CN112717864A - Prevent blockking up type sodium metabisulfite preparation reation kettle - Google Patents

Prevent blockking up type sodium metabisulfite preparation reation kettle Download PDF

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Publication number
CN112717864A
CN112717864A CN202011429749.XA CN202011429749A CN112717864A CN 112717864 A CN112717864 A CN 112717864A CN 202011429749 A CN202011429749 A CN 202011429749A CN 112717864 A CN112717864 A CN 112717864A
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CN
China
Prior art keywords
fixedly connected
sodium metabisulfite
reaction kettle
kettle body
reation kettle
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011429749.XA
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Chinese (zh)
Inventor
刘俊明
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Tonggu County Xianghong Chemical Co ltd
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Tonggu County Xianghong Chemical Co ltd
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Priority to CN202011429749.XA priority Critical patent/CN112717864A/en
Publication of CN112717864A publication Critical patent/CN112717864A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0073Sealings
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01DCOMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
    • C01D5/00Sulfates or sulfites of sodium, potassium or alkali metals in general
    • C01D5/14Preparation of sulfites
    • C01D5/145Pyrosulfites or metabisulfites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/00777Baffles attached to the reactor wall horizontal

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to the technical field of sodium metabisulfite and discloses an anti-blocking type sodium metabisulfite preparation reaction kettle which comprises a reaction kettle body, wherein a supporting block is fixedly connected to one side of the reaction kettle body, a supporting leg is movably connected to the bottom of the supporting block, a connecting rod is fixedly connected to one side of the supporting leg, a vertical plate is fixedly connected to the inner bottom wall of the reaction kettle body, a partition plate is movably connected to the outer wall of the vertical plate, and a through groove is formed in the top of the partition plate. This prevent blockking up type sodium metabisulfite preparation reation kettle, reached convenient to detach's purpose, the problem of general sodium metabisulfite preparation reation kettle not convenient to detach has been solved, the clearance is dismantled to it after using to the reation kettle body of can being convenient for, reduce the reaction of often carrying on some solid-liquid mixture, lead to the long-time accumulational condition that easily causes the material in using reation kettle, the work of being convenient for mix, thereby improve the quality of mixing, convenient to use person's use.

Description

Prevent blockking up type sodium metabisulfite preparation reation kettle
Technical Field
The invention relates to the technical field of sodium metabisulfite, in particular to an anti-blocking type sodium metabisulfite preparation reaction kettle.
Background
The sodium pyrosulfite is white or yellow crystal powder or small crystals, has strong SO2 smell, has a specific gravity of one to four, is dissolved in water, is acidic in aqueous solution, releases SO2 when being contacted with strong acid to generate corresponding salts, and is oxidized into Na2S2O6 when being placed in air for a long time, SO the product cannot be stored for a long time, namely SO2 is decomposed when being higher than 150 ℃, and is used for producing sodium hydrosulfite, sulfamethazine, caprolactam and the like, and purifying chloroform, phenyl sulfone and benzaldehyde, the photographic industry is used as ingredients of fixing agents, the perfume industry is used for producing vanillin, is used as a brewing industry preservative, a rubber coagulant and a dechlorinating agent after cotton bleaching, organic intermediates, dyes, tanning are used as a reducing agent for electroplating industry, the wastewater treatment of oil fields and is used as a mine beneficiation agent of sodium pyrosulfite, and the use of a reaction kettle is particularly important in the preparation production of the sodium pyrosulfite.
However, in the existing market, a general reaction kettle for preparing sodium metabisulfite is inconvenient to disassemble and clean after use, and often reacts with some solid-liquid mixtures, so that the materials are easy to accumulate in the reaction kettle after long-time use, the mixing work is influenced, and the mixing quality is also easy to reduce, so that the existing reaction kettle for preparing sodium metabisulfite cannot meet the use requirements of people, and the work of people is inconvenient.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the anti-blocking type sodium metabisulfite preparation reaction kettle which has the advantages of convenience in disassembly and the like, and solves the problem that a common sodium metabisulfite preparation reaction kettle is inconvenient to disassemble.
(II) technical scheme
In order to realize the purpose that the reaction kettle for preparing the sodium metabisulfite is convenient to disassemble, the invention provides the following technical scheme: the utility model provides a prevent blockking up type sodium metabisulfite preparation reation kettle, includes the reation kettle body, one side fixedly connected with supporting shoe of reation kettle body, the bottom swing joint of supporting shoe has the supporting leg, one side fixedly connected with connecting rod of supporting leg, the interior diapire fixedly connected with riser of reation kettle body, the outer wall swing joint of riser has the baffle, logical groove has been seted up at the top of baffle, the bottom fixedly connected with spring of baffle, the one end fixedly connected with backup pad of spring, the top swing joint of reation kettle body has the apron.
The utility model discloses a reaction kettle, including apron, top fixedly connected with motor, the output shaft of motor passes through shaft coupling fixedly connected with dwang, the outer wall fixedly connected with stirring leaf of dwang, the spacing planking of one side fixedly connected with of apron, the slot has been seted up to one side of reation kettle body, one side swing joint of spacing planking has first screw rod, the outer wall swing joint of spacing planking has solid fixed ring, gu fixed ring's outer wall fixedly connected with fixed block, the top swing joint of fixed block has the second screw rod.
Preferably, the connecting groove has been seted up at the top of fixed block, and the inner wall of connecting groove is provided with the internal thread, and the fixed block passes through internal thread and second screw rod threaded connection.
Preferably, the slot has all been seted up to one side of spacing planking and reation kettle body, and the inner wall of slot is provided with the internal thread, and spacing planking and reation kettle body all pass through internal thread and first screw rod threaded connection.
Preferably, the inside wall fixedly connected with filter screen that leads to the groove, and the shape size that leads to the groove all matches each other with the shape size of filter screen.
Preferably, the top of the cover plate is fixedly connected with a motor box, and the interior of the motor box is movably connected with the outer wall of the motor.
Preferably, the number of baffles and the number of filter screens are two, and each baffle and each filter screen are a set of, and two sets of baffles and filter screens use the perpendicular central line of reation kettle body as symmetry axis symmetry setting.
Preferably, the bottom of the cover plate is fixedly connected with a sealing gasket, the sealing gasket is a hollow sealing gasket, and the sealing gasket is a rubber sealing gasket.
(III) advantageous effects
Compared with the prior art, the invention provides an anti-blocking type sodium metabisulfite preparation reaction kettle which has the following beneficial effects:
1. this prevent blockking up type sodium metabisulfite preparation reation kettle, through the reation kettle body, a cover plate, spacing planking, the slot, first screw rod, gu fixed ring, the use of mutually supporting of fixed block and second screw rod, convenient to detach's purpose has been reached, the problem of general sodium metabisulfite preparation reation kettle convenient to detach is solved, the clearance is dismantled to it after using to the reation kettle body of can being convenient for, reduce the reaction that often carries out some solid-liquid mixture, lead to the long-time accumulational condition that easily causes the material in using reation kettle, the work of being convenient for mix, thereby improve the quality of mixing, people's user demand has further been satisfied, work for people brings the facility.
2. This prevent blockking up type sodium metabisulfite preparation reation kettle, through the use of mutually supporting of riser, baffle, logical groove, filter screen, spring and backup pad, can play the effect of rocking to piling up the material on the baffle, avoid sodium metabisulfite ejection of compact to cause the condition that the discharging pipe blockked up when preparation is accomplished, avoid influencing work efficiency, and reduce the cost of labor of mediation business turn over material mouth, satisfied people's user demand, be worth promoting.
3. This prevent blockking up type sodium metabisulfite preparation reation kettle uses through mutually supporting of apron and sealed pad, can improve this internal leakproofness of reation kettle, avoids this internal relatively poor effect that reduces the internal reaction of leakproofness of reation kettle, reduces the trouble and the loss of unnecessary, has satisfied people's user demand.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a front view of the present invention;
FIG. 3 is a schematic view of a retaining ring according to the present invention;
FIG. 4 is an enlarged view of the invention at A in FIG. 1.
In the figure: 1. a reaction kettle body; 2. a support block; 3. supporting legs; 4. a connecting rod; 5. a vertical plate; 6. a partition plate; 7. a through groove; 8. filtering with a screen; 9. a spring; 10. a support plate; 11. a cover plate; 12. a motor; 13. rotating the rod; 14. a gasket; 15. a limiting outer plate; 16. a slot; 17. a first screw; 18. a fixing ring; 19. a fixed block; 20. a second screw; 21. stirring the leaves.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, an anti-clogging sodium metabisulfite preparation reaction kettle comprises a reaction kettle body 1, wherein one side of the reaction kettle body 1 is fixedly connected with a supporting block 2, the bottom of the supporting block 2 is movably connected with a supporting leg 3, one side of the supporting leg 3 is fixedly connected with a connecting rod 4, the inner bottom wall of the reaction kettle body 1 is fixedly connected with a vertical plate 5, the outer wall of the vertical plate 5 is movably connected with a partition plate 6, the top of the partition plate 6 is provided with a through groove 7, the inner side wall of the through groove 7 is fixedly connected with a filter screen 8, the shape and size of the through groove 7 are matched with the shape and size of the filter screen 8, the number of the partition plates 6 and the number of the filter screens 8 are two, each partition plate 6 and each filter screen 8 are in one group, the two groups of partition plates 6 and filter screens 8, spring 9's one end fixedly connected with backup pad 10, through riser 5, baffle 6, lead to groove 7, filter screen 8, spring 9 and backup pad 10 mutually support and use, can play the effect of rocking to piling up the material on baffle 6, avoid sodium metabisulfite ejection of compact to cause the condition that the discharging pipe blockked up when preparation is accomplished, avoid influencing work efficiency, and reduce the cost of labor of mediation business turn over material mouth, people's user demand has been satisfied, be worth using widely, the top swing joint of reation kettle body 1 has apron 11.
The top of the cover plate 11 is fixedly connected with a motor 12, the top of the cover plate 11 is fixedly connected with a motor box, the interior of the motor box is movably connected with the outer wall of the motor 12, the output shaft of the motor 12 is fixedly connected with a rotating rod 13 through a coupler, the bottom of the cover plate 11 is fixedly connected with a sealing gasket 14, the sealing gasket 14 is a hollow sealing gasket, the sealing gasket 14 is a rubber sealing gasket, rubber is a high-elasticity polymer material with reversible deformation, the rubber is rich in elasticity at room temperature, can generate large deformation under the action of small external force, can recover the original shape after the external force is removed, the sealing property in the reaction kettle body 1 can be improved through the mutual matching use of the cover plate 11 and the sealing gasket 14, the effect of internal reaction caused by poor sealing property in the reaction kettle body 1 is avoided, unnecessary troubles and loss are reduced, the use requirements of people are, one side of the cover plate 11 is fixedly connected with a limiting outer plate 15, one side of the reaction kettle body 1 is provided with a slot 16, one sides of the limiting outer plate 15 and the reaction kettle body 1 are both provided with slots 16, the inner wall of each slot 16 is provided with an internal thread, the limiting outer plate 15 and the reaction kettle body 1 are both in threaded connection with a first screw 17 through the internal thread, one side of the limiting outer plate 15 is movably connected with a first screw 17, the outer wall of the limiting outer plate 15 is movably connected with a fixing ring 18, the outer wall of the fixing ring 18 is fixedly connected with a fixing block 19, the top of the fixing block 19 is provided with a connecting groove, the inner wall of the connecting groove is provided with the internal thread, the fixing block 19 is in threaded connection with a second screw 20 through the internal thread, the reaction kettle body 1, the cover plate 11, the limiting outer plate 15, the slot 16, the first screw 17, the fixing ring, the purpose of convenient to detach has been reached, the problem of general sodium metabisulfite preparation reation kettle inconvenient to detach has been solved, the clearance is dismantled to it after using to reation kettle body 1 of can being convenient for, reduce the reaction of often carrying out some solid-liquid mixture, lead to the long-time accumulational condition that easily causes the material in using reation kettle, the work of the mixture of being convenient for to improve the quality of mixing, further satisfied people's user demand, the work of giving people brings.
The electrical components presented in the document are all electrically connected with an external master controller and 220V mains, and the master controller can be a conventional known device controlled by a computer or the like.
When using, when needing to clear up in the reation kettle body 1, roll out second screw rod 20, be convenient for take off solid fixed ring 18 from reation kettle body 1 is outer, roll out first screw rod 17 from spacing planking 15 and reation kettle body 1, be convenient for take off apron 11, the person of facilitating the use clears up in stirring leaf 21 and reation kettle body 1, filter screen 8 on the baffle 6 can filter the sodium metabisulfite powder piece of not fully stirring simultaneously, sodium metabisulfite powder piece can make spring 9 produce deformation and rock when piling up on baffle 6, baffle 6 reciprocates on riser 5, avoid the jam of discharging pipe when the ejection of compact.
To sum up, this prevent blockking up type sodium metabisulfite preparation reation kettle has solved the problem that general sodium metabisulfite preparation reation kettle is not convenient for dismantle, and not only the person of facilitating the use clears up in to reation kettle body 1, also is convenient for dismantle it simultaneously, further improves reation kettle body 1's practicality, brings the facility for user's use.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. The utility model provides a prevent blockking up type sodium metabisulfite preparation reation kettle, includes reation kettle body (1), its characterized in that: a supporting block (2) is fixedly connected to one side of the reaction kettle body (1), supporting legs (3) are movably connected to the bottom of the supporting block (2), a connecting rod (4) is fixedly connected to one side of each supporting leg (3), a vertical plate (5) is fixedly connected to the inner bottom wall of the reaction kettle body (1), a partition plate (6) is movably connected to the outer wall of each vertical plate (5), a through groove (7) is formed in the top of each partition plate (6), a spring (9) is fixedly connected to the bottom of each partition plate (6), a supporting plate (10) is fixedly connected to one end of each spring (9), and a cover plate (11) is movably connected to the top of the reaction kettle body (1);
the utility model discloses a reaction kettle, including the top fixedly connected with motor (12) of apron (11), the output shaft of motor (12) passes through shaft coupling fixedly connected with dwang (13), the outer wall fixedly connected with stirring leaf (21) of dwang (13), the spacing planking (15) of one side fixedly connected with of apron (11), slot (16) have been seted up to one side of reation kettle body (1), one side swing joint of spacing planking (15) has first screw rod (17), the outer wall swing joint of spacing planking (15) has solid fixed ring (18), the outer wall fixedly connected with fixed block (19) of solid fixed ring (18), the top swing joint of fixed block (19) has second screw rod (20).
2. The anti-blocking sodium metabisulfite preparation reaction kettle according to claim 1, wherein: the connecting groove has been seted up at the top of fixed block (19), and the inner wall of connecting groove is provided with the internal thread, and fixed block (19) pass through internal thread and second screw rod (20) threaded connection.
3. The anti-blocking sodium metabisulfite preparation reaction kettle according to claim 1, wherein: slot (16) have all been seted up to one side of spacing planking (15) and reation kettle body (1), and the inner wall of slot (16) is provided with the internal thread, and just spacing planking (15) and reation kettle body (1) all through internal thread and first screw rod (17) threaded connection.
4. The anti-blocking sodium metabisulfite preparation reaction kettle according to claim 1, wherein: the inside wall fixedly connected with filter screen (8) that lead to groove (7), and the shape size that leads to groove (7) all matches each other with the shape size of filter screen (8).
5. The anti-blocking sodium metabisulfite preparation reaction kettle according to claim 1, wherein: the top of the cover plate (11) is fixedly connected with a motor box, and the interior of the motor box is movably connected with the outer wall of the motor (12).
6. The reactor for preparing sodium metabisulfite with anti-blocking function as claimed in claim 1 and 8, wherein: the quantity of baffle (6) and the quantity of filter screen (8) are two, and each baffle (6) and each filter screen (8) are a set of, and two sets of baffles (6) and filter screen (8) use the perpendicular central line of reation kettle body (1) to set up as symmetry axis symmetry.
7. The anti-blocking sodium metabisulfite preparation reaction kettle according to claim 1, wherein: the bottom fixedly connected with of apron (11) seals up (14), and sealed pad (14) are hollow seal pad, and sealed pad (14) are rubber seal pad.
CN202011429749.XA 2020-12-09 2020-12-09 Prevent blockking up type sodium metabisulfite preparation reation kettle Pending CN112717864A (en)

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Application Number Priority Date Filing Date Title
CN202011429749.XA CN112717864A (en) 2020-12-09 2020-12-09 Prevent blockking up type sodium metabisulfite preparation reation kettle

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Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107185473A (en) * 2017-07-13 2017-09-22 衡阳屹顺化工有限公司 A kind of anticlogging reactor
CN207929209U (en) * 2018-01-19 2018-10-02 天津浩元精细化工股份有限公司 A kind of Chemical Manufacture condensation reaction kettle
CN210206841U (en) * 2019-05-24 2020-03-31 酒泉智捷工业科技有限责任公司 Sodium sulfide preparation reation kettle
CN210279159U (en) * 2019-07-11 2020-04-10 扬州市金诺尔不锈钢有限公司 Stainless steel reation kettle for chemical industry
CN210473988U (en) * 2019-08-17 2020-05-08 龙口佳源颜料有限公司 Reation kettle with filtering capability
CN211358782U (en) * 2019-07-01 2020-08-28 南京承佑树脂有限公司 Screw type directional polymerization device
CN211676386U (en) * 2020-01-03 2020-10-16 湖南复瑞生物医药技术有限责任公司 Crystallization kettle fixing structure

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107185473A (en) * 2017-07-13 2017-09-22 衡阳屹顺化工有限公司 A kind of anticlogging reactor
CN207929209U (en) * 2018-01-19 2018-10-02 天津浩元精细化工股份有限公司 A kind of Chemical Manufacture condensation reaction kettle
CN210206841U (en) * 2019-05-24 2020-03-31 酒泉智捷工业科技有限责任公司 Sodium sulfide preparation reation kettle
CN211358782U (en) * 2019-07-01 2020-08-28 南京承佑树脂有限公司 Screw type directional polymerization device
CN210279159U (en) * 2019-07-11 2020-04-10 扬州市金诺尔不锈钢有限公司 Stainless steel reation kettle for chemical industry
CN210473988U (en) * 2019-08-17 2020-05-08 龙口佳源颜料有限公司 Reation kettle with filtering capability
CN211676386U (en) * 2020-01-03 2020-10-16 湖南复瑞生物医药技术有限责任公司 Crystallization kettle fixing structure

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Application publication date: 20210430