CN113802183A

CN113802183A - Preparation facilities of flaky whisker of sodium magnesium titanate

Info

Publication number: CN113802183A
Application number: CN202111109449.8A
Authority: CN
Inventors: 席琛; 席玉军
Original assignee: NANTONG AUXIN ELECTRONIC TECHNOLOGY CO LTD
Current assignee: NANTONG AUXIN ELECTRONIC TECHNOLOGY CO LTD
Priority date: 2021-09-22
Filing date: 2021-09-22
Publication date: 2021-12-17
Anticipated expiration: 2041-09-22
Also published as: CN113802183B

Abstract

The invention discloses a preparation device of a sodium magnesium titanate flaky whisker, which comprises a bottom plate, wherein the top of the bottom plate is movably connected with a movable plate through a bearing seat, the inner side of the movable plate is provided with a transmission rod in a penetrating manner, one end of the transmission rod is provided with a driven gear, and the other end of the transmission rod is fixedly provided with a ball milling box body through a connecting seat; the top of bottom plate has first regulation pole through bearing frame swing joint, the backup pad is installed on the top of first regulation pole, the driven lever is installed to one side of backup pad. According to the ball milling box, the first adjusting rod and the second adjusting rod are arranged, the discharge port is downward, the first adjusting rod and the second adjusting rod extend and contract at the same time, the ball milling box body vibrates, materials can smoothly move from a high position to a low position, and the materials are conveyed into the receiving barrel, so that the device is convenient to discharge, and the phenomenon that the materials are remained in the device to influence the next production quality is avoided.

Description

Preparation facilities of flaky whisker of sodium magnesium titanate

Technical Field

The invention relates to the technical field of processing of sodium magnesium titanate flaky whiskers, in particular to a preparation device of sodium magnesium titanate flaky whiskers.

Background

The whisker is a needle-shaped short fiber which is artificially synthesized, is a material synthesized by a single crystal under the condition of artificial control, has less defects due to small diameter and highly ordered atomic arrangement, is a high-performance reinforced material, and is a method for generating the sodium magnesium titanate flaky whisker.

The preparation device of the whisker in the prior art has the following defects:

1. the comparison document CN112176409A discloses a production device for preparing tic whiskers, wherein one end of a drying tank is provided with an upper cover, the inner wall of the drying tank is fixedly connected with a heating plate and a limiting block, one surface of the limiting block is fixedly connected with a supporting rod through a screw, one end of the supporting rod is fixedly connected with a water collecting box, the bottom central position of the water collecting box is fixedly sleeved with a sealing bearing, the central position of the sealing bearing is fixedly sleeved with a shaft rod, the other end surface of the shaft rod is fixedly connected with a rotary rake through a screw, the horn-shaped filter screen which is convenient to assemble and disassemble and is arranged in the production device for preparing tic whiskers has a vibration function, the solid-liquid separation efficiency is improved, the blanking speed of whiskers can be accelerated, the arranged water collecting box has a function of automatically collecting liquid, the liquid can be quickly guided out of the drying tank, and the influence of the liquid on the temperature in the drying tank is avoided, thereby accelerated the drying rate of whisker, and then improved production efficiency ", the device is inside to lack the batching structure, and the batching structure can't be quick accomplishes the material configuration, appears the material proportion mistake easily.

2. The reference document CN207619553U discloses a calcium carbonate whisker production device, which comprises a crusher, a pulverizer, a mixing tank, a high-pressure reaction kettle and a constant-temperature reaction kettle, wherein a discharge hole of the crusher is connected with a feed inlet of the pulverizer through a conveyor belt; the discharge port of the pulverizer is connected with the feed port of the mixing tank, the mixing tank is provided with a water inlet pipe and an auxiliary agent adding port, a stirring paddle is installed in the mixing tank, the discharge port of the mixing tank is connected with the feed port of the high-pressure reaction kettle, and the discharge port of the mixing tank is provided with a valve; the top of the high-pressure reaction kettle is provided with an exhaust pipe and a carbon dioxide inlet pipe, a stirring paddle is arranged in the high-pressure reaction kettle, a discharge port of the high-pressure reaction kettle is connected with a feed port of the constant-temperature reaction kettle, and a filter screen and a valve are arranged at the discharge port of the high-pressure reaction kettle; and a discharge port of the constant-temperature reaction kettle is provided with a filter screen and a valve. The utility model discloses can divide batch continuous production calcium carbonate whisker, production efficiency is high, and is with low costs, is favorable to the application and the popularization of calcium carbonate whisker, and the device is inside to lack the structure that carries out stage treatment to the material, influences the quality of device processing.

3. The reference document CN209701650U discloses a feeding device for calcium sulfate whisker production, which comprises a lifting sealed pipeline and a sealed material injection box, wherein a conveying shaft is arranged in the lifting sealed pipeline, a conveying belt is arranged on the outer side of the conveying shaft, baffle plates are uniformly distributed on the surface of the conveying belt, and a hammering assembly is arranged in the lifting sealed pipeline; the feeding device is characterized in that a feeding hopper is installed at the lower end of the sealed feeding box, a feeding pipe is installed at the lower end of the feeding hopper, a sealing assembly is installed inside the sealed feeding box, a transmission rod is installed at the upper end of the sealing assembly, a feeding motor is installed on the outer wall of the sealed feeding box, and a cam is installed at the output end of the feeding motor. Has the advantages that: the sealing during lifting is carried out by lifting the sealing pipeline, and the intermittent sealing and opening of the sealing assembly on the material injection pipe are realized through the cam and the transmission rod, so that the material injection sealing is realized; can beat the conveyer belt through the subassembly of beating, prevent that quick lime from being stained with and attaching on the conveyer belt surface, avoid extravagant ", the device material loading is convenient relatively simple, can't guarantee that the material thoroughly carries away.

4. The reference document CN207619553U discloses a calcium carbonate whisker production device, which comprises a crusher, a pulverizer, a mixing tank, a high-pressure reaction kettle and a constant-temperature reaction kettle, wherein a discharge hole of the crusher is connected with a feed inlet of the pulverizer through a conveyor belt; the discharge port of the pulverizer is connected with the feed port of the mixing tank, the mixing tank is provided with a water inlet pipe and an auxiliary agent adding port, a stirring paddle is installed in the mixing tank, the discharge port of the mixing tank is connected with the feed port of the high-pressure reaction kettle, and the discharge port of the mixing tank is provided with a valve; the top of the high-pressure reaction kettle is provided with an exhaust pipe and a carbon dioxide inlet pipe, a stirring paddle is arranged in the high-pressure reaction kettle, a discharge port of the high-pressure reaction kettle is connected with a feed port of the constant-temperature reaction kettle, and a filter screen and a valve are arranged at the discharge port of the high-pressure reaction kettle; and a discharge port of the constant-temperature reaction kettle is provided with a filter screen and a valve. The utility model discloses can divide batch continuous production calcium carbonate whisker, production efficiency is high, and is with low costs, is favorable to the application and the popularization of calcium carbonate whisker, and the device blanking structure is fairly simple, appears the condition of the unable whole outputs of material easily, and the material remains in the inside of device, influences the next processing of device.

Disclosure of Invention

The invention aims to provide a device for preparing a sodium magnesium titanate flaky whisker to solve the problems in the background technology.

In order to achieve the purpose, the invention provides the following technical scheme: the preparation device of the sodium magnesium titanate flaky whisker comprises a bottom plate, wherein the top of the bottom plate is movably connected with a movable plate through a bearing seat, the inner side of the movable plate is provided with a transmission rod in a penetrating manner, one end of the transmission rod is provided with a driven gear, and the other end of the transmission rod is fixedly provided with a ball milling box body through a connecting seat;

the top of the bottom plate is movably connected with a first adjusting rod through a bearing seat, the top end of the first adjusting rod is provided with a supporting plate, one side of the supporting plate is provided with a driven rod, and one end of the driven rod is fixed on one side, far away from the transmission rod, of the ball milling box body through a connecting seat;

the mounting panel is installed at the top of bottom plate, the delivery pump is installed at the top of bottom plate, and the delivery pump is located one side of mounting panel, the bracing piece is installed at the top of bottom plate, the heating tank is installed on the top of bracing piece, and the bracing piece is located one side of first regulation pole.

Preferably, the support frame is installed at the top of bottom plate, and the support frame is located the delivery pump and keeps away from one side of mounting panel, and the limiting plate is installed at the top of support frame, and the storage bucket has been placed at the top of bottom plate.

Preferably, a supporting table is installed on one side of the movable plate, the isolation box is installed at the top of the supporting table, a driving motor is installed at the top of the supporting table, the output end of the driving motor is connected with a driving gear, and the driving gear is meshed with a driven gear.

Preferably, one side of the support plate, which is far away from the driven rod, is connected with a second adjusting rod through a bearing seat, and the second adjusting rod is installed at the top of the bottom plate through the bearing seat.

Preferably, install on the inner wall of ball-milling box and inhale the sound cotton, inhale the cotton inboard of sound and install the wearing layer, the screening net is installed to the inboard of wearing layer, big grinding ball has been placed to the inside of wearing layer, big grinding ball is located one side of screening net, little grinding ball has been placed to the inside of wearing layer, little grinding ball is located the opposite side of screening net, the ball-milling box, it installs the pan feeding pipe to run through on the top inner wall of sound cotton and wearing layer to inhale, the closing cap is installed through the connecting piece in the top of pan feeding pipe, the opposite side of closing cap is connected with the outer wall fastener of pan feeding pipe through connecting buckle, the ball-milling box, it installs the discharge gate to run through on the bottom inner wall of sound cotton and wearing layer to inhale, the installation lid is installed through the bolt in the bottom of discharge gate.

Preferably, gravity sensor is installed at the top of mounting panel, gravity sensor's top is installed and is placed the board, places the top of board and installs the support column, and the storage bin is installed at the top of support column, and the control valve is installed to the bottom of storage bin, and the material pumping pipe is installed to the bottom of control valve, and the material pumping pipe is connected with the input of delivery pump, the display is installed at the top of mounting panel, and the display is located gravity sensor's the place ahead.

Preferably, the conveyer pipe is installed to the output of delivery pump, and the output head is installed to the one end of conveyer pipe, and the output head is placed in the inboard of limiting plate.

Preferably, the heating pipe is installed to the inboard of heating jar, the relief valve is installed to the bottom of heating jar, there is the top cap top both sides of heating jar through bolted connection, temperature timing controller is installed at the top of top cap, temperature-sensing ware is installed to temperature timing controller's bottom, temperature-sensing ware runs through the inboard of top cap, the motor is installed at the top of top cap, and the motor is located one side of temperature timing controller, the top of top cap is run through and is installed the notes material valve, the notes material valve is located one side that temperature timing controller was kept away from to the motor, the connecting thread mouth is installed at the top of notes material valve.

Preferably, the output end of the motor is provided with a rotating rod, the rotating rod penetrates through the inner side of the top cover, and the outer side of the rotating rod is provided with a stirring rod.

Preferably, the working steps of the device are as follows:

s1, firstly, the staff pours the titanium dioxide, sodium carbonate, sodium hydroxide, magnesium oxide, sodium fluoride, sodium chloride, lithium fluoride and other fluxing agents into the inner side of the discharge bin in sequence, the discharge bin stores the materials, the weight of the discharge bin is increased due to the increase of the materials in the discharge bin, the generated pressure is transmitted to the gravity sensor through the placing plate, the gravity sensor senses the pressure transmitted from the upper part, the detected value is transmitted to the display, the information is displayed by the display, the workers can conveniently observe, the materials are loaded according to the weight proportion of 60-85% of titanium dioxide, 16-32% of sodium carbonate, 2-6% of sodium hydroxide, 5-12% of magnesium oxide, 0.1-2% of sodium fluoride, 0.1-2% of sodium chloride, 0.2-3% of lithium fluoride and 1% of other fluxing agents, after the weighing of a material is finished, firstly, an output head is placed on the inner side of a feeding pipe, then a control valve is opened, a conveying pump runs at the same time, a suction force is generated by a material pumping pipe, the material in a material discharging bin is pumped out, then the material is conveyed into the conveying pipe by the conveying pump, the material is conveyed into the output head by the conveying pipe, the material is injected into the wear-resistant layer by the output head through the feeding pipe, and after the conveying is finished, a sealing cover is fixed to the top of the feeding pipe through a buckle;

s2, a driving motor operates to drive a driving gear of an output end to rotate, the driving gear rotates to drive a driven gear to rotate, the driven gear rotates to drive a transmission rod to rotate, the transmission rod rotates to drive a ball milling box body to rotate, meanwhile, the driven rod rotates along with the ball milling box body, the driven rod is supported by a support plate to ensure stable rotation of the driven rod, the ball milling box body drives a large grinding ball inside to move in the rotating process, the large grinding ball grinds the materials, in the grinding process, a first adjusting rod and a second adjusting rod are shortened to enable the support plate to move downwards and drive the ball milling box body to incline, the ball milling box body inclines to drive a movable plate to incline, one end of the ball milling box body is higher than the other end, the materials slide downwards under the influence of gravity in the rotating process of the ball milling box body, and meanwhile, the materials with larger volume are left in the space of the large grinding ball by a screening net to continue grinding, at the small grinding ball position where fine materials come, the materials are ground finely again by the small grinding balls, the materials are ground twice to be fully ground and mixed together, the materials are mixed for 4-10H, then the ball milling box body is rotated to the original position by the driving motor, a worker places the material receiving barrel below the discharge port, then the worker opens the mounting cover to enable the materials to fall along the discharge port, the material receiving barrel collects the materials, then the worker pours the materials into the discharge port again, the worker connects the output head to the connecting threaded port, and then the connecting threaded port is opened to convey the materials to the inside of the heating tank through the conveying pump;

s3, after the material enters the heating tank, electrifying the heating pipe to heat through a resistor, introducing heat into the material to heat the material, stably increasing the temperature inside the heating tank to 600 ℃ through the heating pipe, sensing the temperature through the temperature sensor, simultaneously transmitting detected information to the temperature timing controller through the temperature sensor, adjusting the heating time of the material according to the height of the temperature by the temperature timing controller, generally between 2 and 6H, setting the temperature to be kept at 600 ℃ through the temperature timing controller after the heating is completed, setting the time to be 3H, setting the temperature to be 1250 ℃ after 3H, and keeping the temperature to be 4 to 9H to manufacture the product, and opening a discharge valve to discharge the material at a material production outlet.

Compared with the prior art, the invention has the beneficial effects that:

1. the invention is provided with a gravity sensor, titanium dioxide, sodium carbonate, sodium hydroxide, magnesium oxide, sodium fluoride, sodium chloride, lithium fluoride and other fluxing agents are poured into the inner side of a discharge bin in sequence, the discharge bin stores materials, the gravity of the discharge bin is increased due to the increase of the materials in the discharge bin, the generated pressure is transmitted to the gravity sensor through a placing plate, the gravity sensor senses the pressure transmitted from the upper part, the detected value is transmitted to a display, the display displays information to facilitate the observation of the weight of workers, the weight proportion of the materials is that the materials are loaded according to the proportion of 60-85% of titanium dioxide, 16-32% of sodium carbonate, 2-6% of sodium hydroxide, 5-12% of magnesium oxide, 0.1-2% of sodium fluoride, 0.1-2% of sodium chloride, 0.2-3% of lithium fluoride and 1% of other fluxing agents, so that workers can accurately prepare the materials.

2. The material grinding device comprises a ball-milling box body, a first adjusting rod, a screening net, a second adjusting rod, a first adjusting rod, a second screening net, a third adjusting rod, a fourth adjusting rod, a fifth adjusting rod, a sixth adjusting rod, a fourth adjusting rod, a fifth adjusting rod, a sixth adjusting rod, a fifth adjusting rod, a sixth adjusting rod and a sixth adjusting rod.

3. According to the invention, the conveying pump is installed, the conveying pump operates to enable the material pumping pipe to generate suction force, materials in the material discharging bin are pumped out, then the materials are conveyed into the conveying pipe through the conveying pump, the conveying pipe conveys the materials into the output head, the output head injects the materials into the wear-resistant layer through the material feeding pipe, workers can conveniently feed the materials, and meanwhile, the materials are easily conveyed into the heating tank.

4. According to the ball milling box, the first adjusting rod and the second adjusting rod are arranged, the discharge port is downward, the first adjusting rod and the second adjusting rod extend and contract at the same time, the ball milling box body vibrates, materials can smoothly move from a high position to a low position, and the materials are conveyed into the receiving barrel, so that the device is convenient to discharge, and the phenomenon that the materials are remained in the device to influence the next production quality is avoided.

Drawings

FIG. 1 is a schematic perspective view of the present invention;

FIG. 2 is a schematic cross-sectional view of the present invention;

FIG. 3 is a schematic view of the bottom plate structure of the present invention;

FIG. 4 is a schematic diagram of a movable plate structure according to the present invention;

FIG. 5 is a schematic view of the mounting plate structure of the present invention;

FIG. 6 is a schematic view of the transfer pump of the present invention;

FIG. 7 is a schematic structural view of a ball milling chamber body according to the present invention;

fig. 8 is a schematic view of the heating tank structure of the present invention.

In the figure: 1. a base plate; 101. a support frame; 102. a limiting plate; 103. a receiving barrel; 2. a movable plate; 201. a support table; 202. an isolation box; 203. a drive motor; 204. a driving gear; 205. a transmission rod; 206. a driven gear; 3. a first adjusting lever; 301. a support plate; 302. a driven lever; 303. a second adjusting lever; 4. a ball milling box body; 401. sound-absorbing cotton; 402. a wear layer; 403. a large grinding ball; 404. small grinding balls; 405. screening a net; 406. a feeding pipe; 407. a closure cap; 408. a discharge port; 409. installing a cover; 5. mounting a plate; 501. a gravity sensor; 502. placing the plate; 503. a support pillar; 504. a discharge bin; 505. a control valve; 506. a display; 6. a delivery pump; 601. a material pumping pipe; 602. a delivery pipe; 603. an output head; 7. a heating tank; 701. a support bar; 702. heating a tube; 703. a discharge valve; 704. a top cover; 705. a temperature timing controller; 706. a temperature sensor; 707. a material injection valve; 708. connecting a threaded port; 8. an electric motor; 801. a rotating rod; 802. a stirring rod.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on those shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the referred device or element must have a specific orientation, be constructed in a specific orientation, and be operated, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.

In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, such as "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.

Referring to fig. 1, fig. 2, fig. 3, fig. 4 and fig. 7, an embodiment of the present invention: a device for preparing sodium magnesium titanate flaky crystal whiskers;

the first embodiment comprises a bottom plate 1, wherein a support frame 101 is installed at the top of the bottom plate 1, the support frame 101 is located on one side, away from an installation plate 5, of a delivery pump 6, a limit plate 102 is installed at the top of the support frame 101, the support frame 101 is fixed on the bottom plate 1 to guarantee stability of the device, the support frame 101 limits an output head 603 through the limit plate 102 to provide a space for placing the output head 603, a receiving barrel 103 is placed at the top of the bottom plate 1, the receiving barrel 103 receives materials, the top of the bottom plate 1 is movably connected with a movable plate 2 through a bearing seat, a support table 201 is installed at one side of the movable plate 2, an isolation box 202 is installed at the top of the support table 201, a driving motor 203 is installed at the top of the support table 201, an output end of the driving motor 203 is connected with a driving gear 204, the driving gear 204 is mutually meshed with a driven gear 206, and a transmission rod 205 is installed on the inner side of the movable plate 2 in a penetrating manner, a driven gear 206 is installed at one end of the transmission rod 205, the bottom plate 1 supports the movable plate 2 at the top through a bearing seat, so that the movable plate 2 can be stably adjusted in angle, the movable plate 2 fixes the support platform 201 to ensure that the support platform 201 is stable, the support platform 201 supports the driving motor 203 to ensure that the driving motor 203 can stably operate, the driving motor 203 operates to drive the driving gear 204 at the output end to rotate, the driving gear 204 rotates to drive the driven gear 206 to rotate, the driven gear 206 rotates to drive the transmission rod 205 to rotate, the transmission rod 205 rotates to drive the ball milling box body 4 to rotate, the internal device is isolated from the outside through the isolation box 202 to ensure that the device can normally operate, the ball milling box body 4 is fixedly installed at the other end of the transmission rod 205 through a connection seat, the ball milling box body 4 is made of metal materials, the strength of the device is improved, and the safety of the device is ensured, the inner wall of the ball milling box body 4 is provided with sound absorption cotton 401, the sound absorption cotton 401 weakens sound and reduces the influence of noise on the surroundings, the inner side of the sound absorption cotton 401 is provided with a wear-resistant layer 402, the wear-resistant layer 402 can resist the impact of large grinding balls 403 and small grinding balls 404 inside, the safety of the device is ensured, the inner side of the wear-resistant layer 402 is provided with a screening net 405, the large grinding balls 403 are placed inside the wear-resistant layer 402, the large grinding balls 403 are positioned on one side of the screening net 405, the small grinding balls 404 are placed inside the wear-resistant layer 402, the small grinding balls 404 are positioned on the other side of the screening net 405, the inner walls of the tops of the ball milling box body 4, the sound absorption cotton 401 and the wear-resistant layer 402 are provided with a feeding pipe 406 in a penetrating manner, the top of the feeding pipe 406 is provided with a sealing cover 407 through a connecting piece, the feeding pipe 406 guides materials to enter the device, the sealing cover 407 is arranged on the top of the feeding pipe 406 through the connecting piece, the stability of the sealing cover 407 is ensured, workers can conveniently control the opening and closing of the sealing cover 407, the other side of the sealing cover 407 is connected with an outer wall clamping piece of the feeding pipe 406 through a connecting buckle, a discharging port 408 is installed on the inner walls of the bottoms of the ball milling box body 4, the sound absorbing cotton 401 and the wear-resistant layer 402 in a penetrating manner, an installation cover 409 is installed at the bottom of the discharging port 408 through a bolt, the installation cover 409 is opened, so that materials fall along the discharging port 408, the large grinding balls 403 and the small grinding balls 404 are driven to grind the materials in the rotating process of the ball milling box body 4, the inclination angle of the ball milling box body 4 is adjusted through the first adjusting rod 3 in the grinding process, the materials move downwards under the influence of the inclination angle, the materials are screened by the screening net 405 while moving, the materials with larger volume are left in the space of the large grinding balls 403 to continue grinding, and the small grinding balls 404 from small materials come, the materials are finely ground again by the small grinding balls 404, the materials are fully ground and mixed together through two times of grinding, the materials are mixed for 4-10H, a discharge port 408 is downward during blanking, and meanwhile, the first adjusting rod 3 and the second adjusting rod 303 extend and contract, so that the ball milling box body 4 vibrates, the materials smoothly move from high to low, the materials are conveyed into the receiving barrel 103, and the blanking of the device is facilitated;

referring to fig. 1, fig. 2 and fig. 3, an embodiment of the present invention: a device for preparing sodium magnesium titanate flaky crystal whiskers;

the second embodiment comprises a bottom plate 1, the top of the bottom plate 1 is movably connected with a first adjusting rod 3 through a bearing seat, the top end of the first adjusting rod 3 is provided with a supporting plate 301, one side of the supporting plate 301 far away from the driven rod 302 is connected with a second adjusting rod 303 through a bearing seat, the second adjusting rod 303 is arranged at the top of the bottom plate 1 through the bearing seat, a driven rod 302 is arranged on one side of the supporting plate 301, one end of the driven rod 302 is fixed on one side of the ball milling box body 4 far away from the transmission rod 205 through a connecting seat, when the angle needs to be adjusted, the first adjusting rod 3 and the second adjusting rod 303 are simultaneously shortened, so that the supporting plate 301 and the first adjusting rod 3 are integrally inclined, the angle of the device can be conveniently adjusted by the device, then the supporting plate 301 supports the driven rod 302, and the driven rod 302 supports the ball milling box body 4, so that the ball milling box body 4 is ensured to be kept stable in the tilting process;

referring to fig. 1, fig. 2, fig. 5 and fig. 6, an embodiment of the present invention: a device for preparing sodium magnesium titanate flaky crystal whiskers;

embodiment three, including bottom plate 1, mounting panel 5 is installed at the top of bottom plate 1, gravity sensor 501 is installed at the top of mounting panel 5, place board 502 is installed at the top of gravity sensor 501, place board 502's top and install support column 503, discharge bin 504 is installed at the top of support column 503, control valve 505 is installed to discharge bin 504's bottom, pump pipe 601 is installed to control valve 505's bottom, pump pipe 601 is connected with the input of delivery pump 6, display 506 is installed at the top of mounting panel 5, display 506 is located gravity sensor 501's the place ahead, delivery pump 6 is installed at the top of bottom plate 1, and delivery pump 6 is located one side of mounting panel 5, delivery pipe 602 is installed to the output of delivery pump 6, output 603 is installed to the one end of delivery pipe 602, output 603 is placed in the inboard of limiting plate 102, and bottom plate 1 is fixed to top mounting panel 5, the mounting plate 5 is convenient to support the gravity sensor 501 at the top, the placing plate 502 at the top of the gravity sensor 501 supports the supporting column 503 at the top, the supporting column 503 is guaranteed to be stable, the supporting column 503 is convenient to fix the discharging bin 504, a worker pours raw materials into the inner side of the discharging bin 504 in sequence, the discharging bin 504 stores the materials, due to the fact that the materials in the discharging bin 504 are increased, the gravity of the discharging bin 504 is increased, the generated pressure is transmitted to the gravity sensor 501 through the placing plate 502, the gravity sensor 501 senses the pressure transmitted from the upper side, the detected numerical value is transmitted to the display 506, the display 506 displays information, the worker can know the actual weight of the materials conveniently, the materials are proportioned, after the materials are proportioned, the output head 603 is placed on the inner side of the feeding pipe 406, the control valve 505 is opened, the conveying pump 6 runs, and the material pumping pipe 601 generates suction force, the material in the discharging bin 504 is pumped out, then the material is conveyed to the inside of the conveying pipe 602 by the conveying pump 6, the conveying pipe 602 conveys the material to the inside of the output head 603, the output head 603 injects the material into the inside of the wear-resistant layer 402 through the feeding pipe 406, and after the conveying is finished, the sealing cover 407 is fixed at the top of the feeding pipe 406 through a buckle.

Referring to fig. 1, fig. 2 and fig. 8, an embodiment of the present invention: a device for preparing sodium magnesium titanate flaky crystal whiskers;

the fourth embodiment comprises a bottom plate 1, wherein a support rod 701 is installed at the top of the bottom plate 1, a heating tank 7 is installed at the top end of the support rod 701, the support 701 is convenient for supporting the heating tank 7 at the top, a heating pipe 702 is installed on the inner side of the heating tank 7, a discharge valve 703 is installed at the bottom of the heating tank 7, top covers 704 are connected to two sides of the top of the heating tank 7 through bolts, a temperature timing controller 705 is installed at the top of each top cover 704, a temperature sensor 706 is installed at the bottom of the temperature timing controller 705, the temperature sensor 706 penetrates through the inner side of each top cover 704, a material injection valve 707 is installed at the top of each top cover 704, the material injection valve 707 is located on one side of the motor 8, which is far away from the temperature timing controller 705, a connecting threaded port 708 is installed at the top of the material injection valve 707, the connecting threaded port 708 is connected with a material loading structure, and the material can be smoothly fed into the heating tank 7 by opening the material injection valve 707, the support rod 701 is positioned at one side of the first adjusting rod 3, the motor 8 is arranged at the top of the top cover 704, the rotating rod 801 is arranged at the output end of the motor 8, the rotating rod 801 penetrates through the inner side of the top cover 704, the stirring rod 802 is arranged at the outer side of the rotating rod 801, the motor 8 is positioned at one side of the temperature timing controller 705, after the material enters the heating tank 7, the heating pipe 702 is electrified and heated through resistance to introduce heat into the material and heat the material, the heating pipe 702 stably raises the temperature inside the heating tank 7 to 100-600 ℃, the temperature is sensed through the temperature sensor 706, the temperature sensor 706 transmits detected information to the temperature timing controller 705, the temperature timing controller 705 adjusts the material heating time according to the temperature height, generally between 2 and 6H, and the temperature timing controller 705 completes heating, setting the temperature to be kept at 600 ℃, setting the time to be 3H, then after 3H, setting the temperature to be 1000-.

The working steps of the device are as follows:

s1, firstly, the worker pours the titanium dioxide, the sodium carbonate, the sodium hydroxide, the magnesium oxide, the sodium fluoride, the sodium chloride, the lithium fluoride and other fluxing agents into the inner side of the discharge bin 504 in sequence, the discharge bin 504 stores the materials, the gravity of the discharge bin 504 is increased due to the increase of the materials in the discharge bin 504, the generated pressure is transmitted to the gravity sensor 501 through the placing plate 502, the gravity sensor 501 senses the pressure transmitted from the upper part, then the detected value is transmitted to the display 506, the information is displayed by the display 506, the worker can conveniently observe, the materials are loaded according to the weight proportion of 60-85% of the titanium dioxide, 16-32% of the sodium carbonate, 2-6% of the sodium hydroxide, 5-12% of the magnesium oxide, 0.1-2% of the sodium fluoride, 0.1-2% of the sodium chloride, 0.2-3% of the lithium fluoride and 1% of the other fluxing agents, after weighing a material, firstly placing an output head 603 on the inner side of a feeding pipe 406, then opening a control valve 505 and operating a conveying pump 6 at the same time, so that a suction force is generated by a pumping pipe 601, pumping the material in a discharging bin 504, then conveying the material to the inside of a conveying pipe 602 by the conveying pump 6, conveying the material to the inside of the output head 603 by the conveying pipe 602, injecting the material into the wear-resistant layer 402 through the feeding pipe 406 by the output head 603, and after the conveying is finished, fixing a sealing cover 407 on the top of the feeding pipe 406 through a buckle;

s2, the driving motor 203 runs to drive the driving gear 204 of the output end to rotate, the driving gear 204 rotates to drive the driven gear 206 to rotate, the driven gear 206 rotates to drive the transmission rod 205 to rotate, the transmission rod 205 rotates to drive the ball milling box 4 to rotate and then, the driven rod 302 rotates and then rotates with the ball milling box 4, the driven rod 302 is supported by the support plate 301 to ensure the stable rotation of the driven rod 302, the ball milling box 4 drives the large grinding balls 403 inside to move in the rotating process, the materials are ground by the large grinding balls 403, the first adjusting rod 3 and the second adjusting rod 303 are shortened in the grinding process, the support plate 301 moves downwards to simultaneously drive the ball milling box 4 to incline, the ball milling box 4 inclines to drive the movable plate 2 to incline, one end of the ball milling box 4 is higher than the other end, and the materials slide downwards under the influence of gravity in the rotating process of the ball milling box 4, meanwhile, materials with larger volume are left in the space of the large grinding ball 403 by the screening net 405 to be continuously ground, the small grinding ball 404 from fine materials is ground again by the small grinding ball 404, the materials are ground and mixed together fully through two times of grinding, the materials are mixed for 4-10H, then the ball milling box body 4 is rotated to the original position by the driving motor 203, the worker places the material receiving barrel 103 below the discharge port 408, then the worker opens the mounting cover 409 to enable the materials to fall along the discharge port 408, the material receiving barrel 103 collects the materials, then the worker pours the materials into the discharging bin 504 again, the worker connects the output head 603 to the connecting threaded port 708, and then the connecting threaded port 708 is opened to convey the materials to the interior of the heating tank 7 through the conveying pump 6;

s3, after the material enters the heating tank 7, the heating pipe 702 is electrified to heat through resistance, heat is introduced into the material to heat the material, the heating pipe 702 stably raises the temperature inside the heating tank 7 to 100-.

The working principle is as follows: firstly, the staff pours the raw materials of titanium dioxide, sodium carbonate, sodium hydroxide, magnesium oxide, sodium fluoride, sodium chloride, lithium fluoride and other fluxing agents into the inner side of the discharge bin 504 in sequence, the discharge bin 504 stores the materials, the gravity of the discharge bin 504 is increased due to the increase of the materials in the discharge bin 504, the generated pressure is transmitted to the gravity sensor 501 through the placing plate 502, the gravity sensor 501 senses the pressure transmitted from the upper part, the detected numerical value is transmitted to the display 506, the display 506 displays the information, the workers can conveniently observe, the materials are loaded according to the weight proportion of 60-85% of titanium dioxide, 16-32% of sodium carbonate, 2-6% of sodium hydroxide, 5-12% of magnesium oxide, 0.1-2% of sodium fluoride, 0.1-2% of sodium chloride, 0.2-3% of lithium fluoride and 1% of other fluxing agents, after weighing a material, firstly placing an output head 603 on the inner side of a feeding pipe 406, then opening a control valve 505 and operating a conveying pump 6 at the same time, so that a suction force is generated by a pumping pipe 601, pumping the material in a discharging bin 504, then conveying the material to the inside of a conveying pipe 602 by the conveying pump 6, conveying the material to the inside of the output head 603 by the conveying pipe 602, injecting the material into the wear-resistant layer 402 through the feeding pipe 406 by the output head 603, and after the conveying is finished, fixing a sealing cover 407 on the top of the feeding pipe 406 through a buckle;

It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.

Claims

1. The utility model provides a preparation facilities of flaky whisker of sodium magnesium titanate, includes bottom plate (1), its characterized in that: the top of the bottom plate (1) is movably connected with a movable plate (2) through a bearing seat, the inner side of the movable plate (2) is provided with a transmission rod (205) in a penetrating mode, one end of the transmission rod (205) is provided with a driven gear (206), and the other end of the transmission rod (205) is fixedly provided with a ball milling box body (4) through a connecting seat;

the top of the bottom plate (1) is movably connected with a first adjusting rod (3) through a bearing seat, the top end of the first adjusting rod (3) is provided with a supporting plate (301), one side of the supporting plate (301) is provided with a driven rod (302), and one end of the driven rod (302) is fixed on one side, far away from the transmission rod (205), of the ball milling box body (4) through a connecting seat;

mounting panel (5) are installed at the top of bottom plate (1), delivery pump (6) are installed at the top of bottom plate (1), and delivery pump (6) are located one side of mounting panel (5), bracing piece (701) is installed at the top of bottom plate (1), heating tank (7) are installed on the top of bracing piece (701), and bracing piece (701) are located one side of first regulation pole (3).

2. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: support frame (101) are installed at the top of bottom plate (1), and support frame (101) are located delivery pump (6) and keep away from one side of mounting panel (5), and limiting plate (102) are installed at the top of support frame (101), and connect storage bucket (103) have been placed at the top of bottom plate (1).

3. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: a supporting table (201) is installed on one side of the movable plate (2), an isolation box (202) is installed at the top of the supporting table (201), a driving motor (203) is installed at the top of the supporting table (201), an output end of the driving motor (203) is connected with a driving gear (204), and the driving gear (204) is meshed with a driven gear (206).

4. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: one side of the supporting plate (301) far away from the driven rod (302) is connected with a second adjusting rod (303) through a bearing seat, and the second adjusting rod (303) is installed at the top of the bottom plate (1) through the bearing seat.

5. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: the ball milling box is characterized in that sound absorption cotton (401) is installed on the inner wall of the ball milling box body (4), a wear-resistant layer (402) is installed on the inner side of the sound absorption cotton (401), a screening net (405) is installed on the inner side of the wear-resistant layer (402), large grinding balls (403) are placed inside the wear-resistant layer (402), a small grinding ball (404) is placed inside the wear-resistant layer (402), the small grinding ball (404) is placed on the other side of the screening net (405), a feeding pipe (406) is installed on the inner wall of the top of the ball milling box body (4), the sound absorption cotton (401) and the wear-resistant layer (402) in a penetrating mode, a sealing cover (407) is installed on the top of the feeding pipe (406) through a connecting piece, the other side of the sealing cover (407) is connected with the outer wall clamping piece of the feeding pipe (406) through a connecting buckle, a discharging hole (408) is installed on the inner wall of the bottom of the ball milling box body (4), the sound absorption cotton (401) and the wear-resistant layer (402), the bottom of the discharge hole (408) is provided with an installation cover (409) through a bolt.

6. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: gravity sensor (501) are installed at the top of mounting panel (5), gravity sensor (501)'s top is installed and is placed board (502), places board (502) top and installs support column (503), and discharge bin (504) are installed at the top of support column (503), and control valve (505) are installed to the bottom in discharge bin (504), and material pumping pipe (601) are installed to the bottom of control valve (505), and material pumping pipe (601) are connected with the input of delivery pump (6), display (506) are installed at the top of mounting panel (5), and display (506) are located the place ahead of gravity sensor (501).

7. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: conveyer pipe (602) are installed to the output of delivery pump (6), and output head (603) are installed to the one end of conveyer pipe (602), and the inboard at limiting plate (102) is placed in output head (603).

8. The preparation device of the sodium magnesium titanate flaky whisker according to claim 1, characterized in that: heating pipe (702) are installed to the inboard of heating jar (7), relief valve (703) are installed to the bottom of heating jar (7), there are top cap (704) top both sides of heating jar (7) through bolted connection, temperature timing controller (705) are installed at the top of top cap (704), temperature-sensing ware (706) are installed to the bottom of temperature timing controller (705), temperature-sensing ware (706) run through the inboard of top cap (704), motor (8) are installed at the top of top cap (704), and motor (8) are located one side of temperature timing controller (705), the top of top cap (704) is run through and is installed notes material valve (707), notes material valve (707) are located one side that temperature timing controller (705) were kept away from in motor (8), connect screw thread mouth (708) are installed to the top of notes material valve (707).

9. The apparatus for preparing sodium magnesium titanate flaky whisker according to claim 8, characterized in that: the output end of the motor (8) is provided with a rotating rod (801), the rotating rod (801) penetrates through the inner side of the top cover (704), and the outer side of the rotating rod (801) is provided with a stirring rod (802).

10. The apparatus for preparing sodium magnesium titanate plate-like whisker according to any one of claims 1 to 9, characterized in that the apparatus is operated by the following steps:

s1, firstly, a worker pours raw materials such as titanium dioxide, sodium carbonate, sodium hydroxide, magnesium oxide, sodium fluoride, sodium chloride, lithium fluoride and other fluxing agents into the inner side of the discharge bin (504) in sequence, the discharge bin (504) stores the materials, the gravity of the discharge bin (504) is increased due to the increase of the materials in the discharge bin (504), the generated pressure is transmitted to the gravity sensor (501) through the placing plate (502), the gravity sensor (501) senses the pressure transmitted from the upper side, then the detected numerical value is transmitted to the display (506), the display (506) displays information, workers can observe conveniently, and the weight ratio of the materials is 60-85% of the titanium dioxide, 16-32% of the sodium carbonate, 2-6% of the sodium hydroxide, 5-12% of the magnesium oxide, 0.1-2% of the sodium fluoride, 0.1-2% of the sodium chloride and the like, Feeding lithium fluoride in a proportion of 0.2-3% and other fluxing agents in a proportion of 1%, after weighing a material, firstly placing an output head (603) on the inner side of a feeding pipe (406), then opening a control valve (505) and operating a conveying pump (6) to enable a pumping pipe (601) to generate suction, pumping the material in a discharging bin (504), then conveying the material to the interior of a conveying pipe (602) by the conveying pump (6), conveying the material to the interior of the output head (603) by the conveying pipe (602), injecting the material into the interior of a wear-resistant layer (402) by the output head (603) through the feeding pipe (406), and after finishing conveying, fixing a sealing cover (407) at the top of the feeding pipe (406) through a buckle;

s2, a driving gear (204) of an output end is driven to rotate by the operation of a driving motor (203), the driving gear (204) rotates to drive a driven gear (206) to rotate, the driven gear (206) rotates to drive a transmission rod (205) to rotate, the transmission rod (205) rotates to drive a ball milling box body (4) to rotate, meanwhile, the driven rod (302) rotates along with the ball milling box body (4), the driven rod (302) is supported by a supporting plate (301), the driven rod (302) is ensured to rotate stably, large grinding balls (403) inside the ball milling box body (4) are driven to move in the rotating process, materials are ground by the large grinding balls (403), in the grinding process, a first adjusting rod (3) and a second adjusting rod (303) are shortened, the supporting plate (301) moves downwards, the ball milling box body (4) is driven to incline simultaneously, the ball milling box body (4) inclines to drive a movable plate (2) to incline by the inclination angle, one end of the ball milling box body (4) is higher than the bottom, in the rotating process of the ball milling box body (4), materials slide downwards under the influence of gravity, meanwhile, the screening net (405) keeps the materials with larger volume in the space of the large grinding ball (403) for continuous grinding, the small grinding ball (404) of the fine materials is used for grinding the materials finely again, the materials are ground and mixed together for 4-10H through two times of grinding, then the ball milling box body (4) is rotated to the original position by the driving motor (203), a worker places the receiving barrel (103) below the discharge port (408), then the worker opens the mounting cover (409) to enable the materials to fall along the discharge port (408), the receiving barrel (103) collects the materials, and then the worker pours the materials into the material placing bin (504) again, a worker connects the output head (603) to the connecting threaded port (708), and then the connecting threaded port (708) is opened to convey the materials to the interior of the heating tank (7) through the conveying pump (6);

s3, after the material enters the heating tank (7), the heating pipe (702) is electrified to heat through resistance, heat is led into the material, the material is heated, the heating pipe (702) stably raises the temperature in the heating tank (7) to 100-600 ℃, the temperature is sensed by a temperature sensor (706), meanwhile, the temperature sensor (706) transmits the detected information to the temperature timing controller (705), the temperature timing controller (705) adjusts the heating time of the material according to the height of the temperature, generally between 2 and 6H, then, when the heating is completed, the temperature is maintained at 600 ℃ for 3H by a temperature timing controller (705), then after 3H, setting the temperature to be 1000-1250 ℃, keeping 4-9H, thereby producing a product, and at the material production outlet, the material is discharged by opening the discharge valve (703).