CN113082086A - Processing method of traditional Chinese medicine decoction pieces - Google Patents
Processing method of traditional Chinese medicine decoction pieces Download PDFInfo
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- CN113082086A CN113082086A CN202110497506.8A CN202110497506A CN113082086A CN 113082086 A CN113082086 A CN 113082086A CN 202110497506 A CN202110497506 A CN 202110497506A CN 113082086 A CN113082086 A CN 113082086A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/64—Orobanchaceae (Broom-rape family)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/10—Laxatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/14—Prodigestives, e.g. acids, enzymes, appetite stimulants, antidyspeptics, tonics, antiflatulents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/19—Preparation or pretreatment of starting material involving fermentation using yeast, bacteria or both; enzymatic treatment
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Abstract
The invention provides a processing method of traditional Chinese medicine decoction pieces, and relates to the technical field of medicinal material processing. The method aims at processing the medicinal material cistanche, and comprises the following steps: the method comprises the steps of washing and drying; crushing at low temperature; performing biological fermentation on the three-dimensional ground product; and fourthly, tabletting and forming. Compared with the prior art, the method has the advantages that the rare rhizome medicinal material cistanche deserticola with high sugar content and large viscosity is crushed after being dried by low-temperature microwave, so that the crushing and drying efficiency and quality are improved, the original medicinal components are well reserved, and the breeding of microorganisms or the deterioration of medicinal properties caused by long-term airing is avoided; after superfine grinding, the cistanche is subjected to anaerobic fermentation, so that the cistanche contains active ingredients of the traditional Chinese medicine, a large amount of probiotics and metabolites thereof, synergy is realized, the medicine property is improved, and the absorption utilization rate is improved; the prepared traditional Chinese medicine decoction pieces have uniform and stable components.
Description
Technical Field
The invention relates to the technical field of medicinal material processing, in particular to a processing method of Chinese medicinal material decoction pieces.
Background
The traditional Chinese medicine decoction pieces are prepared from traditional Chinese medicines according to the traditional Chinese medicine theory and the traditional Chinese medicine preparation method, and can be directly used as traditional Chinese medicines in traditional Chinese medicine clinical practice. The traditional Chinese medicine decoction pieces are one of three main pillars of the Chinese traditional medicine industry, are necessary traditional weapons for clinical syndrome differentiation and treatment of the traditional Chinese medicine, are also important raw materials of the Chinese patent medicine, and have unique processing theory and method without embodying the profound intelligence of the old traditional Chinese medicine. With the continuous perfection and maturity of the processing theory, it has become an important means for preventing and treating diseases in clinical traditional Chinese medicine at present. The Chinese herbal pieces prepared for decoction are used as a special classification in the medicine, and because of the diversity and complexity of the form, the components and the performance, the probability and the degree of quality variation in the storage process are relatively high. Therefore, the method, the standard and the technical requirement for storing and maintaining the traditional Chinese medicine decoction pieces are relatively high, and the application means of the traditional Chinese medicine decoction pieces are also diversified. According to different varieties and different maintenance purposes and seasonal changes, targeted and reasonable measures are taken in the maintenance process. In order to prevent mildew and rot, methods such as airing, ventilation, drying, moisture absorption, fumigation, salting, refrigeration and the like can be adopted; in order to prevent insect damage, methods such as solarization, heating, refrigeration, medicament fumigation and the like can be adopted; in order to prevent volatilization of the medicine property, methods such as sealing, cooling and the like can be adopted; in order to prevent discoloration and oil bleeding, methods such as shading, cooling and the like are adopted.
The superfine grinding technology is a new technology which is rapidly developed in recent years. The active ingredients in the traditional Chinese medicinal materials are mostly distributed in cells, only partial active ingredients can be released when the conventional decoction pieces are decocted, the utilization rate of the active ingredients is low, the wall breaking and crushing technology is adopted, the cell walls of the traditional Chinese medicinal material decoction pieces are broken through a pure physical mode at ultralow temperature, the traditional Chinese medicinal material decoction pieces are crushed into superfine powder with the particle size of less than 45 micrometers, the wall breaking rate of more than 99% of the medicinal material cells is ensured, compared with the traditional Chinese medicinal decoction pieces, the wall breaking decoction pieces are used as full ingredients, all pharmacodynamic ingredients of the traditional Chinese medicine are reserved, the decoction pieces after cell wall breaking are more beneficial to fast dissolution of the pharmacodynamic ingredients, the pharmacodynamic effects of the traditional Chinese medicine are greatly enhanced, the utilization rate of the active ingredients is more than 90.
The cistanche deserticola of cistanche genus plant is dry fleshy stem with scaly leaves, also called cistanche deserticola and herba hyperici japonici, is an extremely rare Chinese medicinal material, is sweet and warm in nature, is salty and moist in quality, and has the effects of tonifying yang but not dryness, warming and dredging kidney yang and tonifying kidney deficiency; nourishing yin without greasiness, moistening intestine, dredging abdomen and treating constipation; the traditional processing method is to obtain the cistanche deserticola decoction pieces by cleaning, moistening, slicing and drying in the sun. The traditional processing method of the traditional Chinese medicine decoction pieces has a plurality of places needing improvement, such as more residual dust, bacteria, mould and the like after airing, the medicinal components are damaged, and the medicinal value is reduced.
Disclosure of Invention
The invention aims to provide a processing method of traditional Chinese medicine decoction pieces, which solves the defects of more dust, bacteria and mould residues and more damage to effective components in the processing of the traditional Chinese medicine decoction pieces.
In order to achieve the purpose, the technical scheme adopted by the invention is a processing method of Chinese herbal medicine decoction pieces, which is used for processing fresh Chinese herbal medicine cistanche and comprises the following specific steps:
washing drying
Washing the surface silt of the dug fresh cistanche deserticola with clear water, draining, atomizing and spraying alcohol with the mass fraction of 70-95% on the surface, then spraying and freezing for 2-5 min by adopting liquid nitrogen with the temperature of-20 to-40 ℃, and then carrying out microwave vacuum drying;
crushing at low temperature
Carrying out airflow superfine grinding at the low temperature of-5 to-10 ℃ to obtain cistanche powder of 300 to 500 meshes;
performing biological fermentation on the ground
Adding sucrose and amino acid into Cistanchis herba powder to obtain pre-fermented material, inoculating beneficial bacteria liquid, and performing anaerobic fermentation;
four preforming shaping
Pressing the fermented material into cistanche slices, and then performing microwave drying to obtain cistanche decoction pieces.
Further, in some preferred embodiments of the present invention, the alcohol is sprayed in an amount of 0.05% to 0.1% by weight of the raw material of cistanche deserticola.
Further, in some preferred embodiments of the present invention, the drying conditions of the microwave vacuum drying are that the microwave power is 5 to 8kW, the vacuum degree is-0.055 to-0.085 MPa, and the temperature is controlled at 40 to 50 ℃ for drying for 45 to 60 min.
Further, in some preferred embodiments of the present invention, the cistanche powder is mixed with sucrose and amino acid in a weight ratio of 96-98:1-2: 1-2.
Further, in some preferred embodiments of the present invention, the beneficial bacteria include, but are not limited to, one or more of lactobacillus plantarum, lactobacillus delbrueckii, and bifidobacterium.
Further, in some preferred embodiments of the present invention, the inoculation amount of the beneficial bacteria liquid is 10-13% of the weight of the pre-fermentation material.
Further, in some preferred embodiments of the present invention, the temperature of the anaerobic fermentation is controlled to be 30-35 ℃, and the fermentation time is 4-6 d.
Further, in some preferred embodiments of the present invention, the cistanche tubulosa has a thickness of 2 to 4mm and a diameter of 1 to 1.5 cm.
Further, in some preferred embodiments of the present invention, the microwave drying is microwave treatment at 60 to 70 ℃ to a water content of 7 to 13%.
Based on the above explanation, compared with the prior art, the invention has the beneficial effects that: aiming at the rare rhizome medicinal material cistanche deserticola with high sugar content and large viscosity, the grinding and drying efficiency and quality are improved by grinding after low-temperature microwave drying, the original medicinal components are well reserved, and the breeding of microorganisms or the deterioration of medicinal properties caused by long-term airing is avoided; after superfine grinding, the cistanche is subjected to anaerobic fermentation, so that the cistanche contains active ingredients of the traditional Chinese medicine, a large amount of probiotics and metabolites thereof, synergy is realized, the medicine property is improved, and the absorption utilization rate is improved; the prepared traditional Chinese medicine decoction pieces have uniform and stable components.
Detailed Description
In order to make those skilled in the art better understand the technical solution of the present invention, the following detailed description of the present invention is provided with reference to specific embodiments.
Example 1
After fresh cistanche is dug, the sediment on the surface is timely washed by clear water, drained and atomized and sprayed with alcohol with the mass fraction of 70 percent, wherein the spraying amount is 0.1 percent of the weight of the cistanche raw material; then spraying and freezing for 5min by adopting liquid nitrogen at the temperature of 40 ℃ below zero, and then performing microwave vacuum drying under the conditions that the microwave power is 8kW, the vacuum degree is 0.085MPa and the temperature is controlled at 50 ℃ for 60 min; performing gas stream ultramicro pulverization at-10 deg.C to obtain 500 mesh Cistanchis herba powder; taking 96g of cistanche deserticola powder, adding 2g of cane sugar and 2g of amino acid into the cistanche deserticola powder to obtain a pre-fermented material, inoculating lactobacillus plantarum liquid, performing anaerobic fermentation, wherein the inoculation amount is 13% of the weight of the pre-fermented material, the fermentation temperature is controlled at 35 ℃, and the fermentation time is 4 d; pressing the fermented material into cistanche slices with the thickness of 2mm and the diameter of 1cm, and performing microwave treatment at 60 ℃ until the water content is 13% to obtain cistanche decoction pieces.
Example 2
After fresh cistanche is dug, the sediment on the surface is timely washed by clear water, drained and atomized and sprayed with alcohol with the mass fraction of 95 percent, wherein the spraying amount is 0.05 percent of the weight of the cistanche raw material; then adopting liquid nitrogen with the temperature of 20 ℃ below zero to spray and freeze for 2min, and then carrying out microwave vacuum drying on the frozen; performing jet superfine grinding at a low temperature of-5 ℃ to obtain cistanche powder of 300 meshes; taking 98g of cistanche deserticola powder, adding 1g of sucrose and 1g of amino acid into the cistanche deserticola powder to obtain a pre-fermented material, inoculating lactobacillus delbrueckii bacterial liquid, and then performing anaerobic fermentation, wherein the inoculation amount is 10% of the weight of the pre-fermented material, the fermentation temperature is controlled at 30 ℃, and the fermentation time is 6 d; pressing the fermented material into a cistanche slice with the thickness of 4mm and the diameter of 1.5cm, and performing microwave treatment at 70 ℃ until the water content is 7% to obtain the cistanche decoction pieces.
Example 3
After fresh cistanche is dug, the sediment on the surface is timely washed by clear water, the sediment is drained, and the surface is atomized and sprayed with alcohol with the mass fraction of 90 percent, wherein the spraying amount is 0.075 percent of the weight of the cistanche raw material; then spraying and freezing for 3min by adopting liquid nitrogen at the temperature of-35 ℃, and then performing microwave vacuum drying for 50min under the drying conditions that the microwave power is 6kW, the vacuum degree is-0.07 MPa and the temperature is controlled at 45 ℃; performing airflow ultramicro pulverization at a low temperature of-8 ℃ to obtain cistanche powder of 400 meshes; 97g of cistanche powder is taken, 2g of cane sugar and 1g of amino acid are added into the cistanche powder to obtain a pre-fermented material, lactobacillus plantarum liquid, lactobacillus delbrueckii liquid and bifidobacterium liquid are mixed according to the volume ratio of 2:2:1 and then inoculated into the pre-fermented material for anaerobic fermentation, the inoculation amount is 12.5 percent of the weight of the pre-fermented material, the fermentation temperature is controlled at 33 ℃, and the fermentation time is 5 days; pressing the fermented material into a cistanche slice with the thickness of 3mm and the diameter of 1.2cm, and performing microwave treatment at 68 ℃ until the water content is 8% to obtain the cistanche decoction pieces.
Example 4
After fresh cistanche is dug, the sediment on the surface is timely washed by clear water, the sediment is drained, and alcohol with the mass fraction of 75% is atomized and sprayed on the surface, wherein the spraying amount is 0.08% of the weight of the cistanche raw material; then spraying and freezing for 4min by adopting liquid nitrogen at the temperature of 25 ℃ below zero, and then performing microwave vacuum drying for 50min under the conditions that the microwave power is 7kW, the vacuum degree is 0.07MPa and the temperature is controlled at 45 ℃; performing airflow ultramicro pulverization at a low temperature of-8 ℃ to obtain cistanche powder of 400 meshes; 97g of cistanche powder is taken, 2g of cane sugar and 1g of amino acid are added into the cistanche powder to obtain a pre-fermented material, lactobacillus plantarum liquid, lactobacillus delbrueckii liquid and bifidobacterium liquid are mixed according to the volume ratio of 1:1:1 and then inoculated into the pre-fermented material for anaerobic fermentation, the inoculation amount is 11 percent of the weight of the pre-fermented material, the fermentation temperature is controlled at 33 ℃, and the fermentation time is 5 days; pressing the fermented material into a cistanche slice with the thickness of 3mm and the diameter of 1.2cm, and performing microwave treatment at 65 ℃ until the water content is 7% to obtain the cistanche decoction pieces.
Example 5
After fresh cistanche is dug, the sediment on the surface is timely washed by clear water, the sediment is drained, and the surface is atomized and sprayed with alcohol with the mass fraction of 85 percent, wherein the spraying amount is 0.09 percent of the weight of the cistanche raw material; then spraying and freezing for 4min by adopting liquid nitrogen at the temperature of-30 ℃, and then performing microwave vacuum drying for 50min under the conditions that the microwave power is 7kW, the vacuum degree is-0.07 MPa and the temperature is controlled at 45 ℃; performing jet superfine grinding at a low temperature of-7 ℃ to obtain 350-mesh cistanche powder; 97g of cistanche powder is taken, 1.5g of cane sugar and 1.5g of amino acid are added into the cistanche powder to obtain a pre-fermented material, lactobacillus plantarum liquid, lactobacillus delbrueckii liquid and bifidobacterium liquid are mixed according to the volume ratio of 1:1:2 and then inoculated into the pre-fermented material for anaerobic fermentation, the inoculation amount is 12 percent of the weight of the pre-fermented material, the fermentation temperature is controlled at 30 ℃, and the fermentation time is 6 d; pressing the fermented material into cistanche slices with the thickness of 3mm and the diameter of 1.2cm, and performing microwave treatment at 68 ℃ until the water content is 7% to obtain cistanche decoction pieces.
The above is only a preferred embodiment of the present invention, and it should be noted that the above preferred embodiment should not be considered as limiting the present invention, and the protection scope of the present invention should be subject to the scope defined by the claims. It will be apparent to those skilled in the art that various modifications and adaptations can be made without departing from the spirit and scope of the invention, and these modifications and adaptations should be considered within the scope of the invention.
Claims (9)
1. A method for processing Chinese herbal medicine decoction pieces is characterized in that fresh medicinal material cistanche is processed, and the method comprises the following specific steps:
washing drying
Washing the surface silt of the dug fresh cistanche deserticola with clear water, draining, atomizing and spraying alcohol with the mass fraction of 70-95% on the surface, then spraying and freezing for 2-5 min by adopting liquid nitrogen with the temperature of-20 to-40 ℃, and then carrying out microwave vacuum drying;
crushing at low temperature
Carrying out airflow superfine grinding at the low temperature of-5 to-10 ℃ to obtain cistanche powder of 300 to 500 meshes;
performing biological fermentation on the ground
Adding sucrose and amino acid into Cistanchis herba powder to obtain pre-fermented material, inoculating beneficial bacteria liquid, and performing anaerobic fermentation;
four preforming shaping
Pressing the fermented material into cistanche slices, and then performing microwave drying to obtain cistanche decoction pieces.
2. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the alcohol spraying amount is 0.05-0.1% of the weight of the cistanche salsa raw material.
3. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the drying conditions of the microwave vacuum drying are that the microwave power is 5-8 kW, the vacuum degree is-0.055-0.085 MPa, and the temperature is controlled at 40-50 ℃ for drying for 45-60 min.
4. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the cistanche powder is mixed with cane sugar and amino acid according to the weight ratio of 96-98:1-2: 1-2.
5. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the beneficial bacteria include but are not limited to one or more of lactobacillus plantarum, lactobacillus delbrueckii and bifidobacterium.
6. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the inoculation amount of the beneficial bacterium liquid is 10-13% of the weight of the pre-fermentation material.
Further, in some preferred embodiments of the present invention, the temperature of the anaerobic fermentation is controlled to be 30-35 ℃, and the fermentation time is 4-6 d.
7. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the cistanche slice is 2-4 mm in thickness and 1-1.5 cm in diameter.
8. The processing method of the traditional Chinese medicine decoction pieces as claimed in claim 1, which is characterized in that: the microwave drying is carried out at the temperature of 60-70 ℃ until the water content is 7-13%.
9. A herbal pieces prepared by the method of processing herbal pieces according to any of claims 1-9.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104544098A (en) * | 2015-01-31 | 2015-04-29 | 张翔 | Cistanche essential tablet and preparation method thereof |
| CN104886254A (en) * | 2015-04-30 | 2015-09-09 | 孟令刚 | Food containing cistanche ferment, and preparation technology of food containing cistanche ferment |
| CN110393745A (en) * | 2019-07-17 | 2019-11-01 | 广东元德中药饮片有限公司 | A kind of Herba Cistanches prepared slices of Chinese crude drugs and preparation method thereof |
| CN111265569A (en) * | 2019-10-22 | 2020-06-12 | 宁夏农林科学院农业生物技术研究中心（宁夏农业生物技术重点实验室） | Preparation method of cistanche superfine powder |
| CN111838486A (en) * | 2020-08-03 | 2020-10-30 | 姜学工 | Cistanche solid particle beverage and preparation method thereof |
-
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- 2021-05-08 CN CN202110497506.8A patent/CN113082086A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104544098A (en) * | 2015-01-31 | 2015-04-29 | 张翔 | Cistanche essential tablet and preparation method thereof |
| CN104886254A (en) * | 2015-04-30 | 2015-09-09 | 孟令刚 | Food containing cistanche ferment, and preparation technology of food containing cistanche ferment |
| CN110393745A (en) * | 2019-07-17 | 2019-11-01 | 广东元德中药饮片有限公司 | A kind of Herba Cistanches prepared slices of Chinese crude drugs and preparation method thereof |
| CN111265569A (en) * | 2019-10-22 | 2020-06-12 | 宁夏农林科学院农业生物技术研究中心（宁夏农业生物技术重点实验室） | Preparation method of cistanche superfine powder |
| CN111838486A (en) * | 2020-08-03 | 2020-10-30 | 姜学工 | Cistanche solid particle beverage and preparation method thereof |
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