CN113731315A - Water reducing agent reaction kettle convenient for sampling detection and sampling method thereof - Google Patents
Water reducing agent reaction kettle convenient for sampling detection and sampling method thereof Download PDFInfo
- Publication number
- CN113731315A CN113731315A CN202111094482.8A CN202111094482A CN113731315A CN 113731315 A CN113731315 A CN 113731315A CN 202111094482 A CN202111094482 A CN 202111094482A CN 113731315 A CN113731315 A CN 113731315A
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- CN
- China
- Prior art keywords
- sampling
- reducing agent
- water reducing
- check valve
- pipe
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
- G01N1/14—Suction devices, e.g. pumps; Ejector devices
Abstract
The invention discloses a water reducing agent reaction kettle convenient for sampling detection and a sampling method thereof, and the water reducing agent reaction kettle comprises a kettle body, wherein the upper part of the kettle body is provided with a sealing cover, the sealing cover is provided with a mounting opening, the mounting opening is hermetically penetrated with a sampling pipe, the lower end of the sampling pipe extends to the inner bottom of the kettle body, a lifting pipe is arranged in the sampling pipe in a sliding manner, and the outer wall of the lifting pipe is hermetically connected with the inner wall of the sampling pipe; the lateral wall of sampling tube sets up a plurality of thief hole along length direction, thief hole department sets up the check valve, the inside of sampling tube sets up the flexible pin of locking check valve, the fall way external connection sampler, when needs sample, the fall way descends and pushes down the flexible pin of elasticity, when the bottom opening of fall way descends to the check valve department of corresponding height, open one-way valve through the sampler suction, the material is through in the fall way suction sampler, move up the fall way after the sample is accomplished, the flexible pin resets and closes one-way valve locking again. Simple structure, the convenience is to the material sample of the internal each height of cauldron, raises the efficiency.
Description
Technical Field
The invention relates to the technical field of water reducing agents, and particularly relates to a water reducing agent reaction kettle convenient for sampling detection and a sampling method thereof.
Background
Reation kettle need be used in the preparation of water-reducing agent, in reation kettle processing procedure, need carry out sample detection to the internal material of a plurality of heights of cauldron, and sampling device structure is complicated, and the sample is inconvenient, and is inefficient.
Disclosure of Invention
The invention aims to provide a water reducing agent reaction kettle convenient for sampling detection.
In order to achieve the purpose, the invention provides the following technical scheme: the water reducing agent reaction kettle convenient for sampling detection comprises a kettle body, wherein a sealing cover is arranged at the upper part of the kettle body, a mounting opening is formed in the sealing cover, a sampling pipe is arranged at the mounting opening in a sealing and penetrating manner, the lower end of the sampling pipe extends to the inner bottom of the kettle body, a lifting pipe is arranged in the sampling pipe in a sliding manner, and the outer wall of the lifting pipe is connected with the inner wall of the sampling pipe in a sealing manner; the lateral wall of sampling tube sets up a plurality of thief hole along length direction, and thief hole department sets up the check valve, and the inside of sampling tube sets up the flexible pin of locking check valve, the fall way external connection sampler. Simple structure, the convenience is to the material sample of the internal each height of cauldron, raises the efficiency.
Furthermore, the elastic telescopic stop lever comprises a stop lever and a return spring, and the lower end of the stop lever is elastically connected with the bottom of the sampling tube through the return spring.
Furthermore, a sealing ring is arranged between the outer wall of the lifting pipe close to the opening at the bottom and the inner wall of the sampling pipe. Make the check valve that only corresponds the position open in the suction process, avoid other check valves to open and cause the sample to obscure.
Further, the sampler is a suction device.
Further, the suction device comprises a pipette, a piston rod and a piston are arranged in the pipette, and an inlet of the pipette is communicated with an external port of the lifting pipe.
Furthermore, the check valve is an automatic reset elastic check valve which is opened towards the interior of the sampling tube.
Furthermore, the upper part of the lifting pipe is provided with a sampling line corresponding to the sampling hole. Make things convenient for operating personnel to observe the decline position of fall way, the sample of being convenient for raises the efficiency.
Furthermore, the upper end lateral part and the sampling tube inside wall sealing connection of flexible pin. The material of other heights has been avoided getting into the fall way, has improved the sampling degree of accuracy.
Furthermore, the opening at the lower end of the lifting pipe is wedge-shaped.
The invention also aims to disclose a sampling method of the water reducing agent reaction kettle, which is convenient for sampling detection, and comprises the following sampling steps: the control fall of fall way pushes down the flexible pin of elasticity, and when the bottom opening of fall way descends to the check valve department of corresponding height, open the check valve through the sampler suction, the material is through the fall way suction to the sampler in, moves the fall way after the sample is accomplished, and the flexible pin resets and locks the check valve again.
The invention has the following technical effects: simple structure, the convenience is to the material sample of the internal each height of cauldron, raises the efficiency.
Drawings
FIG. 1 is a schematic view of the structure of a sampling tube in the example;
FIG. 2 is an enlarged view of portion A of FIG. 1;
fig. 3 is a schematic structural diagram of a sampler in an embodiment.
Reference numerals: 1. a kettle body; 2. sealing the cover; 21. an installation port; 3. a sampling tube; 31. a stop lever; 32. a return spring; 33. a sampling hole; 34. a one-way valve; 4. a lifting pipe; 5. a sampler; 51. a pipette; 52. a piston; 53. a piston rod; 6. and (5) sealing rings.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Examples
As shown in fig. 1-3, a water reducing agent reaction kettle convenient for sampling detection comprises a kettle body 1, wherein a sealing cover 2 is arranged on the upper part of the kettle body 1, a mounting opening 21 is formed in the sealing cover 2, a sampling tube 3 is hermetically arranged at the mounting opening 21 in a penetrating manner, the lower end of the sampling tube 3 extends to the inner bottom of the kettle body 1, a lifting tube 4 is slidably arranged in the sampling tube 3, and the outer wall of the lifting tube 4 is hermetically connected with the inner wall of the sampling tube 3; the lateral wall of sampling tube 3 sets up a plurality of thief hole 33 along length direction, thief hole 33 department sets up check valve 34, the inside of sampling tube 3 sets up the flexible pin of locking check valve 34, 4 external connection samplers 5 of fall way, when needs are at one of them high sample time, 4 descends to push down the flexible pin of fall way 4, when the bottom opening of fall way 4 descends to the check valve 34 department of corresponding height, open check valve 34 through the suction of sampler 5, the material sucks in sampler 5 through fall way 4, move up fall way 4 after the sample is accomplished, the flexible pin resets and locks check valve 34 again. Simple structure, the convenience is to the material sample of each height in the cauldron body 1, raises the efficiency.
The elastic telescopic stop lever comprises a stop lever 31 and a return spring 32, and the lower end of the stop lever 31 is elastically connected with the bottom of the sampling tube 3 through the return spring 32.
A sealing ring 6 is arranged between the outer wall of the lifting pipe 4 close to the opening at the bottom and the inner wall of the sampling pipe 3.
The sampler 5 is a suction device.
The suction means comprises a pipette 51, a piston rod 53 and a piston 52 being provided in the pipette 51, and an inlet of the pipette 51 communicating with an external port of the elevator tube 4. The piston 52 is driven to move in the liquid suction pipe 51 by pulling the piston rod 53, and the material with the corresponding height in the kettle body 1 is sucked into the liquid suction pipe 51 through the lifting pipe 4 by using the pressure.
The check valve 34 is a self-return elastic check valve 34 that opens into the interior of the sampling tube 3. After the sampling is finished, the one-way valve 34 automatically resets, and the sampling device is simple in structure and convenient to operate.
The upper part of the lifting pipe 4 is provided with a sampling line corresponding to the sampling hole 33. Make things convenient for operating personnel to observe the decline position of fall way 4, the sample of being convenient for raises the efficiency.
The upper end lateral part of the elastic telescopic stop lever is connected with the inner side wall of the sampling tube 3 in a sealing way. The material of other heights has been avoided getting into the fall way 4, has improved the sample degree of accuracy. Sealing may be performed using a sealing ring 6.
The lower extreme opening of fall way 4 is the wedge, guarantees when conflicting the flexible pin of elasticity that the opening is opened, makes things convenient for the sample.
The sampling method is as follows: control 4 descends and pushes down the flexible pin of elasticity, and when the bottom opening of fall way 4 descends to the check valve 34 department of corresponding height, open check valve 34 through the suction of sampler 5, the material through 4 suctions of fall way to sampler 5, moves up fall way 4 after the sample is accomplished, and the flexible pin of elasticity resets and locks check valve 34 again.
Although only the preferred embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art, and all changes are encompassed in the scope of the present invention.
Claims (10)
1. The water reducing agent reaction kettle convenient for sampling detection is characterized by comprising a kettle body, wherein a sealing cover is arranged at the upper part of the kettle body, a mounting opening is formed in the sealing cover, a sampling pipe is arranged at the mounting opening in a sealing and penetrating manner, the lower end of the sampling pipe extends to the inner bottom of the kettle body, a lifting pipe is arranged in the sampling pipe in a sliding manner, and the outer wall of the lifting pipe is connected with the inner wall of the sampling pipe in a sealing manner; the lateral wall of sampling tube sets up a plurality of thief hole along length direction, and thief hole department sets up the check valve, and the inside of sampling tube sets up the flexible pin of locking check valve, the fall way external connection sampler.
2. The water reducing agent reation kettle convenient to sample detection of claim 1, characterized in that, the flexible pin includes pin and reset spring, and the lower extreme of pin passes through reset spring elastic connection with the bottom of sampling tube.
3. The water reducing agent reation kettle convenient to sample detection as claimed in claim 1, wherein, set up the sealing washer on the fall pipe between the outer wall that is close to bottom opening department and the sampling tube inner wall.
4. A water reducing agent reation kettle convenient to sample detection as claimed in claim 1, characterized in that, the sampler is suction device.
5. The water reducing agent reation kettle convenient to sample detection as claimed in claim 1, wherein, suction means includes the pipette, sets up piston rod and piston in the pipette, and the import of pipette communicates with the outside port of fall pipe.
6. The water reducing agent reation kettle convenient to sample test of claim 1, characterized in that, the check valve is the automatic reset elasticity check valve of opening to the sampling tube inside.
7. The water reducing agent reaction kettle convenient for sampling detection according to claim 1, wherein a sampling line corresponding to the sampling hole is arranged at the upper part of the lifting pipe.
8. The water reducing agent reation kettle convenient to sample detection of claim 1, characterized in that, the upper end lateral part and the sampling tube inside wall sealing connection of elastic flexible pin.
9. The water reducing agent reaction kettle convenient for sampling detection according to claim 1, wherein the opening at the lower end of the lifting pipe is wedge-shaped.
10. A sampling method for a water reducing agent reaction kettle according to any one of claims 1 to 9, characterized in that the sampling step is as follows: the control fall of fall way pushes down the flexible pin of elasticity, and when the bottom opening of fall way descends to the check valve department of corresponding height, open the check valve through the sampler suction, the material is through the fall way suction to the sampler in, moves the fall way after the sample is accomplished, and the flexible pin resets and locks the check valve again.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202111094482.8A CN113731315A (en) | 2021-09-17 | 2021-09-17 | Water reducing agent reaction kettle convenient for sampling detection and sampling method thereof |
Applications Claiming Priority (1)
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CN202111094482.8A CN113731315A (en) | 2021-09-17 | 2021-09-17 | Water reducing agent reaction kettle convenient for sampling detection and sampling method thereof |
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CN113731315A true CN113731315A (en) | 2021-12-03 |
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CN202111094482.8A Withdrawn CN113731315A (en) | 2021-09-17 | 2021-09-17 | Water reducing agent reaction kettle convenient for sampling detection and sampling method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN116793514A (en) * | 2023-08-29 | 2023-09-22 | 常州乐研分离技术有限公司 | Temperature detection structure of evaporation drying all-in-one machine |
-
2021
- 2021-09-17 CN CN202111094482.8A patent/CN113731315A/en not_active Withdrawn
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN116793514A (en) * | 2023-08-29 | 2023-09-22 | 常州乐研分离技术有限公司 | Temperature detection structure of evaporation drying all-in-one machine |
CN116793514B (en) * | 2023-08-29 | 2023-11-07 | 常州乐研分离技术有限公司 | Temperature detection structure of evaporation drying all-in-one machine |
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Application publication date: 20211203 |