CN112844180A - External forced dispersing device for improving dispersing and mixing capacity of stirring kettle - Google Patents
External forced dispersing device for improving dispersing and mixing capacity of stirring kettle Download PDFInfo
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- CN112844180A CN112844180A CN202011598594.2A CN202011598594A CN112844180A CN 112844180 A CN112844180 A CN 112844180A CN 202011598594 A CN202011598594 A CN 202011598594A CN 112844180 A CN112844180 A CN 112844180A
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- external forced
- static mixer
- electromagnetic valve
- forced dispersion
- downstream
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/82—Combinations of dissimilar mixers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/71—Feed mechanisms
- B01F35/714—Feed mechanisms for feeding predetermined amounts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Accessories For Mixers (AREA)
Abstract
The present disclosure relates to an external forced dispersion device for improving the dispersive mixing capability of a stirred tank. The device comprises a first two-position three-way electromagnetic valve, a pump, a second two-position three-way electromagnetic valve, a feeding device, a bypass pipeline, a static mixer and a controllable flow distribution valve which are sequentially arranged. The pump lift ensures that the pumped liquid has sufficient power to return to the stirred tank through the downstream components. The feeding device consists of a storage hopper and a Venturi tube. The static mixer is connected to the two-position two-way solenoid valve of the charging device and downstream of the bypass line. The controllable flow distribution valve is connected to the static mixer and has two outlets which are respectively connected to the stirred tank and the feeding device. By utilizing the device, the working state of the stirring kettle is kept unchanged, and meanwhile, the processing time of each kettle can be greatly shortened.
Description
Technical Field
The present disclosure relates to stirred tanks, and more particularly to an externally forced dispersion apparatus for improving the dispersive mixing capability of a stirred tank.
Background
The stirring kettle is widely applied to the reaction and mixing processing of chemical liquid products. When a stirred tank is used for preparing a product containing insoluble solid powder and incompatible liquid components, the particle size fineness uniformity and the dispersion uniformity of a dispersed phase in a solution are limited. This problem is mainly caused by two reasons, on one hand, the force applied to the dispersed phase by the solution flow caused by the impact of the two dispersed phases in the solution and the rotation of the stirring paddle is often insufficient, and on the other hand, the effective force is difficult to form and effectively act on the dispersed phase directly.
Disclosure of Invention
In order to solve the problem, the invention improves the traditional stirring kettle and develops an external forced dispersion device for the traditional stirring kettle. The dispersing device mainly comprises a feeding device, a bypass pipeline, a static mixer, a pump, a two-position three-way electromagnetic valve for realizing the switching of the pipeline circulation direction, a two-position two-way electromagnetic valve for controlling the opening and the closing of the pipeline, a controllable flow distribution valve and a pipeline which is connected as necessary.
In order to install the external forced dispersion device, an outlet is required to be arranged at the bottom of the stirring kettle.
According to an aspect of an embodiment of the present disclosure, there is provided an external forced dispersion apparatus for improving a dispersion mixing capability of a stirred tank, the apparatus comprising: the first two-position three-way electromagnetic valve is arranged at the outlet of the stirring kettle, so that the two stations of discharging materials and accessing the external forced dispersion device are switched by the outlet; the pump is connected to the downstream of the first two-position three-way electromagnetic valve, and the pump head of the pump ensures that the pumped liquid has enough power to return to the stirring kettle through a downstream component; a second two-position, three-way solenoid valve connected downstream of the pump; the feeding device is connected to the downstream of the second two-position three-way electromagnetic valve and consists of a storage hopper and a Venturi tube, and the downstream of the feeding device is provided with the two-position two-way electromagnetic valve; a bypass line placed in parallel with the charging device and also connected downstream of the second two-position three-way solenoid valve; a static mixer connected to the two-position, two-way solenoid valve of the charging device and downstream of the bypass line; and the controllable flow distribution valve is connected to the static mixer and is provided with two outlets which are respectively connected into the stirring kettle and the feeding device, wherein the first two-position three-way electromagnetic valve, the pump, the second two-position three-way electromagnetic valve, the feeding device, the bypass pipeline, the static mixer, the controllable flow distribution valve and the stirring kettle are connected through a connecting pipeline.
In an example of the present disclosure, the static mixer is installed in a section of a connecting pipeline, end face sealing flanges are welded to both ends of the section of the connecting pipeline, and the end face sealing flanges are matched with the size of the static mixer.
In an example of the present disclosure, the mixing blade of the static mixer is knife-edged with an angle of less than 60 ° to the wind.
In the disclosed example, the flow rate of the pump ensures both the charging capacity of the charging device and the corresponding shear stress that is generated when the liquid with the dispersed phase passes through the static mixer.
In an example of the disclosure, the venturi tube of the feeding device includes a main flow channel and an auxiliary flow channel, and at a joint position of the main flow channel and the auxiliary flow channel, a tube diameter of the main flow channel is reduced to form a local high-speed area, and a negative pressure is formed at a tube opening of the auxiliary flow channel, so that feeding of materials in the material storage hopper is realized.
In an example of the present disclosure, the second two-position three-way solenoid valve completes the switching of the liquid into the charging device or the bypass line, and the two-position two-way solenoid valve connected to the outlet of the charging device is closed when the second two-position three-way solenoid valve is switched to the station of the bypass line.
In an example of the present disclosure, the charging device includes a storage hopper, and the two outlets of the controllable flow distribution valve are respectively connected to the stirred tank and the storage hopper of the charging device.
In an example of the disclosure, when powder materials are to be added, the second two-position three-way electromagnetic valve is connected to the feeding device for feeding; when the charging is finished, the second two-position three-way electromagnetic valve is connected to the bypass pipeline to realize further external forced dispersion.
In an example of the present disclosure, if the external forced dispersion device is not needed, the first two-position three-way solenoid valve is operated such that the discharge of the material is completed at the outlet of the stirred tank.
In examples of the present disclosure, the static mixers are of different types to achieve mixing of different kinds of materials. For the mixing of the insoluble powder material, an SK type static mixer is recommended. For the mixing of incompatible liquid materials, an SX type static mixer is recommended.
By using the external forced dispersing device for improving the dispersing and mixing capacity of the stirring kettle, the working state of the stirring kettle is kept unchanged, and meanwhile, the processing time of each kettle can be greatly shortened.
It is to be understood that both the foregoing general description and the following detailed description are exemplary and explanatory only and are not restrictive of the disclosure.
Drawings
The accompanying drawings, which are incorporated in and constitute a part of this specification, illustrate embodiments consistent with the present disclosure and, together with the description, serve to explain the principles of the disclosure and are not to be construed as limiting the disclosure.
FIG. 1 is a schematic illustration of a stirred tank equipped with an external forced dispersion apparatus according to an exemplary embodiment of the disclosure. In the figure, 1-a stirring kettle, 2-a discharge port, 3-a two-position three-way electromagnetic valve A, 4-a pump, 5-a two-position three-way electromagnetic valve B, 6-a feeding device, 7-a two-position two-way electromagnetic valve B, 8-a static mixer, 9-a controllable flow distribution valve and 10-a bypass pipeline
Fig. 2 is a schematic view of a structure in which a static mixer line is flange-mounted. In the figure, 8-static mixer, 8-1 is a static mixer inlet side line, and 8-2 is a static mixer outlet side line.
Detailed Description
In order to make the technical solutions of the present disclosure better understood by those of ordinary skill in the art, the technical solutions in the embodiments of the present disclosure will be clearly and completely described below with reference to the accompanying drawings.
It should be noted that the terms "first," "second," and the like in the description and claims of the present disclosure and in the above-described drawings are used for distinguishing between similar elements and not necessarily for describing a particular sequential or chronological order. It is to be understood that the data so used is interchangeable under appropriate circumstances such that the embodiments of the disclosure described herein are capable of operation in sequences other than those illustrated or otherwise described herein. The implementations described in the exemplary embodiments below are not intended to represent all implementations consistent with the present disclosure. Rather, they are merely examples of apparatus and methods consistent with certain aspects of the present disclosure, as detailed in the appended claims.
As shown in FIG. 1, a stirred tank apparatus equipped with the external forced dispersion apparatus of the present invention is shown.
In the example, a discharge port (serial number 2) is formed in the bottom of the stirring kettle (serial number 1), a two-position three-way electromagnetic valve A (serial number 3) is arranged at the downstream of the discharge port (serial number 2), and switching of two stations of a material discharging and connecting external forced dispersing device can be achieved. When 3-1 bit of the two-position three-way electromagnetic valve A (serial number 3) is communicated, material discharge is realized; when the 3-2 position of the two-position three-way electromagnetic valve A (serial number 3) is connected, the material enters the external forced dispersion device.
In the example, the pump (serial No. 4) is used to provide sufficient power to ensure that the liquid has sufficient power to flow through the various stages downstream of the pump (serial No. 4). The downstream of the pump (serial number 4) is a two-position three-way electromagnetic valve B (serial number 5), which can realize the switching of liquid flowing through the feeding device (serial number 6) and the bypass pipeline (serial number 10). When the two-position three-way electromagnetic valve B (serial number 5) is connected to the 5-1 position, the liquid flows through the Venturi tube (serial number 6-1) of the feeding device. The caliber of the main pipeline of the venturi tube (serial number 6-1) is properly reduced at the position crossed with the auxiliary pipeline, and the flow velocity of fluid flowing through the main pipeline is increased, so that relative low pressure is formed at the pipe orifice of the auxiliary pipeline, and powder materials or incompatible liquid materials in the storage hopper (6-2) are pumped into the main pipeline of the venturi tube (serial number 6-1). An electromagnetic valve (serial number 7) is arranged at the outlet of the feeding device (serial number 6).
In an example, when a two-position three-way electromagnetic valve B (serial number 5) is connected to 5-1 bits, an electromagnetic valve (serial number 7) needs to be in an opening state; when the two-position three-way electromagnetic valve B (serial number 5) is connected to 5-2, the electromagnetic valve (serial number 7) needs to be in a closed state to seal the feeding device (serial number 6). The liquid flowing through the feeding device (serial number 6) carries the powder material or the incompatible liquid material to form a mixed material.
In the example, the mixed materials enter the pipeline sections 8-1 and 8-2 provided with the static mixer (serial number 8), and are crushed and corroded while being subjected to flow splitting and confluence mixing by the static mixer (serial number 8). Different types of static mixers can be used depending on the type of dispersed phase. For the mixing of the insoluble powder material, an SK type static mixer is recommended. For the mixing of incompatible liquid materials, an SX type static mixer is recommended. To facilitate the replacement of the static mixer, the present invention installs the static mixer (No. 8) in a section of pipeline, using a flanged connection for replacement (see fig. 2). In order to improve the mixing effect of the static mixer, the windward side of the mixing blades of the static mixer is processed into a blade shape with an angle of less than 60 degrees, so that the crushing of the dispersed phase is further promoted.
Then, the mixed material flows through a controllable flow distribution valve (serial number 9), one part of the mixed material flows back to the stirring kettle (serial number 1), and the other part of the mixed material enters a storage hopper 6-2 of a feeding device (serial number 6). The mixed material entering the storage hopper 6-2 of the feeding device (serial number 6) plays a role in improving the flowability of the powder material or reducing the relative concentration of the incompatible liquid material, and simultaneously plays a role in cleaning the storage hopper 6-2. When powder materials are to be added, a two-position three-way electromagnetic valve B (serial number 5) is switched on to 5-1 position, and an electromagnetic valve B (serial number 7) is opened for feeding; when the feeding is finished, the two-position three-way electromagnetic valve B (serial number 5) is connected to 5-2, the electromagnetic valve (serial number 7) is closed, and the mixed material continuously flows into the pipeline sections 8-1 and 8-2 provided with the static mixer (serial number 8) through the bypass pipeline (serial number 10), so that further external forced dispersion is realized, and the improvement of dispersion and mixing of the stirring kettle on the insoluble powder material or the incompatible liquid material is facilitated.
By using the external forced dispersion device for improving the dispersive mixing capability of the stirrer, the working state of the stirring kettle is not changed, but the processing time of each kettle can be greatly shortened.
Other embodiments of the disclosure will be apparent to those skilled in the art from consideration of the specification and practice of the disclosure disclosed herein. This application is intended to cover any variations, uses, or adaptations of the disclosure following, in general, the principles of the disclosure and including such departures from the present disclosure as come within known or customary practice within the art to which the disclosure pertains. It is intended that the specification and examples be considered as exemplary only, with a true scope and spirit of the disclosure being indicated by the following claims.
In the description of the present disclosure, reference to the description of the terms "one embodiment," "some embodiments," "an example," "a specific example" or "some examples," etc., means that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the present disclosure. In the present disclosure, the schematic representations of the terms described above are not necessarily intended to be the same real-time or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples. Furthermore, various embodiments or examples and features of different embodiments or examples described in this disclosure can be combined and combined by one skilled in the art without contradiction.
It will be understood that the present disclosure is not limited to the precise arrangements described above and shown in the drawings and that various modifications and changes may be made without departing from the scope thereof. The scope of the present disclosure is limited only by the appended claims.
Claims (10)
1. An external forced dispersion device for improving dispersion mixing capability of a stirring kettle, which is characterized by comprising:
the first two-position three-way electromagnetic valve is arranged at the outlet of the stirring kettle, so that the two stations of discharging materials and accessing the external forced dispersion device are switched by the outlet;
the pump is connected to the downstream of the first two-position three-way electromagnetic valve, and the pump head of the pump ensures that the pumped liquid has enough power to return to the stirring kettle through a downstream component;
a second two-position, three-way solenoid valve connected downstream of the pump;
the feeding device is connected to the downstream of the second two-position three-way electromagnetic valve and consists of a storage hopper and a Venturi tube, and the downstream of the feeding device is provided with the two-position two-way electromagnetic valve;
a bypass line placed in parallel with the charging device and also connected downstream of the second two-position three-way solenoid valve;
a static mixer connected to the two-position, two-way solenoid valve of the charging device and downstream of the bypass line; and
a controllable flow distribution valve connected to the static mixer and having two outlets that respectively tap into the stirred tank and the feeding device,
the first two-position three-way electromagnetic valve, the pump, the second two-position three-way electromagnetic valve, the feeding device, the bypass pipeline, the static mixer, the controllable flow distribution valve and the stirring kettle are connected through connecting pipelines.
2. The external forced dispersion device of claim 1, wherein the static mixer is installed into a section of connecting piping, end sealing flanges are welded to both ends of the section of connecting piping, and the end sealing flanges are adapted to the size of the static mixer.
3. The external forced dispersion device of claim 1, wherein the mixing blades of the static mixer are knife-edged with an angle of less than 60 ° on the windward side.
4. An external forced dispersion device according to claim 1, characterized in that the flow rate of the pump guarantees both the feeding capacity of the feeding device and the corresponding shear stress of the liquid with dispersed phase when it passes through the static mixer.
5. The external forced dispersion device of claim 1, wherein the venturi tube of the feeding device comprises a main flow channel and an auxiliary flow channel, and at a joint position of the main flow channel and the auxiliary flow channel, a tube diameter of the main flow channel is reduced to form a local high-speed area, and a negative pressure is formed at a tube opening of the auxiliary flow channel, thereby realizing feeding of the material in the storage hopper.
6. The external forced dispersion device according to claim 1, wherein the second two-position three-way solenoid valve completes the switching of the liquid into the charging device or the bypass line, and when the second two-position three-way solenoid valve is switched to the station of the bypass line, the two-position two-way solenoid valve connected to the outlet of the charging device is closed.
7. The external forced dispersion device of claim 1, wherein the charging device comprises a storage hopper, and the two outlets of the controllable flow distribution valve are connected to the stirred tank and the storage hopper of the charging device, respectively.
8. The external forced dispersion device of claim 1, wherein the second two-position three-way solenoid valve is connected to the feeding device for feeding when powder material is to be fed; when the charging is finished, the second two-position three-way electromagnetic valve is connected to the bypass pipeline to realize further external forced dispersion.
9. The external forced dispersion apparatus of claim 1, wherein if the external forced dispersion apparatus is not needed, the first two-position three-way solenoid valve is operated such that material discharge is accomplished at the outlet of the stirred tank.
10. An external forced dispersion device according to claim 2, characterized in that the static mixers are of different types to achieve mixing of different kinds of materials, SK type static mixers are used for mixing of poorly soluble powder materials, and SX type static mixers are used for mixing of incompatible liquid materials.
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Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
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EP0937495A2 (en) * | 1998-02-23 | 1999-08-25 | Unilever Plc | Mixing immiscible liquids |
CN1785940A (en) * | 2004-12-08 | 2006-06-14 | 北京化工大学 | Technology of ion liquid catalyzing benzene and long chain olefin alkylation reaction and its device |
CN201200888Y (en) * | 2008-06-06 | 2009-03-04 | 东南大学 | High-efficient chemical reactor with combined stirring pot and static mixer |
CN202860460U (en) * | 2012-10-13 | 2013-04-10 | 杨剑英 | Efficient material-liquid mixing complete-set engineering equipment |
CN203329666U (en) * | 2012-12-25 | 2013-12-11 | 上海建安化工设计有限公司 | Naphthalene and air mixing device |
CN105688729A (en) * | 2016-04-13 | 2016-06-22 | 赵扬 | Hydromechanical auto-control three-stage mixing equipment |
CN109200844A (en) * | 2018-09-13 | 2019-01-15 | 重庆腾治科技有限公司 | Additive process units |
CN209338358U (en) * | 2018-11-01 | 2019-09-03 | 左健 | A kind of sludge at low temperature pyrohydrolysis processing unit |
CN211495371U (en) * | 2019-12-24 | 2020-09-15 | 山东泰和水处理科技股份有限公司 | Liquid storage tank device |
-
2020
- 2020-12-29 CN CN202011598594.2A patent/CN112844180A/en active Pending
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0937495A2 (en) * | 1998-02-23 | 1999-08-25 | Unilever Plc | Mixing immiscible liquids |
CN1785940A (en) * | 2004-12-08 | 2006-06-14 | 北京化工大学 | Technology of ion liquid catalyzing benzene and long chain olefin alkylation reaction and its device |
CN201200888Y (en) * | 2008-06-06 | 2009-03-04 | 东南大学 | High-efficient chemical reactor with combined stirring pot and static mixer |
CN202860460U (en) * | 2012-10-13 | 2013-04-10 | 杨剑英 | Efficient material-liquid mixing complete-set engineering equipment |
CN203329666U (en) * | 2012-12-25 | 2013-12-11 | 上海建安化工设计有限公司 | Naphthalene and air mixing device |
CN105688729A (en) * | 2016-04-13 | 2016-06-22 | 赵扬 | Hydromechanical auto-control three-stage mixing equipment |
CN109200844A (en) * | 2018-09-13 | 2019-01-15 | 重庆腾治科技有限公司 | Additive process units |
CN209338358U (en) * | 2018-11-01 | 2019-09-03 | 左健 | A kind of sludge at low temperature pyrohydrolysis processing unit |
CN211495371U (en) * | 2019-12-24 | 2020-09-15 | 山东泰和水处理科技股份有限公司 | Liquid storage tank device |
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