CN113088287A - Preparation method of water-soluble nano luminescent material and water-soluble nano luminescent material - Google Patents
Preparation method of water-soluble nano luminescent material and water-soluble nano luminescent material Download PDFInfo
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- CN113088287A CN113088287A CN202110256570.7A CN202110256570A CN113088287A CN 113088287 A CN113088287 A CN 113088287A CN 202110256570 A CN202110256570 A CN 202110256570A CN 113088287 A CN113088287 A CN 113088287A
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- water
- luminescent material
- soluble nano
- precipitate
- nano luminescent
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- 239000000463 material Substances 0.000 title claims abstract description 49
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 40
- XUJNEKJLAYXESH-UHFFFAOYSA-N cysteine Natural products SCC(N)C(O)=O XUJNEKJLAYXESH-UHFFFAOYSA-N 0.000 claims abstract description 16
- 235000018417 cysteine Nutrition 0.000 claims abstract description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 50
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 36
- 239000002244 precipitate Substances 0.000 claims description 36
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 claims description 34
- 239000008367 deionised water Substances 0.000 claims description 32
- 229910021641 deionized water Inorganic materials 0.000 claims description 32
- 238000001035 drying Methods 0.000 claims description 23
- 239000000203 mixture Substances 0.000 claims description 22
- 238000000926 separation method Methods 0.000 claims description 20
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 claims description 19
- 229960000304 folic acid Drugs 0.000 claims description 19
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 18
- 235000019152 folic acid Nutrition 0.000 claims description 15
- 239000011724 folic acid Substances 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 14
- 238000005406 washing Methods 0.000 claims description 14
- 238000006243 chemical reaction Methods 0.000 claims description 13
- 239000000126 substance Substances 0.000 claims description 12
- 239000012467 final product Substances 0.000 claims description 9
- 239000000047 product Substances 0.000 claims description 9
- 238000005303 weighing Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 238000004140 cleaning Methods 0.000 claims description 7
- 238000001291 vacuum drying Methods 0.000 claims description 7
- XUJNEKJLAYXESH-REOHCLBHSA-N L-Cysteine Chemical compound SC[C@H](N)C(O)=O XUJNEKJLAYXESH-REOHCLBHSA-N 0.000 claims description 3
- 238000012986 modification Methods 0.000 abstract description 7
- 230000004048 modification Effects 0.000 abstract description 6
- 239000002086 nanomaterial Substances 0.000 abstract description 5
- 239000002105 nanoparticle Substances 0.000 description 13
- 239000002994 raw material Substances 0.000 description 7
- 230000035484 reaction time Effects 0.000 description 6
- -1 rare earth ions Chemical class 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 229910052693 Europium Inorganic materials 0.000 description 4
- 239000000090 biomarker Substances 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- 150000001450 anions Chemical class 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- OGPBJKLSAFTDLK-UHFFFAOYSA-N europium atom Chemical compound [Eu] OGPBJKLSAFTDLK-UHFFFAOYSA-N 0.000 description 2
- 238000004020 luminiscence type Methods 0.000 description 2
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000001945 cysteines Chemical class 0.000 description 1
- 238000002059 diagnostic imaging Methods 0.000 description 1
- 239000008204 material by function Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000007146 photocatalysis Methods 0.000 description 1
- 230000001699 photocatalysis Effects 0.000 description 1
- 238000006862 quantum yield reaction Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
- C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
- C09K11/7728—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing europium
- C09K11/7729—Chalcogenides
- C09K11/773—Chalcogenides with zinc or cadmium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y20/00—Nanooptics, e.g. quantum optics or photonic crystals
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
- C09K11/02—Use of particular materials as binders, particle coatings or suspension media therefor
- C09K11/025—Use of particular materials as binders, particle coatings or suspension media therefor non-luminescent particle coatings or suspension media
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B20/00—Energy efficient lighting technologies, e.g. halogen lamps or gas discharge lamps
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Organic Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Composite Materials (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biophysics (AREA)
- Optics & Photonics (AREA)
- Luminescent Compositions (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202110256570.7A CN113088287B (en) | 2021-03-09 | 2021-03-09 | Preparation method of water-soluble nano luminescent material and water-soluble nano luminescent material |
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CN202110256570.7A CN113088287B (en) | 2021-03-09 | 2021-03-09 | Preparation method of water-soluble nano luminescent material and water-soluble nano luminescent material |
Publications (2)
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CN113088287A true CN113088287A (en) | 2021-07-09 |
CN113088287B CN113088287B (en) | 2023-05-12 |
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CN202110256570.7A Active CN113088287B (en) | 2021-03-09 | 2021-03-09 | Preparation method of water-soluble nano luminescent material and water-soluble nano luminescent material |
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101024767A (en) * | 2006-02-21 | 2007-08-29 | 上海师范大学 | Near-ultraviolet or ultraviolet excited semiconductor luminous material and its preparing method |
CN107418560A (en) * | 2017-05-16 | 2017-12-01 | 江西科技师范大学 | A kind of preparation method of efficiently sulfur doping nano zinc oxide material |
-
2021
- 2021-03-09 CN CN202110256570.7A patent/CN113088287B/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101024767A (en) * | 2006-02-21 | 2007-08-29 | 上海师范大学 | Near-ultraviolet or ultraviolet excited semiconductor luminous material and its preparing method |
CN107418560A (en) * | 2017-05-16 | 2017-12-01 | 江西科技师范大学 | A kind of preparation method of efficiently sulfur doping nano zinc oxide material |
Non-Patent Citations (4)
Title |
---|
WANG XIAOXUAN ET AL.,: ""Synthesis and Photoluminescence Properties of Water-Soluble ZnS Quantum Dots for Biomarkers"", 《MATERIAL SCIENCE AND ENGINEERING CONFERENCE SERIES》 * |
XIAOXIA LI ET AL.,: ""Synthesis and photoluminescence of Eu3+ and O2- co-doped ZnS nanoparticles with yellow emission synthesized by a solid-state reaction"", 《JOURNAL OF LUMINESCENCE》 * |
XIAOXUAN WANG ET AL.,: ""Effects of L-cysteine on the photoluminescence, electronic and cytotoxicity properties of ZnS: O quantum dots"", 《JOURNAL OF ALLOYS AND COMPOUNDS》 * |
ZHONG CHEN ET AL.,: ""Strong blue luminescence of O2−-doped ZnS nanoparticles synthesized by a low temperature solid state reaction method"", 《MATERIALS SCIENCE IN SEMICONDUCTOR PROCESSING》 * |
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Publication number | Publication date |
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CN113088287B (en) | 2023-05-12 |
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Effective date of registration: 20240206 Address after: 100086 208, 2f, building 1, Mantingfangyuan community, Qingyun Li, Haidian District, Beijing Patentee after: Quanku (Beijing) Technology Co.,Ltd. Country or region after: China Address before: Room 306, building B, Longyong apartment, no.26-1, liuhengli, Fengxiang Road, Qiongshan District, Haikou City, Hainan Province, 571100 Patentee before: Hainan Daowu Biomedical Technology Co.,Ltd. Country or region before: China |
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Application publication date: 20210709 Assignee: Tangshan Gangwen Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003266 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240326 Application publication date: 20210709 Assignee: Tangshan Chenhuan Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003264 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240326 Application publication date: 20210709 Assignee: Tangshan Cenyi Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003261 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240326 Application publication date: 20210709 Assignee: Tangshan Caijia Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003255 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240326 Application publication date: 20210709 Assignee: Tangshan Guitao Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003273 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240327 Application publication date: 20210709 Assignee: Tangshan Guangou Technology Co.,Ltd. Assignor: Quanku (Beijing) Technology Co.,Ltd. Contract record no.: X2024980003268 Denomination of invention: A method for preparing water-soluble nano luminescent materials and water-soluble nano luminescent materials Granted publication date: 20230512 License type: Common License Record date: 20240327 |