CN112957303B - Waterproof and sweat-proof eyebrow pencil containing multiple plant essences and preparation method thereof - Google Patents
Waterproof and sweat-proof eyebrow pencil containing multiple plant essences and preparation method thereof Download PDFInfo
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- CN112957303B CN112957303B CN202110206826.3A CN202110206826A CN112957303B CN 112957303 B CN112957303 B CN 112957303B CN 202110206826 A CN202110206826 A CN 202110206826A CN 112957303 B CN112957303 B CN 112957303B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/38—Percompounds, e.g. peracids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/927—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of insects, e.g. shellac
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a waterproof and anti-sweat eyebrow pencil containing multiple plant essences and a preparation method thereof, wherein the waterproof and anti-sweat eyebrow pencil comprises the following components in parts by weight: 10 to 25 parts of filling agent, 20 to 32 parts of colorant, 5 to 15 parts of Japan wax, 3 to 10 parts of polyethylene glycol wax, 0.1 to 1.5 parts of ginger extract, 0.1 to 1 part of calendula extract, 0.1 to 1 part of honeysuckle extract, 1 to 5 parts of hydrogenated castor oil and 2 to 5 parts of glycerol tri (ethyl acetate). The eyebrow pencil provided by the invention solves the problem of separation of wax and colorant by adjusting the formula composition, and the obtained product has good appearance and stability, has the functions of water resistance and sweat resistance, can effectively keep makeup, is smooth in use, is easy to develop color and has a good use effect.
Description
Technical Field
The invention belongs to the technical field of cosmetics. More particularly, relates to a waterproof and sweat-proof eyebrow pencil containing multiple plant essences and a preparation method thereof.
Background
The eyebrow pencil lead is made from materials including grease, wax and pigment, wherein the wax is paraffin, japan wax, beeswax, ozokerite, lanolin, carnauba wax, cocoa butter and the like, the wax mainly has thickening, solidifying and shaping effects in the formula, the melting point of the wax is generally between 45 and 110 ℃, and the wax is required to be firstly melted and then changed into flowing liquid by raising the temperature to be mixed with coloring agent, filling agent and the like when the eyebrow pencil is prepared. But in the subsequent preparation process, the temperature is inevitably reduced for 2 to 3 times, and in the process, the separation of grease and colorant is easily caused, and the delamination of the product is caused.
Shellac, also known as shellac, shellac and the like, is a fatty resin, is currently used as a component of legal cosmetics in the countries of the united states, japan and the like, which are leading in cosmetic science and technology, is commonly used in hair-setting products such as hair spray, conditioning hair spray and the like, and is also used in eyeliner cosmetics. It has not been shown to be used in eyebrow pencils to overcome the separation of wax from toner.
In addition, after the eyebrow pencil is made up, because the skin of a human body can secrete grease and sweat, the eyebrow pencil without the water-proof and oil-proof functions can be made up, and therefore, the eyebrow pencil with the water-proof and sweat-proof functions is needed.
Disclosure of Invention
The invention aims to solve the technical problem of overcoming the defects of the existing eyebrow pencil and provides the eyebrow pencil which contains multiple plant essences and has the functions of water resistance and sweat resistance.
The above purpose of the invention is realized by the following technical scheme: a waterproof and sweat-proof eyebrow pencil containing multiple plant essences comprises the following components in parts by weight: 10 to 25 parts of filling agent, 20 to 32 parts of colorant, 5 to 15 parts of Japan wax, 3 to 10 parts of polyethylene glycol wax, 0.1 to 1.5 parts of ginger extract, 0.1 to 1 part of calendula extract, 0.1 to 1 part of honeysuckle extract, 1 to 5 parts of hydrogenated castor oil and 2 to 5 parts of glycerol tri (ethyl acetate).
Preferably, the eyebrow pencil comprises the following components in parts by weight: 15 to 25 portions of filling agent, 25 to 32 portions of colorant, 10 to 15 portions of Japan wax, 6 to 10 portions of polyethylene glycol wax, 0.5 to 1.5 portions of ginger extract, 0.3 to 1 portion of calendula extract, 0.3 to 1 portion of honeysuckle extract, 2 to 4 portions of hydrogenated castor oil and 2 to 4 portions of glycerol tri (ethyl acetate).
Preferably, the eyebrow pencil further comprises shellac.
Preferably, in the eyebrow pencil, the weight ratio of the Japan wax, the polyethylene glycol wax and the shellac is 3:1 to 2:0.1 to 1.5.
Preferably, in the eyebrow pencil, the weight ratio of the Japan wax, the polyethylene glycol wax and the shellac is 3:1.2:0.8.
preferably, the colorant is selected from at least one of CI77499, CI77492, CI77491 and CI 77891.
Preferably, the filler is selected from one or both of mica and silica.
Preferably, the filler is selected from mica.
The invention provides a method for preparing the waterproof and sweat-proof eyebrow pencil, which comprises the following steps:
s1, mechanically crushing Japan wax, polyethylene glycol wax, a coloring agent and a filling agent respectively for later use;
s2, putting Japan wax and polyethylene glycol wax into a melting pot, heating to melt, adding hydrogenated castor oil and glycerol tri (ethyl acetate), and stirring and mixing uniformly;
s3, cooling to 60-80 ℃, adding the filler, the colorant, the ginger extract, the calendula extract and the honeysuckle extract, and uniformly stirring; grinding; and (5) molding to obtain the product.
Preferably, the step S1 also comprises the step of adding the shellac in the process of mechanical crushing; the step S2 also comprises the step of putting the crushed lac, the Japan wax and the polyethylene glycol wax into a melting pot.
The invention adopts the Japan wax as the main wax to play the roles of solidification and shaping, but the repeated temperature change in the subsequent process causes the wax to be separated from the colorant, and the product has more heterochromatic spots. It has been unexpectedly found that the addition of shellac can overcome the separation between the wax and the colorant, and the inventors speculate that this may be due to the specific amphiphilic block copolymer nature of shellac. The lac has hydrophilic and hydrophobic part concurrently, has a large amount of functional groups simultaneously such as hydroxyl and carboxyl, can act as the effect of bridging between toner and wax class, and in addition, the lac has ionizable carboxyl, possesses certain polyelectrolyte polymer nature, can provide two electron layer stabilizing action and steric hindrance effect simultaneously, and the dispersion in the system is strong to play the separation effect of curbing wax and colorant.
But the lac is very unstable due to a large number of functional groups, and the product is found to have a delamination phenomenon in long-term storage tests. In this regard, the inventors further found through experiments that the addition of the polyethylene glycol wax based on the above results in the improvement of the overall stability of the product, and the effect of the polyethylene glycol wax is considered to be mainly due to the stabilizing effect of the polyethylene glycol wax on the shellac.
The invention has the following beneficial effects:
the eyebrow pencil provided by the invention solves the problem of separation of wax and colorant by adjusting the formula composition, the obtained product has good appearance and stability, and the eyebrow pencil has the functions of water resistance and sweat resistance, is added with multiple plant essences, can effectively keep makeup appearance, is smooth in use, is easy to develop color, and has a good use effect.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Unless otherwise indicated, reagents and materials used in the following examples are commercially available.
EXAMPLES 1 TO 3 PEN WITH WATER-PROOF AND ANTI-SWEAT FUNCTION AND ITS FORMULATION (IN WEIGHT PARTS)
| Components | Example 1 | Example 2 | Example 3 | Example 4 |
| Mica | 10 | 16 | 20 | 23 |
| Japanese wax | 9 | 6 | 12 | 15 |
| Polyethylene glycol wax | 3.6 | 4 | 4 | 5 |
| Lacca | 2.4 | 3 | 2 | 1.5 |
| Hydrogenated castor oil | 1.5 | 2.5 | 3 | 5 |
| Glycerol tri (ethyl acetate) | 2 | 3 | 4 | 5 |
| CI77499 | 5 | 6 | 7 | 8 |
| CI77492 | 5 | 6 | 7 | 8 |
| CI77491 | 5 | 6 | 7 | 8 |
| CI77891 | 5 | 6 | 7 | 8 |
| Ginger extract | 1 | 0.6 | 1.2 | 1.5 |
| Calendula extract | 0.5 | 1 | 0.8 | 0.5 |
| Honeysuckle flower extract | 0.5 | 1 | 0.8 | 0.5 |
The preparation method comprises the following steps:
s1, mechanically crushing Japan wax, polyethylene glycol wax, a coloring agent, a filling agent and lac for later use respectively;
s2, putting Japan wax, polyethylene glycol wax and lac into a melting material pot, heating to melt, adding hydrogenated castor oil and glycerol tri (ethyl acetate), and stirring and mixing uniformly;
s3, cooling to 60 ℃, adding the filler, the colorant, the ginger extract, the polygonum multiflorum root extract and the honeysuckle flower extract, and uniformly stirring; grinding until the powder is uniformly dispersed;
s4, placing the powder at a constant temperature of 25 ℃ for 12 hours, pouring the powder into a plodder, extruding a refill, placing the refill until the hardness is recovered, and packaging the refill after the color matching is qualified.
Comparative example 1 differs from example 1 in that no shellac was added and the remaining parameters were the same as in example 1.
Comparative example 2, which is different from example 1 in that no polyethylene glycol wax was added, and the remaining parameters were the same as in example 1.
Comparative example 3 differs from example 1 in that beeswax is used instead of polyethylene glycol wax and the remaining parameters are the same as in example 1.
Test I, sensory index and physicochemical index test
The cartridges prepared in examples 1 to 4 and comparative examples 1 to 3 were tested according to the sensory index and physicochemical index test methods in the national standard GB/T27575-2011 "cosmetic pencil, cosmetic cartridge", and the test results are shown in tables 1 and 2 below.
TABLE 1 sensory index test results
TABLE 2 results of physical and chemical index testing
As can be seen from the above table, the pen refills prepared in embodiments 1 to 4 of the present invention have good sensory and physicochemical indexes, and analysis of test results of other comparative examples shows that the problem of separation of wax from toner in the eyebrow pencil can be solved by adding shellac, and that adding polyethylene glycol wax is beneficial to improving the stability of shellac, so that the cold resistance and heat resistance of the eyebrow pencil are improved, but the effect disappears when beeswax is used to replace polyethylene glycol wax.
Test example two, long-term storage test
The lead cores of the eyebrow pencils prepared in examples 1 to 4 and comparative examples 1 to 3 were stored for 36 months under conditions of temperature of 25. + -. 2 ℃ and humidity of 60%. + -. 5% RH, and the appearance of the lead cores was observed, and the test results are shown in Table 3 below.
| Sample (I) | Stability test results |
| Example 1 | The refill has no fracture and delamination |
| Example 2 | The refill has no fracture and delamination |
| Example 3 | The refill has no fracture and delamination |
| Example 4 | The refill has no fracture and delamination |
| Comparative example 1 | The refill has no fracture and delamination |
| Comparative example 2 | The refill has obvious layering phenomenon |
| Comparative example 3 | The layered phenomenon of the pen core |
As can be seen from the above table, examples 1 to 4 according to the present invention have excellent stability, and the shelf life thereof is as long as 36 months, whereas the refills prepared in comparative examples 2 to 3 have a significant delamination phenomenon, indicating poor stability.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such modifications are intended to be included in the scope of the present invention.
Claims (6)
1. The waterproof and anti-sweat eyebrow pencil containing multiple plant essences is characterized by being prepared from the following components in parts by weight: 10 to 25 parts of a filler, 20 to 32 parts of a colorant, 5 to 15 parts of Japan wax, 3 to 5 parts of polyethylene glycol wax, 0.1 to 1.5 parts of a ginger extract, 0.1 to 1 part of a calendula extract, 0.1 to 1 part of a honeysuckle extract, 1 to 5 parts of hydrogenated castor oil and 2 to 5 parts of triglyceride (ethyl acetate); the eyebrow pencil further comprises shellac, wherein the weight ratio of the Japan wax, the polyethylene glycol wax and the shellac is 3:1 to 2:0.3 to 1.5.
2. The waterproof and sweat-proof eyebrow pencil as recited in claim 1, wherein the weight ratio of japan wax, polyethylene glycol wax and shellac is 3:1.2:0.8.
3. the waterproof and antiperspirant eyebrow pencil of claim 1 or claim 2, wherein the colorant is at least one selected from the group consisting of CI77499, CI77492, CI77491 and CI 77891.
4. The waterproof and antiperspirant eyebrow pencil of claim 1 or claim 2, wherein the filler is selected from one or both of mica and silica.
5. The waterproof sweatproof eyebrow pencil of claim 4 wherein said filler is selected from mica.
6. A process for preparing a waterproof and antiperspirant eyebrow pencil according to claim 1 or 2, comprising the steps of:
s1, mechanically crushing Japan wax, polyethylene glycol wax, a coloring agent and a filling agent respectively for later use;
s2, putting the Japan wax and the polyethylene glycol wax into a melting material pot, heating to melt, adding the hydrogenated castor oil and the glycerol tri (ethyl acetate), and stirring and mixing uniformly;
s3, cooling to 60-80 ℃, adding a filler, a colorant, a ginger extract, a calendula extract and a honeysuckle extract, and uniformly stirring; grinding; molding to obtain the product;
the step S1 also comprises a step of adding lac in the mechanical crushing process; the step S2 also comprises the step of putting the crushed lac, the Japan wax and the polyethylene glycol wax into a melting pot.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110206826.3A CN112957303B (en) | 2021-02-24 | 2021-02-24 | Waterproof and sweat-proof eyebrow pencil containing multiple plant essences and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110206826.3A CN112957303B (en) | 2021-02-24 | 2021-02-24 | Waterproof and sweat-proof eyebrow pencil containing multiple plant essences and preparation method thereof |
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| CN112957303B true CN112957303B (en) | 2022-12-27 |
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Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111000736A (en) * | 2019-12-24 | 2020-04-14 | 张士飞 | Preparation method of eyebrow pencil lead |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS60208904A (en) * | 1984-03-31 | 1985-10-21 | Pentel Kk | Liquid cosmetic for pen-type cosmetic |
| CN106265225B (en) * | 2016-08-10 | 2019-05-31 | 云南尚呈生物科技有限公司 | A kind of eyebrow pencil composition and preparation method thereof |
| DE202018100825U1 (en) * | 2018-02-15 | 2019-05-20 | Schwan-Stabilo Cosmetics Gmbh & Co. Kg | powder mines |
| CN108294971A (en) * | 2018-03-21 | 2018-07-20 | 浙江美密科技发展有限公司 | A kind of tearable type eyeliner and preparation method thereof |
| CN110314123A (en) * | 2019-07-01 | 2019-10-11 | 上海欧润化妆品有限公司 | A kind of eyebrow pencil and preparation method thereof |
| CN111529433A (en) * | 2020-04-27 | 2020-08-14 | 浙江美雪化妆品有限公司 | Solid paste eyebrow pencil |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111000736A (en) * | 2019-12-24 | 2020-04-14 | 张士飞 | Preparation method of eyebrow pencil lead |
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| Title |
|---|
| 紫胶蜡及其在化妆品的应用;刘新民;《广西轻工业》;19950630(第02期);第11-16页 * |
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