CN112959539B - Continuous dewatering mixed pouring device and process for high-viscosity filler-containing heat-insulating coating - Google Patents
Continuous dewatering mixed pouring device and process for high-viscosity filler-containing heat-insulating coating Download PDFInfo
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7466—Combinations of similar mixers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/81—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles
- B01F33/813—Combinations of similar mixers, e.g. with rotary stirring devices in two or more receptacles mixing simultaneously in two or more mixing receptacles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/02—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type
- B29B7/06—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices
- B29B7/10—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary
- B29B7/12—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with single shaft
- B29B7/16—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type with movable mixing or kneading devices rotary with single shaft with paddles or arms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/02—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type
- B29B7/22—Component parts, details or accessories; Auxiliary operations
- B29B7/28—Component parts, details or accessories; Auxiliary operations for measuring, controlling or regulating, e.g. viscosity control
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/02—Mixing; Kneading non-continuous, with mechanical mixing or kneading devices, i.e. batch type
- B29B7/22—Component parts, details or accessories; Auxiliary operations
- B29B7/28—Component parts, details or accessories; Auxiliary operations for measuring, controlling or regulating, e.g. viscosity control
- B29B7/286—Component parts, details or accessories; Auxiliary operations for measuring, controlling or regulating, e.g. viscosity control measuring properties of the mixture, e.g. temperature, density
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B7/00—Mixing; Kneading
- B29B7/74—Mixing; Kneading using other mixers or combinations of mixers, e.g. of dissimilar mixers ; Plant
- B29B7/7476—Systems, i.e. flow charts or diagrams; Plants
- B29B7/7485—Systems, i.e. flow charts or diagrams; Plants with consecutive mixers, e.g. with premixing some of the components
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C39/00—Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor
- B29C39/22—Component parts, details or accessories; Auxiliary operations
- B29C39/24—Feeding the material into the mould
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C39/00—Shaping by casting, i.e. introducing the moulding material into a mould or between confining surfaces without significant moulding pressure; Apparatus therefor
- B29C39/22—Component parts, details or accessories; Auxiliary operations
- B29C39/44—Measuring, controlling or regulating
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- Mixers Of The Rotary Stirring Type (AREA)
- Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
Abstract
The invention discloses a high-viscosity filler-containing heat-insulating coating continuous dewatering mixed pouring device and a process, which comprises a mixing tank I for placing a component A and a mixing tank II for placing a component B, wherein a stirring paddle, a jacket, a vacuum port, a vacuum pipeline, a nitrogen port, a nitrogen pipeline, a discharge port, a metering pump, an electromagnetic valve, a pressure regulating valve and a three-way electromagnetic valve are arranged on the mixing tanks I and II; the tail ends of the pipelines of the mixing tank I and the mixing tank II are connected to a continuous mixing head; the whole mixing process comprises the steps of dewatering and continuous mixed casting, the whole dewatering, mixing and casting process of the materials of the heat-insulating coating layer is carried out in a closed system, nitrogen is adopted for balancing pressure, secondary contact of moisture in air in the mixed casting process is avoided, the yield of products is improved from 60% to more than 95%, and the efficiency is improved by more than 750% compared with that of the traditional manual process; the problems of low efficiency and low product yield of the traditional mixed casting process of the high-viscosity filler-containing heat-insulating coating are solved.
Description
Technical Field
The invention belongs to the field of heat-insulating coating layers, relates to the field of heat-insulating coating layers with high viscosity and high solid content, and particularly relates to a continuous dewatering and mixed pouring device and process for a heat-insulating coating layer with high viscosity and filler.
Background
A common application area for high solids content and high viscosity insulating coatings is that of propellant products. The heat-insulating coating material contains solid-phase components such as organic filler, carbon fiber material and the like, and the solid-phase content is generally 10% -60%. The high solid-phase filler enables the viscosity of the heat-insulating coating layer to be extremely high and the fluidity to be extremely poor, the production mode at the present stage is mainly full manual operation, firstly, the adhesive and the solid-phase filler are mixed into a component A by adopting a kneading machine and a three-roll calender; when the catalyst is used, the component A and the component B are respectively placed in a heated vacuum box for vacuumizing for about 30min, then the component A and the component B are poured into a container according to the proportion, and simultaneously the catalyst is added and stirred by a manual hand-held stirring rod for about 1 min. Stirring is increasingly difficult because, after the addition of the catalyst, the component A and the component B undergo a curing reaction. And in the stirring process, the mixture is directly contacted with the air, so that the moisture in the air is brought into the mixture, the moisture in the air and the component A react to generate carbon dioxide, and the carbon dioxide gas generates pores in the mixture, so that the product contains pores and the quality of the product is influenced.
After stirring is finished, pouring the stirred mixture into a mold manually, wherein the stirring time is long, so that the reaction time of the component A and the component B is long, the viscosity is increased, and the pouring is difficult; the process bubbles wrapped in the mixture in the casting process can not smoothly overflow.
Based on the characteristics of the high-solid-content and high-viscosity heat-insulation coating material, the processing technology mainly has the advantages of long process period, more process links and low product yield caused by bubbles generated in the process; in summer weather with high humidity, the product yield is even less than 60%.
Disclosure of Invention
Aiming at the defects and shortcomings in the prior art, the invention aims to provide a continuous dewatering and mixing pouring device and a continuous dewatering and mixing pouring process for a high-viscosity filler-containing heat-insulating coating.
In order to achieve the purpose, the invention adopts the following technical scheme:
a high-viscosity filler-containing heat-insulating coating continuous dewatering mixed pouring device is used for mixing and pouring a component A and a component B containing solid-phase filler to obtain a high-viscosity filler-containing heat-insulating coating, wherein the solid-phase content of the heat-insulating coating is 10% -60%; the device comprises a mixing tank I for placing a component A and a mixing tank II for placing a component B;
a stirring paddle I is arranged in the mixing tank I and extends out of the top of the mixing tank I, a jacket I is sleeved on the outer wall of the mixing tank I, and the jacket I is connected with a component A temperature control unit; the top of the mixing tank I is also provided with a vacuum port I and a nitrogen port I, the vacuum port I is connected with a vacuum pipeline I, the vacuum pipeline I is provided with a first electromagnetic valve I, the nitrogen port I is connected with a nitrogen pipeline I, and a second electromagnetic valve I and a pressure regulating valve I are sequentially arranged on the nitrogen pipeline I; the bottom of the mixing tank I is provided with a discharge port I which is connected with a discharge pipeline I, the discharge pipeline I is provided with a first-component metering pump, the tail end of the discharge pipeline I is connected with an inlet I of a three-way electromagnetic valve I, a first outlet I of the three-way electromagnetic valve I is connected with a return pipe I, the tail end of the return pipe I is connected into the mixing tank I, a second outlet I of the three-way electromagnetic valve I is connected with the pipeline I, and the pipeline I is provided with a third electromagnetic valve I; the end of the pipeline I is connected to a continuous mixing head;
a stirring paddle II is arranged in the mixing tank II and extends out of the top of the mixing tank II, a jacket II is sleeved on the outer wall of the mixing tank II, and the jacket II is connected with a component B temperature control unit; the top of the mixing tank II is also provided with a vacuum port II and a nitrogen port II, the vacuum port II is connected with a vacuum pipeline II, the vacuum pipeline II is provided with a first electromagnetic valve II, the nitrogen port II is connected with a nitrogen pipeline II, and the nitrogen pipeline II is sequentially provided with a second electromagnetic valve II and a pressure regulating valve II; a discharge port II is arranged at the bottom of the mixing tank II, the discharge port II is connected with a discharge pipeline II, a component B metering pump is arranged on the discharge pipeline II, the tail end of the discharge pipeline II is connected with an inlet II of a three-way electromagnetic valve II, a first outlet II of the three-way electromagnetic valve II is connected with a return pipe II, the tail end of the return pipe II is connected into the mixing tank II, a second outlet II of the three-way electromagnetic valve II is connected with a pipeline II, and a third electromagnetic valve II is arranged on the pipeline II; the tail end of the pipeline II is connected to the continuous mixing head;
the first electromagnetic valve I, the second electromagnetic valve I, the third electromagnetic valve I, the pressure regulating valve I, the first component metering pump, the first component temperature control unit, the first electromagnetic valve II, the second electromagnetic valve II, the third electromagnetic valve II, the pressure regulating valve II, the second component metering pump, the second component temperature control unit and the continuous mixing head are controlled by a computer control program.
The invention also comprises the following technical characteristics:
specifically, the third electromagnetic valve I and the third electromagnetic valve II are close to the continuous mixing head.
Specifically, the outer surfaces of the discharge pipeline I, the return pipe I and the pipeline I are covered with jackets; the outer surfaces of the discharge pipeline II, the return pipe II and the pipeline II are all covered with a jacket.
Specifically, the part of the return pipe I connected with the mixing tank I is higher than the liquid level in the mixing tank I, and the part of the return pipe II connected with the mixing tank II is higher than the liquid level in the mixing tank II.
Specifically, the nitrogen pipeline I and the nitrogen pipeline II are connected to a nitrogen bottle.
A high-viscosity filler-containing heat-insulating coating layer continuous water removal mixed casting process comprises the following steps:
A. dewatering: adding the component A and the catalyst into the mixing tank I, and adding the component B into the mixing tank II; the third electromagnetic valve I and the third electromagnetic valve II are closed; an inlet I and a first outlet I of the three-way electromagnetic valve I are opened, a second outlet I is closed, an inlet II and a first outlet II of the three-way electromagnetic valve II are opened, and a second outlet II is closed; the loop arrangement ensures that under the condition that the outlet is closed, the component A in the mixing tank I and the return pipe I thereof can be circulated, and the component B in the mixing tank II and the return pipe II thereof can be circulated;
closing a second electromagnetic valve I of the nitrogen port I and a second electromagnetic valve II of the nitrogen port II; opening a first electromagnetic valve I of the vacuum port I and a first electromagnetic valve II of the vacuum port II for vacuumizing; the stirring paddle I and the stirring paddle II work; heating the jacket I and the jacket II; after the material temperature reaches the set temperature, the component A metering pump and the component B metering pump are started; under the condition of stirring circulation, the component A and the component B are subjected to vacuum pumping to remove the water in the components A and B, and the water removal time is 10-30min;
B. continuous mixed casting: closing a first electromagnetic valve I of a vacuum port I and a first electromagnetic valve II of a vacuum port II, opening a second electromagnetic valve I of a nitrogen port I and a second electromagnetic valve II of the nitrogen port II, and setting the pressure of a pressure regulating valve I and the pressure of the pressure regulating valve I; then opening a second outlet I of the three-way electromagnetic valve I and a second outlet II of the three-way electromagnetic valve II; setting a pouring speed;
controlling the continuous mixing head to rotate through a computer; within 0.5s-1s after the continuous mixing head rotates, the third electromagnetic valve I and the third electromagnetic valve II are opened simultaneously; stopping the continuous mixing head after pouring is finished;
C. intermittent continuous mixed casting: setting the pouring time T and pouring interval time Delta T of a single product through calculating the material density; the control program of opening and closing the third electromagnetic valve I and the third electromagnetic valve II and the rotation and stop of the continuous mixing head is the same as the step B; the time from the opening to the closing of the third electromagnetic valve I and the third electromagnetic valve II is T; the time from the closing to the opening of the third electromagnetic valve I and the third electromagnetic valve II is delta T.
In the step A:
the component A is in a viscous state containing solid-phase filler, the mass percentage of the solid-phase filler is 20-80%, and the viscosity is 10-200Pa.s;
the component B is single-component liquid with the viscosity of 2-20Pa.s;
the mass ratio of the component A to the component B is (1-3) to 1;
the content of the catalyst accounts for 0.05-0.2% of the total mass of the component A and the component B.
In the step A:
vacuumizing until the vacuum degree is-85 kPa to-100 kPa;
the rotating speeds of the stirring paddle I and the stirring paddle II are respectively 10-40rpm and 10-100rpm;
the temperature in the jacket I and the jacket II is 50-75 ℃ and 40-60 ℃ respectively;
the flow rates of the component A metering pump and the component B metering pump are both 0.5L/min to 5L/min.
In the step B, the pressure of the pressure regulating valve I and the pressure regulating valve I are 100kPa-120kPa; setting the pouring speed to be 0.5L-10L/min; the rotating speed of the continuous mixing head is 1000-3000rpm.
Compared with the prior art, the invention has the beneficial technical effects that:
(1) The process is automatic and continuous in the whole process, and compared with the traditional manual mixed pouring process, the efficiency is improved by over 600 percent; (2) Moisture in the process link is isolated, and the product qualification rate is improved from less than 60 percent to more than 95 percent.
Drawings
FIG. 1 is a schematic view of a continuous dewatering and mixing casting device and a process flow of the high-viscosity filler-containing heat-insulating coating layer.
The reference numerals have the meanings given below: 101. mixing tanks I,102, stirring paddles I,103, jackets I,104, a component A temperature control unit, 105, vacuum ports I,106, nitrogen ports I,107, first electromagnetic valves I,108, second electromagnetic valves I,109, pressure regulating valves I,110, discharge ports I,111, a component A metering pump, 112, three-way electromagnetic valves I,113, inlets I,114, first outlets I,115, return pipes I,116, second outlets I,117 and a third electromagnetic valve I;
201. mixing tanks II,202, stirring paddles II,203, jackets II,204, a component B temperature control unit, 205, vacuum ports II,206, nitrogen ports II,207, first electromagnetic valves II,208, second electromagnetic valves II,209, pressure regulating valves II,210, discharge ports II,211, a component B metering pump, 212, three-way electromagnetic valves II,213, inlet II,214, first outlets II,215, return pipes II,216, second outlets II,217 and a third electromagnetic valve II;
300. continuous mixing head, 400 nitrogen cylinder.
Detailed Description
According to the product characteristics of the high-solid-content heat-insulating coating layer, the equipment and the process are improved, so that the production process is automated and continuous, the process links are reduced, the contact between materials and air in the process is avoided, the moisture is isolated, the product quality is improved, the process efficiency is improved, and the manual labor intensity is reduced.
A high-viscosity filler-containing heat-insulating coating continuous dewatering mixed pouring device is used for mixing and pouring a component A and a component B containing solid-phase filler to obtain a high-viscosity filler-containing heat-insulating coating, wherein the solid-phase content of the heat-insulating coating is 10% -60%; the device is including the blending tank I101 of placing first component and the blending tank II201 of placing second component, and blending tank I101 and blending tank II201 are all airtight.
A stirring paddle I102 is arranged in the mixing tank I101, the stirring paddle I102 extends out of the top of the mixing tank I101, a jacket I103 is sleeved on the outer wall of the mixing tank I101, and the jacket I103 is connected with a component A temperature control unit 104; the top of the mixing tank I101 is also provided with a vacuum port I105 and a nitrogen port I106, the vacuum port I105 is connected with a vacuum pipeline I, the vacuum pipeline I is provided with a first electromagnetic valve I107, the nitrogen port I106 is connected with a nitrogen pipeline I, and the nitrogen pipeline I is sequentially provided with a second electromagnetic valve I108 and a pressure regulating valve I109; a discharge port I110 is arranged at the bottom of the mixing tank I101, the discharge port I110 is connected with a discharge pipeline I, a component A metering pump 111 is arranged on the discharge pipeline I, the tail end of the discharge pipeline I is connected with an inlet I113 of a three-way electromagnetic valve I112, a first outlet I114 of the three-way electromagnetic valve I112 is connected with a return pipe I115, the tail end of the return pipe I115 is connected into the mixing tank I101, a second outlet I116 of the three-way electromagnetic valve I112 is connected with a pipeline I, and a third electromagnetic valve I117 is arranged on the pipeline I; line I terminates to a continuous mixing head 300.
A stirring paddle II202 is arranged in the mixing tank II201, the stirring paddle II202 extends out of the top of the mixing tank II201, a jacket II203 is sleeved on the outer wall of the mixing tank II201, and the jacket II203 is connected with a component B temperature control unit 204; the top of the mixing tank II201 is also provided with a vacuum port II205 and a nitrogen port II206, the vacuum port II205 is connected with a vacuum pipeline II, the vacuum pipeline II is provided with a first electromagnetic valve II207, the nitrogen port II206 is connected with a nitrogen pipeline II, and the nitrogen pipeline II is sequentially provided with a second electromagnetic valve II208 and a pressure regulating valve II209; a discharge port II210 is arranged at the bottom of the mixing tank II201, the discharge port II210 is connected with a discharge pipeline II, a component B metering pump 211 is arranged on the discharge pipeline II, the tail end of the discharge pipeline II is connected with an inlet II213 of a three-way electromagnetic valve II212, a first outlet II214 of the three-way electromagnetic valve II212 is connected with a return pipe II215, the tail end of the return pipe II215 is connected into the mixing tank II201, a second outlet II216 of the three-way electromagnetic valve II212 is connected with a pipeline II, and a third electromagnetic valve II217 is arranged on the pipeline II; line II terminates in a continuous mixing head 300.
The first electromagnetic valve I107, the second electromagnetic valve I108, the third electromagnetic valve I117, the pressure regulating valve I109, the component A metering pump 111, the component A temperature control unit 104, the first electromagnetic valve II207, the second electromagnetic valve II208, the third electromagnetic valve II217, the pressure regulating valve II209, the component B metering pump 211, the component B temperature control unit 204 and the continuous mixing head 300 are all controlled by a computer control program.
Third solenoid valve I117 and third solenoid valve II217 are in close proximity to continuous mixing head 300. Specifically, the distance between the third electromagnetic valve I and the third electromagnetic valve II and the continuous mixing head is less than 10cm.
The outer surfaces of the discharge pipeline I, the return pipe I115 and the pipeline I are covered with jackets; the outer surfaces of the discharge pipeline II, the return pipe II215 and the pipeline II are covered with jackets. In the embodiment, the discharge pipeline I, the return pipeline I and the jacket internal control Wen Gongzhi covered by the outer surface of the pipeline I are the same as the jacket I; the inner control of the jacket Wen Gongzhi covered by the outer surfaces of the discharge pipeline II, the return pipeline II and the pipeline II is the same as the jacket II.
The part of the return pipe I115 connected with the mixing tank I101 is higher than the liquid level in the mixing tank I101, and the part of the return pipe II215 connected with the mixing tank II201 is higher than the liquid level in the mixing tank II 201; and (5) uniformly mixing the auxiliary materials.
The nitrogen line I and the nitrogen line II are connected to a nitrogen cylinder 400.
The embodiment also provides a continuous dewatering mixed pouring process for the high-viscosity filler-containing heat-insulating coating, which comprises the following steps:
A. dewatering: adding the component A and the catalyst into the mixing tank I, and adding the component B into the mixing tank II; the third electromagnetic valve I and the third electromagnetic valve II are closed; an inlet I and a first outlet I of the three-way electromagnetic valve I are opened, a second outlet I is closed, an inlet II and a first outlet II of the three-way electromagnetic valve II are opened, and a second outlet II is closed; the loop arrangement ensures that under the condition that the outlet is closed, the component A in the mixing tank I and the return pipe I thereof can be circulated, and the component B in the mixing tank II and the return pipe II thereof can be circulated;
closing a second electromagnetic valve I of the nitrogen port I and a second electromagnetic valve II of the nitrogen port II; opening a first electromagnetic valve I of the vacuum port I and a first electromagnetic valve II of the vacuum port II for vacuumizing; the stirring paddle I and the stirring paddle II work; heating the jacket I and the jacket II; after the material temperature reaches the set temperature, the component A metering pump and the component B metering pump are started; under the condition of stirring circulation, the component A and the component B are subjected to vacuum pumping to remove the water in the components A and B, and the water removal time is 10-30min;
in step a of the present embodiment:
the component A is in a viscous state containing solid-phase filler, the mass of the solid-phase filler accounts for 20-80% of the total mass of the component A, and the viscosity is 10-200Pa.s;
the component B is single-component liquid with the viscosity of 2-20Pa.s;
the mass ratio of the component A to the component B is (1-3) to 1;
the catalyst accounts for 0.05-0.2% of the total mass of the component A and the component B;
vacuumizing until the vacuum degree is-85 kPa to-100 kPa;
the rotating speeds of the stirring paddle I and the stirring paddle II are respectively 10-40rpm and 10-100rpm;
the temperature in the jacket I and the jacket II is 50-75 ℃ and 40-60 ℃ respectively;
the flow rates of the component A metering pump and the component B metering pump are both 0.5L/min to 5L/min.
B. Continuous mixed casting: closing a first electromagnetic valve I of a vacuum port I and a first electromagnetic valve II of a vacuum port II, opening a second electromagnetic valve I of a nitrogen port I and a second electromagnetic valve II of the nitrogen port II, and setting the pressure of a pressure regulating valve I and the pressure of the pressure regulating valve I; then opening a second outlet I of the three-way electromagnetic valve I and a second outlet II of the three-way electromagnetic valve II; setting a pouring speed;
controlling the continuous mixing head to rotate through a computer; within 0.5s-1s after the continuous mixing head rotates, the third electromagnetic valve I and the third electromagnetic valve II are opened simultaneously; stopping the rotation of the continuous mixing head after the pouring is finished;
in the step B, the pressure of the pressure regulating valve I and the pressure of the pressure regulating valve I are 100kPa-120kPa; setting the pouring speed to be 0.5L-10L/min through a control system, and enabling a metering pump to adapt to the rotating speed according to the set pouring speed to realize pouring; the rotating speed of the continuous mixing head is 1000-3000rpm.
C. Intermittent continuous mixed casting: setting the pouring time T and pouring interval time Delta T of a single product through calculating the material density; the control program of opening and closing the third electromagnetic valve I and the third electromagnetic valve II and the rotation and stop of the continuous mixing head is the same as the step B; the time from the opening to the closing of the third electromagnetic valve I and the third electromagnetic valve II is T; the time from the closing to the opening of the third electromagnetic valve I and the third electromagnetic valve II is delta T.
The present invention is not limited to the following embodiments, and equivalent changes made on the basis of the technical solutions of the present invention fall within the scope of the present invention.
Example 1:
in this example, the mixture casting of the heat-insulating coating layer was carried out on the dewatering mixture casting apparatus, the viscosity of the component a was 150pa.s (at 50 ℃), the component a contained 40% by mass of the solid-phase filler with a particle size of 29um and 25% by mass of the solid-phase filler with a particle size of 13um, and 0.1% of the catalyst was added to the component a at the same time; the component B is a single phase, and the viscosity at 50 ℃ is 2.6Pa.s. The temperatures in the jacket I and the jacket II were 55 ℃ and 50 ℃ respectively; when the temperatures of the component A and the component B respectively reach 45 ℃, starting a stirring paddle, wherein the rotating speeds of the stirring paddle I and the stirring paddle II are respectively 20rpm and 20rpm; when the component A mixing tank I and the component B mixing tank II are vacuumized, the vacuum degrees are both-92 kPa.
Vacuum dewatering for 20min; the pouring speed was set at 300g/10s, i.e. the pouring time T was 10s, corresponding to 1.2L/min. The mass ratio of the component A to the component B is 180. The rotating speed of the continuous mixing head is 2800rpm; and (3) 0.5s after the continuous mixing head 8 starts to rotate, simultaneously opening the third electromagnetic valve I and the third electromagnetic valve II for mixing and pouring.
40 shots of cast products were continuously mixed, and the casting interval time DeltaT between each shot of products was 10s for switching the molds, and the casting weights obtained were as shown in Table 1 below.
TABLE 1 quality of the cast product
The average charging mass of 40 pieces of products is 300.52g, the precision reaches 0.18 percent, and the product design requirement is met; the total time consumption is 40 × 10s +40 × 10s =800s. The manual mixing time of a single product in the traditional process is 100s, the manual pouring time is 40s, the switching time of the middle die is 10s, the actual time consumption for producing 40 products is 6000s, and the efficiency of the continuous mixing and pouring process is improved by 750 percent compared with that of the traditional process. After the obtained product is cured, the product is detected to be 38, the number of the products is completely qualified, the number of the products needs to be repaired is 2, and the yield is 95%.
Claims (4)
1. A high-viscosity filler-containing heat-insulating coating continuous dewatering mixed pouring device is used for mixing and pouring a component A and a component B containing solid-phase filler to obtain a high-viscosity filler-containing heat-insulating coating, wherein the solid-phase content of the heat-insulating coating is 10% -60%; the device is characterized by comprising a mixing tank I (101) for placing a component A and a mixing tank II (201) for placing a component B;
a stirring paddle I (102) is arranged in the mixing tank I (101), the stirring paddle I (102) extends out of the top of the mixing tank I (101), a jacket I (103) is sleeved on the outer wall of the mixing tank I (101), and the jacket I (103) is connected with a component A temperature control unit (104); the top of the mixing tank I (101) is also provided with a vacuum port I (105) and a nitrogen port I (106), the vacuum port I (105) is connected with a vacuum pipeline I, the vacuum pipeline I is provided with a first electromagnetic valve I (107), the nitrogen port I (106) is connected with a nitrogen pipeline I, and the nitrogen pipeline I is sequentially provided with a second electromagnetic valve I (108) and a pressure regulating valve I (109); a discharge port I (110) is arranged at the bottom of the mixing tank I (101), the discharge port I (110) is connected with a discharge pipeline I, a component A metering pump (111) is arranged on the discharge pipeline I, the tail end of the discharge pipeline I is connected with an inlet I (113) of a three-way electromagnetic valve I (112), a first outlet I (114) of the three-way electromagnetic valve I (112) is connected with a return pipe I (115), the tail end of the return pipe I (115) is connected into the mixing tank I (101), a second outlet I (116) of the three-way electromagnetic valve I (112) is connected with a pipeline I, and a third electromagnetic valve I (117) is arranged on the pipeline I; the end of the pipeline I is connected to a continuous mixing head (300);
a stirring paddle II (202) is arranged in the mixing tank II (201), the stirring paddle II (202) extends out of the top of the mixing tank II (201), a jacket II (203) is sleeved on the outer wall of the mixing tank II (201), and the jacket II (203) is connected with a component B temperature control unit (204); the top of the mixing tank II (201) is also provided with a vacuum port II (205) and a nitrogen port II (206), the vacuum port II (205) is connected with a vacuum pipeline II, the vacuum pipeline II is provided with a first electromagnetic valve II (207), the nitrogen port II (206) is connected with a nitrogen pipeline II, and the nitrogen pipeline II is sequentially provided with a second electromagnetic valve II (208) and a pressure regulating valve II (209); a discharge port II (210) is arranged at the bottom of the mixing tank II (201), the discharge port II (210) is connected with a discharge pipeline II, a component B metering pump (211) is arranged on the discharge pipeline II, the tail end of the discharge pipeline II is connected with an inlet II (213) of a three-way electromagnetic valve II (212), a first outlet II (214) of the three-way electromagnetic valve II (212) is connected with a return pipe II (215), the tail end of the return pipe II (215) is connected into the mixing tank II (201), a second outlet II (216) of the three-way electromagnetic valve II (212) is connected with a pipeline II, and a third electromagnetic valve II (217) is arranged on the pipeline II; the end of the pipeline II is connected to the continuous mixing head (300);
the first electromagnetic valve I (107), the second electromagnetic valve I (108), the third electromagnetic valve I (117), the pressure regulating valve I (109), the component A metering pump (111), the component A temperature control unit (104), the first electromagnetic valve II (207), the second electromagnetic valve II (208), the third electromagnetic valve II (217), the pressure regulating valve II (209), the component B metering pump (211), the component B temperature control unit (204) and the continuous mixing head (300) are controlled by a computer control program;
the outer surfaces of the discharge pipeline I, the return pipe I (115) and the pipeline I are covered with jackets; the outer surfaces of the discharge pipeline II, the return pipe II (215) and the pipeline II are covered with jackets;
the connection part of the return pipe I (115) and the mixing tank I (101) is higher than the liquid level in the mixing tank I (101), and the connection part of the return pipe II (215) and the mixing tank II (201) is higher than the liquid level in the mixing tank II (201).
2. The continuous dewatering mixing casting device for the high-viscosity filler-containing heat-insulating coating layer according to claim 1, characterized in that the third solenoid valve I (117) and the third solenoid valve II (217) are close to the continuous mixing head (300).
3. The continuous dehydrating hybrid casting apparatus for a highly viscous, filled, insulating coating according to claim 1, wherein the nitrogen line I and the nitrogen line II are connected to a nitrogen gas cylinder (400).
4. A continuous water-removing mixed pouring process for the high-viscosity filler-containing heat-insulating coating layer, which is realized by the continuous water-removing mixed pouring device for the high-viscosity filler-containing heat-insulating coating layer, as claimed in claim 1, and comprises the following steps:
A. dewatering: adding the component A and the catalyst into the mixing tank I, and adding the component B into the mixing tank II; the third electromagnetic valve I and the third electromagnetic valve II are closed; an inlet I and a first outlet I of the three-way electromagnetic valve I are opened, a second outlet I is closed, an inlet II and a first outlet II of the three-way electromagnetic valve II are opened, and a second outlet II is closed; the loop arrangement ensures that under the condition that the outlet is closed, the component A in the mixing tank I and the return pipe I thereof can be circulated, and the component B in the mixing tank II and the return pipe II thereof can be circulated;
closing a second electromagnetic valve I of the nitrogen port I and a second electromagnetic valve II of the nitrogen port II; opening a first electromagnetic valve I of the vacuum port I and a first electromagnetic valve II of the vacuum port II for vacuumizing; the stirring paddle I and the stirring paddle II work; heating the jacket I and the jacket II; after the material temperature reaches the set temperature, the component A metering pump and the component B metering pump are started; under the condition of stirring circulation, the component A and the component B are subjected to vacuum pumping to remove the water in the components A and B, and the water removal time is 10-30min;
B. continuous mixed casting: closing a first electromagnetic valve I of a vacuum port I and a first electromagnetic valve II of a vacuum port II, opening a second electromagnetic valve I of a nitrogen port I and a second electromagnetic valve II of the nitrogen port II, and setting the pressure of a pressure regulating valve I and the pressure of the pressure regulating valve I; then opening a second outlet I of the three-way electromagnetic valve I and a second outlet II of the three-way electromagnetic valve II; setting a pouring speed;
the continuous mixing head is controlled to rotate by a computer; within 0.5s-1s after the continuous mixing head rotates, the third electromagnetic valve I and the third electromagnetic valve II are opened simultaneously; stopping the continuous mixing head after pouring is finished;
C. intermittent continuous mixed casting: setting the pouring time T and pouring interval time Delta T of a single product through calculating the material density; the control program of opening and closing the third electromagnetic valve I and the third electromagnetic valve II and the rotation and stop of the continuous mixing head is the same as the step B; the time from the opening to the closing of the third electromagnetic valve I and the third electromagnetic valve II is T; the time from the closing to the opening of the third electromagnetic valve I and the third electromagnetic valve II is delta T;
in the step A:
the component A is in a viscous state containing solid phase filler, the mass percentage of the solid phase filler is 20-80%, and the viscosity is 10-200Pa.s;
the component B is single-component liquid, and the viscosity is 2-20Pa.s;
the mass ratio of the component A to the component B is (1-3) to 1;
the catalyst accounts for 0.05-0.2% of the total mass of the component A and the component B;
in the step A:
vacuumizing to the vacuum degree of-85 kPa to-100 kPa;
the rotating speeds of the stirring paddle I and the stirring paddle II are respectively 10-40rpm and 10-100rpm;
the temperature in the jacket I and the jacket II is 50-75 ℃ and 40-60 ℃ respectively;
the flow rates of the component A metering pump and the component B metering pump are both 0.5L/min to 5L/min;
in the step B, the pressure of the pressure regulating valve I and the pressure regulating valve I are 100kPa-120kPa; setting the pouring speed to be 0.5L-10L/min; the rotating speed of the continuous mixing head is 1000-3000rpm.
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CN202428611U (en) * | 2011-12-31 | 2012-09-12 | 洛阳智颢工程塑料有限公司 | High-pressure reaction injection molding device |
CN102806611A (en) * | 2012-08-20 | 2012-12-05 | 湘潭方棱聚氨酯机器有限公司 | Continuous automatic double-component adhesive mixing machine |
CN203409948U (en) * | 2013-07-08 | 2014-01-29 | 河南科技大学 | Small-sized reaction injection molding device |
CN206762815U (en) * | 2017-05-22 | 2017-12-19 | 中山凯旋真空技术工程有限公司 | Vacuum Mixture system |
CN110180470B (en) * | 2019-04-29 | 2024-01-26 | 中国科学院山西煤炭化学研究所 | Kettle type continuous slurry bed reactor and use method thereof |
CN112045964B (en) * | 2020-07-31 | 2023-03-31 | 聊城鲁西聚碳酸酯有限公司 | Polycarbonate additive adding device and adding process |
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