CN112646441A - Building indoor emulsion paint and preparation method thereof - Google Patents
Building indoor emulsion paint and preparation method thereof Download PDFInfo
- Publication number
- CN112646441A CN112646441A CN202011553104.7A CN202011553104A CN112646441A CN 112646441 A CN112646441 A CN 112646441A CN 202011553104 A CN202011553104 A CN 202011553104A CN 112646441 A CN112646441 A CN 112646441A
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- glass beads
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- latex paint
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/22—Luminous paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses indoor latex paint for a building and a preparation method thereof, and belongs to the technical field of indoor latex paint. The composition is prepared from the following raw materials in parts by weight: 15-40 parts of acrylic emulsion; 5-15 parts of fluorescent glass beads; 5-15 parts of nano titanium dioxide; 15-25 parts of calcium carbonate; 2-5 parts of a film-forming assistant; 0.3-0.5 part of wetting agent; 0.2-1.5 parts of a dispersant; 0.2-1 part of defoaming agent; 0.1-0.5 part of thickening agent; 0.2-1 part of preservative; 25-40 parts of deionized water. The fluorescent glass beads are added into the common emulsion paint, the fluorescent glass beads adopt the hollow glass beads doped with the fluorescent powder, the hollow glass beads are light in weight, small in density and good in heat insulation performance, and the fluorescent glass beads can have a fluorescent effect after being doped with the fluorescent powder; the fluorescent powder is protected in the glass beads, has the wear-resistant characteristic, prolongs the service life of the fluorescent powder, and has better crystal clear fluorescent effect because the glass beads are in a transparent state.
Description
Technical Field
The invention relates to indoor latex paint for buildings and a preparation method thereof, belonging to the technical field of indoor latex paint.
Background
The emulsion paint is a water paint prepared by adding pigment, filler and various auxiliary agents into synthetic resin emulsion serving as a base material, is also called synthetic resin emulsion paint, and is one of organic paints. The latex paint mainly comprises polyvinyl acetate latex paint, ethylene propylene latex paint, pure acrylic latex paint and the like, and can be divided into two types of inner wall latex paint and outer wall latex paint according to different application environments of products. The inner wall latex paint adopting the acrylic emulsion is widely applied. The acrylic emulsion is milky white or nearly transparent viscous liquid. The acrylic emulsion is an emulsion prepared by copolymerizing pure acrylic monomers, is an emulsion with small particle size, multiple purposes and outstanding performance, is suitable for various coating formulations, has outstanding water resistance and weather resistance, and particularly has excellent performance in high-gloss and semi-gloss coatings. The acrylic emulsion has good water resistance, alkali resistance and dirt resistance, has good adhesion to the surfaces of masonry, wood and steel, can be used for preparing flat, semi-gloss and high-gloss emulsion paints, and can also be used for preparing high-quality finishing paints for floors, cement encaustic tiles and tennis courts.
At present, the interior wall latex paint mainly comprises emulsion, pigment, filling material and auxiliary agent, wherein the pigment mainly adopts two kinds of white pigments of titanium dioxide or lithopone (lithopone) which are harmless to human bodies, and the latex paint is also doped with light-colored pigment, and the colored pigment is also made of materials harmless to human bodies. Some hold the indoor wall of building of activity, in order to reach the more dazzling effect of turning off the light, mix phosphor powder in ordinary emulsion paint usually, after phosphor powder absorbed light, under the condition of turning off the light, can also continuously send fluorescence for the activity scene is dazzling more.
However, the fluorescent powder doped in the common latex paint is not protected, and the fluorescent effect is lost after long-time use. Therefore, the design is the building indoor latex paint and the preparation method thereof, and the building indoor latex paint can protect the fluorescent powder in the glass beads, can be used for a long time and can also keep the fluorescent effect.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: the indoor latex paint for the building and the preparation method thereof are provided, and the problems that the existing indoor latex paint added with fluorescent powder is not protected and the service life of the fluorescent powder needs to be prolonged are solved.
The technical problem to be solved by the invention is realized by adopting the following technical scheme:
the indoor latex paint for the building is prepared from the following raw materials in parts by weight:
15-40 parts of acrylic emulsion;
5-15 parts of fluorescent glass beads;
5-15 parts of nano titanium dioxide;
15-25 parts of calcium carbonate;
2-5 parts of a film-forming assistant;
0.3-0.5 part of wetting agent;
0.2-1.5 parts of a dispersant;
0.2-1 part of defoaming agent;
0.1-0.5 part of thickening agent;
0.2-1 part of preservative;
25-40 parts of deionized water;
the fluorescent glass beads adopt hollow glass beads doped with fluorescent powder.
As a preferable example, the dispersant is at least one of sodium polyacrylate, styrene maleic anhydride copolymer, sodium hexametaphosphate and ammonium salt.
As a preferred example, the defoaming agent is at least one of a polyether defoaming agent, a silicone oil defoaming agent, and mineral oil.
As a preferred example, the thickener is a polyurethane thickener.
As a preferred example, the preservative is 1, 2 benzisothiazolin-3-one/2-methyl-4 isothiazolin-3-one preservative.
A preparation method of indoor latex paint for buildings comprises the following steps:
(1) manufacturing fluorescent glass beads:
a. using water glass (Na)2O·nSiO2) As raw material, preparing a catalyst containing H2Water glass solution of O55.9%;
b. according to the mass parts, taking 500 parts of water glass solution, 5-50 parts of inorganic fluorescent powder and 500 parts of 10% ammonium pentaborate aqueous solution, and stirring until the materials are uniformly mixed to form mixed aqueous solution containing the inorganic fluorescent powder;
c. spraying the mixed aqueous solution into a spray drying tower, wherein the inlet temperature of the drying tower is 390-420 ℃, the outlet temperature of the drying tower is 140-160 ℃, and the recovered microspheres are dried to form fluorescent glass microspheres;
(2) adding 15-40 parts of acrylic emulsion, 0.2-1.5 parts of dispersant and 0.2-1 part of defoamer into a material cylinder of a stirrer, and uniformly stirring;
(3) continuously adding 5-15 parts of fluorescent glass beads, 5-15 parts of nano titanium dioxide and 15-25 parts of calcium carbonate into a material cylinder of a stirrer, and uniformly dispersing and stirring;
(4) finally, 2-5 parts of film forming auxiliary agent, 0.3-0.5 part of wetting agent, 0.1-0.5 part of thickening agent, 0.2-1 part of preservative and 25-40 parts of deionized water are put into a material cylinder of a stirrer and are uniformly mixed and stirred to prepare the building indoor emulsion paint.
The invention has the beneficial effects that: the fluorescent glass beads are added into the common emulsion paint, the fluorescent glass beads adopt the hollow glass beads doped with the fluorescent powder, the hollow glass beads are light in weight, small in density and good in heat insulation performance, and the fluorescent glass beads can have a fluorescent effect after being doped with the fluorescent powder; the fluorescent powder is protected in the glass beads, has the wear-resistant characteristic, prolongs the service life of the fluorescent powder, and has better glittering and translucent fluorescent effect because the glass beads are in a transparent state; the fluorescent glass beads are prepared by adopting water glass as a raw material, can be matched with inorganic fluorescent powder to prepare the glass beads with the fluorescent effect, and are simple in preparation method and convenient for batch production.
Detailed Description
In order to make the technical means, the original characteristics, the achieved purpose and the efficacy of the invention easily understood, the invention is further described with reference to the following embodiments.
Example 1
The indoor latex paint for the building is prepared from the following raw materials in parts by weight:
15 parts of acrylic emulsion;
15 parts of fluorescent glass beads;
15 parts of nano titanium dioxide;
15 parts of calcium carbonate;
2 parts of a film-forming additive;
0.3 part of wetting agent;
0.2 part of a dispersant;
0.2 part of defoaming agent;
0.1 part of thickening agent;
0.2 part of preservative;
30 parts of deionized water.
The dispersing agent is sodium polyacrylate, the defoaming agent is a polyether defoaming agent, the thickening agent is a polyurethane thickening agent, the preservative is 1, 2-benzisothiazolin-3-one preservative, the film-forming additive is 2, 2, 4-trimethyl-1, 3-pentanediol monoisobutyrate, and the wetting agent is alkylphenol ethoxylate.
Example 2
The indoor latex paint for the building is prepared from the following raw materials in parts by weight:
30 parts of acrylic emulsion;
15 parts of fluorescent glass beads;
10 parts of nano titanium dioxide;
15 parts of calcium carbonate;
3 parts of a film-forming assistant;
0.4 part of wetting agent;
0.8 part of a dispersant;
0.5 part of defoaming agent;
0.3 part of thickening agent;
0.3 part of preservative;
30 parts of deionized water.
The dispersing agent is styrene maleic anhydride copolymer, the defoaming agent is silicone oil defoaming agent, the thickening agent is polyurethane thickening agent, the preservative adopts 2-methyl-4 isothiazoline-3-ketone preservative, the film forming additive is 2, 2, 4-trimethyl-1, 3-pentanediol monoisobutyrate, and the wetting agent adopts alkylphenol polyoxyethylene ether.
Example 3
40 parts of acrylic emulsion;
15 parts of fluorescent glass beads;
15 parts of nano titanium dioxide;
25 parts of calcium carbonate;
5 parts of a film-forming assistant;
0.5 part of wetting agent;
1.5 parts of a dispersing agent;
1 part of a defoaming agent;
0.5 part of thickening agent;
1 part of preservative;
25 parts of deionized water.
The dispersing agent is sodium hexametaphosphate, the defoaming agent is mineral oil, the thickening agent is a polyurethane thickening agent, the preservative is 1, 2-benzisothiazolin-3-one preservative, the film-forming auxiliary agent is 2, 2, 4-trimethyl-1, 3-pentanediol monoisobutyrate, and the wetting agent is alkylphenol ethoxylate.
The formulation according to the above example was prepared using the following preparation method:
a preparation method of indoor latex paint for buildings comprises the following steps:
(1) manufacturing fluorescent glass beads:
a. water glass (Na 2O. nSiO2) is used as a raw material to prepare a water glass solution containing H2O 55.9.9%;
b. according to the mass parts, taking 500 parts of water glass solution, 5-50 parts of inorganic fluorescent powder and 500 parts of 10% ammonium pentaborate aqueous solution, and stirring until the materials are uniformly mixed to form mixed aqueous solution containing the inorganic fluorescent powder;
c. spraying the mixed aqueous solution into a spray drying tower, wherein the inlet temperature of the drying tower is 390-420 ℃, the outlet temperature of the drying tower is 140-160 ℃, and the recovered microspheres are dried to form fluorescent glass microspheres;
(2) adding the acrylic emulsion, the dispersing agent and the defoaming agent into a material cylinder of the stirrer, and uniformly stirring;
(3) continuously adding the fluorescent glass beads, the nano titanium dioxide and the calcium carbonate into a material cylinder of the stirrer, and uniformly dispersing and stirring;
(4) finally, the film forming auxiliary agent, the wetting agent, the thickening agent, the preservative and the deionized water are put into a material cylinder of the stirrer, and the materials are mixed and stirred uniformly to prepare the building indoor emulsion paint.
The prepared indoor latex paint has the following advantages: the fluorescent glass beads are added into the common emulsion paint, the fluorescent glass beads adopt the hollow glass beads doped with the fluorescent powder, the hollow glass beads are light in weight, small in density and good in heat insulation performance, and the fluorescent glass beads can have a fluorescent effect after being doped with the fluorescent powder; the fluorescent powder is protected in the glass beads, has the wear-resistant characteristic, prolongs the service life of the fluorescent powder, and has better glittering and translucent fluorescent effect because the glass beads are in a transparent state; the fluorescent glass beads are prepared by adopting water glass as a raw material, can be matched with inorganic fluorescent powder to prepare the glass beads with the fluorescent effect, and are simple in preparation method and convenient for batch production.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and that various changes and modifications may be made without departing from the spirit and scope of the invention as defined in the appended claims. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (6)
1. The indoor latex paint for the building is characterized by comprising the following raw materials in parts by weight:
15-40 parts of acrylic emulsion;
5-15 parts of fluorescent glass beads;
5-15 parts of nano titanium dioxide;
15-25 parts of calcium carbonate;
2-5 parts of a film-forming assistant;
0.3-0.5 part of wetting agent;
0.2-1.5 parts of a dispersant;
0.2-1 part of defoaming agent;
0.1-0.5 part of thickening agent;
0.2-1 part of preservative;
25-40 parts of deionized water;
the fluorescent glass beads adopt hollow glass beads doped with fluorescent powder.
2. The building interior latex paint of claim 1, wherein said dispersant is at least one of sodium polyacrylate, styrene maleic anhydride copolymer, sodium hexametaphosphate and ammonium salt.
3. The building interior latex paint of claim 1, wherein said defoamer is at least one of polyether defoamer, silicone defoamer and mineral oil.
4. The architectural interior latex paint of claim 1, wherein said thickener is a polyurethane thickener.
5. The architectural interior latex paint according to claim 1, wherein said preservative is 1, 2 benzisothiazolin-3-one/2-methyl-4 isothiazolin-3-one preservative.
6. The method for preparing the indoor latex paint for the building according to claim 1, which is characterized by comprising the following steps:
(1) manufacturing fluorescent glass beads:
a. using water glass (Na)2O·nSiO2) As raw material, preparing a catalyst containing H2Water glass solution of O55.9%;
b. according to the mass parts, taking 500 parts of water glass solution, 5-50 parts of inorganic fluorescent powder and 500 parts of 10% ammonium pentaborate aqueous solution, and stirring until the materials are uniformly mixed to form mixed aqueous solution containing the inorganic fluorescent powder;
c. spraying the mixed aqueous solution into a spray drying tower, wherein the inlet temperature of the drying tower is 390-420 ℃, the outlet temperature of the drying tower is 140-160 ℃, and the recovered microspheres are dried to form fluorescent glass microspheres;
(2) adding 15-40 parts of acrylic emulsion, 0.2-1.5 parts of dispersant and 0.2-1 part of defoamer into a material cylinder of a stirrer, and uniformly stirring;
(3) continuously adding 5-15 parts of fluorescent glass beads, 5-15 parts of nano titanium dioxide and 15-25 parts of calcium carbonate into a material cylinder of a stirrer, and uniformly dispersing and stirring;
(4) finally, 2-5 parts of film forming auxiliary agent, 0.3-0.5 part of wetting agent, 0.1-0.5 part of thickening agent, 0.2-1 part of preservative and 25-40 parts of deionized water are put into a material cylinder of a stirrer and are uniformly mixed and stirred to prepare the building indoor emulsion paint.
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CN202011553104.7A CN112646441A (en) | 2020-12-24 | 2020-12-24 | Building indoor emulsion paint and preparation method thereof |
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CN202011553104.7A CN112646441A (en) | 2020-12-24 | 2020-12-24 | Building indoor emulsion paint and preparation method thereof |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115093729A (en) * | 2022-07-26 | 2022-09-23 | 富思特新材料科技发展股份有限公司 | Self-luminous stain-resistant fireproof material and preparation method and application thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115093729A (en) * | 2022-07-26 | 2022-09-23 | 富思特新材料科技发展股份有限公司 | Self-luminous stain-resistant fireproof material and preparation method and application thereof |
CN115093729B (en) * | 2022-07-26 | 2024-01-02 | 富思特新材料科技发展股份有限公司 | Self-luminous pollution-resistant fireproof material and preparation method and application thereof |
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Application publication date: 20210413 |