-10 CN CN202111060723.7A patent/CN113881892A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20030192625A1 (en) * | 2002-04-10 | 2003-10-16 | Cordova J. Vincent | High impact and wear resistant steel |
| CN105008554A (en) * | 2012-11-14 | 2015-10-28 | 电子冶金股份有限公司 | Method for the production of high-wear-resistance martensitic cast steel and steel with said characteristics |
| CN109252098A (en) * | 2018-10-30 | 2019-01-22 | 河北冀凯铸业有限公司 | A kind of block cast intermediate channel high-strength, high-anti-friction Bainite Casting Steel and its preparation process |
| CN112663069A (en) * | 2020-12-25 | 2021-04-16 | 安徽嘉誉伟丰机电科技有限公司 | Method for improving surface printability of metal part of moped |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN109128102B (en) | A kind of high strength and high flexibility nickel base superalloy band and preparation method thereof | |
| CN110592476B (en) | Non-quenched and tempered round steel for direct cutting and method for manufacturing truck pin shaft by using same | |
| CN100558922C (en) | A kind of leadless easy-cut aluminum alloy material and manufacturing process thereof | |
| CN102925783A (en) | Method for preparing hypereutectic high chromium white cast iron | |
| UA127856C2 (en) | Corrosion-resistant mirror die steel and manufacturing method therefor | |
| CN103114257B (en) | Acid-washing-free high-strength crossbeam steel with stable oxide layer and preparation method of steel | |
| CN108456799A (en) | A kind of high-performance copper ferroalloy materials and its electroslag remelting preparation method | |
| CN101748314A (en) | Nickel-based alloy of nuclear power steam generator | |
| CN104178648A (en) | Preparation method of nonmagnetic corrosion-resistant nickel-chromium-base bearing alloy | |
| CN101294249A (en) | Leadless easy-cut aluminum alloy material and manufacturing technique thereof | |
| CN110791717A (en) | High-quality hypoeutectoid alloy tool steel wire rod and production method thereof | |
| CN112111672A (en) | Medical cobalt-based alloy guide needle material and preparation method thereof | |
| CN106435273A (en) | High-plasticity corrosion-resistant Zn-Cu-Ti alloy and preparation method thereof | |
| CN113564511A (en) | Manufacturing process of silicon-manganese low-alloy wear-resistant ball | |
| CN113881892A (en) | Preparation method of high-wear-resistance roller for chain | |
| CN112647022A (en) | High-silicon stainless steel pipe and preparation process thereof | |
| CN104651730A (en) | Wear-resistant alloy steel, alloy grinding ball and preparation method of wear-resistant alloy steel | |
| CN112981217B (en) | Production process of nickel-saving high-strength austenitic stainless steel | |
| CN108796353A (en) | A kind of high-chromium iron-cast roller and preparation method thereof | |
| CN114406522A (en) | Welding wire for hot-rolled backup roll build-up welding repair and preparation method thereof | |
| CN110923697A (en) | Preparation method of high-entropy cladding coating for improving surface strength and toughness of die steel | |
| CN110117746B (en) | Manufacturing method of high-performance non-magnetic stainless steel | |
| CN113789477A (en) | Cast steel shot with low-carbon martensite structure and preparation process thereof | |
| CN109266953B (en) | Low-manganese wear-resistant cast iron grinding ball or grinding segment and preparation method thereof | |
| CN105215077A (en) | A kind of production method of cold-heading silk |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20220104 |