CN112742327A - Reaction kettle for continuous chlorination - Google Patents
Reaction kettle for continuous chlorination Download PDFInfo
- Publication number
- CN112742327A CN112742327A CN202011590053.5A CN202011590053A CN112742327A CN 112742327 A CN112742327 A CN 112742327A CN 202011590053 A CN202011590053 A CN 202011590053A CN 112742327 A CN112742327 A CN 112742327A
- Authority
- CN
- China
- Prior art keywords
- stirring
- reation kettle
- kettle body
- hydraulic
- pivot
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D19/00—Degasification of liquids
- B01D19/0073—Degasification of liquids by a method not covered by groups B01D19/0005 - B01D19/0042
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The application relates to a reation kettle is used in continuous method chlorination relates to chlorination process equipment's field, and it includes the reation kettle body, is provided with on the reation kettle body to be used for carrying out the stirring subassembly that stirs to reation kettle body inside, is provided with on the reation kettle body inner wall to carry out abluent washing subassembly to reation kettle body inner wall, and the position that the reation kettle body is close to the top is provided with control stirring subassembly and washs subassembly joint complex hydraulic component. This application has the effect of being convenient for wash inside the reation kettle.
Description
Technical Field
The application relates to the field of chlorination process equipment, in particular to a reaction kettle for continuous chlorination.
Background
The chlorination process of the current continuous method has the advantages of convenient operation, labor saving and easy control of product quality in production engineering. It mainly lets in every reation kettle respectively from the distributor through chlorine, and the reaction mass is squeezed into first reation kettle with the pump, and follow-up reation kettle of rethread overflow entering in proper order realizes continuous chlorination, and wherein reation kettle is the most important equipment that realizes chlorination.
The reaction kettle is a container for chemical reaction or physical reaction, and the functions of heating, evaporation, cooling and the like required by the process can be realized through the structural design and parameter configuration of the reaction kettle. The reaction kettle is widely applied to the fields of petroleum, chemical industry, medicine, metallurgy and the like, and the reaction kettle is generally made of carbon manganese steel, stainless steel, nickel-based alloy, other composite materials and the like. After the reaction time in the reaction kettle lasts for a long time, a crystallization layer is formed on the inner wall of the reaction kettle, and if the crystallization layer is not cleaned, the smooth proceeding of the reaction between different reactants in the next round can be influenced, so that an operator needs to clean the reaction kettle frequently.
In view of the above-mentioned related art, the inventors considered that there was a drawback that it was inconvenient for an operator to clean the inside of the reaction tank.
Disclosure of Invention
In order to improve the problem of being not convenient for carry out abluent inside the reation kettle, this application provides a reation kettle is used in continuous method chlorination.
The application provides a reation kettle for continuous process chlorination adopts following technical scheme:
the utility model provides a reation kettle is used in continuous method chlorination, includes the reation kettle body, is provided with on the reation kettle body to be used for carrying out the stirring subassembly that stirs to reation kettle body inside, is provided with on the reation kettle body inner wall to carry out abluent washing subassembly to reation kettle body inner wall, and the position that the reation kettle body is close to the top is provided with the hydraulic component of control stirring subassembly and washing subassembly joint complex.
Through adopting above-mentioned technical scheme, when carrying out the chlorination reaction of material, start the stirring subassembly and stir the inside material of reation kettle body, need wash the inner wall of reation kettle body, it makes stirring subassembly and washing subassembly joint fixed to start hydraulic assembly, the stirring subassembly can drive and wash the subassembly and rotate in order to wash the inner wall of reation kettle body, this application can utilize the power supply of stirring subassembly to carry out automatic clearance with the inner wall to the reation kettle body, intersect in the washing of manpower, have the cleaning efficiency high cleaning effect good advantage.
Preferably, the stirring subassembly is including agitator motor, agitator motor fixes the position that the reation kettle body is close to the top, agitator motor's output shaft fixedly connected with stirring pivot, the stirring pivot is the structure that has annular cavity in inside, one side that the stirring pivot is close to agitator motor is provided with the intubate, intubate and the inside cavity intercommunication of stirring pivot, intubate and hydraulic component intercommunication, all be provided with hydraulic oil in the cavity of stirring pivot and the hydraulic component, the periphery department of stirring pivot is provided with a plurality of puddlers along axial and circumference all fixed, the puddler is the inside hollow structure of both ends opening, the puddler deviates from the one end of stirring pivot and inserts and is equipped with telescopic stirring rod, telescopic stirring rod and puddler sliding fit and the axis of slip axis perpendicular to puddler self, the inside cavity of puddler and the inside cavity intercommunication of stirring pivot.
Through adopting above-mentioned technical scheme, when needs stir the inside material of reation kettle body, start agitator motor, agitator motor's output shaft drives the stirring pivot and rotates to make the stirring pivot drive the puddler and produce the rotation, the puddler rotates the effect of stirring the mixing to the material. When the inner wall of reation kettle body was washd to needs, operating personnel controlled hydraulic assembly for stirring telescopic link is moving towards the direction that deviates from the stirring pivot under hydraulic pressure's effect, and until stirring telescopic link and the cooperation of the joint between the washing subassembly, start agitator motor this moment and can make agitator motor drive washing subassembly produce the rotation, thereby make the washing subassembly play better cleaning performance to the inner wall of reation kettle body.
Preferably, it is including the support ring frame to wash the subassembly, the support ring frame is provided with two, the support ring frame is the annular setting, two support ring frames set up respectively in inside top and bottom department of reation kettle body, support ring frame and reation kettle body normal running fit and axis of rotation are on a parallel with the axis of stirring pivot, be provided with a plurality of washing boards between two support ring frames, the both ends of wasing the board respectively with two support ring frame fixed connection, it is close to the fixed brush hair that is provided with in one side of reation kettle body inner wall to wash the board, brush hair and the cooperation of reation kettle body inner wall butt, it has seted up the joint groove to wash one side that the board is close to the stirring pivot, the joint groove cooperates with the one end joint that stirring rod deviates from the.
Through adopting above-mentioned technical scheme, when starting hydraulic assembly and making the continuous washing board that is close to of stirring rod, stirring rod's one end finally can peg graft at the joint inslot to the washing board can rotate along with stirring rod's rotation, makes agitator motor's rotation can drive the brush hair and play abluent effect to the inner wall of reation kettle body.
Preferably, the one end that stirring telescopic link deviates from the puddler is the chamfer setting, and the chamfer is by the puddler to the stirring telescopic link in the direction shape that the circumference size constantly reduces.
Through adopting above-mentioned technical scheme, stirring telescopic link's chamfer setting has improved stirring telescopic link and has inserted accuracy and the smoothness nature of advancing the joint groove, has been convenient for the grafting cooperation in stirring telescopic link and joint groove.
Preferably, the inner wall of joint groove opening orientation with the one end that stirring telescopic link deviates from the puddler all is fixed and is provided with the magnet of inter attraction.
Through adopting above-mentioned technical scheme, the setting of magnet for when stirring telescopic link is close to the joint groove soon, wash board and stirring telescopic link can be under the magnetic force adsorption of magnet, make the washing board can be automatic just right with the joint groove, further improvement stirring telescopic link and joint groove grafting complex smoothness nature and rapidity.
Preferably, the supporting ring frame has been seted up the spout near one side of wasing the board, and the spout is provided with the location extension spring towards on the inner wall of wasing the board, the one end of location extension spring and the inner wall fixed connection of spout, the other end and the washing board fixed connection of location extension spring, the axis of washing board and spout sliding fit and slip direction perpendicular to stirring pivot self.
Through adopting above-mentioned technical scheme, the setting of location extension spring for the cleaning plate when need not wasing the inner wall of reation kettle body, can make the cleaning plate be in the position that the spout deviates from reation kettle body inner wall through the effect of pulling force, the inner wall of brush hair and reation kettle body is not the butt on the cleaning plate this moment, has reduced the condition that the brush hair brought the damage with reation kettle body inner wall butt for a long time.
Preferably, the bristles are inclined in the following directions: inclined along the circumferential direction of the support ring frame.
Through adopting above-mentioned technical scheme, the washing setting of brush hair has improved the brush hair and has resisted the ability of stress when rotating along reation kettle body inner wall for the difficult harm of brush hair has improved the area of contact of brush hair with reation kettle body inner wall simultaneously, has improved the cleaning performance of brush hair to reation kettle body inner wall.
Preferably, the hydraulic pressure subassembly is including the hydraulic pressure case, the top surface fixed connection of hydraulic pressure case and reation kettle body, and the top surface of hydraulic pressure case is fixed to be provided with the push rod motor, and the fixed hydraulic plate that is provided with of output shaft of push rod motor, the hydraulic pressure board sets up inside the hydraulic pressure case, the hydraulic pressure board all around with the sealed butt of hydraulic pressure incasement wall, the position intercommunication that the hydraulic pressure case is close to the bottom is provided with the hydraulic pressure pipe, the hydraulic pressure pipe deviates from the one end and the intubate intercommunication setting of hydraulic pressure case.
Through adopting above-mentioned technical scheme, with the cooperation of pegging graft of hydraulic pressure pipe and intubate, start the push rod motor for the output shaft of push rod motor drives hydraulic pressure board and promotes hydraulic oil, thereby hydraulic oil promotes stirring telescopic link and removes towards the direction that deviates from the stirring pivot, and then makes stirring telescopic link can and wash the cooperation of joint between the board.
Preferably, the periphery department of stirring pivot is provided with the tooth, the tooth meshing of stirring pivot periphery department has connecting gear, the periphery department that the stirring pivot is provided with the tooth is provided with rotates the cover, it is on a parallel with the axis of stirring pivot self with stirring pivot normal running fit and axis of rotation to rotate the cover, annular holding tank has been seted up to the inside of rotating the cover, connecting gear sets up in the holding tank, connecting gear and holding tank normal running fit and axis of rotation are on a parallel with the axis of stirring pivot self, the fixed tooth that is provided with on the inner wall of holding tank periphery, tooth and the connecting gear meshing in the holding tank periphery, the fixed a plurality of defoaming poles that are provided with in periphery department of rotating the cover.
Through adopting above-mentioned technical scheme, when starting agitator motor and making the puddler stir the inside material of reation kettle body, the tooth in the puddler periphery also can produce the rotation, connect the gear this moment and can rotate along with the rotation of tooth on the puddler, it can drive the motion that the cover produced with the puddler opposite direction to connect the gear, it drives the defoaming pole and produces the rotation to rotate the cover, at this in-process, the cooperation of defoaming pole and puddler opposite rotation, can make the liquid material produce better disorder, make the more even that the material mixes, the slew velocity of defoaming pole is slower simultaneously, can play the effect of certain breaing up to chlorine gas bubble.
Preferably, the fixed a plurality of barbs that are provided with in the periphery of defoaming pole, the barb is the slope setting, and the direction of slope is: away from the defoaming rod in the direction away from the stirring rotating shaft.
By adopting the technical scheme and the arrangement of the barbs, the bubbles of the chlorine gas can be further scattered, so that the bubbles of the chlorine gas are smaller, the contact area between the chlorine gas and the material is increased, and the reaction between the chlorine gas and the material is quicker and more sufficient; simultaneously, the slope setting of barb has improved the area of contact between barb and the liquid material under the prerequisite of guaranteeing barb and defoaming pole fixed strength, has improved the effect of breaing up of barb to the chlorine bubble as far as.
In summary, the present application includes at least one of the following beneficial technical effects:
1. due to the arrangement of the stirring assembly, the effect of better and uniform mixing of the materials in the reaction kettle body can be achieved;
2. the cleaning component and the hydraulic component are arranged, so that the power source of the stirring component can be utilized to play a cleaning effect on the inner wall of the reaction kettle body;
3. the defoaming subassembly sets up, can break up the chlorine bubble, has improved the area of contact between chlorine and the material, has improved the chlorination reaction rate of material.
Drawings
FIG. 1 is a schematic view of a reaction kettle for continuous chlorination in accordance with an embodiment of the present disclosure;
FIG. 2 is a schematic partial sectional view for explaining the internal structure of a reaction vessel body;
FIG. 3 is an enlarged schematic view of section A of FIG. 1;
FIG. 4 is an enlarged schematic view of section B of FIG. 2;
FIG. 5 is an enlarged schematic view of section C of FIG. 2;
fig. 6 is an enlarged schematic view of a portion D in fig. 2.
Description of reference numerals: 1. a reaction kettle body; 2. a stirring assembly; 21. a stirring motor; 22. a stirring rotating shaft; 221. a slot; 222. inserting a tube; 223. a cavity; 23. a stirring rod; 24. stirring the telescopic rod; 3. cleaning the assembly; 31. a support ring frame; 311. a chute; 32. cleaning the plate; 321. a clamping groove; 33. brushing; 34. positioning a tension spring; 4. a defoaming assembly; 41. a defoaming rod; 411. a barb; 42. rotating the sleeve; 421. accommodating grooves; 43. a connecting gear; 5. a hydraulic assembly; 51. a hydraulic tank; 52. a hydraulic tube; 53. a push rod motor; 54. a hydraulic plate; 6. and a magnet.
Detailed Description
The present application is described in further detail below with reference to figures 1-6.
The embodiment of the application discloses reation kettle is used in continuous method chlorination.
Referring to fig. 1 and 2, a reaction kettle for continuous chlorination comprises a reaction kettle body 1, a stirring assembly 2, a cleaning assembly 3, a defoaming assembly 4 and a hydraulic assembly 5. The stirring assembly 2 is arranged at the position, close to the central axis, of the reaction kettle body 1, and plays a role in uniformly stirring and mixing substances in the reaction kettle body 1 to improve the reaction rate; the defoaming component 4 is arranged on the inner wall of the reaction kettle body 1 and is driven by the stirring component 2 to rotate, so that the reaction completeness rate of the materials is improved on the premise of improving the uniform mixing degree of the materials, and meanwhile, the chlorine bubbles in the reaction liquid are broken smaller, so that the contact area between the chlorine and the materials is increased, the combination degree of the chlorine and the reaction substances is improved, and the reaction speed of chlorination is increased; wash subassembly 3 and set up in the inner wall department of reation kettle body 1, through control hydraulic assembly 5, can be so that stirring subassembly 2 cooperates or removes the joint with 3 joints of washing subassembly to make stirring subassembly 2 can drive and wash subassembly 3 and rotate, wash to reation kettle body 1 inner wall, thereby make reation kettle body 1 have wash automatic, convenient and fast's advantage.
Referring to fig. 2 and 3, the stirring assembly 2 includes a stirring motor 21, a stirring rotating shaft 22, a stirring rod 23, and a stirring telescopic rod 24. Agitator motor 21 installation is fixed at the top surface of reation kettle body 1, and the center department of reation kettle body 1 is worn to locate by stirring pivot 22, and stirring pivot 22 is vertical with 1 normal running fit of reation kettle body and rotation axis, and slot 221 has been seted up to the top surface of stirring pivot 22, and agitator motor 21's output shaft is pegged graft in slot 221, and the outer axle of stirring pivot 22 is worn to be equipped with the output shaft of bolt with agitator motor 21 and stirring pivot 22 fixed coordination. Stirring pivot 22 is the cylinder structure that has annular cavity 223 in inside, and one side that stirring pivot 22 is close to agitator motor 21 is provided with intubate 222, and intubate 222 and the inside cavity 223 intercommunication of stirring pivot 22, hydraulic assembly 5 is through intubate 222 and the inside cavity 223 intercommunication of stirring pivot 22, and the inside cavity 223 of stirring pivot 22 is filled with hydraulic oil. The puddler 23 is provided with a plurality ofly along stirring pivot 22's circumference and axial, and this embodiment sets up puddler 23 and is provided with threely along stirring pivot 22's circumference, and the three puddler 23 of circumference is a set of, is provided with two sets ofly on the stirring pivot 22. The stirring rod 23 is fixedly connected with the stirring rotating shaft 22, and the stirring rod 23 is of a hollow tubular structure with two open ends. Stirring rod 24 sets up the one end that deviates from stirring pivot 22 at puddler 23, and stirring rod 24's periphery and the sealed sliding fit of puddler 23 internal circumference and the axis of sliding direction perpendicular to stirring pivot 22 self.
When needs stir the inside material of reation kettle body 1, start agitator motor 21, agitator motor 21's output shaft drives stirring pivot 22 and rotates to make stirring pivot 22 drive puddler 23 and produce and rotate, puddler 23 rotates the effect of stirring the mixing to the material. When needs wash reation kettle body 1's inner wall, operating personnel controls hydraulic assembly 5 for stirring telescopic link 24 is moving towards the direction that deviates from stirring pivot 22 under hydraulic effect, until stirring telescopic link 24 and wash the cooperation of joint between the subassembly 3, start agitator motor 21 this moment and can make agitator motor 21 drive and wash subassembly 3 and produce the rotation, thereby make and wash subassembly 3 and play better cleaning performance to reation kettle body 1's inner wall.
Referring to fig. 4 and 5, the cleaning assembly 3 includes a support ring frame 31, a cleaning plate 32, bristles 33, and a positioning tension spring 34. Support ring frame 31 is provided with two, and two support ring frames 31 set up respectively in the inside position that is close to top and bottom of reation kettle body 1, and support ring frame 31 is the annular setting, and support ring frame 31 and reation kettle body 1 normal running fit and axis of rotation are on a parallel with the axis of stirring pivot 22 self. The cleaning plate 32 is provided with a plurality ofly, and the quantity that this embodiment set up cleaning plate 32 is three, and three cleaning plate 32 evenly sets up along the circumference of support ring frame 31, cleaning plate 32 and the cooperation of stirring telescopic link 24 joint. The supporting ring frame 31 is close to one side of cleaning plate 32 and has been seted up spout 311, and the one end of location extension spring 34 is fixed on the inner wall of spout 311 orientation cleaning plate 32, and the other end and the cleaning plate 32 fixed connection of location extension spring 34, cleaning plate 32 both ends insert respectively in the spout 311 of two cleaning plates 32, cleaning plate 32 and spout 311 sliding fit and the axis of slip direction perpendicular to stirring pivot 22. Brush hair 33 sets up in the one side that wash plate 32 deviates from stirring pivot 22, and brush hair 33 cooperates with the inner wall butt of reation kettle body 1, and brush hair 33 is the direction that the slope set up and slope and does: horizontally inclined along the circumferential direction of the support ring frame 31.
When starting hydraulic assembly 5 and making stirring telescopic link 24 be continuous near the cleaning plate 32, the one end of stirring telescopic link 24 finally can be pegged graft in joint groove 321, and hydraulic assembly 5 can continue to promote stirring telescopic link 24 towards the direction that is close to cleaning plate 32 this moment to make stirring telescopic link 24 promote cleaning plate 32 and move towards the direction that is close to reation kettle body 1 inner wall, this moment location extension spring 34 is in tensile state. When the inner wall to reation kettle body 1 need not wash, start hydraulic assembly 5 and make and break away from between stirring telescopic link 24 and the cleaning plate 32, thereby make stirring assembly 2's rotation can not drive cleaning assembly 3 and remove, the loss to the energy among the stirring process has been reduced, and when breaking away from between stirring telescopic link 24 and the cleaning plate 32, cleaning plate 32 breaks away from reation kettle body 1's inner wall under the effect of location extension spring 34, the long-term butt of brush hair 33 has been reduced and the condition that brush hair 33 damaged has been made on reation kettle body 1's inner wall.
For the convenience of explaining the clamping matching mode of the stirring telescopic rod 24 and the cleaning plate 32, referring to fig. 5, a clamping groove 321 is formed in one side, close to the stirring telescopic rod 24, of the cleaning plate 32, the stirring telescopic rod 24 is in splicing matching with the clamping groove 321, one end, close to the cleaning plate 32, of the stirring telescopic rod 24 is arranged in a chamfer, and the chamfer is in a shape that the circumferential size is continuously reduced in the direction from the stirring rod 23 to the stirring telescopic rod 24. Equal fixedly connected with magnet 6 on one side that stirring telescopic link 24 is close to cleaning plate 32 and the inner wall of joint groove 321 opening orientation, magnet 6 on the stirring telescopic link 24 and the inside magnet 6 inter attraction of joint groove 321.
When needs peg graft in joint groove 321 with stirring telescopic link 24, operating personnel starts hydraulic assembly 5 and will stir telescopic link 24 and be continuous near cleaning plate 32, when stirring telescopic link 24 will be near cleaning plate 32, extract hydraulic pressure pipe 52 from intubate 222, then operating personnel rotates agitator motor 21 and makes stirring telescopic link 24 just can be to joint groove 321, insert hydraulic pressure pipe 52 on intubate 222 once more, continue to start hydraulic assembly 5 and make stirring telescopic link 24 finally insert in joint groove 321. The chamfer setting of the stirring telescopic rod 24 improves the accuracy and the fluency of the stirring telescopic rod 24 inserted into the clamping groove 321, and facilitates the insertion and connection matching of the stirring telescopic rod 24 and the clamping groove 321. And magnet 6's setting for when stirring telescopic link 24 is close to joint groove 321 soon, cleaning plate 32 and stirring telescopic link 24 can be under magnet 6's magnetic force adsorption, make cleaning plate 32 just right with joint groove 321 automatically, further improvement stirring telescopic link 24 and joint groove 321 grafting complex smoothness nature and rapidity.
Referring to fig. 1 and 2, the hydraulic assembly 5 includes a hydraulic tank 51, a hydraulic pipe 52, a push rod motor 53, and a hydraulic plate 54. The hydraulic tank 51 is fixedly arranged at the top end of the reaction kettle body 1, hydraulic oil is filled in the hydraulic tank 51, and the push rod motor 53 is fixedly arranged at the top end of the hydraulic tank 51. The hydraulic plate 54 is arranged in the hydraulic tank 51, the periphery of the hydraulic plate 54 is in butt joint and sealing with the inner wall of the hydraulic tank 51, and the hydraulic plate 54 is fixedly connected with the output shaft of the push rod motor 53. One end of the hydraulic tube 52 communicates with the hydraulic tank 51, and the other end of the hydraulic tube 52 communicates with the insert tube 222.
The hydraulic pushing principle of the hydraulic component 5 on the stirring telescopic rod 24 is as follows: the hydraulic pipe 52 is in plug-in fit with the insertion pipe 222, the push rod motor 53 is started, so that the output shaft of the push rod motor 53 drives the hydraulic plate 54 to push hydraulic oil, and the hydraulic oil pushes the stirring telescopic rod 24 to move towards the direction away from the stirring rotating shaft 22.
Referring to fig. 2 and 6, the defoaming assembly 4 includes a defoaming lever 41, a rotating sleeve 42, and a connecting gear 43. The rotating sleeve 42 is sleeved on the periphery of the stirring rotating shaft 22, the rotating sleeve 42 is arranged between the two stirring rods 23 in the axial direction of the stirring rotating shaft 22, and the rotating sleeve 42 is in rotating fit with the stirring rotating shaft 22 and the rotating axis is parallel to the axis of the stirring rotating shaft 22. An annular accommodating groove 421 is formed in the rotating sleeve 42, and the accommodating groove 421 penetrates through the inner periphery of the rotating sleeve 42. Connecting gear 43 is provided with a plurality ofly, this example sets up the quantity of connecting dimension and is six, six connecting gear 43 evenly arrange along stirring pivot 22's periphery, connecting gear 43 sets up the inside at holding tank 421, connecting gear 43 and the axis that the rotating sleeve 42 normal running fit and axis of rotation are on a parallel with stirring pivot 22 self, stirring pivot 22 is located the inside periphery department of holding tank 421 and is provided with the tooth, also be provided with the tooth on the inner wall of holding tank 421 periphery, connecting gear 43 and the equal meshing of tooth in stirring pivot 22 and the holding tank 421 periphery. Defoaming pole 41 is provided with a plurality ofly, and the quantity that this embodiment set up defoaming pole 41 is three, and three defoaming pole 41 evenly sets up along the circumference that rotates cover 42, defoaming pole 41 with rotate cover 42 fixed connection, fixed being provided with a plurality of barbs 411 in defoaming pole 41's the periphery, barb 411 is the slope setting, and the direction of slope is: away from the defoaming lever 41 in a direction away from the stirring rotation shaft 22.
When stirring subassembly 2 stirs the inside material of reation kettle body 1, the rotation of stirring pivot 22 can drive the rotation of stirring pivot 22 periphery going up the tooth, thereby it produces the rotation to drive connecting gear 43, connecting gear 43 rotates and drives and rotate cover 42 and produce the rotation, and the rotation direction that rotates cover 42 is opposite with the rotation direction of stirring pivot 22, it takes place to rotate cover 42 and drives defoaming pole 41 and rotate, barb 411 can be more garrulous of beating the chlorine bubble in the liquid material on the defoaming pole 41, the area of contact of chlorine and material has been improved, thereby the reaction rate of chlorine and material has been improved, defoaming pole 41 is for the antiport of puddler 23 simultaneously, the disorder degree that the material flows has been improved, make the material mix more even, further improvement the reaction rate of chlorine and material.
The implementation principle of a reaction kettle for continuous chlorination is as follows: when the chlorination reaction of the materials in the reaction kettle body 1 needs to be carried out, the stirring motor 21 is started, and the stirring telescopic rod 24 is positioned in the stirring rod 23 at the moment, so that the stress applied when the stirring rod 23 rotates is reduced, and the damage of the stirring rod 23 is reduced; in the stirring process, the stirring rod 23 and the defoaming rod 41 play a role in uniformly stirring the mixture of the materials, and meanwhile, the barbs 411 on the defoaming rod 41 can break up the bubbles of the chlorine, so that the reaction rate is further improved. Finish when the material chlorination, when needing to clear up reation kettle body 1's inner wall, operating personnel starts hydraulic assembly 5 and makes stirring rod 24 remove towards the direction that deviates from puddler 23, it is fixed until joint groove 321 joint on stirring rod 24 and the cleaning plate 32, and when continuing to promote brush hair 33 butt on cleaning plate 32 on the inner wall of reation kettle body 1, operating personnel starts agitator motor 21 and can make cleaning plate 32 rotate in order to play the effect of clearance to reation kettle body 1 inner wall.
The above embodiments are preferred embodiments of the present application, and the protection scope of the present application is not limited by the above embodiments, so: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.
Claims (10)
1. A reation kettle is used in continuous method chlorination which characterized in that: including reation kettle body (1), be provided with on reation kettle body (1) and be used for carrying out the stirring subassembly (2) that stir to reation kettle body (1) inside, be provided with on reation kettle body (1) inner wall and carry out abluent washing subassembly (3) to reation kettle body (1) inner wall, the position that reation kettle body (1) is close to the top is provided with control stirring subassembly (2) and washs subassembly (3) joint complex hydraulic component (5).
2. The reaction kettle for continuous chlorination according to claim 1, wherein: stirring subassembly (2) including agitator motor (21), agitator motor (21) are fixed in the position that reation kettle body (1) is close to the top, the output shaft fixedly connected with stirring pivot (22) of agitator motor (21), stirring pivot (22) are the structure that has annular cavity (223) in inside, one side that stirring pivot (22) are close to agitator motor (21) is provided with intubate (222), intubate (222) and stirring pivot (22) inside cavity (223) intercommunication, intubate (222) and hydraulic component (5) intercommunication, all be provided with hydraulic oil in cavity (223) and the hydraulic component (5) of stirring pivot (22), the periphery department of stirring pivot (22) is all fixed along axial and circumference and is provided with a plurality of puddlers (23), puddler (23) are the inside hollow structure of both ends opening, puddler (23) deviate from the one end of stirring pivot (22) and insert and are equipped with stirring telescopic link (24), the stirring telescopic rod (24) is in sliding fit with the stirring rod (23), the sliding axis is perpendicular to the axis of the stirring rod (23), and the inner cavity (223) of the stirring rod (23) is communicated with the inner cavity (223) of the stirring rotating shaft (22).
3. The reaction kettle for continuous chlorination according to claim 2, wherein: wash subassembly (3) including support ring frame (31), support ring frame (31) are provided with two, support ring frame (31) are the annular setting, two support ring frame (31) set up respectively in inside top and bottom department of reation kettle body (1), support ring frame (31) and reation kettle body (1) normal running fit and axis of rotation are on a parallel with the axis of stirring pivot (22), be provided with a plurality of washing board (32) between two support ring frame (31), the both ends of wasing board (32) respectively with two support ring frame (31) fixed connection, it is fixed brush hair (33) that one side that washing board (32) are close to reation kettle body (1) inner wall is provided with, brush hair (33) and reation kettle body (1) inner wall butt cooperation, joint groove (321) have been seted up to one side that washing board (32) are close to stirring pivot (22), joint groove (321) and the one end joint cooperation that stirring rod (23) deviate from with stirring rod (24).
4. The continuous chlorination reactor of claim 3, wherein: one end of the stirring telescopic rod (24) deviating from the stirring rod (23) is in a chamfer angle, and the chamfer angle is in a shape that the circumferential size is continuously reduced in the direction from the stirring rod (23) to the stirring telescopic rod (24).
5. The continuous chlorination reactor of claim 3, wherein: the inner wall of joint groove (321) opening orientation with stirring telescopic link (24) deviates from the one end of puddler (23) and all fixedly is provided with magnet (6) of inter attraction.
6. The continuous chlorination reactor of claim 3, wherein: one side that the supporting ring frame (31) is close to the cleaning plate (32) has been seted up spout (311), spout (311) are provided with location extension spring (34) on the inner wall towards cleaning plate (32), the one end of location extension spring (34) and the inner wall fixed connection of spout (311), the other end and the cleaning plate (32) fixed connection of location extension spring (34), cleaning plate (32) and spout (311) sliding fit and the axis of slip direction perpendicular to stirring pivot (22) self.
7. The continuous chlorination reactor of claim 3, wherein: the bristles (33) are inclined in the following directions: is inclined along the circumferential direction of the support ring frame (31).
8. The reaction kettle for continuous chlorination according to claim 2, wherein: hydraulic assembly (5) is including hydraulic tank (51), the top surface fixed connection of hydraulic tank (51) and reation kettle body (1), the fixed push rod motor (53) that is provided with of top surface of hydraulic tank (51), the fixed hydraulic plate (54) that is provided with of output shaft of push rod motor (53), hydraulic plate (54) set up inside hydraulic tank (51), all around with hydraulic tank (51) inner wall sealing butt of hydraulic plate (54), hydraulic tank (51) are close to the position intercommunication of bottom and are provided with hydraulic pressure pipe (52), hydraulic pressure pipe (52) deviate from the one end and intubate (222) intercommunication setting of hydraulic tank (51).
9. The reaction kettle for continuous chlorination according to claim 2, wherein: the periphery department of stirring pivot (22) is provided with the tooth, the tooth meshing of stirring pivot (22) periphery department has connecting gear (43), the periphery department that stirring pivot (22) was provided with the tooth is provided with rotates cover (42), it is parallel to the axis of stirring pivot (22) self with stirring pivot (22) normal running fit and axis of rotation to rotate cover (42), annular holding tank (421) have been seted up to the inside of rotating cover (42), connecting gear (43) set up in holding tank (421), connecting gear (43) and holding tank (421) normal running fit and axis of rotation are parallel to the axis of stirring pivot (22) self, the fixed tooth that is provided with on the inner wall of holding tank (421) periphery, holding tank (421) tooth in the periphery and connecting gear (43) meshing, the fixed a plurality of defoaming poles (41) that are provided with in periphery department of rotating cover (42).
10. The continuous chlorination reactor of claim 9, wherein: fixed a plurality of barbs (411) that are provided with in the periphery of defoaming pole (41), barb (411) are the slope setting, and the direction of slope is: away from the defoaming rod (41) in the direction away from the stirring rotating shaft (22).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011590053.5A CN112742327A (en) | 2020-12-29 | 2020-12-29 | Reaction kettle for continuous chlorination |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011590053.5A CN112742327A (en) | 2020-12-29 | 2020-12-29 | Reaction kettle for continuous chlorination |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112742327A true CN112742327A (en) | 2021-05-04 |
Family
ID=75646579
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011590053.5A Pending CN112742327A (en) | 2020-12-29 | 2020-12-29 | Reaction kettle for continuous chlorination |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112742327A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115557843A (en) * | 2022-10-19 | 2023-01-03 | 宁夏中盛新科技有限公司 | Process for preparing 2, 4-dinitro-6-chloroaniline by sulfuric acid method |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017101596A1 (en) * | 2015-12-16 | 2017-06-22 | 吴伟峰 | Novel chemical reactor |
| CN210675200U (en) * | 2019-09-12 | 2020-06-05 | 广东新辉化学有限公司 | Reation kettle with cleaning function |
| CN111321064A (en) * | 2020-03-09 | 2020-06-23 | 安徽环球基因科技有限公司 | Bioreactor for preparing monoclonal antibody |
| CN211800816U (en) * | 2020-01-20 | 2020-10-30 | 易洁维(辽宁)能源科技有限公司 | Reation kettle for chemical production with reciprocal stirring function |
-
2020
- 2020-12-29 CN CN202011590053.5A patent/CN112742327A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2017101596A1 (en) * | 2015-12-16 | 2017-06-22 | 吴伟峰 | Novel chemical reactor |
| CN210675200U (en) * | 2019-09-12 | 2020-06-05 | 广东新辉化学有限公司 | Reation kettle with cleaning function |
| CN211800816U (en) * | 2020-01-20 | 2020-10-30 | 易洁维(辽宁)能源科技有限公司 | Reation kettle for chemical production with reciprocal stirring function |
| CN111321064A (en) * | 2020-03-09 | 2020-06-23 | 安徽环球基因科技有限公司 | Bioreactor for preparing monoclonal antibody |
Non-Patent Citations (1)
| Title |
|---|
| 杨耀东 等: "《液压与气动技术》", 31 August 2017, 北京理工大学出版社 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115557843A (en) * | 2022-10-19 | 2023-01-03 | 宁夏中盛新科技有限公司 | Process for preparing 2, 4-dinitro-6-chloroaniline by sulfuric acid method |
| CN115557843B (en) * | 2022-10-19 | 2023-10-13 | 宁夏中盛新科技有限公司 | Process for preparing 2, 4-binitro-6-chloroaniline by sulfuric acid method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN212417825U (en) | Industrial stirring equipment with cleaning function | |
| CN112742327A (en) | Reaction kettle for continuous chlorination | |
| CN113578119A (en) | Automatic hypochlorous acid solution preparation device | |
| CN208642443U (en) | A kind of lithium battery electrolytes agitating device | |
| CN213703966U (en) | Hollow brick double-shaft mixer | |
| CN109761198A (en) | A kind of equipment of automatic production liquor natrii hypochloritis | |
| CN216198031U (en) | Composite acid injection device | |
| CN108211920A (en) | A kind of coating automatic stirring and cleaning device | |
| CN107935249A (en) | A kind of new PET production modifying porcelain device | |
| CN113115934A (en) | Automatic boiling equipment for donkey-hide gelatin | |
| CN208894125U (en) | A kind of production system based on mildy wash production | |
| CN215611039U (en) | Stirring device for wall heat-insulating material | |
| CN220276737U (en) | Mixing device for food additives | |
| CN213563492U (en) | Cement paste mixer | |
| CN214439015U (en) | A reation kettle for preparing strontium fluoride | |
| CN214261591U (en) | Stirring barrel for producing hard alloy material | |
| CN216704264U (en) | Composite printing paste preparation device | |
| CN220779930U (en) | Dynamic and static stirrer | |
| CN218131239U (en) | Agitating unit is used in detergent production | |
| CN108404773A (en) | A kind of printing and dyeing raw material blending device | |
| CN213467772U (en) | Reation kettle for chemical production | |
| CN209549356U (en) | A kind of preparation facilities of polymolecularity acid dyes | |
| CN219567880U (en) | Camellia oil stirring decoloration device | |
| CN220003858U (en) | Mixing tank convenient to wash | |
| CN219342568U (en) | Dyeing device of blending machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20210504 |
|
| RJ01 | Rejection of invention patent application after publication |