CN112680297A - Soap grain formula and production process - Google Patents
Soap grain formula and production process Download PDFInfo
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- CN112680297A CN112680297A CN202011640509.4A CN202011640509A CN112680297A CN 112680297 A CN112680297 A CN 112680297A CN 202011640509 A CN202011640509 A CN 202011640509A CN 112680297 A CN112680297 A CN 112680297A
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Abstract
The invention discloses a soap grain formula and a production process, and relates to the technical field of soap grain production, wherein the soap grain comprises the following raw materials in percentage by mass: water content of 18.5-19.5%, glycine of 0.3-0.7%, free fatty acid of 0.1-0.5%, alkali liquor of 0.01-0.03%, sodium chloride solution of 0.4-0.6%, ethanol of 0.5-1.0%, EDTA of 0.03-0.05% and HEDP of 0.03-0.05%, and fatty acid as the rest solvent. The invention is suitable for the continuous production of large-batch soap particles, can provide unusual economic benefits for manufacturers, can also meet the increasing requirement of the soap particles in society, can replace phosphorus-containing washing powder to clean clothes, prevents phosphorus-containing substances from flowing into river water to cause river water eutrophication, and plays a role in protecting the environment.
Description
Technical Field
The invention relates to the technical field of soap grain production, in particular to a soap grain formula and a production process.
Background
The soap grain mainly refers to a complex mixture of fatty acid sodium salts, has excellent wetting, dispersing and cleaning capabilities, and is suitable for soaping after textile dyeing and quick washing of production equipment. The soap grain is mainly used for producing perfumed soap, laundry soap, transparent soap and the like, the soap powder is used for washing powder and other hard soap cleaning products, and the basic character and appearance are as follows: white granular solids (mostly vegetable oil soap particles) creamy yellow granular solids (animal based soap particles).
However, in the prior art, the traditional soap granule production process is complex, and large-batch continuous production cannot be carried out, so that the production speed is reduced, which directly results in that the increasingly-increased soap granule requirement in society cannot be met.
Disclosure of Invention
The invention aims to provide a soap particle formula and a production process, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
the soap grain formula comprises the following raw materials in percentage by mass: water content of 18.5-19.5%, glycine of 0.3-0.7%, free fatty acid of 0.1-0.5%, alkali liquor of 0.01-0.03%, sodium chloride solution of 0.4-0.6%, ethanol of 0.5-1.0%, EDTA of 0.03-0.05% and HEDP of 0.03-0.05%, and fatty acid as the rest solvent.
As a further scheme of the invention: the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of the sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
As a still further scheme of the invention: and a first heater is arranged in the first mixer in the second step, and the heating temperature is 65-98 ℃.
As a still further scheme of the invention: and a second heater is arranged in the second mixer in the third step, and the heating temperature is 65-98 ℃.
As a still further scheme of the invention: and a third heater is arranged in the third mixer in the fourth step, and the heating temperature is 65-98 ℃.
As a still further scheme of the invention: and step ten, additionally arranging a metal separator, conveying the unqualified soap particles to the metal separator for metal separation, conveying the soap particles subjected to metal separation to the metal detector again, and continuously detecting whether metal exists or not until the soap particles are qualified.
Compared with the prior art, the invention has the beneficial effects that: the invention is suitable for the continuous production of large-batch soap particles, can provide unusual economic benefits for manufacturers, can also meet the increasing requirement of the soap particles in society, can replace phosphorus-containing washing powder to clean clothes, prevents phosphorus-containing substances from flowing into river water to cause river water eutrophication, and plays a role in protecting the environment.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The first embodiment is as follows:
a soap grain formula comprises the following raw materials in percentage by mass: 18.5% of water, 0.3% of glycine, 0.1% of free fatty acid, 0.01% of alkali liquor, 0.4% of sodium chloride solution, 0.5% of ethanol, 0.03% of EDTA and 0.03% of HEDP, and the rest of terminal solvent is fatty acid.
Wherein the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
And a first heater is arranged in the first mixer in the step two, the heating temperature is 81.5 ℃, a second heater is arranged in the second mixer in the step three, the heating temperature is 81.5 ℃, a third heater is arranged in the third mixer in the step four, the heating temperature is 81.5 ℃, a metal separator is additionally arranged in the step ten, the soap particles which are detected to be unqualified are conveyed into the metal separator for metal separation operation, the soap particles which are subjected to metal separation are conveyed into the metal detector again, and the metal detection is continuously carried out until the detection is qualified.
Example two:
a soap grain formula comprises the following raw materials in percentage by mass: 19.5% of water, 0.7% of glycine, 0.5% of free fatty acid, 0.03% of alkali liquor, 0.6% of sodium chloride solution, 1.0% of ethanol, 0.05% of EDTA and 0.05% of HEDP, and the rest of terminal solvent is fatty acid.
Wherein the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
And a first heater is arranged in the first mixer in the step two, the heating temperature is 81.5 ℃, a second heater is arranged in the second mixer in the step three, the heating temperature is 81.5 ℃, a third heater is arranged in the third mixer in the step four, the heating temperature is 81.5 ℃, a metal separator is additionally arranged in the step ten, the soap particles which are detected to be unqualified are conveyed into the metal separator for metal separation operation, the soap particles which are subjected to metal separation are conveyed into the metal detector again, and the metal detection is continuously carried out until the detection is qualified.
Example three:
a soap grain formula comprises the following raw materials in percentage by mass: 19% of water, 0.5% of glycine, 0.3% of free fatty acid, 0.02% of alkali liquor, 0.5% of sodium chloride solution, 0.75% of ethanol, 0.04% of EDTA and 0.04% of HEDP, and the balance of the terminal solvent is fatty acid.
Wherein the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
And a first heater is arranged in the first mixer in the step two, the heating temperature is 81.5 ℃, a second heater is arranged in the second mixer in the step three, the heating temperature is 81.5 ℃, a third heater is arranged in the third mixer in the step four, the heating temperature is 81.5 ℃, a metal separator is additionally arranged in the step ten, the soap particles which are detected to be unqualified are conveyed into the metal separator for metal separation operation, the soap particles which are subjected to metal separation are conveyed into the metal detector again, and the metal detection is continuously carried out until the detection is qualified.
Example four:
a soap grain formula comprises the following raw materials in percentage by mass: 19% of water, 0.5% of glycine, 0.3% of free fatty acid, 0.02% of alkali liquor, 0.5% of sodium chloride solution, 0.75% of ethanol, 0.04% of EDTA and 0.04% of HEDP, and the balance of the terminal solvent is fatty acid.
Wherein the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
And a first heater is arranged in the first mixer in the step two, the heating temperature is 65 ℃, a second heater is arranged in the second mixer in the step three, the heating temperature is 65 ℃, a third heater is arranged in the third mixer in the step four, the heating temperature is 65 ℃, a metal separator is additionally arranged in the step ten, the soap particles which are detected to be unqualified are conveyed into the metal separator for metal separation operation, the soap particles which are subjected to metal separation are conveyed into the metal detector again, and the metal detection is continuously carried out until the detection is qualified.
Example five:
a soap grain formula comprises the following raw materials in percentage by mass: 19% of water, 0.5% of glycine, 0.3% of free fatty acid, 0.02% of alkali liquor, 0.5% of sodium chloride solution, 0.75% of ethanol, 0.04% of EDTA and 0.04% of HEDP, and the balance of the terminal solvent is fatty acid.
Wherein the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of sodium hydroxide in the alkali liquor is 30-50%.
A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
And step ten, additionally arranging a metal separator, conveying the unqualified soap particles to the metal separator for metal separation, conveying the soap particles subjected to metal separation to the metal detector again, and continuously detecting whether metal exists or not until the qualified soap particles are detected.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.
Claims (7)
1. A soap particle formula, which is characterized in that: the soap particles comprise the following raw materials in percentage by mass: water content of 18.5-19.5%, glycine of 0.3-0.7%, free fatty acid of 0.1-0.5%, alkali liquor of 0.01-0.03%, sodium chloride solution of 0.4-0.6%, ethanol of 0.5-1.0%, EDTA of 0.03-0.05% and HEDP of 0.03-0.05%, and fatty acid as the rest solvent.
2. The soap pellet formulation of claim 1 wherein: the alkali liquor is sodium hydroxide solution, the alkali liquor is at normal temperature, and the concentration of the sodium hydroxide in the alkali liquor is 30-50%.
3. A production process of soap particles comprises the following steps:
the method comprises the following steps: firstly, weighing and proportioning raw materials according to mass percentage for later use;
step two: conveying fatty acid, water and free fatty acid to a first mixer, and mixing and heating to form a first mixture;
step three: conveying the alkali liquor and the sodium chloride solution to a second mixer, and mixing and heating to form a second mixture;
step four: conveying glycine, ethanol, EDTA and HEDP into a third mixer, mixing and heating to form a third mixer;
step five: simultaneously conveying the first mixture, the second mixture and the third mixture to a first homogenizer, and mixing and stirring to form a fourth mixture;
step six: conveying the mixture IV into a soap reactor for saponification reaction to prepare a product;
step seven: conveying the resultant into a bar making machine, and extruding the resultant into soap granules;
step nine: conveying the soap particles into a three-roller grinding machine, grinding the soap particles, and conveying the ground soap particles into a refining machine through a first belt conveyor for refining;
step ten: conveying the refined soap particles into a metal detector through a second belt conveyor to detect whether metal exists or not;
step eleven: and conveying the qualified soap particles to a packaging machine for packaging the soap particles.
4. A process for the production of soap pellets as claimed in claim 3 wherein: and a first heater is arranged in the first mixer in the second step, and the heating temperature is 65-98 ℃.
5. A process for the production of soap pellets as claimed in claim 3 wherein: and a second heater is arranged in the second mixer in the third step, and the heating temperature is 65-98 ℃.
6. A process for the production of soap pellets as claimed in claim 3 wherein: and a third heater is arranged in the third mixer in the fourth step, and the heating temperature is 65-98 ℃.
7. The process for producing soap pellets as claimed in claim 1, wherein: and step ten, additionally arranging a metal separator, conveying the unqualified soap particles to the metal separator for metal separation, conveying the soap particles subjected to metal separation to the metal detector again, and continuously detecting whether metal exists or not until the soap particles are qualified.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011640509.4A CN112680297A (en) | 2020-12-31 | 2020-12-31 | Soap grain formula and production process |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011640509.4A CN112680297A (en) | 2020-12-31 | 2020-12-31 | Soap grain formula and production process |
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| CN112680297A true CN112680297A (en) | 2021-04-20 |
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| CN202011640509.4A Pending CN112680297A (en) | 2020-12-31 | 2020-12-31 | Soap grain formula and production process |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104017674A (en) * | 2014-06-20 | 2014-09-03 | 益海（东莞）油化工业有限公司 | Anti-freezing soap grain and production method thereof |
| CN110003998A (en) * | 2019-04-25 | 2019-07-12 | 湖南日用化学科学研究所有限公司 | A kind of long-acting fluorescent brightener added detergent and preparation method thereof with highly effective chelating ability |
-
2020
- 2020-12-31 CN CN202011640509.4A patent/CN112680297A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104017674A (en) * | 2014-06-20 | 2014-09-03 | 益海（东莞）油化工业有限公司 | Anti-freezing soap grain and production method thereof |
| CN110003998A (en) * | 2019-04-25 | 2019-07-12 | 湖南日用化学科学研究所有限公司 | A kind of long-acting fluorescent brightener added detergent and preparation method thereof with highly effective chelating ability |
Non-Patent Citations (1)
| Title |
|---|
| 章永年，等: "工业及公共设施洗涤剂", 中国轻工业出版社, pages: 115 - 116 * |
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Address after: 515000 plot a11-2, Shantou Free Trade Zone, Shantou City, Guangdong Province (7 buildings in total) Applicant after: Guangdong kaiqia Oil Technology Co.,Ltd. Address before: 515071 plot a11-2, Shantou Free Trade Zone, Shantou City, Guangdong Province (7 buildings in total) Applicant before: SHANTOU KAIQIA CHEMICAL Co.,Ltd. |
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