CN112645286B - Hydrogen fluoride high-efficient purification processing integrated device - Google Patents
Hydrogen fluoride high-efficient purification processing integrated device Download PDFInfo
- Publication number
- CN112645286B CN112645286B CN202011528773.9A CN202011528773A CN112645286B CN 112645286 B CN112645286 B CN 112645286B CN 202011528773 A CN202011528773 A CN 202011528773A CN 112645286 B CN112645286 B CN 112645286B
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- device body
- hydrogen fluoride
- circulating pump
- fixedly connected
- cavity
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- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 229910000040 hydrogen fluoride Inorganic materials 0.000 title claims abstract description 31
- 238000000746 purification Methods 0.000 title claims abstract description 18
- 238000003756 stirring Methods 0.000 claims abstract description 34
- 230000005540 biological transmission Effects 0.000 claims abstract description 8
- 239000007789 gas Substances 0.000 claims description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 238000006243 chemical reaction Methods 0.000 abstract description 4
- 238000010438 heat treatment Methods 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 abstract description 4
- 239000000376 reactant Substances 0.000 abstract description 4
- 239000007858 starting material Substances 0.000 abstract description 3
- 239000002253 acid Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- -1 hydrogen halides Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 150000007522 mineralic acids Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000002341 toxic gas Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B7/00—Halogens; Halogen acids
- C01B7/19—Fluorine; Hydrogen fluoride
- C01B7/191—Hydrogen fluoride
- C01B7/195—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention discloses an integrated device for high-efficiency purification and processing of hydrogen fluoride, which comprises a bottom plate, wherein a circulating pump is arranged on the upper surface of the bottom plate, a heater is arranged on one side of the circulating pump, a device body is arranged on the other side of the circulating pump, a hot oil cavity is arranged in the device body, and a transmission case is arranged on the upper surface of the device body. This high-efficient purification processing integrated device of hydrogen fluoride through the setting of circulating pump, the heater, the hot oil pocket, motor and temperature sensor, when carrying out the hydrogen fluoride preparation, the starter motor, the motor drives the pivot and rotates, the pivot drives stirring structure and rotates, stir the reactant, start circulating pump and heater simultaneously, the circulating pump will pass through the hot oil of heater heating and let in the hot oil pocket, it is even to make the reaction be heated, temperature sensor carries out real-time supervision to the inside temperature of device body, in this constant temperature state of holding device, improve the production efficiency of hydrogen fluoride.
Description
Technical Field
The invention relates to the technical field of purification devices, in particular to an integrated device for high-efficiency purification and processing of hydrogen fluoride.
Background
Hydrogen fluoride is an inorganic acid, has the chemical formula of HF, is a colorless and toxic gas with pungent smell under normal conditions, has very strong hygroscopicity, generates white smoke when being contacted with air, is easy to dissolve in water, can be infinitely mutually dissolved with water to form hydrofluoric acid, has hydrogen bonds among hydrogen fluoride molecules, can show abnormal properties such as boiling points which are much higher than those of other hydrogen halides, has very strong chemical reactivity and can react with a plurality of compounds, and hydrogen fluoride is taken as a solute to be a weak acid, and pure hydrogen fluoride is taken as a strong acid.
In the prior art, the hydrogen fluoride production efficiency is low, and the use is inconvenient, so that an integrated device for high-efficiency purification and processing of hydrogen fluoride is provided.
Disclosure of Invention
(one) solving the technical problems
Aiming at the defects of the prior art, the invention provides an integrated device for high-efficiency purification and processing of hydrogen fluoride, which solves the problems in the prior art.
(II) technical scheme
In order to achieve the above purpose, the invention is realized by the following technical scheme: the utility model provides a high-efficient purification processing integrated device of hydrogen fluoride, includes the bottom plate, the upper surface of bottom plate is provided with the circulating pump, one side of circulating pump is provided with the heater, the opposite side of circulating pump is provided with the device body, the inside of device body is provided with hot oil pocket, the upper surface of device body is provided with the transmission case, fixedly connected with motor between the inside wall of transmission case, the output fixedly connected with pivot of motor, the surface of pivot is provided with the mounting hole, the internally mounted of mounting hole has stirring structure, the inside wall fixedly connected with temperature sensor of device body.
Optionally, stirring structure includes blade, cavity, spring, sliding plate, inserted bar and toggle rod, the inside of blade is provided with the cavity, the interior bottom wall fixedly connected with spring of cavity, the one end fixedly connected with sliding plate of spring, one side fixedly connected with inserted bar of sliding plate, one side of inserted bar is provided with the toggle rod.
Optionally, the spout has been seted up to inside wall one side of cavity, the internal surface sliding connection of spout has the slider, one side and the inserted bar fixed connection of slider, the stirring groove has been seted up to the inside wall opposite side of cavity.
Optionally, the upper surface of device body is pegged graft and is had the gas exit tube, one side of gas exit tube is provided with the feeder hopper.
Optionally, an oil inlet pipe is arranged between the device body and the circulating pump, and a return pipe is arranged between the device body and the heater.
Optionally, the lower surface of device body is provided with the supporting legs, the quantity of supporting legs is three.
(III) beneficial effects
The invention provides an integrated device for high-efficiency purification and processing of hydrogen fluoride, which has the following beneficial effects:
1. this high-efficient purification processing integrated device of hydrogen fluoride through the setting of circulating pump, the heater, the hot oil pocket, motor and temperature sensor, when carrying out the hydrogen fluoride preparation, the starter motor, the motor drives the pivot and rotates, the pivot drives stirring structure and rotates, stir the reactant, start circulating pump and heater simultaneously, the circulating pump will pass through the hot oil of heater heating and let in the hot oil pocket, it is even to make the reaction be heated, temperature sensor carries out real-time supervision to the inside temperature of device body, in this constant temperature state of holding device, improve the production efficiency of hydrogen fluoride.
2. This high-efficient purification processing integrated device of hydrogen fluoride stirs the pole through mounting hole and stirring structure's setting to both sides, and the spring is compressed, drives the inserted bar shrink simultaneously, when the inserted bar breaks away from the mounting hole, can take off stirring structure to be convenient for change stirring structure, simultaneously through the setting of spout and slider, make the structure more stable, extension stirring structure's life.
Drawings
FIG. 1 is a schematic diagram of the front structure of the present invention;
FIG. 2 is a schematic cross-sectional view of the body of the device of the present invention;
fig. 3 is an enlarged schematic view of the structure a in fig. 2 according to the present invention.
In the figure: 1. a bottom plate; 2. a circulation pump; 3. a heater; 4. a device body; 5. a hot oil chamber; 6. a transmission case; 7. a motor; 8. a rotating shaft; 9. a mounting hole; 10. a stirring structure; 1001. a blade; 1002. a cavity; 1003. a spring; 1004. a sliding plate; 1005. a rod; 1006. a toggle rod; 11. a temperature sensor; 12. a chute; 13. a slide block; 14. a toggle groove; 15. a gas outlet pipe; 16. a feed hopper; 17. an oil inlet pipe; 18. a return pipe; 19. and supporting the feet.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments.
Referring to fig. 1 to 3, the present invention provides a technical solution: the utility model provides a high-efficient purification processing integrated device of hydrogen fluoride, including bottom plate 1, the upper surface of bottom plate 1 is provided with circulating pump 2, one side of circulating pump 2 is provided with heater 3, the opposite side of circulating pump 2 is provided with device body 4, the upper surface of device body 4 is pegged graft and is had gas exit tube 15, through the setting of gas exit tube 15, be convenient for hydrogen fluoride gas collection, one side of gas exit tube 15 is provided with feeder hopper 16, be provided with oil feed pipe 17 between device body 4 and the circulating pump 2, be provided with back flow 18 between device body 4 and the heater 3, the lower surface of device body 4 is provided with supporting legs 19, the quantity of supporting legs 19 is three, the inside of device body 4 is provided with hot oil pocket 5, the upper surface of device body 4 is provided with transmission case 6, fixedly connected with motor 7 between the inside wall of transmission case 6, the output fixedly connected with pivot 8 of motor 7, the surface of pivot 8 is provided with mounting hole 9, the stirring structure 10 is arranged in the mounting hole 9, the stirring structure 10 comprises a blade 1001, a cavity 1002, a spring 1003, a sliding plate 1004, an inserting rod 1005 and a stirring rod 1006, the cavity 1002 is arranged in the blade 1001, the spring 1003 is fixedly connected with the inner bottom wall of the cavity 1002, one end of the spring 1003 is fixedly connected with the sliding plate 1004, one side of the sliding plate 1004 is fixedly connected with the inserting rod 1005, one side of the inserting rod 1005 is provided with the stirring rod 1006, the stirring rod 1006 is stirred to two sides through the mounting hole 9 and the setting of the stirring structure 10, the spring 1003 is compressed, meanwhile, the inserting rod 1005 is driven to shrink, when the inserting rod 1005 is separated from the mounting hole 9, the stirring structure 10 can be taken down, thereby facilitating the replacement of the stirring structure 10, a sliding groove 12 is arranged on one side of the inner side wall of the cavity 1002, the inner surface of the sliding groove 12 is slidably connected with a sliding block 13, one side of the sliding block 13 is fixedly connected with the inserting rod 1005, through the setting of spout 12 and slider 13, make the structure more stable, the life of extension stirring structure 10, stir groove 14 has been seted up to the inside wall opposite side of cavity 1002, the inside wall fixedly connected with temperature sensor 11 of device body 4, through circulating pump 2, heater 3, hot oil chamber 5, motor 7 and temperature sensor 11's setting, when carrying out the hydrogen fluoride preparation, starter motor 7, motor 7 drives pivot 8 and rotates, pivot 8 drives stirring structure 10 and stirs the reactant, start circulating pump 2 and heater 3 simultaneously, circulating pump 2 will be heated in the hot oil chamber 5 through the hot oil of heater 3 heating, make the reaction be heated evenly, temperature sensor 11 carries out real-time supervision to the inside temperature of device body 4, in order to keep device body 4 in constant temperature state, improve the production efficiency of hydrogen fluoride.
To sum up, this high-efficient purification integrated device of hydrogen fluoride, when using, through circulating pump 2, the heater 3, hot oil chamber 5, motor 7 and temperature sensor 11's setting, when carrying out the hydrogen fluoride preparation, start motor 7, motor 7 drives pivot 8 rotation, pivot 8 drives stirring structure 10 and rotates, stir the reactant, simultaneously start circulating pump 2 and heater 3, circulating pump 2 will pass through the hot oil of heater 3 heating and let in hot oil chamber 5, make the reaction heated evenly, temperature sensor 11 carries out real-time supervision to the inside temperature of device body 4, in order to keep device body 4 in the constant temperature state, improve the production efficiency of hydrogen fluoride, stir the pole 1006 to both sides through the setting of mounting hole 9 and stirring structure 10, spring 1003 is compressed, drive the shrinkage of inserted bar 1005 simultaneously, when inserted bar 1005 breaks away from mounting hole 9, can take off stirring structure 10, thereby be convenient for change stirring structure 10, simultaneously through the setting up of spout 12 and slider 13, make the structure more stable, and the life of stirring structure 10 is prolonged.
The foregoing is only a preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art, who is within the scope of the present invention, should make equivalent substitutions or modifications according to the technical scheme of the present invention and the inventive concept thereof, and should be covered by the scope of the present invention.
Claims (4)
1. The utility model provides a high-efficient purification processing integrated device of hydrogen fluoride, includes bottom plate (1), its characterized in that: the device is characterized in that a circulating pump (2) is arranged on the upper surface of the bottom plate (1), a heater (3) is arranged on one side of the circulating pump (2), a device body (4) is arranged on the other side of the circulating pump (2), a hot oil cavity (5) is arranged in the device body (4), a transmission case (6) is arranged on the upper surface of the device body (4), a motor (7) is fixedly connected between the inner side walls of the transmission case (6), a rotating shaft (8) is fixedly connected to the output end of the motor (7), a mounting hole (9) is formed in the surface of the rotating shaft (8), a stirring structure (10) is arranged in the mounting hole (9), and a temperature sensor (11) is fixedly connected to the inner side walls of the device body (4);
the stirring structure (10) comprises a blade (1001), a cavity (1002), a spring (1003), a sliding plate (1004), an inserting rod (1005) and a poking rod (1006), wherein the cavity (1002) is arranged in the blade (1001), the spring (1003) is fixedly connected to the inner bottom wall of the cavity (1002), the sliding plate (1004) is fixedly connected to one end of the spring (1003), the inserting rod (1005) is fixedly connected to one side of the sliding plate (1004), and the poking rod (1006) is arranged on one side of the inserting rod (1005);
the sliding groove (12) is formed in one side of the inner side wall of the cavity (1002), the sliding block (13) is connected to the inner surface of the sliding groove (12) in a sliding mode, one side of the sliding block (13) is fixedly connected with the inserted link (1005), and the poking groove (14) is formed in the other side of the inner side wall of the cavity (1002).
2. The integrated device for efficient purification and processing of hydrogen fluoride according to claim 1, wherein: the upper surface of device body (4) is pegged graft and is had gas exit tube (15), one side of gas exit tube (15) is provided with feeder hopper (16).
3. The integrated device for efficient purification and processing of hydrogen fluoride according to claim 1, wherein: an oil inlet pipe (17) is arranged between the device body (4) and the circulating pump (2), and a return pipe (18) is arranged between the device body (4) and the heater (3).
4. The integrated device for efficient purification and processing of hydrogen fluoride according to claim 1, wherein: the lower surface of the device body (4) is provided with supporting feet (19), and the number of the supporting feet (19) is three.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011528773.9A CN112645286B (en) | 2020-12-22 | 2020-12-22 | Hydrogen fluoride high-efficient purification processing integrated device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011528773.9A CN112645286B (en) | 2020-12-22 | 2020-12-22 | Hydrogen fluoride high-efficient purification processing integrated device |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112645286A CN112645286A (en) | 2021-04-13 |
| CN112645286B true CN112645286B (en) | 2023-10-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011528773.9A Active CN112645286B (en) | 2020-12-22 | 2020-12-22 | Hydrogen fluoride high-efficient purification processing integrated device |
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| Country | Link |
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| CN (1) | CN112645286B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112897467B (en) * | 2021-03-18 | 2022-09-30 | 福建省建阳金石氟业有限公司 | Production method of electronic-grade hydrofluoric acid |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN207175464U (en) * | 2017-05-31 | 2018-04-03 | 格林斯达(北京)环保科技有限公司 | A kind of hydrogen chloride equipment for purifying |
| CN108217599A (en) * | 2018-03-19 | 2018-06-29 | 衢州市鼎盛化工科技有限公司 | A kind of reaction unit that hydrogen fluoride is prepared suitable for calcirm-fluoride |
| CN108972931A (en) * | 2018-07-26 | 2018-12-11 | 芜湖市黄山松工业地坪新材料有限公司 | Agitating device is used in a kind of processing of epoxide resin material |
| CN208244718U (en) * | 2018-03-30 | 2018-12-18 | 江西新明展实业有限公司 | A kind of reaction kettle of plastic cement production |
| CN208320619U (en) * | 2018-05-16 | 2019-01-04 | 龙川绿油农业发展有限公司 | Blender is used in a kind of processing of tea oil |
| CN210313531U (en) * | 2019-07-31 | 2020-04-14 | 江西天行化工有限责任公司 | Hydrogen fluoride purification device |
-
2020
- 2020-12-22 CN CN202011528773.9A patent/CN112645286B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN207175464U (en) * | 2017-05-31 | 2018-04-03 | 格林斯达(北京)环保科技有限公司 | A kind of hydrogen chloride equipment for purifying |
| CN108217599A (en) * | 2018-03-19 | 2018-06-29 | 衢州市鼎盛化工科技有限公司 | A kind of reaction unit that hydrogen fluoride is prepared suitable for calcirm-fluoride |
| CN208244718U (en) * | 2018-03-30 | 2018-12-18 | 江西新明展实业有限公司 | A kind of reaction kettle of plastic cement production |
| CN208320619U (en) * | 2018-05-16 | 2019-01-04 | 龙川绿油农业发展有限公司 | Blender is used in a kind of processing of tea oil |
| CN108972931A (en) * | 2018-07-26 | 2018-12-11 | 芜湖市黄山松工业地坪新材料有限公司 | Agitating device is used in a kind of processing of epoxide resin material |
| CN210313531U (en) * | 2019-07-31 | 2020-04-14 | 江西天行化工有限责任公司 | Hydrogen fluoride purification device |
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| CN112645286A (en) | 2021-04-13 |
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