CN112755937A - High-efficient reliable hydrogenation cauldron - Google Patents

High-efficient reliable hydrogenation cauldron Download PDF

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Publication number
CN112755937A
CN112755937A CN201911000795.5A CN201911000795A CN112755937A CN 112755937 A CN112755937 A CN 112755937A CN 201911000795 A CN201911000795 A CN 201911000795A CN 112755937 A CN112755937 A CN 112755937A
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CN
China
Prior art keywords
kettle body
drawing plate
driving
hydrogen
box
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Pending
Application number
CN201911000795.5A
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Chinese (zh)
Inventor
钱君
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhongqi Petrochemical Equipment Wuxi Co ltd
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Zhongqi Petrochemical Equipment Wuxi Co ltd
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Publication date
Application filed by Zhongqi Petrochemical Equipment Wuxi Co ltd filed Critical Zhongqi Petrochemical Equipment Wuxi Co ltd
Priority to CN201911000795.5A priority Critical patent/CN112755937A/en
Publication of CN112755937A publication Critical patent/CN112755937A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00245Avoiding undesirable reactions or side-effects
    • B01J2219/00256Leakage

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to a high-efficiency reliable hydrogenation reaction kettle, which comprises a kettle body, wherein the outer side of the kettle body is connected with a steam heat exchange cavity, the upper part and the lower part of the steam heat exchange cavity are respectively connected with a steam inlet and a lower condensate outlet, the upper end of the kettle body is provided with a feed inlet, the lower end of the kettle body is connected with a discharge outlet, the upper end of the kettle body is connected with a hydrogen inlet pipe, the upper end of the hydrogen inlet pipe is positioned at the upper end of the kettle body, the lower end of the hydrogen inlet pipe is positioned above the bottom of the kettle body, the kettle body is connected with a drive shaft through a bearing in a rotating way, the upper end of the drive shaft is connected with the drive end of a drive motor, the lower end of the drive shaft is connected with a rotating shaft, the drive motor is connected with an impeller on the kettle body through a bracket, the outer side of the drive shaft on the, can improve the reaction efficiency, prevent hydrogen leakage and ensure safe production.

Description

High-efficient reliable hydrogenation cauldron
Technical Field
The invention relates to a reaction kettle, in particular to a high-efficiency and reliable hydrogenation reaction kettle.
Background
Hydrogenation reation kettle is the container that is used for realizing hydrogen and material reaction, and traditional hydrogenation reation kettle wears to react slow problem, and in addition, the reactor is used for a long time, and the sealed probably damage that appears of drive shaft, and hydrogen is probably leaked outside the cauldron again, has the potential safety hazard.
Disclosure of Invention
The applicant carries out research and improvement aiming at the defects and provides a high-efficiency and reliable hydrogenation reaction kettle.
A high-efficiency reliable hydrogenation reaction kettle comprises a kettle body, wherein a steam heat exchange cavity is connected to the outer side of the kettle body, the upper part and the lower part of the steam heat exchange cavity are respectively connected with an upper steam inlet and a lower condensate outlet, a feed inlet is arranged at the upper end of the kettle body, a discharge outlet is connected at the lower end of the kettle body, a hydrogen inlet pipe is connected at the upper end of the kettle body, the upper end of the hydrogen inlet pipe is positioned above the bottom of the kettle body, a drive shaft is connected on the kettle body in a rotating manner through a bearing, the upper end of the drive shaft is connected with a drive end of a drive motor, the lower end of the drive shaft is connected with a rotating shaft through a coupler, an impeller is connected on the rotating shaft, the drive motor is connected on the kettle body through a bracket, a leakage-proof box is connected outside the drive shaft on the kettle body, the leakage-, and a drawing plate is arranged between the two pore plates.
As a further improvement of the above technical solution:
and a sleeve is arranged between the two pore plates in a matching manner with the driving shaft, and a sealing ring is arranged between the sleeve and the driving shaft.
The drawing plate comprises a left drawing plate and a right drawing plate, the left drawing plate and the right drawing plate are respectively connected with a left transverse moving driving part and a right transverse moving driving part, and a sealing strip is arranged between the left drawing plate and the right drawing plate.
The left transverse moving driving part and the right transverse moving driving part are driving cylinders.
The invention has the following beneficial effects: high-efficient reliable hydrogenation cauldron makes hydrogen deliver to the cauldron bottom through advancing hydrogen pipe, because hydrogen density is lower can the upward movement, and it is long when area of contact and the contact that can increase the reaction improve reaction efficiency, in addition through preventing leaking the box, when hydrogen reveals, can start the exhaust tube and take away the collection, prevent that hydrogen from revealing, eliminate the potential safety hazard, guarantee production safety.
Drawings
FIG. 1 is a schematic structural diagram of a high-efficiency and reliable hydrogenation reactor provided by the invention.
FIG. 2 is a cross-sectional view of a leak-proof box of the high-efficiency and reliable hydrogenation reactor provided by the invention.
FIG. 3 is a schematic diagram of the high-efficiency and reliable hydrogenation reactor provided by the invention when the left and right drawing plates are closed.
FIG. 4 is a schematic diagram of the high-efficiency and reliable hydrogenation reactor provided by the invention when the left and right drawing plates are opened.
In the figure: 1. a kettle body; 11. a feed inlet; 12. a hydrogen inlet pipe; 13. a discharge port; 2. a vapor heat exchange cavity; 21. an upper vapor inlet; 22. a lower condensate outlet; 3. a drive shaft; 4. a drive motor; 5. a rotating shaft; 6. a leak-proof box; 61. an orifice plate; 611. a sleeve; 612. a seal ring; 62. putting the box on; 622. an air exhaust pipe; 63. a box is lowered; 631. a hydrogen sensor; 64. a left drawing plate; 641. a left traverse driving member; 65. a right drawing plate; 651. a right traverse driving member; 66. a sealing strip.
Detailed Description
The following describes a specific embodiment of the present embodiment with reference to the drawings.
As shown in fig. 1 to 4, the high-efficiency reliable hydrogenation reaction kettle of the present embodiment comprises a kettle body 1, a steam heat exchange cavity 2 is connected to the outer side of the kettle body 1, the upper part and the lower part of the steam heat exchange cavity 2 are respectively connected with an upper steam inlet 21 and a lower condensed water outlet 22, a feed inlet 11 is arranged at the upper end of the kettle body 1, a discharge outlet 13 is connected to the lower end of the kettle body 1, a hydrogen inlet pipe 12 is connected to the upper end of the kettle body 1, the lower end of the hydrogen inlet pipe 12 is positioned above the bottom of the kettle body 1, a drive shaft 3 is rotatably connected to the kettle body 1 through a bearing, the upper end of the drive shaft 3 is connected to the drive end of a drive motor 4, the lower end of the drive shaft 3 is connected to a rotating shaft 5 through a coupler, an impeller is connected to the rotating shaft 5, the drive motor 4 is connected to the kettle body 1 through a bracket, a leakage-proof box 6 is, and a sleeve 611 is arranged between the two pore plates 61 in a matching manner with the driving shaft 3, a sealing ring 612 is arranged between the sleeve 611 and the driving shaft 3, a hydrogen sensor 631 is arranged in the lower box 63, the upper box 62 is connected with an exhaust pipe 622, a pumping plate is arranged between the two pore plates 61, the pumping plate comprises a left pumping plate 64 and a right pumping plate 65, the left pumping plate 64 and the right pumping plate 65 are respectively connected with a left traverse driving part 641 and a right traverse driving part 651, the left traverse driving part 641 and the right traverse driving part 651 are driving cylinders, and a sealing strip 66 is arranged between the left pumping plate 64 and the right pumping plate 65.
When the high-efficiency and reliable hydrogenation reaction kettle of the embodiment is used, firstly, materials are sent into the kettle body 1 from the feeding hole 11, meanwhile, the driving motor 4 drives the rotating shaft 5 and the impeller to rotate through the driving shaft 3, the materials are stirred, then, hydrogen is sent to the bottom of the kettle body 1 from the hydrogen inlet pipe 12, the hydrogen can move upwards due to low hydrogen density, and can fully contact with the materials, so that the reaction efficiency of the materials and the hydrogen is improved, the reaction time is shortened, the production efficiency is improved, the materials are discharged and collected from the discharging hole 13 after the reaction is finished, if the seal is damaged, the hydrogen can leak to the outer side of the kettle body 1 from the seal and enter the lower box 63 of the leakage-proof box 6, when the hydrogen concentration reaches the induction concentration of the hydrogen sensor 631, the hydrogen sensor 631 can control the left traverse driving part 641 and the right traverse driving part 651 to drive the left drawing plate 64 and the right drawing plate 65 to move towards two sides, the hydrogen, meanwhile, the hydrogen sensor 631 is used for extracting and collecting hydrogen in the upper box 62 through the matching of air extracting equipment, and meanwhile, an operator can be reminded that the sealing is damaged and leaked, and after the reaction is finished, the sealing part of the driving shaft 3 can be replaced in time.
The foregoing description is illustrative of the present invention and is not to be construed as limiting thereof, the scope of the invention being defined by the appended claims, which may be modified in any manner without departing from the basic structure thereof.

Claims (4)

1. The utility model provides a high-efficient reliable hydrogenation reation kettle which characterized in that: comprises a kettle body (1), wherein a steam heat exchange cavity (2) is connected with the outer side of the kettle body (1), the upper part and the lower part of the steam heat exchange cavity (2) are respectively connected with a steam inlet (21) and a lower condensate outlet (22), a feed inlet (11) is arranged at the upper end of the kettle body (1), a discharge outlet (13) is connected with the lower end of the kettle body (1), a hydrogen inlet pipe (12) is connected with the upper end of the kettle body (1), the upper end of the hydrogen inlet pipe (12) is positioned at the upper end of the kettle body (1), the lower end of the hydrogen inlet pipe (12) is positioned above the bottom of the kettle body (1), a driving shaft (3) is connected with the kettle body (1) in a rotating way through a bearing, the upper end of the driving shaft (3) is connected with a driving end of a driving motor (4), the lower end of the driving shaft (3) is connected with a rotating shaft (, it prevents leaking box (6) to lie in drive shaft (3) outside connection on the cauldron body (1), prevent leaking box (6) and separate into through two orifice plates (61) and go up box (62) and lower box (63), set up hydrogen sensor (631) in lower box (63), go up box (62) and connect exhaust tube (622), two set up between orifice plate (61) and take out the board.
2. The efficient and reliable hydrogenation reactor according to claim 1, wherein: a sleeve (611) is arranged between the two pore plates (61) in a matched mode and is matched with the driving shaft (3), and a sealing ring (612) is arranged between the sleeve (611) and the driving shaft (3).
3. The efficient and reliable hydrogenation reactor according to claim 1, wherein: the drawing plate comprises a left drawing plate (64) and a right drawing plate (65), the left drawing plate (64) and the right drawing plate (65) are respectively connected with a left transverse moving driving component (641) and a right transverse moving driving component (651), and a sealing strip (66) is arranged between the left drawing plate (64) and the right drawing plate (65).
4. The efficient and reliable hydrogenation reactor according to claim 3, wherein: the left traverse driving component (641) and the right traverse driving component (651) are driving cylinders.
CN201911000795.5A 2019-10-21 2019-10-21 High-efficient reliable hydrogenation cauldron Pending CN112755937A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201911000795.5A CN112755937A (en) 2019-10-21 2019-10-21 High-efficient reliable hydrogenation cauldron

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201911000795.5A CN112755937A (en) 2019-10-21 2019-10-21 High-efficient reliable hydrogenation cauldron

Publications (1)

Publication Number Publication Date
CN112755937A true CN112755937A (en) 2021-05-07

Family

ID=75691633

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201911000795.5A Pending CN112755937A (en) 2019-10-21 2019-10-21 High-efficient reliable hydrogenation cauldron

Country Status (1)

Country Link
CN (1) CN112755937A (en)

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202224166U (en) * 2011-09-21 2012-05-23 成都德美精英化工有限公司 Reactor sealing device
CN207680599U (en) * 2017-11-17 2018-08-03 中国石油天然气股份有限公司 A kind of Zeolite synthesis device
CN207970852U (en) * 2018-01-30 2018-10-16 浙江鸿盛化工有限公司 A kind of hydrogenation reaction kettle
CN208407007U (en) * 2018-04-24 2019-01-22 浙江华洲药业有限公司 A kind of hydrogenation reaction kettle
CN109289740A (en) * 2018-11-12 2019-02-01 阜阳洁平日化有限公司 Reaction kettle is used in a kind of toilet cleaner production of anti-leak

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202224166U (en) * 2011-09-21 2012-05-23 成都德美精英化工有限公司 Reactor sealing device
CN207680599U (en) * 2017-11-17 2018-08-03 中国石油天然气股份有限公司 A kind of Zeolite synthesis device
CN207970852U (en) * 2018-01-30 2018-10-16 浙江鸿盛化工有限公司 A kind of hydrogenation reaction kettle
CN208407007U (en) * 2018-04-24 2019-01-22 浙江华洲药业有限公司 A kind of hydrogenation reaction kettle
CN109289740A (en) * 2018-11-12 2019-02-01 阜阳洁平日化有限公司 Reaction kettle is used in a kind of toilet cleaner production of anti-leak

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Application publication date: 20210507

RJ01 Rejection of invention patent application after publication