CN113088897A - Preparation method of low-temperature low-pressure vapor deposition coating textile - Google Patents

Preparation method of low-temperature low-pressure vapor deposition coating textile Download PDF

Info

Publication number
CN113088897A
CN113088897A CN202110365631.3A CN202110365631A CN113088897A CN 113088897 A CN113088897 A CN 113088897A CN 202110365631 A CN202110365631 A CN 202110365631A CN 113088897 A CN113088897 A CN 113088897A
Authority
CN
China
Prior art keywords
textile
coating
temperature
vapor deposition
equipment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN202110365631.3A
Other languages
Chinese (zh)
Inventor
郑奇标
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Suzhou Fanershi New Material Technology Co ltd
Original Assignee
Suzhou Fanershi New Material Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Suzhou Fanershi New Material Technology Co ltd filed Critical Suzhou Fanershi New Material Technology Co ltd
Priority to CN202110365631.3A priority Critical patent/CN113088897A/en
Priority to PCT/CN2021/104214 priority patent/WO2022213497A1/en
Publication of CN113088897A publication Critical patent/CN113088897A/en
Withdrawn legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/24Vacuum evaporation
    • C23C14/32Vacuum evaporation by explosion; by evaporation and subsequent ionisation of the vapours, e.g. ion-plating
    • C23C14/325Electric arc evaporation
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/54Controlling or regulating the coating process
    • C23C14/542Controlling the film thickness or evaporation rate

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Vapour Deposition (AREA)
  • Physical Vapour Deposition (AREA)

Abstract

The invention discloses a preparation method of low-temperature low-pressure vapor deposition coated textiles, which comprises the following steps of S1, preparing a textile vapor deposition coating device Q1 with a high-voltage current arc target evaporation ionization source and a textile coating reaction device Q2, checking the tightness of the devices, S2, and then connecting a temperature adjusting mechanism Q3 and an air pressure adjusting mechanism Q4 with the textile coating reaction device Q2 through adjusting pipelines, S3: the raw materials required by the coating are put into a textile vapor deposition coating device Q1, and the high-voltage current arc target evaporation ionization source decomposes the coating raw materials into gaseous plasmas. In the invention, the textile vapor deposition coating equipment converts the coating raw material into an ionic state and enters the textile coating reaction equipment to coat the textile under the action of the temperature regulating mechanism and the air pressure regulating mechanism, so that the textile is firmer and more durable, and the service life of the textile is prolonged.

Description

Preparation method of low-temperature low-pressure vapor deposition coating textile
Technical Field
The invention relates to the technical field of textiles, in particular to a preparation method of a low-temperature low-pressure vapor deposition coating textile.
Background
The textile is a product formed by processing and weaving textile fibers, occupies a great position in daily life, is widely applied to various aspects such as production life, chemical industry and the like, and the continuous innovation of the textile continuously improves the life quality of people. However, the textile is worn due to various reasons in the daily use process, the service life is generally short, and the existing textiles have poor tensile property and electrical conductivity, are not high-temperature resistant and are easy to deform after being soaked in hot water and the like.
In order to solve the problem of the existing textile, the textile is more durable in a coating mode, however, the existing textile coating mode is single, most of the textile can feel coated in a chemical mode, the coating cost is high, the production cost of the textile is increased, and the economical and practical performance is poor.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of a low-temperature low-pressure vapor deposition coating textile.
The invention provides a preparation method of a low-temperature low-pressure vapor deposition coating textile, which comprises the following steps:
s1: early preparation: preparing a textile vapor deposition coating device Q1 and a textile coating reaction device Q2 which are provided with high-voltage current arc target evaporation ionization sources, checking the sealing performance of the textile vapor deposition coating device Q1 and the textile coating reaction device Q2, arranging a textile placing mechanism which can be adjusted along with the size of a textile inside the textile coating reaction device Q2, connecting the textile vapor deposition coating device Q1 and the textile coating reaction device Q2 through a connecting pipeline, and arranging a control valve for opening or closing the connecting pipeline on the connecting pipeline;
s2: the auxiliary mechanism is connected: then, a temperature adjusting mechanism Q3 and an air pressure adjusting mechanism Q4 are connected with a textile coating reaction device Q2 through an adjusting pipeline, a control mechanism is arranged to control the opening and closing of the adjusting pipeline, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 are both positioned at the bottom of the textile coating reaction device Q2, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 enable the air inside the textile coating reaction device Q2 to circulate from top to bottom, the tightness of the connected textile coating reaction device Q2 is checked again, and the situation that the air leakage of the device influences the preparation of textiles in the preparation process is avoided;
s3: decomposition of plating raw materials: putting raw materials required by a coating into textile vapor deposition coating equipment Q1, decomposing the coating raw materials into gaseous plasma through a high-voltage current arc target evaporation ionization source, then putting the textile into textile coating reaction equipment Q2, and after the textile raw materials are placed, opening a connecting pipeline between the textile vapor deposition coating equipment Q1 and the textile coating reaction equipment Q2 so that free ions in the textile vapor deposition coating equipment Q1 enter the textile coating reaction equipment Q2;
s4: coating the textile: after the free ions enter the textile coating reaction equipment Q2, respectively starting the temperature regulating mechanism Q3 and the air pressure regulating mechanism Q4, regulating the temperature and the air pressure inside the textile coating reaction equipment Q2, and accumulating the free ions on the surface layer of the textile under the conditions of low temperature and low pressure so as to form a deposited film layer;
s5: data collection: the forming speed of the coating also changes correspondingly with the continuous change of the temperature and the air pressure, at the moment, the data acquisition equipment collects and arranges the numerical values of the temperature T and the air pressure P in the textile coating reaction equipment Q2 to obtain related data, the influence of the temperature T and the air pressure P on the textile coating effect is researched along with the change of the data, and the condition which is most beneficial to the textile coating forming is researched, so that the optimal coating scheme is obtained, the production resources are saved, and the production cost is reduced.
Preferably, the data acquisition device comprises a temperature sensor, a pressure sensor, a computer and a data collector.
According to the invention, the textile vapor deposition coating equipment converts the coating raw material into an ionic state and enters the textile coating reaction equipment, and the textile is coated on the progress under the action of the temperature adjusting mechanism and the air pressure adjusting mechanism.
Drawings
FIG. 1 is a schematic view of the preparation process of a low-temperature low-pressure vapor deposition coated textile according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Referring to fig. 1, a method for preparing a low-temperature low-pressure vapor deposition coated textile comprises the following steps:
s1: early preparation: preparing a textile vapor deposition coating device Q1 and a textile coating reaction device Q2 which are provided with high-voltage current arc target evaporation ionization sources, checking the sealing performance of the textile vapor deposition coating device Q1 and the textile coating reaction device Q2, arranging a textile placing mechanism which can be adjusted along with the size of a textile inside the textile coating reaction device Q2, connecting the textile vapor deposition coating device Q1 and the textile coating reaction device Q2 through a connecting pipeline, and arranging a control valve for opening or closing the connecting pipeline on the connecting pipeline;
s2: the auxiliary mechanism is connected: then, a temperature adjusting mechanism Q3 and an air pressure adjusting mechanism Q4 are connected with a textile coating reaction device Q2 through an adjusting pipeline, a control mechanism is arranged to control the opening and closing of the adjusting pipeline, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 are both positioned at the bottom of the textile coating reaction device Q2, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 enable the air inside the textile coating reaction device Q2 to circulate from top to bottom, the tightness of the connected textile coating reaction device Q2 is checked again, and the situation that the air leakage of the device influences the preparation of textiles in the preparation process is avoided;
s3: decomposition of plating raw materials: putting raw materials required by a coating into textile vapor deposition coating equipment Q1, decomposing the coating raw materials into gaseous plasma through a high-voltage current arc target evaporation ionization source, then putting the textile into textile coating reaction equipment Q2, and after the textile raw materials are placed, opening a connecting pipeline between the textile vapor deposition coating equipment Q1 and the textile coating reaction equipment Q2 so that free ions in the textile vapor deposition coating equipment Q1 enter the textile coating reaction equipment Q2;
s4: coating the textile: after the free ions enter the textile coating reaction equipment Q2, respectively starting the temperature regulating mechanism Q3 and the air pressure regulating mechanism Q4, regulating the temperature and the air pressure inside the textile coating reaction equipment Q2, and accumulating the free ions on the surface layer of the textile under the conditions of low temperature and low pressure so as to form a deposited film layer;
s5: data collection: along with the continuous change of the temperature and the air pressure, the forming speed of the coating also changes correspondingly, at the moment, the data acquisition equipment collects and arranges the numerical values of the temperature T and the air pressure P in the textile coating reaction equipment Q2 to obtain related data, the influence of the temperature T and the air pressure P on the coating effect of the textile is researched along with the change of the data, and the condition which is most beneficial to the forming of the coating of the textile is researched, so that the optimal coating scheme is obtained, the production resources are saved, and the production cost is reduced.
According to the invention, the textile vapor deposition coating equipment Q1 converts the coating raw material into an ionic state and enters the textile coating reaction equipment Q2, and the textile is coated under the action of the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (2)

1. The preparation method of the low-temperature low-pressure vapor deposition coating textile is characterized by comprising the following steps of:
s1: early preparation: preparing a textile vapor deposition coating device Q1 and a textile coating reaction device Q2 which are provided with high-voltage current arc target evaporation ionization sources, checking the sealing performance of the textile vapor deposition coating device Q1 and the textile coating reaction device Q2, arranging a textile placing mechanism which can be adjusted along with the size of a textile inside the textile coating reaction device Q2, connecting the textile vapor deposition coating device Q1 and the textile coating reaction device Q2 through a connecting pipeline, and arranging a control valve for opening or closing the connecting pipeline on the connecting pipeline;
s2: the auxiliary mechanism is connected: then, a temperature adjusting mechanism Q3 and an air pressure adjusting mechanism Q4 are connected with a textile coating reaction device Q2 through an adjusting pipeline, a control mechanism is arranged to control the opening and closing of the adjusting pipeline, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 are both positioned at the bottom of the textile coating reaction device Q2, the temperature adjusting mechanism Q3 and the air pressure adjusting mechanism Q4 enable the air inside the textile coating reaction device Q2 to circulate from top to bottom, the tightness of the connected textile coating reaction device Q2 is checked again, and the situation that the air leakage of the device influences the preparation of textiles in the preparation process is avoided;
s3: decomposition of plating raw materials: putting raw materials required by a coating into textile vapor deposition coating equipment Q1, decomposing the coating raw materials into gaseous plasma through a high-voltage current arc target evaporation ionization source, then putting the textile into textile coating reaction equipment Q2, and after the textile raw materials are placed, opening a connecting pipeline between the textile vapor deposition coating equipment Q1 and the textile coating reaction equipment Q2 so that free ions in the textile vapor deposition coating equipment Q1 enter the textile coating reaction equipment Q2;
s4: coating the textile: after the free ions enter the textile coating reaction equipment Q2, respectively starting the temperature regulating mechanism Q3 and the air pressure regulating mechanism Q4, regulating the temperature and the air pressure inside the textile coating reaction equipment Q2, and accumulating the free ions on the surface layer of the textile under the conditions of low temperature and low pressure so as to form a deposited film layer;
s5: data collection: the forming speed of the coating also changes correspondingly with the continuous change of the temperature and the air pressure, at the moment, the data acquisition equipment collects and arranges the numerical values of the temperature T and the air pressure P in the textile coating reaction equipment Q2 to obtain related data, the influence of the temperature T and the air pressure P on the textile coating effect is researched along with the change of the data, and the condition which is most beneficial to the textile coating forming is researched, so that the optimal coating scheme is obtained, the production resources are saved, and the production cost is reduced.
2. The method for preparing the low-temperature low-pressure vapor deposition coated textile according to claim 1, wherein the data acquisition equipment comprises a temperature sensor, a pressure sensor, a computer and a data acquisition unit.
CN202110365631.3A 2021-04-06 2021-04-06 Preparation method of low-temperature low-pressure vapor deposition coating textile Withdrawn CN113088897A (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
CN202110365631.3A CN113088897A (en) 2021-04-06 2021-04-06 Preparation method of low-temperature low-pressure vapor deposition coating textile
PCT/CN2021/104214 WO2022213497A1 (en) 2021-04-06 2021-07-02 Preparation method for low temperature low pressure vapor deposition-coated textile

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202110365631.3A CN113088897A (en) 2021-04-06 2021-04-06 Preparation method of low-temperature low-pressure vapor deposition coating textile

Publications (1)

Publication Number Publication Date
CN113088897A true CN113088897A (en) 2021-07-09

Family

ID=76673762

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202110365631.3A Withdrawn CN113088897A (en) 2021-04-06 2021-04-06 Preparation method of low-temperature low-pressure vapor deposition coating textile

Country Status (2)

Country Link
CN (1) CN113088897A (en)
WO (1) WO2022213497A1 (en)

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20050205206A1 (en) * 2004-03-19 2005-09-22 Robert Lembersky Apparatus for materials processing by stimulated light emission and method of its utilization
CN101037765A (en) * 2006-12-30 2007-09-19 苏州大学 Method for metallization treatment of textile surface
CN104831238B (en) * 2015-03-31 2017-07-18 嘉兴中科奥度新材料有限公司 Composite ion plating nano-metal technique and its product
CN108823540A (en) * 2018-07-18 2018-11-16 无锡爱尔华精机有限公司 A kind of Ion Aided Film Coating evaporation equipment
CN111748777B (en) * 2020-06-08 2022-07-15 季华实验室 Variable-angle variable-diameter magnetic filtration cathode arc film deposition equipment and method
CN111741582A (en) * 2020-07-02 2020-10-02 安徽纯源镀膜科技有限公司 Transmission channel device for plasma transmission and coating equipment

Also Published As

Publication number Publication date
WO2022213497A1 (en) 2022-10-13

Similar Documents

Publication Publication Date Title
CN105671654B (en) A kind of ion induction type artificial skin array structure and preparation method thereof
EP2980281B1 (en) Apparatus and method for forming metal coating film
Zhao et al. Highly stretchable, breathable and negative resistance variation textile strain sensor with excellent mechanical stability for wearable electronics
CN102784517B (en) Ultra-fine glass fiber coated substrate and preparation method thereof
CN103696230A (en) Continuous treatment method for conductive yarns and device for method
CN112680967B (en) Piezoresistive sensing fabric with unidirectional moisture-conducting function and preparation method thereof
CN113088897A (en) Preparation method of low-temperature low-pressure vapor deposition coating textile
Huang et al. Multifunctional MXene-decorated cotton fabric with different weaves, outstanding photothermal effect, and rapid response
Yan et al. Research progress of fabrics with different geometric structures for triboelectric nanogenerators in flexible and wearable electronics
CN107402068A (en) A kind of ultraviolet light transducer based on metal nanometer line/nano zinc oxide material
CN111763922A (en) Vacuum coating machine capable of realizing continuous coating function
CN107575748A (en) Steam tracing device
CN107475945B (en) Starching and shaping system for carbon fiber and sizing technique
CN201485666U (en) Western-style suit wetting device
CN105887471A (en) Organic fiber surface chromium-plating method
Manjakkal et al. Cloth based biocompatiable temperature sensor
CN205501409U (en) Intelligent vacuum coating machine
CN213507527U (en) Humidification device is used in weaving
CN107938220A (en) A kind of cut pile fabric final finishing device
CN210159580U (en) Processing sulfur dioxide buffer kettle for heartleaf houttuynia herb
CN211394617U (en) Graphene film roll-to-roll production device
CN208336251U (en) Flexible solar battery copper indium gallium selenide manufacturing equipment
CN111703163A (en) PTFE (polytetrafluoroethylene) film-coated garment fabric with nano silver ion layer and manufacturing process
CN207072970U (en) Reinforced graphite alkene coating thin film equipment based on PECVD
CN208212205U (en) A kind of energy-efficient medicine processing device

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication

Application publication date: 20210709

WW01 Invention patent application withdrawn after publication