CN113440422A - Matte eyeliner and preparation method thereof - Google Patents
Matte eyeliner and preparation method thereof Download PDFInfo
- Publication number
- CN113440422A CN113440422A CN202110739833.XA CN202110739833A CN113440422A CN 113440422 A CN113440422 A CN 113440422A CN 202110739833 A CN202110739833 A CN 202110739833A CN 113440422 A CN113440422 A CN 113440422A
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- CN
- China
- Prior art keywords
- eyeliner
- matte
- mixture
- water
- silica
- Prior art date
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- Granted
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- 238000002360 preparation method Methods 0.000 title abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 44
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 26
- 239000000843 powder Substances 0.000 claims abstract description 24
- 239000002738 chelating agent Substances 0.000 claims abstract description 8
- 239000000945 filler Substances 0.000 claims abstract description 8
- 239000003906 humectant Substances 0.000 claims abstract description 8
- 239000003755 preservative agent Substances 0.000 claims abstract description 8
- 230000002335 preservative effect Effects 0.000 claims abstract description 8
- 239000012153 distilled water Substances 0.000 claims abstract description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 67
- 239000000203 mixture Substances 0.000 claims description 46
- 239000000377 silicon dioxide Substances 0.000 claims description 33
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 22
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 20
- 229920001577 copolymer Polymers 0.000 claims description 19
- 150000002148 esters Chemical class 0.000 claims description 17
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 16
- 238000003756 stirring Methods 0.000 claims description 15
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 11
- 238000002156 mixing Methods 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 7
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 6
- 238000000034 method Methods 0.000 claims description 6
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 4
- LRCFXGAMWKDGLA-UHFFFAOYSA-N dioxosilane;hydrate Chemical compound O.O=[Si]=O LRCFXGAMWKDGLA-UHFFFAOYSA-N 0.000 claims description 4
- 229960004029 silicic acid Drugs 0.000 claims description 4
- 239000002202 Polyethylene glycol Substances 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 238000004806 packaging method and process Methods 0.000 claims description 3
- 229920001223 polyethylene glycol Polymers 0.000 claims description 3
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims description 2
- CLAHOZSYMRNIPY-UHFFFAOYSA-N 2-hydroxyethylurea Chemical compound NC(=O)NCCO CLAHOZSYMRNIPY-UHFFFAOYSA-N 0.000 claims description 2
- RMTFNDVZYPHUEF-XZBKPIIZSA-N 3-O-methyl-D-glucose Chemical compound O=C[C@H](O)[C@@H](OC)[C@H](O)[C@H](O)CO RMTFNDVZYPHUEF-XZBKPIIZSA-N 0.000 claims description 2
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 2
- ODHCTXKNWHHXJC-VKHMYHEASA-N 5-oxo-L-proline Chemical compound OC(=O)[C@@H]1CCC(=O)N1 ODHCTXKNWHHXJC-VKHMYHEASA-N 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 2
- YDNKGFDKKRUKPY-JHOUSYSJSA-N C16 ceramide Natural products CCCCCCCCCCCCCCCC(=O)N[C@@H](CO)[C@H](O)C=CCCCCCCCCCCCCC YDNKGFDKKRUKPY-JHOUSYSJSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 claims description 2
- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 claims description 2
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims description 2
- CRJGESKKUOMBCT-VQTJNVASSA-N N-acetylsphinganine Chemical compound CCCCCCCCCCCCCCC[C@@H](O)[C@H](CO)NC(C)=O CRJGESKKUOMBCT-VQTJNVASSA-N 0.000 claims description 2
- 239000004721 Polyphenylene oxide Substances 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 2
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims description 2
- 241001506047 Tremella Species 0.000 claims description 2
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims description 2
- 229920006322 acrylamide copolymer Polymers 0.000 claims description 2
- 239000001361 adipic acid Substances 0.000 claims description 2
- 235000011037 adipic acid Nutrition 0.000 claims description 2
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims description 2
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 2
- 239000004202 carbamide Substances 0.000 claims description 2
- 229940106189 ceramide Drugs 0.000 claims description 2
- ZVEQCJWYRWKARO-UHFFFAOYSA-N ceramide Natural products CCCCCCCCCCCCCCC(O)C(=O)NC(CO)C(O)C=CCCC=C(C)CCCCCCCCC ZVEQCJWYRWKARO-UHFFFAOYSA-N 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 229920006037 cross link polymer Polymers 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims description 2
- ACCCMOQWYVYDOT-UHFFFAOYSA-N hexane-1,1-diol Chemical compound CCCCCC(O)O ACCCMOQWYVYDOT-UHFFFAOYSA-N 0.000 claims description 2
- 229940031575 hydroxyethyl urea Drugs 0.000 claims description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims description 2
- VVGIYYKRAMHVLU-UHFFFAOYSA-N newbouldiamide Natural products CCCCCCCCCCCCCCCCCCCC(O)C(O)C(O)C(CO)NC(=O)CCCCCCCCCCCCCCCCC VVGIYYKRAMHVLU-UHFFFAOYSA-N 0.000 claims description 2
- 229940101267 panthenol Drugs 0.000 claims description 2
- 235000020957 pantothenol Nutrition 0.000 claims description 2
- 239000011619 pantothenol Substances 0.000 claims description 2
- 239000000419 plant extract Substances 0.000 claims description 2
- 229920000058 polyacrylate Polymers 0.000 claims description 2
- 229920000570 polyether Polymers 0.000 claims description 2
- 229920001451 polypropylene glycol Polymers 0.000 claims description 2
- 229920001282 polysaccharide Polymers 0.000 claims description 2
- 239000005017 polysaccharide Substances 0.000 claims description 2
- 229920002635 polyurethane Polymers 0.000 claims description 2
- 239000004814 polyurethane Substances 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims description 2
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims description 2
- 229940079889 pyrrolidonecarboxylic acid Drugs 0.000 claims description 2
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 2
- 239000001540 sodium lactate Substances 0.000 claims description 2
- 229940005581 sodium lactate Drugs 0.000 claims description 2
- 235000011088 sodium lactate Nutrition 0.000 claims description 2
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- 229960002920 sorbitol Drugs 0.000 claims description 2
- 229940045136 urea Drugs 0.000 claims description 2
- 239000000811 xylitol Substances 0.000 claims description 2
- 235000010447 xylitol Nutrition 0.000 claims description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims description 2
- 229960002675 xylitol Drugs 0.000 claims description 2
- SNAAJJQQZSMGQD-UHFFFAOYSA-N aluminum magnesium Chemical compound [Mg].[Al] SNAAJJQQZSMGQD-UHFFFAOYSA-N 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 21
- 239000007788 liquid Substances 0.000 abstract description 12
- 239000002994 raw material Substances 0.000 abstract description 10
- 239000000463 material Substances 0.000 abstract description 9
- 239000002537 cosmetic Substances 0.000 abstract description 6
- 230000002688 persistence Effects 0.000 abstract 1
- 230000006641 stabilisation Effects 0.000 description 26
- 238000011105 stabilization Methods 0.000 description 26
- 238000012360 testing method Methods 0.000 description 16
- 238000011084 recovery Methods 0.000 description 11
- 239000002562 thickening agent Substances 0.000 description 6
- 230000001804 emulsifying effect Effects 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 3
- 229960005323 phenoxyethanol Drugs 0.000 description 3
- 230000035807 sensation Effects 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 229920006243 acrylic copolymer Polymers 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 239000003086 colorant Substances 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 238000005485 electric heating Methods 0.000 description 2
- 239000003995 emulsifying agent Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- 210000003128 head Anatomy 0.000 description 2
- KWLMIXQRALPRBC-UHFFFAOYSA-L hectorite Chemical compound [Li+].[OH-].[OH-].[Na+].[Mg+2].O1[Si]2([O-])O[Si]1([O-])O[Si]([O-])(O1)O[Si]1([O-])O2 KWLMIXQRALPRBC-UHFFFAOYSA-L 0.000 description 2
- 229910000271 hectorite Inorganic materials 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- AEIJTFQOBWATKX-UHFFFAOYSA-N octane-1,2-diol Chemical compound CCCCCCC(O)CO AEIJTFQOBWATKX-UHFFFAOYSA-N 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- -1 polyethylene Polymers 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 239000011863 silicon-based powder Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000000725 suspension Substances 0.000 description 2
- GYDYJUYZBRGMCC-INIZCTEOSA-N (2s)-2-amino-6-(dodecanoylamino)hexanoic acid Chemical compound CCCCCCCCCCCC(=O)NCCCC[C@H](N)C(O)=O GYDYJUYZBRGMCC-INIZCTEOSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004288 Sodium dehydroacetate Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- GQEZCXVZFLOKMC-UHFFFAOYSA-N n-alpha-hexadecene Natural products CCCCCCCCCCCCCCC=C GQEZCXVZFLOKMC-UHFFFAOYSA-N 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000007764 o/w emulsion Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 229960001866 silicon dioxide Drugs 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 125000004469 siloxy group Chemical group [SiH3]O* 0.000 description 1
- 229940079839 sodium dehydroacetate Drugs 0.000 description 1
- 235000019259 sodium dehydroacetate Nutrition 0.000 description 1
- 159000000000 sodium salts Chemical class 0.000 description 1
- DSOWAKKSGYUMTF-GZOLSCHFSA-M sodium;(1e)-1-(6-methyl-2,4-dioxopyran-3-ylidene)ethanolate Chemical compound [Na+].C\C([O-])=C1/C(=O)OC(C)=CC1=O DSOWAKKSGYUMTF-GZOLSCHFSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/412—Microsized, i.e. having sizes between 0.1 and 100 microns
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/432—Direct dyes
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a matte eyeliner and a preparation method thereof, wherein the eyeliner mainly comprises the following components in percentage by mass: powder filler: 1-10%, preservative: 0.1-1%, film-forming agent: 5-40% of a humectant: 1-10%, color paste: 10-50%, chelating agent: 0.01-0.2% and distilled water to 100%. The invention has the advantages that a novel matte eyeliner is developed, the added powder raw materials can be uniformly distributed in the material body, the pen point is not blocked, and the liquid outlet is smooth. The powder raw materials and the film-forming agent are mixed according to a specific proportion, so that the eyeliner has good matte effect and strong persistence. The invention belongs to the technical field of cosmetics.
Description
Technical Field
The invention belongs to the field of cosmetics, and particularly relates to eyeliner and a preparation method thereof.
Background
The eye liner products are color cosmetics which are commonly used for eyes to lead eyes to have spirit and increase the outline feeling, are deeply loved by beauty lovers, and the existing eye liner products comprise four categories of eye liners, dipping type eye liners, eye liner glue pens and eye liner liquid pens. Most of eyeliner pens in the market are bright, and the market demand of matte eyeliner pens is more and more increased due to the popularity of mist makeup. Most film forming agents of the eyeliner pen are bright, and the matte effect is difficult to present in direct-liquid eyeliner. The matte light sensation of cosmetics can be reached to silicon powder usually, but because the discharge gate of eyeliner liquid is thin very easily leads to the nib to block up, and solid particle can produce simultaneously and subside and make the play water not smooth, and the matte effect can not last, and the eyeliner is usually made in order to satisfy the requirement of user to matte light sensation on the market, and the eyeliner is a solid-like eyeliner product that contains the wax base, has certain hardness, and the use sense is not very good.
Patent CN202011388816.8 discloses an eyeliner based on hectorite lipophilic thickener and a preparation method thereof. The eyeliner comprises a lipophilic thickening agent, and the eyeliner comprises, by weight, 0.2-1% of hectorite lipophilic thickening agent, 5-10% of polyethylene, 0-0.8% of mica, 1-5% of VP/hexadecene copolymer, 11.5-15% of adhesive, 23.4-26% of colorant, 0.5-2% of phenyl dimethyl siloxy silicate, 1-3% of lauroyl lysine, 0.5-3% of polyhydroxystearic acid, 18-20% of humectant, 25-35% of film forming agent and 0.1% of antioxidant. The oily thickener composition has excellent dispersing performance in oily environment, so that the micro particles of the toner are uniformly distributed, and the color of the product is improved. But the eye liner is not easy to remove and remove, simultaneously, the skin of the eyes is sensitive and fine, the hardness of the eye liner gel pen is stronger to the pulling feeling of the eyes, and the eye liner gel pen has less irritation under the general condition than the eye liner liquid pen.
Patent CN201810657569.3 discloses an eyeliner and a preparation method thereof. The composition comprises the following substances in parts by weight: 30-50 parts of acrylate copolymer, 10-20 parts of polyethylene glycol, 5-8 parts of propylene glycol, 3-8 parts of isopropyl palmitate, 1-3 parts of titanium dioxide, 3-10 parts of colorant and 50-120 parts of water. The eyeliner liquid disclosed by the invention adopts the acrylate copolymer, so that the addition amount of a surfactant which has irritation to the skin is reduced, the prepared eyeliner liquid has texture after being smeared, the line feeling is quite clear, the makeup is lasting, the makeup is not easy to be blurry, the brightness is high, and the water resistance and the oil resistance are good. It belongs to bright eyeliner.
Patent CN202010825975.3 discloses a pearlescent eyeliner and a preparation method thereof. The raw materials of the invention comprise the following components in parts by weight: the pearlescent eyeliner provided by the invention has good centrifugal stability and high-temperature storage stability, can uniformly and continuously discharge water in a liquid pen, and is saturated and uniform in color. The patent also uses a plurality of powder raw materials and adds a plurality of thickening suspending agents to stabilize the system, but the influence on the viscosity is great, so the material body is thick, the viscosity is great, and the formula can achieve stable and continuous liquid output without adding or adding a few thickening agents.
The invention relates to an aqueous matte eyeliner and a preparation method thereof, the raw materials of the eyeliner are simple, easy to obtain, safe and nontoxic, the predispersed aqueous color paste is selected to be perfectly matched with a system, and the film forming agent and the powder of the eyeliner are screened and prepared by multiple particle sizes and proportions and are tightly attached to the skin, so that the makeup holding effect is improved. The matte effect of the formula is mainly provided by silica which is matched by selecting various particle sizes, the matte effect is good and easy to disperse, the silica is suspended in a material body under the combined action of the thickening agent and the film forming agent and is uniformly distributed on the film forming agent after being coated, so that each stroke has an extremely high matte effect.
Disclosure of Invention
The invention mainly aims to provide an innovative matte eyeliner pen which has better durability and is not easy to be tinged compared with an eyeliner pen.
The invention provides a matte eyeliner which is characterized in that the raw materials in percentage by mass of the composition are as follows: powder filler: 1-10%, preservative: 0.1-1%, film-forming agent: 10-40% of a humectant: 1-10%, color paste: 10-50%, chelating agent: 0.01-0.2% and distilled water to 100%.
The matte eyeliner provided by the invention has the characteristics that the powder filler is silica. When light irradiates an object and is directly reflected back to generate mirror reflection, because the selected silica is porous spherical silicon dioxide, when the light irradiates the surface of the silicon powder, the light propagation direction at the interface is diffused towards the periphery to generate diffuse reflection so as to achieve the matte effect. The selected silica particle size is 10-12000nm, the refractive indexes of different forms of silica with different particle sizes are different, the suspension stability is different, and the optimal diffuse reflection and the optimal suspension stability are achieved by matching silica with different sizes and blending according to a specific proportion. The specific surface area of the silica selected here is 180-300m2/g, 2 kinds of silica are selected, which are respectively gas phase method silica of 10-20nm and mesoporous spherical silica of 1-6 microns, the specific surface areas of the two kinds of silica are very large, the optimum is 200-260 m2/g, and the optimum is 1-10% of silica dosage, 2-6%. The silica can be used in matte eyeliner, oil-in-water emulsion, foundation make-up, and oil control cosmetic water to achieve good matte effect.
The matte eyeliner provided by the invention can also have the characteristic that the film-forming agent can be one or a mixture of more than two of aqueous film-forming agents, polyvinylpyrrolidone, polyvinyl alcohol, acrylate/octylacrylamide copolymer, acrylic acid (ester)/acrylamide copolymer, adipic acid/diethylene glycol/glycerol cross-linked polymer, styrene/acrylic acid (ester) copolymer, polyacrylate, methyl methacrylate/acrylonitrile copolymer, acrylic acid (ester) copolymer and aqueous polyurethane. Different film forming agents have different film forming effects, the same type of film forming agents with different molecular weights have different durability and friction resistance, and the film forming effect is good and durable without influencing the matte effect by screening different types of film forming agents with different molecular weights. The film forming agent is an acrylic acid (ester) copolymer with different molecular weights and a styrene/acrylic acid (ester) copolymer are the preferable scheme.
The matte eyeliner provided by the invention can also be characterized in that the humectant is one or a mixture of more than two of glycerin, butanediol, propylene glycol, polyethylene glycol, hexanediol, xylitol, polypropylene glycol, sorbitol, pyrrolidone carboxylic acid, sodium lactate, urea, hydroxyethyl urea, methyl glucose polyether, trehalose, tremella polysaccharide, sodium hyaluronate, panthenol, ceramide and natural plant extracts.
The matte eyeliner provided by the invention can also have the characteristic that the color paste is one or a mixture of more than two of water-based organic color pastes and water-based inorganic color pastes. Wherein the organic color paste comprises organic toner lake water dispersion paste such as CI 74160/CI 124905/CI 75470/CI19140/CI42090/CI 16035 and the like; the inorganic color paste comprises inorganic toner water dispersion paste such as CI 77266/CI77891/CI 77491/CI 77492/CI 77510/CI77007/CI77288 and the like.
The matte eyeliner provided by the invention can also have the characteristic that the prepared material can be used in ball brush heads, ball cotton heads and cotton core cotton head wrapping materials.
The preparation method of the matte eyeliner comprises the following steps.
(1) According to the mass fraction, 10-20% of water and the chelating agent are stirred by a stirrer at the rotating speed of 150rpm, the mixture is stirred to be completely dissolved uniformly to obtain a mixture 1, and the mixture is heated to 85-90 ℃ by a water bath kettle.
(2) Dispersing and mixing the powder in a specific proportion uniformly by an airflow crushing and dispersing machine, stirring 5-20% of water and the dispersed powder by a stirrer at the rotating speed of 150rpm according to the mass fraction, stirring to completely and uniformly disperse the water and the powder to obtain a mixture 2, homogenizing the mixture for 5min at the rotating speed of 10000rpm by a homogenizing and emulsifying machine, and heating the mixture to 85-90 ℃ by a water bath kettle.
(3) Uniformly mixing the preservative, the film forming agent and the humectant according to mass fraction, stirring with a stirrer at the rotating speed of 200rpm to obtain a mixture 3, homogenizing with a homogenizing emulsifier at the rotating speed of 10000rpm for 6-10min, and heating to 85-90 ℃ with a water bath kettle.
(4) Adding mixture 1 and mixture 2 into mixture 3 in sequence, stirring with a stirrer at 200rpm, stirring to mix completely, and homogenizing with a homogenizing emulsifier at 10000rpm for 2min to obtain mixture 4.
(5) And stirring the mixture 4 by a stirrer at the rotating speed of 200rpm and cooling to 45-50 ℃.
(6) Adding the color paste into the mixture 4 slowly under stirring to completely mix uniformly, and homogenizing for 5-10min at 10000rpm by using a homogenizing emulsifying machine.
(7) Filtering with 200 mesh filter cloth to obtain matte eyeliner, and packaging.
According to the matte eyeliner, silica with different particle sizes is selected, so that the matte effect of the material body is good; the used water-based color paste has high dispersibility, so that the color is more saturated and uniform; different film forming agents are selected and matched, so that the film forming effect is firm and durable, the matte light sensation cannot be weakened, and finally the eye liner liquid body is moderate in viscosity, smooth in water outlet, good in matte effect and strong in durability.
Detailed Description
In order to make the technical means, the creation features, the achievement purposes and the effects of the invention easy to understand, the invention is specifically described with the embodiment below.
The raw materials used in the examples are all common raw materials sold in the market; the relevant description is as follows:
film-forming agent: the main components are as follows: trade names of acrylic acid (ester) copolymer, water, phenoxyethanol: kingcova PA-36 manufacturer: jiangxi sheath science, Inc.;
film-forming agent: the main components are as follows: styrene/acrylic acid (ester) copolymer, water, sodium dehydroacetate trade name: kingcova PA-59 manufacturer: jiangxi sheath science, Inc., wherein the styrene/acrylic acid (ester) copolymer is a common raw material for cosmetics;
powder: silica, trade name: kingsica 3022 manufacturer: jiangxi sheath science, Inc.;
powder: silica, trade name: kingsica 5020 manufacturer: jiangxi sheath science, Inc.;
powder: hydrated silica, trade name: zeodent 165 manufacturer: win special chemistry (shanghai) limited;
preservative: phenoxyethanol, caprylyl glycol = 6.5: 3.5; trade name: microcare PHG manufacturer: turker specialty Chemicals (Zhenjiang) Co., Ltd;
color paste: carbon Black W-306 manufacturer: jiangxi sheath science, Inc. with the composition: water, CI 77266, ceteareth-25, caprylyl glycol, phenoxyethanol.
Examples 1 to 7
Examples 8 to 13:
| example 8 | Example 9 | Example 10 | Example 11 | Example 12 | Example 13 | ||
| Name of raw materials | The content of the components is% | The content of the components is% | The content of the components is% | The content of the components is% | The content of the components is% | The content of the components is% | |
| Chelating agents | EDTA 2 sodium salt | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 | 0.05 |
| Powder body | Silica (3022) | 5 | 5 | 5 | 5 | 5 | 5 |
| Preservative | Microcare PHG | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 | 0.5 |
| Film forming agent | Kingcova PA-36 | 5 | 10 | 15 | 25 | 30 | / |
| Film forming agent | Kingcova PA-59 | 25 | 20 | 15 | 5 | / | 30 |
| Moisture-retaining agent | Propylene glycol | 10 | 10 | 10 | 10 | 10 | 10 |
| Color paste | Carbon Black W-306 | 20 | 20 | 20 | 20 | 20 | 20 |
| Deionized water | Deionized water | TO100 | TO100 | TO100 | TO100 | TO100 | TO100 |
The operation steps are as follows.
(1) According to the mass fraction, 10-20% of water and the chelating agent are stirred for 5 minutes by a stirrer at the rotating speed of 150rpm to obtain a mixture 1, and then the mixture is heated to 90 ℃ by a water bath kettle.
(2) Dispersing and mixing the powder in a specific proportion for 5 minutes by using an airflow crushing and dispersing machine, stirring 5-20% of water and the dispersed powder for 5 minutes by using a stirrer at the rotating speed of 150rpm according to the mass fraction to obtain a mixture 2, homogenizing for 5 minutes by using a homogenizing and emulsifying machine at the rotating speed of 10000rpm, and heating to 90 ℃ by using a water bath kettle.
(3) Uniformly mixing the preservative and the film-forming agent according to mass fraction, stirring for 5 minutes by using a stirrer at the rotating speed of 200rpm to obtain a mixture 3, homogenizing for 8 minutes by using a homogenizing emulsifying machine at the rotating speed of 10000rpm, and heating to 90 ℃ by using a water bath kettle.
(4) The mixture 1 and the mixture 2 were sequentially added to the mixture 3, stirred with a stirrer at 200rpm for 8 minutes, and then homogenized with a homogenizer at 10000rpm for 2 minutes to obtain a mixture 4.
(5) The mixture 4 was stirred with a stirrer at 200rpm until the temperature had dropped to 50 ℃.
(6) And adding the color paste into the mixture 4 at a low speed during stirring to ensure that the color paste is completely and uniformly mixed, and homogenizing for 8 minutes by using a homogenizing and emulsifying machine at the rotating speed of 10000 rpm.
(7) Filtering with 200 mesh filter cloth to obtain matte eyeliner, and packaging.
Comparative test 1: and (5) testing water resistance.
The eyeliner of examples 1-13 was applied to the skin of the back of the human hand with a film 3mm wide and 100mm long, a small amount of the applied film was dipped with finger pad, the number of application was recorded when the film began to fall off, each group of samples was tested 10 times, the maximum and minimum values of each group were discarded, and the remaining average value was taken. The test results are shown in Table 1.
TABLE 1 Water-resistant test Effect table
| Group of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 | Example 13 |
| Number of times of starting to drop | 17 | 17.2 | 16.5 | 16.2 | 16.4 | 15.1 | 17.5 | 15.5 | 15.2 | 13.9 | 13.2 | 12.5 | 16 |
As can be seen from Table 1, examples 1 to 4 show that silica 3022 together with acrylic and styrene/acrylic copolymers has excellent water repellency at 20:10, the amount of silica slightly affects the water repellency, examples 5 to 7 show that ordinary silica alone affects the water repellency, and the water repellency is the best without adding silica at all, and examples 8 to 13 show that styrene/acrylic has superior water repellency to acrylic copolymers.
Comparative test 2: and (5) testing the matte effect.
The samples 1 to 13 were uniformly applied to materials of consistent gloss, and the gloss meter was used to perform the test, the meter was placed on the material to be tested, the test data was immediately displayed, the power key was pressed, the current test data was recorded, and the maximum, minimum, average, and mean square deviation values were automatically calculated. A smaller mean square error value indicates a more uniform gloss of the surface of the measured material. The test results are shown in Table 2.
TABLE 2 matte test effect table
| Group of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 | Example 13 |
| Mean value of | 16 | 13.2 | 13 | 13 | 17.6 | 14.5 | 48.6 | 14.2 | 13.9 | 13.5 | 13.2 | 13 | 14.5 |
| Mean square error value | 0.01 | 0.01 | 0.01 | 0.01 | 0.01 | 0.03 | 0.01 | 0.01 | 0.01 | 0.01 | 0.01 | 0.01 | 0.01 |
The test results show that the gloss is matte below 20GU, semi-matte between 20GU and 40GU, and bright above 40 GU.
As can be seen from Table 2, example 7 shows that the gloss is obtained without adding silica, examples 2, 5 and 6 show that the matte effect of silica 3022 is better than that of hydrated silica or ordinary silica alone, examples 1 to 4 show that the optimum matte effect is obtained when the amount of silica 3022 is 5 points, examples 8 to 13 show that the brightness of styrene/acrylic acid (ester) is slightly higher than that of acrylic acid (ester) copolymer, and that ordinary silica is not uniform in variance.
Comparative test 3: the eye liner liquid has cold resistance and heat resistance.
An electric heating constant temperature incubator and a refrigerator are adopted.
And (3) experimental operation: adjusting an electric heating constant temperature incubator to 48 ℃ in advance, adjusting a refrigerator to-18 ℃, taking 10ml of a sample to be detected into a 15ml inspection bottle, vertically putting the bottle into the constant temperature incubator or the refrigerator, and taking out the bottle for observation within a specified time (judging the stable condition according to the conditions of sedimentation and water outlet). The results are shown in Table 3.
TABLE 3 eye liner liquid cold and heat resistance test result table
| Group of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 | Example 13 |
| Heat resistance (48 ℃ C.) | Stabilization for 30d | Stabilization for 30d | Stabilization for 20d | Stabilization of 10d | Stabilization for 20d | Stabilization of 7d | Stabilization for 30d | Stabilization for 30d | Stabilization for 30d | Stabilization for 30d | Stabilization of 29d | Stabilization of 26d | Stabilization for 30d |
| Cold resistance (-18 ℃ C.) | Stabilization for 30d | Stabilization for 30d | Stabilization of 22d | Stabilization of 13d | Stabilization for 25d | Stabilization of 10d | Stabilization for 30d | Stabilization of 18d | Stabilization of 22d | Stabilization of 26d | Stabilization for 30d | Stabilization for 30d | Stabilization of 12d |
As can be seen from Table 3, examples 1 to 4 show that the heat and cold resistance stability is worse at a powder content of 8% or more, examples 5 and 6 show that the heat and cold resistance stability is worse with ordinary silica or hydrated silica alone, and example 8 to 13 show that the cold resistance stability is affected by an excessive styrene/acrylic acid (ester) ratio.
Comparative test 4: and (4) centrifugal testing.
Samples of samples to be detected in examples 1 to 13 are respectively filled with samples with the same weight in a centrifuge tube, and the samples are taken out for observation of sedimentation after being centrifuged for 30min by a centrifuge at the rotating speed of 2500 rpm. The results are shown in Table 4.
TABLE 4
| Group of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 | Example 11 | Example 12 | Example 13 |
| Whether or not to settle | Is that | Is that | Is that | Is that | Is that | Is that | Whether or not | Is that | Is that | Is that | Is that | Is that | Is that |
| Recovery from jolt | Recovery | Recovery | Recovery | Recovery | Recovery | Does not recover | — | Does not recover | Recovery | Recovery | Recovery | Recovery | Does not recover |
As can be seen from Table 4, example 6 illustrates that the settling cannot be recovered by using ordinary silica alone, and examples 8 and 13 illustrate that too high a styrene/acrylic acid (ester) content also affects the recovery.
The applicant declares that the present invention is described by the above embodiments as the detailed features and the detailed methods of the present invention, but the present invention is not limited to the above detailed features and the detailed methods, that is, it is not meant that the present invention must be implemented by relying on the above detailed features and the detailed methods. It will be apparent to those skilled in the art that any modification of the present invention, equivalent substitutions of selected components of the present invention, additions of auxiliary components, selection of specific modes and the like, are within the scope and disclosure of the present invention.
Claims (10)
1. The matte eyeliner is characterized by comprising the following components in percentage by mass: powder filler: 1-10%, preservative: 0.1-1%, film-forming agent: 5-40% of a humectant: 1-10%, color paste: 10-50%, chelating agent: 0.01-0.2%, and the balance of distilled water.
2. The matte eyeliner of claim 1, wherein: the powder filler is one or more of silica, hydrated silica and magnesium aluminum silicate.
3. The matte eyeliner of claim 1, wherein: the mass percentage of the powder filler is 1-10% of silica.
4. The matte eyeliner of claim 1, wherein: the mass percentage of the powder filler is 2-6% of silica.
5. A matte eyeliner according to claims 1-4, wherein: the powder filler is silica with the particle size of 10nm-12000 nm.
6. The matte eyeliner of claim 1, wherein: the film forming agent is one or a mixture of more than two of polyvinylpyrrolidone, polyvinyl alcohol, acrylate/octylacrylamide copolymer, acrylic acid (ester)/acrylamide copolymer, styrene/acrylic acid (ester) copolymer, methyl methacrylate/acrylonitrile copolymer, adipic acid/diethylene glycol/glycerol cross-linked polymer, polyacrylate, acrylic acid (ester) copolymer and waterborne polyurethane.
7. The matte eyeliner of claim 1, wherein: the film forming agent is a mixture of styrene/acrylic acid (ester) copolymer and acrylic acid (ester) copolymer.
8. The matte eyeliner of claim 1, wherein: the humectant is one or more of glycerol, butanediol, propylene glycol, polyethylene glycol, hexanediol, xylitol, polypropylene glycol, sorbitol, pyrrolidone carboxylic acid, sodium lactate, urea, hydroxyethyl urea, methyl glucose polyether, trehalose, Tremella polysaccharide, sodium hyaluronate, panthenol, ceramide, and natural plant extract.
9. The matte eyeliner of claim 1, wherein: the color paste is one or a mixture of more than two of water-based organic color pastes and water-based inorganic color pastes.
10. The method for preparing matte eyeliner according to claim 1, wherein the method comprises the following steps:
(1) mixing 10-20% of water and a chelating agent according to the mass fraction, stirring to completely dissolve the water and the chelating agent uniformly to obtain a mixture 1, and heating to 85-90 ℃;
(2) mixing 5-20% of water and the pre-dispersed powder according to the mass fraction, stirring to uniformly disperse the water and the pre-dispersed powder to obtain a mixture 2, homogenizing for 3-8min, and heating to 85-90 ℃;
(3) uniformly mixing the preservative, the film-forming agent and the humectant according to the mass fraction to obtain a mixture 3, homogenizing for 6-10min, and heating to 85-90 ℃;
(4) sequentially adding the mixture 1 and the mixture 2 into the mixture 3, stirring to completely and uniformly mix the mixture, and homogenizing for 1-5min to obtain a mixture 4;
(5) stirring the mixture 4 and cooling to 45-50 ℃;
(6) adding the color paste into the mixture 4 slowly under stirring to completely mix uniformly, and homogenizing for 5-10 min;
(7) filtering with 200 mesh filter cloth to obtain matte eyeliner, and packaging.
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| CN114788808A (en) * | 2022-05-12 | 2022-07-26 | 广州多多化妆品有限公司 | Agile rainbow eyeliner and preparation method thereof |
| CN115969734A (en) * | 2022-12-31 | 2023-04-18 | 上海联锴新材料有限公司 | Aqueous eyeliner and preparation method thereof |
| CN116270304A (en) * | 2022-12-31 | 2023-06-23 | 广州联锴粉体科技有限公司 | Eyeliner and preparation method thereof |
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| CN115969734A (en) * | 2022-12-31 | 2023-04-18 | 上海联锴新材料有限公司 | Aqueous eyeliner and preparation method thereof |
| CN116270304A (en) * | 2022-12-31 | 2023-06-23 | 广州联锴粉体科技有限公司 | Eyeliner and preparation method thereof |
| CN116270304B (en) * | 2022-12-31 | 2023-12-08 | 广州联锴粉体科技有限公司 | Eyeliner and preparation method thereof |
| CN115969734B (en) * | 2022-12-31 | 2024-02-13 | 上海联锴新材料有限公司 | Aqueous eyeliner and preparation method thereof |
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