CN113143802B - 一种鲑鱼蛋白多糖保湿护肤乳液制备方法 - Google Patents
一种鲑鱼蛋白多糖保湿护肤乳液制备方法 Download PDFInfo
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Abstract
本发明涉及一种鲑鱼蛋白多糖保湿护肤乳液制备方法，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖10‑15％、乳香精油8‑12％、橄榄油2‑4％、牡蛎甾醇3‑5％、单硬脂酸甘油酯3‑6％、十八醇2‑4％、麦醇溶蛋白2‑6％、水解棉籽蛋白1‑5％、丙三醇1‑4％、聚赖氨酸0.1‑0.5％和去离子水60‑68％，所述制备方法包括以下步骤：(1)水相的制备：按重量百分比，将丙三醇1‑4％、麦醇溶蛋白2‑6％和水解棉籽蛋白1‑5％依次加入去离子水中，搅拌均匀并加热至75‑85℃；(2)油相的制备：按重量百分比，将乳香精油8‑12％、橄榄油2‑4％、牡蛎甾醇3‑5％、单硬脂酸甘油酯3‑6％和十八醇2‑4％混合加热熔融。本发明具有保湿、紧致、延缓衰老等作用，添加的天然提取物可以代替传统的化妆品生产中化学成分，产品天然、安全。
Description
技术领域
本发明涉及护肤品技术领域，具体是指一种鲑鱼蛋白多糖保湿护肤乳液制备方法。
背景技术
鲑鱼，又称三文鱼，属硬骨鱼纲、鲑形目、鲑属，鲑鱼肉有补虚劳、健脾胃、暖胃和中的功能。蛋白多糖是蛋白和糖的复合体，由糖链和肽链共价结合形成的生物大分子，多数蛋白多糖分子由1个核心蛋白与1条或多条糖胺聚糖(GAG)链经共价连接组成，分子量从1万至20几万，其中糖链是由二糖重复单位组成的线性杂多糖。由于蛋白多糖的巨大分子量及其高度聚阴离子的特点，能够结合大量的水。胶原纤维、弹性纤维形成的网架结构就沉浸在这一水合基质中，二者共同维持皮肤充盈、紧致、水润的外观质感。皮肤中蛋白多糖组分随龄变化趋势相当明显，首先是蛋白多糖总量下降，其次蛋白多糖集聚体结构断裂。主要原因是由于蛋白多糖的更新比胶原迅速，随着岁月的流失和环境的影响，细胞合成蛋白多糖的能力下降，导致其机械强度变弱，水合能力下降，皮肤看上去不够水润，而且肤色暗哑。
“绿色”是21世纪化妆品的主题，天然活性化妆品顺应回归大自然的发展潮流和人们的消费心理。目前多糖等生物活性成分在化妆品中得到广泛的应用，具有较大的前景和市场，因此，研发一种以天然原料为主要成分的保湿润肤乳很有必要。
发明内容
本发明的目的是提供一种鲑鱼蛋白多糖保湿护肤乳液制备方法，该产品具有保湿、紧致、延缓衰老等作用，添加的天然提取物可以代替传统的化妆品生产中化学成分，产品天然、安全。
为解决上述技术问题，本发明提供的技术方案为：
一种鲑鱼蛋白多糖保湿护肤乳液制备方法，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖10-15％、乳香精油8-12％、橄榄油2-4％、牡蛎甾醇3-5％、单硬脂酸甘油酯3-6％、十八醇2-4％、麦醇溶蛋白2-6％、水解棉籽蛋白1-5％、丙三醇1-4％、聚赖氨酸0.1-0.5％和去离子水60-68％，所述制备方法包括以下步骤：
(1)水相的制备：按重量百分比，将丙三醇1-4％、麦醇溶蛋白2-6％和水解棉籽蛋白1-5％依次加入去离子水60-68％中，搅拌均匀并加热至75-85℃，静置保温10-40min；
(2)油相的制备：按重量百分比，将乳香精油8-12％、橄榄油2-4％、牡蛎甾醇3-5％、单硬脂酸甘油酯3-6％和十八醇2-4％混合加热熔融，温度升高至75-85℃，静置保温10-40min；
(3)乳化：将步骤(2)得到的产物迅速加入到步骤(1)的产物中，以8000-10000r/min的转速均质5-10min，均质后75-85℃静置保温20-40min；
(4)冷却：温度降至40-50℃时，加入鲑鱼蛋白多糖10-15％和聚赖氨酸0.1-0.5％，搅拌混合均匀，继续降温至30-35℃；
(5)陈化、灌装：将制得的膏体陈化48-72h，经检验合格后进行灌装。
进一步的，所述鲑鱼蛋白多糖的提取制备方法为：将鲑鱼软骨水煮洗净后放入鼓风干燥机中烘干，粉碎，加入5％NaOH溶液，45℃超声提取5h，提取液离心过滤，保留上清液备用，上清液pH调至7.0，然后加入95％乙醇沉淀10h，去除上清液，减压抽滤后保留沉淀，沉淀置于65℃下干燥至恒重，制得鲑鱼蛋白多糖。
进一步的，所述麦醇溶蛋白的提取制备方法为：中筋小麦粉与65％乙醇溶液按固液比1:10的比例溶解混合搅拌，搅拌均匀的溶液4000r/min离心20min，取上清液备用，上清液加水稀释并调解液pH至6.3，静置1h，溶液4000r/min离心20min，取沉淀，沉淀置于65℃下干燥至恒重，制得麦醇溶蛋白。
进一步的，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖12％、乳香精油10％、橄榄油3％、牡蛎甾醇4％、单硬脂酸甘油酯5％、十八醇3％、麦醇溶蛋白4％、水解棉籽蛋白3％、丙三醇3％、聚赖氨酸0.4％，去离子水52.6％。
采用以上制备方法后，本发明具有如下优点：
本发明中添加的鲑鱼蛋白多糖具有非常强的结合水的能力，使护肤乳液具有保湿、紧致和延缓皮肤衰老等功效；乳香精油具有抗老化、提升皮肤紧致、改善皮肤敏感、干燥和发炎的效果，散发着温馨清纯的木质香气，又透出淡淡的果香，甚至有一点柠檬的味道，可令人感受从未有过的放松和舒缓；麦醇溶蛋白是一种植物蛋白，来源于小麦、大麦或其他麦科植物的种子，含有大量的谷氨酸，麦醇溶蛋白具有表面活性、可稳定乳状液、增强起泡性和泡沫稳定性，易为皮肤和毛发表面吸附，在护肤品中使用，都能降低皮肤的粗糙度，具有保湿功能；水解棉籽蛋白提取自棉仁，成分以寡肽为主，有一定的乳化能力，且具有抗氧作用；牡蛎甾醇是从牡蛎脂质中分离制得，具有表面活性，有助乳化、稳定乳状液的作用，还在皮肤细胞赋活、抗皱等方面器作用；聚赖氨酸是一种天然来源的氨基酸聚合物，是一种广谱抑菌剂，具有安全、无毒、生物可降解等；本发明中添加的天然提取成分，可以代替传化妆品生产中添加的表面活性剂、防腐剂等化学成分，使用更加安全健康，这些成分还具有多种护肤功效，增加了润肤乳的其他功能。
具体实施方式
下面结合实施例对本发明做进一步的详细说明。
实施例一
一种鲑鱼蛋白多糖保湿护肤乳液制备方法，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖10％、乳香精油8％、橄榄油4％、牡蛎甾醇5％、单硬脂酸甘油酯3％、十八醇4％、麦醇溶蛋白2％、水解棉籽蛋白5％、丙三醇2％、聚赖氨酸0.2％，去离子水56.8％，所述制备方法包括以下步骤：
(1)水相的制备：按重量百分比，将丙三醇2％、麦醇溶蛋白2％和水解棉籽蛋白5％依次加入去离子水56.8％中，搅拌均匀并加热至75℃，静置保温40min；
(2)油相的制备：按重量百分比，将乳香精油8％、橄榄油4％、牡蛎甾醇5％、单硬脂酸甘油酯3％和十八醇4％混合加热熔融，温度升高至75℃，静置保温40min；
(3)乳化：将步骤(2)得到的产物迅速加入到步骤(1)的产物中，以8000r/min的转速均质10min，均质后75℃静置保温40min；
(4)冷却：温度降至40℃时，加入鲑鱼蛋白多糖10％和聚赖氨酸0.2％，搅拌混合均匀，继续降温至30℃；
(5)陈化、灌装：将制得的膏体陈化48h，经检验合格后进行灌装。
所述鲑鱼蛋白多糖的提取制备方法为：将鲑鱼软骨水煮洗净后放入鼓风干燥机中烘干，粉碎，加入5％NaOH溶液，45℃超声提取5h，提取液离心过滤，保留上清液备用，上清液pH调至7.0，然后加入95％乙醇沉淀10h，去除上清液，减压抽滤后保留沉淀，沉淀置于65℃下干燥至恒重，制得鲑鱼蛋白多糖。
所述麦醇溶蛋白的提取制备方法为：中筋小麦粉与65％乙醇溶液按固液比1:10的比例溶解混合搅拌，搅拌均匀的溶液4000r/min离心20min，取上清液备用，上清液加水稀释并调解液pH至6.3，静置1h，溶液4000r/min离心20min，取沉淀，沉淀置于65℃下干燥至恒重，制得麦醇溶蛋白。
实施例二
一种鲑鱼蛋白多糖保湿护肤乳液制备方法，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖15％、乳香精油10％、橄榄油3％、牡蛎甾醇3％、单硬脂酸甘油酯4％、十八醇3％、麦醇溶蛋白6％、水解棉籽蛋白5％、丙三醇3％、聚赖氨酸0.5％，去离子水42.5％，所述制备方法包括以下步骤：
(1)水相的制备：按重量百分比，将丙三醇3％、麦醇溶蛋白6％和水解棉籽蛋白5％依次加入去离子水42.5％中，搅拌均匀并加热至85℃，静置保温10min；
(2)油相的制备：按重量百分比，将乳香精油10％、橄榄油3％、牡蛎甾醇3％、单硬脂酸甘油酯4％和十八醇3％混合加热熔融，温度升高至85℃，静置保温10min；
(3)乳化：将步骤(2)得到的产物迅速加入到步骤(1)的产物中，10000r/min的转速均质5min，均质后85℃静置保温20min；
(4)冷却：温度降至50℃时，加入鲑鱼蛋白多糖15％和聚赖氨酸0.5％，搅拌混合均匀，继续降温至35℃；
(5)陈化、灌装：将制得的膏体陈化72h，经检验合格后进行灌装。
所述鲑鱼蛋白多糖的提取制备方法为：将鲑鱼软骨水煮洗净后放入鼓风干燥机中烘干，粉碎，加入5％NaOH溶液，45℃超声提取5h，提取液离心过滤，保留上清液备用，上清液pH调至7.0，然后加入95％乙醇沉淀10h，去除上清液，减压抽滤后保留沉淀，沉淀置于65℃下干燥至恒重，制得鲑鱼蛋白多糖。
所述麦醇溶蛋白的提取制备方法为：中筋小麦粉与65％乙醇溶液按固液比1:10的比例溶解混合搅拌，搅拌均匀的溶液4000r/min离心20min，取上清液备用，上清液加水稀释并调解液pH至6.3，静置1h，溶液4000r/min离心20min，取沉淀，沉淀置于65℃下干燥至恒重，制得麦醇溶蛋白。
实施例三
一种鲑鱼蛋白多糖保湿护肤乳液制备方法，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖13％、乳香精油10％、橄榄油3％、牡蛎甾醇4％、单硬脂酸甘油酯5％、十八醇3％、麦醇溶蛋白4％、水解棉籽蛋白3％、丙三醇3％、聚赖氨酸0.4％，去离子水51.6％，所述制备方法包括以下步骤：
(1)水相的制备：按重量百分比，将丙三醇3％、麦醇溶蛋白4％和水解棉籽蛋白3％依次加入去离子水51.6％中，搅拌均匀并加热至80℃，静置保温20min；
(2)油相的制备：按重量百分比，将乳香精油10％、橄榄油3％、牡蛎甾醇4％、单硬脂酸甘油酯5％和十八醇3％混合加热熔融，温度升高至80℃，静置保温20min；
(3)乳化：将步骤(2)得到的产物迅速加入到步骤(1)的产物中，以10000r/min的转速均质5min，均质后80℃静置保温30min；
(4)冷却：温度降至45℃时，加入鲑鱼蛋白多糖13％和聚赖氨酸0.4％，搅拌混合均匀，继续降温至335℃；
(5)陈化、灌装：将制得的膏体陈化60h，经检验合格后进行灌装。
所述鲑鱼蛋白多糖的提取制备方法为：将鲑鱼软骨水煮洗净后放入鼓风干燥机中烘干，粉碎，加入5％NaOH溶液，45℃超声提取5h，提取液离心过滤，保留上清液备用，上清液pH调至7.0，然后加入95％乙醇沉淀10h，去除上清液，减压抽滤后保留沉淀，沉淀置于65℃下干燥至恒重，制得鲑鱼蛋白多糖。
所述麦醇溶蛋白的提取制备方法为：中筋小麦粉与65％乙醇溶液按固液比1:10的比例溶解混合搅拌，搅拌均匀的溶液4000r/min离心20min，取上清液备用，上清液加水稀释并调解液pH至6.3，静置1h，溶液4000r/min离心20min，取沉淀，沉淀置于65℃下干燥至恒重，制得麦醇溶蛋白。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。
Claims (3)
1.一种鲑鱼蛋白多糖保湿护肤乳液的制备方法，其特征在于，按重量百分比，由以下原材料组成：鲑鱼蛋白多糖10-15％、乳香精油8-12％、橄榄油2-4％、牡蛎甾醇3-5％、单硬脂酸甘油酯3-6％、十八醇2-4％、麦醇溶蛋白2-6％、水解棉籽蛋白1-5％、丙三醇1-4％、聚赖氨酸0.1-0.5％和去离子水60-68％，所述制备方法包括以下步骤：
(1)水相的制备：按重量百分比，将丙三醇1-4％、麦醇溶蛋白2-6％和水解棉籽蛋白1-5％依次加入去离子水60-68％中，搅拌均匀并加热至75-85℃，静置保温10-40min；
(2)油相的制备：按重量百分比，将乳香精油8-12％、橄榄油2-4％、牡蛎甾醇3-5％、单硬脂酸甘油酯3-6％和十八醇2-4％混合加热熔融，温度升高至75-85℃，静置保温10-40min；
(3)乳化：将步骤(2)得到的产物迅速加入到步骤(1)的产物中，以8000-10000r/min的转速均质5-10min，均质后75-85℃静置保温20-40min；
(4)冷却：温度降至40-50℃时，加入鲑鱼蛋白多糖10-15％和聚赖氨酸0.1-0.5％，搅拌混合均匀，继续降温至30-35℃；
(5)陈化、灌装：将制得的膏体陈化48-72h，经检验合格后进行灌装。
2.根据权利要求1所述的一种鲑鱼蛋白多糖保湿护肤乳液的制备方法，其特征在于，所述鲑鱼蛋白多糖的提取制备方法为：将鲑鱼软骨水煮洗净后放入鼓风干燥机中烘干，粉碎，加入5％NaOH溶液，45℃超声提取5h，提取液离心过滤，保留上清液备用，上清液pH调至7.0，然后加入95％乙醇沉淀10h，去除上清液，减压抽滤后保留沉淀，沉淀置于65℃下干燥至恒重，制得鲑鱼蛋白多糖。
3.根据权利要求1所述的一种鲑鱼蛋白多糖保湿护肤乳液的制备方法，其特征在于，所述麦醇溶蛋白的提取制备方法为：中筋小麦粉与65％乙醇溶液按固液比1:10的比例溶解混合搅拌，搅拌均匀的溶液4000r/min离心20min，取上清液备用，上清液加水稀释并调解液pH至6.3，静置1h，溶液4000r/min离心20min，取沉淀，沉淀置于65℃下干燥至恒重，制得麦醇溶蛋白。
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