CN113559556A - Oil-water separation device - Google Patents
Oil-water separation device Download PDFInfo
- Publication number
- CN113559556A CN113559556A CN202110996739.2A CN202110996739A CN113559556A CN 113559556 A CN113559556 A CN 113559556A CN 202110996739 A CN202110996739 A CN 202110996739A CN 113559556 A CN113559556 A CN 113559556A
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- oil
- porous
- plate
- water separator
- outlet
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0202—Separation of non-miscible liquids by ab- or adsorption
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0211—Separation of non-miscible liquids by sedimentation with baffles
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G33/00—Dewatering or demulsification of hydrocarbon oils
- C10G33/06—Dewatering or demulsification of hydrocarbon oils with mechanical means, e.g. by filtration
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Removal Of Floating Material (AREA)
Abstract
The invention discloses an oil-water separation device, which comprises a separation tank, wherein one end of the separation tank is provided with a liquid inlet, the other end of the separation tank is provided with an oil outlet, and the bottom of the separation tank is provided with a liquid outlet, and the oil-water separation device is characterized in that: the oil-out separation device is characterized in that a porous aggregation plate which is inclined relative to the horizontal plane is arranged in the separation tank, the lower end of the porous aggregation plate is located at the bottom of the separation tank, the upper end of the porous aggregation plate is located above the liquid level, the porous aggregation plate is gradually inclined towards the direction of the oil outlet from bottom to top, and the liquid outlet is formed between the porous aggregation plate and the oil outlet. The porous aggregation plate is gradually inclined towards the oil outlet from bottom to top, so that the contact length of the porous aggregation plate and liquid is changed, the movement track of oil droplets is prolonged, the collision probability among a plurality of oil droplets can be increased, and the oil-water separation efficiency is further improved.
Description
Technical Field
The invention belongs to the technical field of oil-water separation, and particularly relates to an oil-water separation device.
Background
A large amount of oily sludge is generated in the processes of oil exploitation, gathering and transportation and refining. In order to avoid direct discharge of oily sludge to pollute the environment and waste of oil and gas resources in the oily sludge, pyrolysis technology is generally adopted to treat the oily sludge and recover petroleum resources. The sludge pyrolysis is to utilize the thermal instability of organic matters in the sludge, heat the organic matters under the anaerobic condition, thermally crack the organic matters to form pyrolysis gas with a utilization value, and after the part of the pyrolysis gas is condensed by a quench tower to form an oil-water mixture, the oil-water separation needs to be carried out on the part of the oil-water mixture, so that the recovery of petroleum resources is realized.
In the related technology, a gravity method is generally adopted to separate an oil-water mixture, namely, the oil-water mixture is guided into an oil-water separation pool or a separation tank by utilizing different oil-water densities and is kept stand for a period of time to naturally separate the oil-water mixture.
The oil-water mixture is separated by adopting a gravity method, and in order to ensure that the oil-water mixture is fully layered, the volume and the occupied area of an oil-water separation pool are large, and the production cost is high. And after the oil-water mixture is stood for a long time, the problem of incomplete separation of oil phase and water phase still exists, and the oil-water separation efficiency is low.
Therefore, further improvement is required for the existing oil-water separation device.
Disclosure of Invention
The invention aims to solve the technical problem of providing an oil-water separation device with high oil-water separation efficiency.
The technical scheme adopted by the invention for solving the technical problems is as follows: the utility model provides an oil-water separator, includes the knockout drum, the one end of knockout drum is equipped with the inlet, the other end of knockout drum is equipped with the oil-out, the bottom of knockout drum is equipped with liquid outlet, its characterized in that: the oil-out separation device is characterized in that a porous aggregation plate which is inclined relative to the horizontal plane is arranged in the separation tank, the lower end of the porous aggregation plate is located at the bottom of the separation tank, the upper end of the porous aggregation plate is located above the liquid level, the porous aggregation plate is gradually inclined towards the direction of the oil outlet from bottom to top, and the liquid outlet is formed between the porous aggregation plate and the oil outlet.
Preferably, the included angle alpha between the porous aggregation plate and the horizontal plane is 50-80 degrees. Within the angle range, the motion trail of the oil drops is prolonged, meanwhile, the oil drops are more favorably collided, and the aggregation efficiency is improved.
Preferably, the porous aggregate plate comprises a plurality of porous corrugated plates arranged at intervals along the direction of the fluid. Porous buckled plate has increased the area of contact of oil dripping with panel, and the ripple shape more is favorable to the aggregation and the collision of oil dripping, and the oil dripping after the aggregation floats and passes in the hole of porous buckled plate, and oil dripping constantly aggregates when passing the porous buckled plate of polylith along fluidic direction and grows up, finally discharges from the oil-out.
Preferably, each porous corrugated plate is in a continuous W shape, the length L of each side forming the W shape is 40-60 mm, and the included angle beta of adjacent sides is 85-95 degrees. Through the angle of placing of porous buckled plate and mutually supporting of its wave form for the rivers that have the oil globule secretly move the in-process on porous buckled plate, the movement track of oil globule can prolong, and can increase the collision probability between a plurality of oil globules, thereby improve the water oil separating precision of buckled plate coalescer.
Preferably, the extension direction of each W-shape is identical to the inclination direction of the porous aggregate plate. The W-shaped arrangement is beneficial to the continuous aggregation and floating of oil drops along the W-shaped grooves.
Preferably, the diameter of each of the porous corrugated plates is 1 to 10mm, and the diameter of each of the porous corrugated plates gradually increases from the bottom to the top of the porous corrugated plate. Oil drops collide and aggregate gradually in the floating process, so that the pore diameter of each porous corrugated plate is gradually increased from the bottom to the top, and the collision and the passing of the aggregated oil drops are facilitated.
Preferably, the open pore ratio of each porous corrugated plate is 60 to 80%, and the open pore ratios of adjacent porous corrugated plates are sequentially increased by 3 to 5% in the fluid direction. Along with the flowing of the liquid, oil drops grow gradually, so that the opening rate of the porous corrugated plate is increased gradually along the flowing direction of the liquid.
Preferably, the liquid inlet comprises an outlet end located in the separation tank, and the outlet end is upward. The outlet end is upward, so that the liquid has an upward speed when entering the separation tank, and the small oil drops are promoted to float upwards and gather.
Preferably, a buffer plate for buffering fluid is arranged between the outlet end and the porous aggregation plate, and the top end of the buffer plate is higher than the outlet end. The top end of the buffer plate is higher than the outlet end, so that the liquid can be pre-separated, and the collision among oil drops is increased.
Preferably, an oil spilling partition plate is arranged between the porous aggregation plate and the oil outlet, and the top end of the oil spilling partition plate is located below the liquid level and higher than the upper edge of the oil outlet. The top end of the oil spilling partition plate is higher than the upper edge of the oil outlet, so that the separation of collected oil is facilitated, and the collected oil is prevented from being directly discharged from the oil outlet.
Compared with the prior art, the invention has the advantages that: according to the invention, the porous aggregation plate which is inclined relative to the horizontal plane is arranged in the separation tank, after liquid enters the separation tank from the liquid inlet, the liquid flows along the axial direction of the separation tank, oil drops in the liquid can be adsorbed on the porous aggregation plate and are collided and aggregated continuously, the aggregated oil drops float upwards to realize oil-water separation, and the oil-water separation efficiency is improved; the porous aggregation plate is gradually inclined towards the oil outlet from bottom to top, the contact length of the porous aggregation plate and liquid is changed, the motion track of oil droplets can be prolonged, the collision probability among a plurality of oil droplets can be increased, and the oil-water separation efficiency is further improved. The oil-water separation device provided by the invention has the advantages that the oil-water separation efficiency is improved, the size of the separation tank is reduced, and the equipment investment is reduced.
Drawings
FIG. 1 is a cross-sectional view of an embodiment of the present invention;
FIG. 2 is a schematic structural view of a corrugated porous plate according to an embodiment of the present invention;
FIG. 3 is a cross-sectional view taken along direction A of FIG. 2;
fig. 4 is a partial schematic view of 4 perforated corrugated sheets spaced apart in the direction of flow in an embodiment of the present invention.
Detailed Description
The invention is described in further detail below with reference to the accompanying examples.
Referring to fig. 1 to 4, a preferred embodiment of the oil-water separating device includes a separation tank 1, a porous aggregate plate 2, a buffer plate 4, and an oil spill baffle 5.
One end of the separation tank 1 is provided with a liquid inlet 11, the other end of the separation tank 1 is provided with an oil outlet 12, and the bottom of the separation tank 1 is provided with a liquid outlet 13. Referring to fig. 1, a liquid inlet 11 is arranged at the bottom of one end of the separation tank 1, and an oil outlet 12 is arranged at the middle upper part of the other end of the separation tank 1, which is favorable for pre-separation of fluid and fine separation of oil and water. The liquid inlet 11 comprises an outlet end 11a located in the separation tank 1, the outlet end 11a being directed upwards. The outlet end 11a is upward, so that the liquid has an upward speed when entering the separation tank 1, and the floating and gathering of the oil droplets are promoted.
Porous board 2 of gathering sets up in knockout drum 1 relative to the horizontal plane slope, and the lower extreme of porous board 2 of gathering is located the bottom of knockout drum 1, and the upper end of porous board 2 of gathering is located the top of liquid level, and porous board 2 of gathering inclines towards oil-out 12 directions from bottom to top gradually, and liquid outlet 13 is seted up between porous board 2 of gathering and oil-out 12. In this embodiment, the angle α between the perforated collector plate 2 and the horizontal plane is 60 °. The porous aggregation plate 2 comprises 4 porous corrugated plates 3 arranged at intervals along the fluid direction, each porous corrugated plate 3 is in a continuous W shape, the length L of each side forming the W shape is 50mm, and the included angle beta of adjacent sides is 90 degrees, which is shown in figure 3. The extension direction of each W-shape coincides with the inclination direction of the perforated collector plate 2, see fig. 2. The collected and floated oil drops sequentially pass through the 4 porous corrugated plates 3, and in the process, the oil drops continuously collide, are collected and grow up and are finally discharged from the oil outlet 12. The design of the W-shaped corrugated plate is more beneficial to floating of oil drops along the grooves, and is beneficial to collision and growth of the oil drops, and the oil-water separation efficiency is improved. The aperture of the 4 porous corrugated plates 3 is phi 1-phi 10mm, the aperture range is favorable for the adsorption and the passing of oil drops, and the aperture range gradually increases from the bottom to the top of the porous corrugated plates 3, as shown in fig. 4, the 4 porous corrugated plates 3 are a first corrugated plate 31, a second corrugated plate 32, a third corrugated plate 33 and a fourth corrugated plate 34 in sequence along the fluid direction, and the aperture ratio is 67%, 70%, 75% and 78% respectively.
The buffer plate 4 is disposed between the outlet end 11a and the porous aggregate plate 2, and the top end of the buffer plate 4 is higher than the outlet end 11 a. The liquid entering the separation tank is reduced in speed after passing through the buffer plate 4, pre-separation of oil drops is realized, aggregation on the porous aggregation plate 2 is facilitated, and energy storage is provided for subsequent collision and growth.
The oil spilling partition plate 5 is arranged between the porous aggregation plate 2 and the oil outlet 12, and the top end of the oil spilling partition plate 5 is positioned below the liquid level and is higher than the upper edge of the oil outlet 12. The gathered floating oil crosses the oil spilling partition plate 5 and then flows into the oil outlet 12 to be discharged.
Claims (10)
1. The utility model provides an oil-water separator, includes knockout drum (1), the one end of knockout drum (1) is equipped with inlet (11), the other end of knockout drum (1) is equipped with oil-out (12), the bottom of knockout drum (1) is equipped with liquid outlet (13), its characterized in that: be equipped with porous board (2) of gathering of relative horizontal plane slope in knockout drum (1), the lower extreme of porous board (2) of gathering is located the bottom of knockout drum (1), the upper end of porous board (2) of gathering is located the top of liquid level, and porous board (2) of gathering from bottom to top gradually towards oil-out (12) direction slope, liquid outlet (13) are seted up between porous board (2) of gathering and oil-out (12).
2. The oil-water separator according to claim 1, wherein: the included angle alpha between the porous aggregation plate (2) and the horizontal plane is 50-80 degrees.
3. The oil-water separator according to claim 1, wherein: the porous aggregation plate (2) comprises a plurality of porous corrugated plates (3) which are arranged at intervals along the fluid direction.
4. The oil-water separator according to claim 1, wherein: each porous corrugated plate (3) is continuous W-shaped, the length L of each side forming the W-shape is 40-60 mm, and the included angle beta of adjacent sides is 85-95 degrees.
5. The oil-water separator according to claim 4, wherein: the extension direction of each W-shape is consistent with the inclination direction of the porous collecting plate (2).
6. The oil-water separator according to claim 4, wherein: the aperture of each porous corrugated plate (3) is phi 1-phi 10mm, and the aperture gradually increases from the bottom to the top of each porous corrugated plate (3).
7. The oil-water separator according to claim 4, wherein: the aperture ratio of each porous corrugated plate (3) is 60-80%, and the aperture ratios of adjacent porous corrugated plates (3) are sequentially increased by 3-5% along the fluid direction.
8. The oil-water separator according to claim 1, wherein: the liquid inlet (11) comprises an outlet end (11a) positioned in the separation tank (1), and the direction of the outlet end (11a) faces upwards.
9. The oil-water separator according to claim 8, wherein: a buffer plate (4) for buffering fluid is arranged between the outlet end (11a) and the porous aggregation plate (2), and the top end of the buffer plate (4) is higher than the outlet end (11 a).
10. The oil-water separator according to claim 1, wherein: an oil spilling partition plate (5) is arranged between the porous aggregation plate (2) and the oil outlet (12), and the top end of the oil spilling partition plate (5) is located below the liquid level and is higher than the upper edge of the oil outlet (12).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202110996739.2A CN113559556A (en) | 2021-08-27 | 2021-08-27 | Oil-water separation device |
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CN202110996739.2A CN113559556A (en) | 2021-08-27 | 2021-08-27 | Oil-water separation device |
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CN113559556A true CN113559556A (en) | 2021-10-29 |
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CN202110996739.2A Pending CN113559556A (en) | 2021-08-27 | 2021-08-27 | Oil-water separation device |
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2021
- 2021-08-27 CN CN202110996739.2A patent/CN113559556A/en active Pending
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