CN1136282C - Method for producing bone glue, bone oil and bone powder simultaneously - Google Patents
Method for producing bone glue, bone oil and bone powder simultaneously Download PDFInfo
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- CN1136282C CN1136282C CNB981138314A CN98113831A CN1136282C CN 1136282 C CN1136282 C CN 1136282C CN B981138314 A CNB981138314 A CN B981138314A CN 98113831 A CN98113831 A CN 98113831A CN 1136282 C CN1136282 C CN 1136282C
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- bone
- glue
- steam
- high pressure
- animal oil
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
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- Fertilizers (AREA)
- Fodder In General (AREA)
Abstract
The present invention relates to a method for producing bone glue, bone oil and bone meal by one step by fresh ox bones, which comprises the following steps: putting fresh ox bones in a high-pressure steaming tank, and injecting high-pressure saturated steam in the high-pressure steaming tank; closing an air inlet valve when pressure reaches 0.25 to 0.3MPa, opening a lower exhaust valve to discharge steam, and closing the exhaust valve after discharging the steam; injecting steam into the tank, closing the air inlet valve when the pressure reaches 0.35 to 0.45MPa, carrying out dry steaming for 1.5 to 3.0 hours, and discharging the steam in the tank; after carrying out stewing and depositing for 0.5 to 1.5 hours, opening a glue discharging valve and an oil discharging valve to discharge bone glue and glue oil, and then, producing bone meal by degreasing bones. The bone glue, the bone oil and the bone meal which are produced by using the method of the present invention have no benzene pollution.
Description
(1) technical field
The present invention relates to the production method of a kind of gelatine, animal oil, bone meal, particularly relating to a kind of is raw material with bright ox bone, adopts the method for the disposable production gelatine of saturation steam, animal oil, bone meal.
(2) technical background
Bone meal is important fertilizer, has the raising crop yield, improves the effect that fruit eats quality and improves the soil, and also is the good feed of domestic animals such as pig, ox, chicken, poultry simultaneously.
Animal oil is the fatty oil that extracts from bone, is rich in lipid acid, is to make additives such as perfumed soap, feed.
Gelatine in textile industries such as cotton, silk, felt, printing and dyeing, is indispensable tackiness agent, also is the important additives of products such as starching in papermaking, printing, the leather processing industry or lustering agent and manufacturing sand paper, emery wheel, emery cloth, match.
The conventional production method of gelatine, animal oil, bone meal is:
A, aggregate is ground into certain particle size (30-40mm) with pulverizer after, will go into to carry oil tank, through long-time benzene gas high temperature extraction, output animal oil.
B, with the aggregate behind the extract oil through mill bone, smoked bone, wash multiple tracks art breading such as bone after, with steam and the rare glue of hot water extraction.
Fixture behind C, the extraction glue is bone meal.
There is following shortcoming in conventional method of producing gelatine, animal oil, bone meal:
1, complex process, and production cycle long (extract rare glue and need about 72 hours approximately) from being dosed into.
2, owing to adopt the benzene extraction process, making has residual benzene to exist in bone meal, gelatine and the animal oil.To making the animal oil can not be as fodder additives.Particularly, use this bone meal, can make residual benzene enter in the meat of domestic animal, poultry or during crop really ate, the people ate this domestic animal, poultry or crop and really eats, and is deleterious to people's body and mind health as feed and fertilizer owing to residual in the bone meal benzene arranged.
3, benzene is inflammable explosive article, and its flash-point is-11 ℃, and potential safety hazard is very big.In addition, benzene gas is poisonous, and the mankind are had direct injury, and contaminate environment.
4, owing to the easy alkene of benzene gas, explosive, and poisonous, in benzene gas extraction process, require the equipment precision height, need explosion-proof equipment, so facility investment is big.
(3) summary of the invention
Purpose of the present invention is at the problems referred to above, and providing a kind of is raw material with bright ox bone, adopts the method for the disposable production gelatine of saturation steam, animal oil, bone meal.The technical scheme that adopts is:
One, raw material adopts bright ox bone;
Two, bright ox bone classification, get the bright ox bone (as excellent bone) of same class, monoblock drops in the high pressure steaming jar.
Three, secondary extracts gelatine, animal oil to bright ox bone with high-pressure saturated steam.
For the first time the process that extracts gelatine, animal oil with high-pressure saturated steam is:
1, the upper and lower jar mouth of high pressure steaming jar is closed after, open the steam inlet valve, in the high pressure steaming jar, import high-pressure saturated steam, to bright ox bone carry out disinfection and blowdown (therebetween, high-pressure saturated steam contacts with cold bone, after the cold and hot exchange, vapor condensation Cheng Shui as spray, cleans aggregate), when vapor pressure reached 0.25-0.3Mpa, the steam off intake valve was opened down vent valve, jar interior steam is discharged, when tensimeter was designated as zero, exhaust finished, and closes vent valve;
2, dry blowing.After the sterilization blowdown is finished, open the steam inlet valve, in the high pressure steaming jar, import high-pressure saturated steam, when tensimeter is designated as 0.35-0.45Mpa, the steam off intake valve, beginning dry blowing 1.5-3.0 hour, after the dry blowing time arrives, open vent valve, begin to discharge the steam in the high pressure steaming jar, be designated as zero up to tensimeter, staticly settled 1-1.5 hour;
3, discharging gelatine, animal oil.After sedimentation time arrives, open and put glue valve, oil drain valve, emit rare glue respectively, emit thick animal oil.
4, thick animal oil is put into the essential oil jar and carry out refining.With rare glue of emitting, behind vacuum suction filter, enter the falling liquid film shell and tube evaporator and concentrate, surveying Baume concentration in the time of 75 ℃ is 18-20 ° of Be.Add the sterilization sanitas simultaneously.After glue reaches requirement concentration, put into storage glue jar, adopt the oxidation style decolouring, adopt ordinary method moulding, drying then.The rare glue of 1m3 adds sterilization, sanitas company=S-WAT 500g.Oxidation style decolouring be concentrate reach 18-20 ° of Be after, at 1m
3Add discoloring agent hydrogen peroxide (H in the dense glue
2O
2) 6000-10000mL, stir at a slow speed, make it abundant reaction.
Extract for the second time gelatine, animal oil technology, be after having put rare glue and thick animal oil, close and put glue valve and oil drain valve, open the steam inlet valve, input high pressure saturated vapo(u)r in the high pressure steaming jar, all the other technological processs extract gelatine with the first time, animal oil technology is basic identical, and its difference is to be 0.5 2 hours the dry blowing time.
After discharging for the second time thin liquid and thick animal oil, in the high pressure steaming jar, take out the degreasing bone, through pulverizing, make bone meal.
After dry blowing 1.5-3.0 hour, when opening the vent valve exhaust, when high pressure steaming jar internal pressure is discharged to 0.1-0.2Mpa, can be crack following jar mouthful, improve exhaust velocity, adopt this method, the quality that can increase substantially animal oil, gelatine reaches glue, separating of oil purpose.
Adopt high-pressure saturated steam that the production method of the disposable extraction gelatine of bright ox bone, animal oil, bone meal is had following advantage:
1, do not have residual benzene in animal oil and the bone meal, can be used as the additive of green feed and make senior perfumed soap.
2, owing to do not contain residual benzene in the bone meal, can be used as green organic fertilizer, not only can be used for improving the domestic quality that has crop really to eat, and can export in a large number and earn foreign exchange.
3, owing in production technique, there is not benzene gas, therefore fundamentally eliminated pollution to environment.
4, do not need to adopt antiknock device, can produce quality products, invest little, instant effect with common equipment.
5, with short production cycle.Only need 5-8 hour from being dosed into out animal oil and gelatine, thereby reduced production cost, particularly the oil yield height can reach 17-18%.And rare glue only adds sanitas, discoloring agent, does not need to smoke complicated conventional process operations such as bone, just can reach the color and luster requirement of high-quality gelatine.
(4) embodiment
Embodiment
One, bright ox rod bone is put into the high pressure steaming jar, on the high pressure steaming jar, after following jar of mouth closed, beat, in the high pressure steaming jar, import high-pressure saturated steam in the steam inlet valve, bright ox bone is carried out disinfection and blowdown, when vapor pressure reached 0.3Mpa, the steam off intake valve was opened down vent valve, jar interior steam is discharged, exhaust is closed down vent valve after finishing, and opens the steam inlet valve again, in the high pressure steaming jar, import high-pressure saturated steam again, when pressure reaches 0.45Mpa, the steam off intake valve, dry blowing is after 3 hours, open vent valve, exhaust, when high pressure steaming jar internal pressure is 0.2Mpa, crack following jar mouthful of exhaust, until pressure is zero, after staticly settling at 1.5 o'clock, open and put glue valve and oil drain valve, emit rare glue and animal oil respectively.The animal oil of emitting places the essential oil jar to carry out refining.The alkene glue of emitting is regulated pH value between 6.5-6.8 with sulfuric acid, behind vacuum suction filter, enters the falling liquid film shell and tube evaporator and concentrates, in the time of 75 ℃, when the survey degree Beaume is 20 ° of Be, at 1m
3Add sterilization sanitas V-Brite B 500g in rare glue, glue reaches to be put into storage glue jar after the 18-20 ° of Be concentration and carries out oxidative decoloration, and used discoloring agent is hydrogen peroxide (H
2O
2), add-on is at 1m
3Add 8000mL in the dense glue, stir at a slow speed, make its sufficient reacting, adopt conventional method moulding, drying then.
Two, for the first time bright ox rod bone is extracted gelatine, animal oil with high-pressure saturated steam after, carry out extraction second time with high-pressure saturated steam, its technological process is basic identical with the first time, its difference is to be 2 hours the dry blowing time.
Three, take out degreasing bone in the high pressure steaming jar, drying is pulverized, and makes bone meal.
Claims (3)
1, with the production method of the disposable production gelatine of bright ox bone, animal oil, bone meal, comprise reextraction gelatine, animal oil technology, the thick animal oil that extracts is put into the refining of essential oil jar and is gone out qualified animal oil, and the rare glue that extracts enters the falling liquid film shell and tube evaporator and concentrates, when survey Baume concentration is 18-20 ° of Be in the time of 75 ℃, add the sterilization sanitas, after glue reaches requirement concentration, pass through oxidative decoloration, carry out drying, moulding again, it is characterized in that:
A, the technology that bright ox bone is extracted gelatine, animal oil for the first time are:
1, with bright ox bone classification, get the bright ox bone of same class, monoblock drops in the high pressure steaming jar;
2, the upper and lower jar mouth of high pressure steaming jar is closed after, open the steam inlet valve, the full steam that closes of input high pressure in the high pressure steaming jar, when vapor pressure reached 0.25-0.3MPa, the steam off intake valve was opened down the vent valve steam discharge, when high pressure steaming jar internal pressure is zero, close down vent valve;
3, open the steam inlet valve, in the high pressure steaming jar, import the full steam that closes of high pressure again, when pressure reaches 0.35-0.45MPa, the steam off intake valve dry blowing 1.5-3.0 hour, is opened the vapor cock exhaust vapour, when pressure is zero, quiescent setting 0.5-1.5 hour, open respectively and put glue valve, oil drain valve, extract rare glue and thick animal oil;
Extract B, the described second time gelatine, animal oil technology, be after having put rare glue and thick animal oil, close and put glue valve, oil drain valve, open the steam inlet valve, in the high pressure steaming jar, import the full steam that closes of high pressure once more, all the other technological processs extract gelatine with the first time, animal oil technology is basic identical, and its difference is to be 0.5-2 hour the dry blowing time.
2, the production method of the disposable production gelatine of bright ox bone according to claim 1, animal oil, bone meal, it is characterized in that after described dry blowing 1.5-3.0 hour, open the vent valve steam discharge, when high pressure steaming jar internal pressure reaches 0.1-0.2MPa, can crack high pressure steaming jar following jar mouthful.
3, the production method of the disposable production gelatine of bright ox bone according to claim 1, animal oil, bone meal is characterized in that the decolouring of described oxidation style, is that glue is when reaching concentration 18-20 ° of Be, at 1m
3Put into hydrogen peroxide 6000-10000mL in the dense glue, stir at a slow speed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB981138314A CN1136282C (en) | 1998-03-11 | 1998-03-11 | Method for producing bone glue, bone oil and bone powder simultaneously |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB981138314A CN1136282C (en) | 1998-03-11 | 1998-03-11 | Method for producing bone glue, bone oil and bone powder simultaneously |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1193647A CN1193647A (en) | 1998-09-23 |
| CN1136282C true CN1136282C (en) | 2004-01-28 |
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ID=5223529
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB981138314A Expired - Fee Related CN1136282C (en) | 1998-03-11 | 1998-03-11 | Method for producing bone glue, bone oil and bone powder simultaneously |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1136282C (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103843970A (en) * | 2012-11-30 | 2014-06-11 | 闫云霞 | Production method for preparing ossein oligopeptide meal, bone oil and bone meal |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102648723B (en) * | 2012-05-25 | 2014-07-09 | 内蒙古蒙都羊业食品有限公司 | Method for coproducing beef bone oil, beef bone meal and beef flavor seasoning through beef bone oil extracts |
| CN107513466A (en) * | 2017-10-10 | 2017-12-26 | 寻甸中盛生物科技有限公司 | A kind of production technology and its production system of low-temperature atmosphere-pressure extraction animal oil |
| CN112939636B (en) * | 2021-04-22 | 2022-10-28 | 嘉兴大胃蛙环保科技有限公司 | Utilize kitchen discarded object preparation fertilizer equipment |
-
1998
- 1998-03-11 CN CNB981138314A patent/CN1136282C/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103843970A (en) * | 2012-11-30 | 2014-06-11 | 闫云霞 | Production method for preparing ossein oligopeptide meal, bone oil and bone meal |
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| Publication number | Publication date |
|---|---|
| CN1193647A (en) | 1998-09-23 |
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