CN113445322B - Anti-aging sphygmomanometer wrapping belt and manufacturing method thereof - Google Patents
Anti-aging sphygmomanometer wrapping belt and manufacturing method thereof Download PDFInfo
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- CN113445322B CN113445322B CN202110580827.4A CN202110580827A CN113445322B CN 113445322 B CN113445322 B CN 113445322B CN 202110580827 A CN202110580827 A CN 202110580827A CN 113445322 B CN113445322 B CN 113445322B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/285—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acid amides or imides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61B—DIAGNOSIS; SURGERY; IDENTIFICATION
- A61B5/00—Measuring for diagnostic purposes; Identification of persons
- A61B5/02—Detecting, measuring or recording pulse, heart rate, blood pressure or blood flow; Combined pulse/heart-rate/blood pressure determination; Evaluating a cardiovascular condition not otherwise provided for, e.g. using combinations of techniques provided for in this group with electrocardiography or electroauscultation; Heart catheters for measuring blood pressure
- A61B5/021—Measuring pressure in heart or blood vessels
- A61B5/022—Measuring pressure in heart or blood vessels by applying pressure to close blood vessels, e.g. against the skin; Ophthalmodynamometers
- A61B5/02233—Occluders specially adapted therefor
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
- D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
- D04C1/02—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof made from particular materials
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04C—BRAIDING OR MANUFACTURE OF LACE, INCLUDING BOBBIN-NET OR CARBONISED LACE; BRAIDING MACHINES; BRAID; LACE
- D04C1/00—Braid or lace, e.g. pillow-lace; Processes for the manufacture thereof
- D04C1/06—Braid or lace serving particular purposes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
- D06M13/51—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond
- D06M13/513—Compounds with at least one carbon-metal or carbon-boron, carbon-silicon, carbon-selenium, or carbon-tellurium bond with at least one carbon-silicon bond
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/25—Resistance to light or sun, i.e. protection of the textile itself as well as UV shielding materials or treatment compositions therefor; Anti-yellowing treatments
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
- D10B2201/02—Cotton
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
Abstract
The application relates to the field of blood pressure monitoring equipment parts, and particularly discloses an anti-aging sphygmomanometer covering belt and a manufacturing method thereof. An anti-aging sphygmomanometer wrapping belt is prepared from raw materials such as polyester yarns, cotton fibers and modified water-absorbent resin, wherein the modified water-absorbent resin is prepared from the following raw materials in parts by weight: water-absorbent resin: 50-70 parts of silicon nitride ceramic powder: 18-26 parts of a silane coupling agent: 4-8 parts of starch: 5.5-7.5 parts; the manufacturing method comprises the following steps: s1, adding the modified water-absorbing resin into the polyester fiber and the cotton fiber, and performing ball milling for 50-80min at the ball milling speed of 200-300rad/min to ensure that the modified water-absorbing resin is coated on the outer sides of the polyester fiber and the cotton fiber to obtain modified mixed fiber; s2, twisting the modified mixed fiber into roving after the modified mixed fiber is made into strips; and S3, weaving the roving into a wrapping belt. The coating belt prepared by the method has better ultraviolet aging resistance.
Description
Technical Field
The application relates to the field of blood pressure monitoring equipment parts, in particular to an anti-aging sphygmomanometer coating belt and a manufacturing method thereof.
Background
Blood pressure is an important index for diagnosing the health condition of a human body, and currently, clinically, blood pressure is mainly measured by measuring the lateral pressure of a blood vessel wall through a sphygmomanometer. The main principle of the sphygmomanometer is to pressurize air to a local artery, and to apply pressure to stop fluctuation of the local artery, thereby measuring the blood flow pressure during this period.
Currently, the related art sphygmomanometer generally includes three parts, i.e., a balloon, a cover tape and a pressure detector. Wherein, the wrapping belt is wrapped with an inflatable bag which is respectively connected with the balloon and the pressure detector through two pipelines, and the three form a closed pipeline system. When the device is used, the wrapping band is bound at the arm, and then the pressure detector is started to detect.
When summer weather is hotter, people generally sweat easily, and for the travelling comfort of people when surveying blood pressure as much as possible, the present cover band generally has better moisture absorption function. However, since bacteria are easily grown in sweat remaining on the cover tape after the cover tape absorbs a large amount of sweat for a long period of time, it is generally necessary to periodically place the cover tape under an ultraviolet lamp for sterilization.
However, after the wrapping tape in the related art is sterilized by the ultraviolet lamp, the wrapping tape is easy to age, and the subsequent use of the wrapping tape is affected.
Disclosure of Invention
In order to solve the problem that the conventional cover belt is easy to age to influence subsequent use, the application provides an anti-aging sphygmomanometer cover belt and a manufacturing method thereof.
In a first aspect, the application provides an anti-aging sphygmomanometer cover belt, which adopts the following technical scheme:
an anti-aging sphygmomanometer wrapping belt is prepared from the following raw materials in parts by weight:
polyester yarn: 70 to 90 portions of
Cotton fiber: 55 to 75 portions of
Modified water-absorbent resin: 28 to 36 portions of
The modified water-absorbing resin is prepared from the following raw materials in parts by weight:
water-absorbent resin: 50 to 70 portions of
Silicon nitride ceramic powder: 18-26 parts of
Silane coupling agent: 4 to 8 portions of
Starch: 5.5 to 7.5 portions of
Wherein the particle size range of the water-absorbing resin is 300-500nm, and the particle size range of the silicon nitride ceramic powder is 40-60 nm.
After the water-absorbing resin is modified by adopting the silicon nitride ceramic powder, the silane coupling agent and the starch, the problem that the wrapping belt is easy to age after being disinfected by ultraviolet irradiation can be solved, and meanwhile, the problem that the moisture absorption performance of the wrapping belt is greatly reduced after being disinfected by ultraviolet irradiation can be solved.
Preferably, the modified water-absorbent resin is prepared from the following raw materials in parts by weight:
water-absorbent resin: 60 to 65 portions of
Silicon nitride ceramic powder: 20-24 parts of
Silane coupling agent: 6 to 8 portions of
Starch: 6.2 to 6.8 portions of
Wherein the particle size range of the water-absorbing resin is 300-500nm, and the particle size range of the silicon nitride ceramic powder is 40-60 nm.
By adopting the technical scheme, when the coating belt is prepared from the modified water-absorbent resin prepared according to the proportion, the polyester yarns and the cotton fibers, the obtained coating belt has good aging resistance, and the reduction range of the water absorption rate of the coating belt after ultraviolet disinfection is reduced.
Preferably, the modified water-absorbent resin is produced by the following method:
(1) uniformly mixing starch and silicon nitride ceramic powder, and performing ball milling for 30-50min at the ball milling speed of 320-480rad/min to obtain a silicon nitride ceramic powder-starch mixture;
(2) burning the silicon nitride ceramic powder-starch mixture at the temperature of 700-800 ℃ for 1-2h, taking out and cooling to obtain modified silicon nitride ceramic powder;
(3) after the modified silicon nitride ceramic powder and the silane coupling agent are uniformly mixed, the water-absorbing resin is continuously added, and the ball milling is carried out for 20-40min at the ball milling speed of 100-120rad/min, thus obtaining the modified water-absorbing resin.
By adopting the technical scheme, after the water-absorbent resin is modified by adopting the method, the obtained modified water-absorbent resin can effectively improve the aging resistance of the coating belt, and the reduction range of the water absorption rate of the coating belt after ultraviolet disinfection is reduced.
Preferably, the water-absorbing resin is one or a mixture of more of polyacrylamide, starch-acrylate polymer and sodium polyacrylate.
By adopting the technical scheme, the polyacrylamide, the starch-acrylate polymer, the sodium polyacrylate and the like have better water absorption performance, and can realize the rapid absorption of sweat of a human body.
Preferably, the water-absorbent resin comprises polyacrylamide and sodium polyacrylate, and the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: (0.4-0.8).
By adopting the technical scheme, when the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: (0.4-0.8), the ultraviolet-sterilized coating belt has good aging resistance, and the water absorption rate is further reduced.
Preferably, the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: 0.6.
by adopting the technical scheme, when the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: when 0.6 hour, the ultraviolet sterilized coating band not only has better aging resistance, but also has the minimum reduction range of the water absorption rate.
Preferably, the molecular weight of the water-absorbent resin is in the range of 100-200 ten thousand.
By adopting the technical scheme, when the molecular weight of the water-absorbing resin is 100-200 ten thousand, the aging resistance of the prepared coating band is enhanced, and the water-absorbing rate of the coating band is reduced after the coating band is sterilized by ultraviolet irradiation.
Preferably, the silane coupling agent is any one or a mixture of several of KH550, KH560 and KH 570.
By adopting the technical scheme, the compatibility of the silicon nitride ceramic powder and the water-absorbent resin can be improved by adding the silane coupling agents KH550, KH560 and KH 570.
In a second aspect, the present application provides a method for manufacturing an anti-aging sphygmomanometer cover tape, which adopts the following technical scheme:
a manufacturing method of an anti-aging sphygmomanometer covering belt is characterized by comprising the following steps:
s1, adding the modified water-absorbing resin into the polyester fiber and the cotton fiber, and performing ball milling for 50-80min at the ball milling speed of 200-300rad/min to ensure that the modified water-absorbing resin is coated on the outer sides of the polyester fiber and the cotton fiber to obtain modified mixed fiber;
s2, twisting the modified mixed fiber into roving after the modified mixed fiber is made into strips;
and S3, weaving the roving into a wrapping belt.
When adopting above-mentioned technical scheme production cladding belt, not only have step simple, convenient operation's advantage, the ultraviolet resistance of the cladding belt who makes moreover promotes, and the hygroscopic property of cladding belt after the ultraviolet irradiation disinfection changes little.
In summary, the present application has the following beneficial effects:
1. after the water-absorbing resin is modified by adopting the silicon nitride ceramic powder, the silane coupling agent and the starch, the problem that the coating belt is easy to age after being sterilized by ultraviolet irradiation can be solved, and meanwhile, the problem that the moisture absorption performance of the coating belt is greatly reduced after being sterilized by ultraviolet irradiation can be solved.
2. When the weight ratio of polyacrylamide to sodium polyacrylate is 1: (0.4-0.8), the ultraviolet-sterilized coating belt has good aging resistance, and the water absorption rate is further reduced.
Detailed Description
The present application will be described in further detail with reference to examples and comparative examples.
The raw materials adopted in the application are all commercially available, wherein:
dacron silk is purchased from Shenzhen special power chemical fiber GmbH.
Cotton fibers were purchased from Intelligent fiber products, Inc. of Dongguan.
Polyacrylamide is available from hua navigation chemical technology ltd, suzhou.
Sodium polyacrylate was purchased from Ofu Biotech, Inc., Jiangsu.
The silicon carbide ceramic powder is prepared by crushing the waste silicon nitride sealing ring of Shenzhen Xinlongrun precision ceramics Limited company.
Preparation examples
The raw material compositions and proportions of the modified water-absorbent resins of preparation examples 1 to 4 are as follows in Table 1.
TABLE 1 raw Material composition (unit/kg) of modified Water-absorbent resin in preparation examples 1 to 4
Starting materials | Preparation example 1 | Preparation example 2 | Preparation example 3 | Preparation example 4 |
Water-absorbent resin | 50 | 60 | 65 | 70 |
Silicon nitride ceramic powder | 18 | 20 | 24 | 26 |
Silane coupling agent | 4 | 6 | 8 | 8 |
Starch | 4.5 | 6.2 | 6.8 | 7.5 |
Preparation example 1
A modified water-absorbent resin, the proportion of each raw material is referred to preparation example 1 in Table 1, and the preparation method comprises the following steps:
(1) uniformly mixing starch and silicon nitride ceramic powder with the particle size range of 40-60nm, and performing ball milling at the ball milling speed of 320rad/min for 50min to obtain a silicon nitride ceramic powder-starch mixture;
(2) firing the silicon nitride ceramic powder-starch mixture at 700 ℃ for 2h, taking out and cooling to obtain modified silicon nitride ceramic powder;
(3) uniformly mixing the modified silicon nitride ceramic powder with a silane coupling agent KH550, continuously adding water-absorbent resin, and performing ball milling at a ball milling speed of 100rad/min for 40min to obtain the modified water-absorbent resin; wherein, the water-absorbing resin in the preparation example is polyacrylamide with the particle size range of 300-500nm and the molecular weight of 100 ten thousand.
Preparation example 2
A modified water-absorbent resin differing from preparation example 1 in that: the proportions of the respective raw materials are referred to in table 1, preparation example 2.
Preparation example 3
A modified water-absorbent resin differing from preparation example 1 in that: the proportions of the respective raw materials are referred to in table 1, preparation example 3.
Preparation example 4
A modified water-absorbent resin differing from preparation example 1 in that: the compounding ratio of each raw material was referred to preparation example 4 in table 1.
Preparation example 5
A modified water-absorbent resin which is different from the preparation example 3 in that:
the ball milling speed in the step (1) is 480rad/min, and the ball milling time is 30 min;
the burning temperature in the step (2) is 800 ℃, and the burning time is 1 h;
the silane coupling agent in the step (3) is silane coupling agent 570, the ball milling speed is 120rad/min, and the ball milling time is 20 min.
Preparation example 6
A modified water-absorbent resin which is different from the preparation example 3 in that:
the water-absorbing resin in the step (3) is polyacrylamide with the particle size range of 300-500nm and the molecular weight of 200 ten thousand.
Preparation example 7
A modified water-absorbent resin which is different from the resin obtained in preparation example 3 in that:
the water-absorbing resin in the step (3) is polyacrylamide with the particle size range of 300-500nm and the molecular weight of 20 ten thousand.
Preparation example 8
A modified water-absorbent resin which is different from the preparation example 3 in that:
the water-absorbing resin in the step (3) comprises polyacrylamide and sodium polyacrylate, the weight ratio of the polyacrylamide to the sodium polyacrylate is 1:0.4, the particle size ranges of the polyacrylamide and the sodium polyacrylate are both 300-500nm, and the molecular weights of the polyacrylamide and the sodium polyacrylate are both 100 ten thousand.
Preparation example 9
A modified water-absorbent resin which is different from that in preparation example 8 in that:
in the step (3), the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: 0.6.
Preparation example 10
A modified water-absorbent resin which is different from the modified water-absorbent resin prepared in preparation example 8 in that:
in the step (3), the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: 0.8.
Examples
The compositions and proportions of the raw materials for the coated tapes of examples 1-3 are given in Table 2 below.
TABLE 2 composition and ratio (unit/kg) of raw materials for the wrapping tape in examples 1-3
Raw materials | Example 1 | Example 2 | Example 3 |
Polyester yarn | 70 | 80 | 90 |
Cotton fiber | 55 | 65 | 75 |
Modified water-absorbent resin | 28 | 32 | 36 |
Example 1
An anti-aging sphygmomanometer covering belt, the proportion of each raw material is referred to example 1 in a table 2, and the manufacturing method comprises the following steps:
s1, adding the modified water-absorbent resin into polyester yarns and cotton fibers, and performing ball milling for 80min at a ball milling speed of 200rad/min to ensure that the modified water-absorbent resin prepared in the preparation example 1 is coated on the outer sides of the polyester yarns and the cotton fibers to obtain modified mixed fibers;
s2, twisting the modified mixed fiber into roving after the modified mixed fiber is made into strips;
and S3, weaving the roving into a wrapping tape.
Example 2
An aging-resistant sphygmomanometer covering tape, differing from example 1 in that:
the proportions of the raw materials are referred to example 2 in table 2;
the ball milling speed in the step S1 is 250rad/min, and the ball milling time is 65 min.
Example 3
An aging-resistant sphygmomanometer covering tape, differing from example 1 in that:
the proportions of the raw materials are referred to example 3 in table 2;
the ball milling speed in step S1 is 300rad/min, and the ball milling time is 50 min.
Example 4
An aging-resistant sphygmomanometer covering belt, which is different from the embodiment 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 2 was used.
Example 5
An aging-resistant sphygmomanometer covering belt, which is different from the embodiment 2 in that:
modified Water-absorbent resin the modified water-absorbent resin prepared in preparation example 3 was used.
Example 6
An aging-resistant sphygmomanometer covering belt, which is different from the embodiment 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 4 was used.
Example 7
An aging-resistant sphygmomanometer covering belt, which is different from the embodiment 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 5 was used.
Example 8
An aging-resistant sphygmomanometer covering tape, differing from example 2 in that:
modified Water-absorbent resin the modified water-absorbent resin prepared in preparation example 6 was used.
Example 9
An aging-resistant sphygmomanometer covering tape, differing from example 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 7 was used.
Example 10
An aging-resistant sphygmomanometer covering tape, differing from example 2 in that:
modified Water-absorbent resin the modified water-absorbent resin prepared in preparation example 8 was used.
Example 11
An aging-resistant sphygmomanometer covering tape, differing from example 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 9 was used.
Example 12
An aging-resistant sphygmomanometer covering belt, which is different from the embodiment 2 in that:
modified Water-absorbent resin the modified water-absorbent resin obtained in preparation example 10 was used.
Comparative example
Comparative example 1
A sphygmomanometer cuff belt, differing from example 2 in that:
the silicon nitride ceramic powder in the modified water-absorbing resin is replaced by diatomite with the same quantity and the same particle size.
Comparative example 2
A sphygmomanometer cuff belt, differing from example 2 in that:
the silane coupling agent in the modified water-absorbing resin is replaced by the same amount of silicon nitride ceramic powder.
Comparative example 3
A sphygmomanometer cuff belt, differing from example 2 in that:
the starch in the modified water-absorbing resin is replaced by the same amount of diatomite.
Detection method/test method
Water absorption rate: referring to the evaluation part 2 of moisture absorption and quick drying of textiles in the national standard GB/T21655.2-2019: dynamic moisture transfer method the moisture absorption performance of the wrapping tapes in examples 1-12 and comparative examples 1-3 was tested.
Tearing strength: referring to the national standard GB/T3917.1-2009 part 1 of tearing performance of textile fabrics: determination of tear Strength by impact pendulum method the tear strength of the cover tapes in examples 1 to 12 and comparative examples 1 to 3 was tested.
Table 3 performance data for coated tapes of examples 1-12 and comparative examples 1-3
Detecting items | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
Water absorption Rate (%/s) before Disinfection | 52.3 | 54.2 | 53.1 | 54.9 | 55.1 |
Water absorption Rate (%/s) after Disinfection | 43.9 | 45.3 | 44.6 | 47.8 | 48.2 |
Tearing strength before disinfection (N) | 63 | 68 | 66 | 69 | 70 |
Sterilized and tornBreak strong force (N) | 58 | 62 | 60 | 63 | 62 |
Detecting items | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 |
Water absorption Rate (%/s) before Disinfection | 54.6 | 55.4 | 55.3 | 48.9 | 56.1 |
Water absorption Rate (%/s) after Disinfection | 45.7 | 48.5 | 49.5 | 38.2 | 52.2 |
Tearing strength before disinfection (N) | 67 | 69 | 70 | 69 | 70 |
Tearing strength after disinfection (N) | 60 | 63 | 64 | 62 | 63 |
Detecting items | Example 11 | Example 12 | Comparative example 1 | Comparative example 2 | Comparative example 3 |
Water absorption Rate (%/s) before Disinfection | 56.8 | 56.4 | 53.9 | 54.2 | 54.4 |
Water absorption Rate (%/s) after Disinfection | 54.1 | 52.6 | 30.1 | 30.4 | 30.6 |
Tearing strength before disinfection (N) | 69 | 72 | 68 | 70 | 69 |
Tearing strength after disinfection (N) | 63 | 68 | 49 | 41 | 45 |
It can be seen from the combination of example 2 and comparative examples 1 to 3 and table 3 that the silicon nitride ceramic powder, the silane coupling agent and the starch have a synergistic effect on the modification of the water-absorbent resin, and the problem that the wrapping tape is easy to age after being sterilized by ultraviolet radiation can be solved only by simultaneously modifying the water-absorbent resin by the silicon nitride ceramic powder, the silane coupling agent and the starch, and the problem that the moisture absorption performance of the wrapping tape is greatly reduced after being sterilized by ultraviolet radiation can be solved.
As can be seen by combining example 5 with examples 8 to 9 and Table 3, when the molecular weight of the water-absorbent resin was in the range of 100-.
As can be seen from the combination of example 5 and examples 10 to 12 and table 3, when the mixture of polyacrylamide and sodium polyacrylate is used as the water-absorbing resin, the water-absorbing rate of the coated tape after sterilization by ultraviolet irradiation is further decreased, and the other conditions are not changed, wherein when the weight ratio of polyacrylamide to sodium polyacrylate is 1: at 0.6, the water absorption rate of the coated belt is reduced to the minimum.
The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.
Claims (6)
1. An anti-aging sphygmomanometer covering belt is characterized by being prepared from the following raw materials in parts by weight:
polyester yarn: 70 to 90 portions of
Cotton fiber: 55 to 75 portions of
Modified water-absorbent resin: 28-36 parts
The water-absorbing resin is one or a mixture of more of polyacrylamide, starch-acrylate polymer and sodium polyacrylate;
the method for preparing the modified water-absorbing resin comprises the following steps:
(1) uniformly mixing 5.5-7.5 parts by weight of starch and 20-24 parts by weight of silicon nitride ceramic powder with the particle size range of 40-60nm, and performing ball milling at the ball milling speed of 320-480rad/min for 30-50min to obtain a silicon nitride ceramic powder-starch mixture;
(2) burning the silicon nitride ceramic powder-starch mixture at the temperature of 700-800 ℃ for 1-2h, taking out and cooling to obtain modified silicon nitride ceramic powder;
(3) uniformly mixing the modified silicon nitride ceramic powder with 6-8 parts by weight of silane coupling agent, continuously adding 60-65 parts by weight of water-absorbing resin with the particle size range of 300-;
the anti-aging sphygmomanometer coating belt adopts the following manufacturing method:
s1, adding the modified water-absorbing resin into the polyester fiber and the cotton fiber, and performing ball milling for 50-80min at the ball milling speed of 200-300rad/min to ensure that the modified water-absorbing resin is coated on the outer sides of the polyester fiber and the cotton fiber to obtain modified mixed fiber;
s2, twisting the modified mixed fiber into roving after the modified mixed fiber is made into strips;
and S3, weaving the roving into a wrapping belt.
2. The covered belt for an anti-aging sphygmomanometer as claimed in claim 1, wherein the water-absorbent resin is 60 to 65 parts by weight, the silicon nitride ceramic powder is 20 to 24 parts by weight, the silane coupling agent is 6 to 8 parts by weight, and the starch is 6.2 to 6.8 parts by weight.
3. The aging-resistant sphygmomanometer covering belt according to claim 1, wherein the water-absorbent resin comprises polyacrylamide and sodium polyacrylate, and the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: (0.4-0.8).
4. The aging-resistant sphygmomanometer covering belt according to claim 3, wherein the weight ratio of the polyacrylamide to the sodium polyacrylate is 1: 0.6.
5. the aging-resistant sphygmomanometer covering tape according to claim 1, wherein the silane coupling agent is any one or a mixture of several of KH550, KH560 and KH 570.
6. The method for manufacturing the aging-resistant sphygmomanometer covering belt according to any one of claims 1 to 5, comprising the steps of:
s1, adding the modified water-absorbent resin into the polyester yarns and the cotton fibers, and performing ball milling for 50-80min at a ball milling speed of 200 plus 300rad/min to ensure that the modified water-absorbent resin is coated on the outer sides of the polyester yarns and the cotton fibers to obtain modified mixed fibers;
s2, twisting the modified mixed fiber into roving after the modified mixed fiber is made into strips;
and S3, weaving the roving into a wrapping tape.
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CN104631122B (en) * | 2015-02-26 | 2016-12-07 | 河南科技大学 | The preparation method of high-modulus shock resistance carbon fibre composite |
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