CN112629287A - Heating/vaporizing device comprising built-in coil - Google Patents

Heating/vaporizing device comprising built-in coil Download PDF

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Publication number
CN112629287A
CN112629287A CN201910908761.XA CN201910908761A CN112629287A CN 112629287 A CN112629287 A CN 112629287A CN 201910908761 A CN201910908761 A CN 201910908761A CN 112629287 A CN112629287 A CN 112629287A
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CN
China
Prior art keywords
heating
heat
barrel
coil
built
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201910908761.XA
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Chinese (zh)
Inventor
钱震
曹宏成
李俊诚
菅青娥
关怀
武靖为
高源�
王海国
秦艳
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Inner Mongolia Yitai Coal Based New Materials Research Institute Co Ltd
Original Assignee
Inner Mongolia Yitai Coal Based New Materials Research Institute Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Inner Mongolia Yitai Coal Based New Materials Research Institute Co Ltd filed Critical Inner Mongolia Yitai Coal Based New Materials Research Institute Co Ltd
Priority to CN201910908761.XA priority Critical patent/CN112629287A/en
Publication of CN112629287A publication Critical patent/CN112629287A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/04Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being spirally coiled
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F24HEATING; RANGES; VENTILATING
    • F24HFLUID HEATERS, e.g. WATER OR AIR HEATERS, HAVING HEAT-GENERATING MEANS, e.g. HEAT PUMPS, IN GENERAL
    • F24H7/00Storage heaters, i.e. heaters in which the energy is stored as heat in masses for subsequent release
    • F24H7/02Storage heaters, i.e. heaters in which the energy is stored as heat in masses for subsequent release the released heat being conveyed to a transfer fluid
    • F24H7/0208Storage heaters, i.e. heaters in which the energy is stored as heat in masses for subsequent release the released heat being conveyed to a transfer fluid using electrical energy supply
    • F24H7/0233Storage heaters, i.e. heaters in which the energy is stored as heat in masses for subsequent release the released heat being conveyed to a transfer fluid using electrical energy supply the transfer fluid being water
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F27/00Control arrangements or safety devices specially adapted for heat-exchange or heat-transfer apparatus

Abstract

The utility model provides a heating/vapourizing unit including built-in coil pipe, includes the barrel, the both ends of barrel are sealed through the apron, it has heat-conducting medium to fill in the barrel, heat-conducting medium be provided with built-in coil pipe in the barrel, the one end and the import union coupling of built-in coil pipe, the other end is connected with the outlet pipe, the outer wall of barrel is provided with electric heating tape, electric heating tape links to each other with temperature controller. The heating/vaporizing device has simple structure, and can controllably and fully heat and heat or vaporize the raw materials in an indirect heating mode.

Description

Heating/vaporizing device comprising built-in coil
Technical Field
The invention belongs to the technical field of heating equipment, and particularly relates to a heating/vaporizing device comprising a built-in coil.
Background
In the laboratory, the flow of the experimental feedstock is small and there is generally no steam as a source of steady heat. When the experimental raw materials need to be heated/vaporized continuously, the heating/vaporizing method commonly used by large-scale chemical devices is difficult to be directly applied due to small flow, and a proper heating/vaporizing device is difficult to find.
Common continuous heating/vaporization methods include:
(1) electric heating jacket heating/vaporization method: the flask filled with the experimental raw materials is arranged in the electric heating sleeve, and an electric heating program is started for heating. The method has controllable heating and simple operation. However, the raw materials are usually added at one time and used for the batch distillation of liquid raw materials, so that the continuous heating is difficult to realize.
(2) Electric heating rod heating/vaporization method: an electric heating rod provided with an electric heating element is extended into the heating/vaporizing device to heat the experimental raw materials and heat or vaporize the experimental raw materials. The method has the advantages of rapid temperature rise and low equipment material cost. Because the temperature of the electric heating rod is high and the temperature rise is fast, local overheating of a contact part area of the electric heating rod can be caused, and raw materials are coked or decomposed. The temperature rise and the temperature drop are fast, and the temperature rise and the temperature drop are difficult to control.
(3) Electric heating/vaporizing method for outer wall of hollow tube: the electric heating belt is wound on the outer wall of the hollow pipe, the electric heating belt heats the outer wall of the hollow pipe, and the outer wall transfers heat to the raw materials in the hollow pipe to heat or vaporize the raw materials. The method has the advantages of simple equipment structure, low equipment manufacturing difficulty and low material cost. However, the pipe wall is directly heated, and the temperature difference exists in the radial direction of the pipe, so that hot spots can be formed on the local inner wall of the pipe, the experimental raw materials are coked or decomposed, and the central temperature of the pipe is low, so that the raw materials are not heated completely.
(4) Straight tube outside jacket oil bath heating/vaporization method: the hollow pipe is externally provided with a jacket, heat conduction oil is filled in the jacket, a heat conduction oil circulating heating oil bath system is externally arranged, the heat conduction oil is heated through the oil bath system, the heat conduction oil transfers heat to the outer wall of the hollow pipe and then transfers heat to the raw material, and the raw material is heated or vaporized. The method has the advantages of high heating precision, uniform heating, no local hot spot and high safety. But the heat transfer coefficient of the pure pipe wall is small, the heat exchange area per unit length is small, and the method is not suitable for occasions with limited length.
(5) Tube oil bath heating/vaporization method: the heating/vaporizer is of a tubular structure, a tube pass is taken by general raw materials, a shell pass is taken by heat conduction oil, a heat conduction oil heating circulating oil bath system is arranged outside, the heat conduction oil is heated by the oil bath system, the heat conduction oil transfers heat to the heat exchange tubes, and then the heat is transferred to the raw materials, so that the raw materials are heated or vaporized. The method has the advantages of large heat exchange area, strong heating capacity, uniform heating, no local hot spot and high safety. However, the internal parts are more, the sealing points are arranged in the internal parts, leakage is easy to occur, the structure is complex, the manufacturing difficulty is higher, the cost is higher, and the maintenance is difficult.
Disclosure of Invention
In view of the above, the present invention provides a heating/vaporizing device with simple principle and reasonable structure, wherein the heating/vaporizing device is internally provided with a metal coil pipe with a spiral structure, and a cylinder body is filled with heat conducting oil. Through the indirect heating mode, the problem that continuous uniform nondestructive heating/vaporization cannot be realized in the prior art is solved by utilizing the high heat transfer performance of the metal coil pipe and the high heat capacity of the heat transfer oil and adopting a reasonable temperature control scheme, and the device is particularly suitable for heating/vaporization of small-flow experimental raw materials.
In order to achieve the purpose, the invention adopts the following technical scheme:
the utility model provides a heating/vapourizing unit including built-in coil pipe, includes the barrel, the both ends of barrel are sealed through the apron, it has heat-conducting medium to fill in the barrel, heat-conducting medium be provided with built-in coil pipe in the barrel, the one end and the import union coupling of built-in coil pipe, the other end is connected with the outlet pipe, the outer wall of barrel is provided with electric heating tape, electric heating tape links to each other with temperature controller.
In some embodiments, the top of the cylinder is provided with a heat-conducting medium expansion tank, and the bottom is provided with a guide shower.
In some embodiments, the outer wall of the barrel is provided with a barrel wall thermometer, and the barrel wall thermometer is connected with the temperature controller.
In some embodiments, a heat-conducting medium thermometer is disposed on the barrel for detecting the temperature of the heat-conducting medium.
The heating/vaporizing device comprises a barrel, wherein two ends of the barrel are sealed through cover plates, a heat-conducting medium is filled in the barrel, the barrel is internally provided with the built-in coil, one end of the built-in coil is connected with an inlet pipe, the other end of the built-in coil is connected with an outlet pipe, and the barrel is connected with a heat-conducting medium circulating heating unit.
In some embodiments, the heat transfer medium is a heat transfer oil.
In some embodiments, a heat-conducting medium thermometer is arranged on the cylinder, and the heat-conducting medium thermometer is connected with the heat-conducting medium circulating heating unit.
In some embodiments, an outlet thermometer is disposed on the outlet tube.
In some embodiments, the cover plate is connected to the barrel by a clip connection, a threaded connection, or a flanged connection for ease of disassembly, preferably a clip connection.
In some embodiments, the connection between the internal coil and the cover plate is in a bayonet, screw, or flange connection for easy removal, preferably a bayonet connection.
In some embodiments, the internal coil is connected to the inlet and outlet pipes in a manner that facilitates a detachable snap-fit connection, a threaded connection, or a flanged connection, preferably a snap-fit connection.
In some embodiments, the material of the internal coil is carbon steel, stainless steel, alloy steel, copper or aluminum.
In some embodiments, the diameter of the built-in coil is 1/20-1/10, such as 1/18, 1/15 or 1/12, of the inner diameter of the cylinder, and preferably, the diameter of the coil helix is 1/5-4/5, such as 2/5 or 3/5, of the inner diameter of the cylinder.
Compared with the prior art, the invention has the following beneficial effects:
the coil adopts a spiral structure, the heat exchange area in unit height in the heating/vaporizer cylinder is large, the raw material pipeline is fully contacted with heat-conducting oil, no heating dead point exists, and the raw material is completely heated;
the heating mode is indirect heating, no local hot spot exists in the heating/vaporizing device (including the inner wall of the inner pipe), and raw materials are not easy to coke and decompose;
the heat conducting oil is filled in the cylinder body, and the heat capacity of the heat conducting oil is large, so that the temperature rise and the temperature reduction are not too fast;
the spiral structure is beneficial to the flow of experimental raw materials, is convenient for the complete discharge of the experiment and can not generate liquid accumulation;
the heating/vaporizing device has no other internal components except the coil pipe, and has no risk of internal leakage;
the inner coil pipe and the cover plate can be easily disassembled by adopting a detachable connection mode;
according to the requirements of the properties of raw materials, the flow rate, the temperature change and the like, internal coil pipes and connecting pieces with different specifications can be prepared in advance to carry out experiments under different working conditions;
simple structure, easy manufacture and low cost.
Drawings
FIG. 1 is a schematic view of a heating/vaporizing apparatus according to an embodiment of the present invention;
fig. 2 is a schematic structural view of a heating/vaporizing apparatus according to another embodiment of the present invention.
Description of reference numerals:
1-a cylinder body; 2, arranging a coil pipe inside; 3-lower cover; 4-lower tube cap connector; 5, covering the upper cover; 6-upper tube cover connecting piece; 7-a heat conducting oil expansion tank; 8-conducting oil spraying; 9-an inlet pipe; 10-inlet tube connections; 11-an outlet pipe; 12-outlet pipe connection; 13-an electrical heating belt; 14-cartridge wall temperature controller; 15-cylinder wall thermometer; 16-cylinder wall thermometer sleeve; 17-a heat transfer oil thermometer; 18-conduction oil thermo-well tube; 19-an outlet thermometer; 20-outlet thermowell; 21-heat conducting oil circulation heating unit.
Detailed Description
In order that the objects, technical solutions and advantages of the present invention will become more apparent, the present invention will be further described in detail with reference to the accompanying drawings in conjunction with the following specific embodiments.
The invention provides a heating/vaporizing device with simple principle and reasonable structure, which is particularly suitable for continuous, uniform and nondestructive heating or vaporization of raw materials in a laboratory or a miniaturized device.
As shown in fig. 1, the heating/vaporizing apparatus in the embodiment of the present invention includes a cylinder 1, an internal coil 2, a lower cover plate 3, an upper cover plate 5, a heat-conducting oil expansion tank 7, a heat-conducting oil spray 8, an electric heating belt 13, a temperature controller 14, a lower cover plate connector 4 for connecting the lower cover plate, the cylinder 1, and an extension of the internal coil, an upper cover plate connector 6 for connecting the upper cover plate, the cylinder 1, and the extension of the internal coil, an inlet pipe connector 10 for connecting the extension of the internal coil to an inlet pipe 9, and an inlet pipe connector 12 for connecting the extension of the internal coil to an outlet pipe 11.
Wherein, the cylinder body 1 can be a metal straight cylinder, and a heat-conducting medium, such as heat-conducting oil, is injected into the cylinder body; the outer wall of the barrel 1 can be provided with a barrel wall thermometer sleeve 16 and a heat conduction oil thermometer sleeve 18 which are respectively used for placing a barrel wall thermometer 15 and a heat conduction oil thermometer 17.
The built-in coil 2 is of a spiral structure, can be made of carbon steel, stainless steel, alloy steel, copper or aluminum and other metals with heat conductivity coefficient, and does not react with raw materials and heat-conducting media.
The diameter of the built-in coil is 1/20-1/10, such as 1/18, 1/15 or 1/12, of the inner diameter of the cylinder body 1, and the diameter of the coil spiral structure is 1/5-4/5, such as 2/5 or 3/5, of the inner diameter of the cylinder body 1.
The lower cover plate 3 and the upper cover plate 5 can be both disc-shaped.
The heat-conducting oil expansion tank is positioned at the top of the cylinder body 1 and plays a role in adding heat-conducting oil and providing an expansion space in a temperature rise stage; the heat conduction oil guide shower is positioned at the bottom of the cylinder body 1 and used for discharging heat conduction oil after heating is stopped.
The upper cover, the lower cover and the cylinder body are connected in a manner of conveniently detachable hoop connection, screw thread connection or flange connection, and preferably hoop connection; the connection mode among the built-in coil pipe, the lower cover plate and the upper cover plate is clamping sleeve connection, screw thread connection or flange connection which is convenient to disassemble, and clamping sleeve connection is preferred; the connection mode of the extension part of the built-in coil pipe and the inlet pipe and the outlet pipe is clamping sleeve connection, screw thread connection or flange connection which is convenient to disassemble, and preferably clamping sleeve connection is adopted; the built-in coil pipe 2, the lower cover plate 3 and the upper cover plate 5 can be detached and replaced.
An outlet thermometer sleeve 20 may be provided on the outlet tube for receiving an outlet thermometer 19.
The cylinder wall temperature controller 14 is connected with an electric heating belt 13 wound on the outer wall of the cylinder body 1 and a cylinder wall thermometer 15 arranged in the sleeve, and is used for controlling the temperature of the outer wall of the cylinder and heating or vaporizing the raw materials in an indirect heating mode, namely, the electric heating belt → the outer wall of the cylinder body → heat conducting oil → the outer wall of the material pipe → the raw materials.
The heating/vaporizing device adopts a barrel body which is internally provided with a coil pipe with a spiral structure and is filled with heat conducting oil, and the outer wall of the barrel body is wound with an electric heating belt. The method for sequentially transferring heat to the cylinder, the heat transfer oil, the built-in coil and the experimental raw materials through the electric heating belt solves the problem of continuous, uniform and nondestructive heating of the small-flow experimental raw materials, and the built-in coil can be replaced according to different working condition requirements.
As shown in fig. 2, the heating/vaporizing device in another embodiment of the present invention includes a cylinder 1, an internal coil 2, a lower cover plate 3, an upper cover plate 5, a heat transfer oil circulation heating unit 21, a heat transfer oil guide shower 8, a lower cover plate connector 4 for connecting the lower cover plate, the cylinder 1 and an extension of the internal coil, an upper cover plate connector 6 for connecting the upper cover plate, the cylinder 1 and the extension of the internal coil, an inlet pipe connector 10 for connecting the extension of the internal coil to an inlet pipe 9, and an inlet pipe connector 12 for connecting the extension of the internal coil to an outlet pipe 11.
The cylinder 1 is filled with a heat conducting medium, such as heat conducting oil, a heat conducting oil thermometer sleeve 18 can be arranged on the outer wall of the cylinder 1 and used for placing a heat conducting oil thermometer 17, and an outlet thermometer sleeve 20 can be arranged on the outlet pipe 11 and used for placing an outlet thermometer 19.
The heat conducting oil circulation heating unit 21 is used for heating heat conducting oil, heating modes such as oil bath can be adopted, and the heat conducting oil circulation heating unit 21 is connected with the heat conducting oil thermometer 17 and used for detecting and controlling the temperature of the heat conducting oil.
In the embodiment of the invention, the raw material is heated or vaporized by indirect heating, namely the heat conduction oil circulation heating unit → the outer wall of the cylinder → the heat conduction oil → the outer wall of the material pipe → the raw material.
The above-mentioned embodiments are intended to illustrate the objects, technical solutions and advantages of the present invention in further detail, and it should be understood that the above-mentioned embodiments are only exemplary embodiments of the present invention and are not intended to limit the present invention, and any modifications, equivalents, improvements and the like made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (10)

1. The utility model provides a heating/vapourizing unit including built-in coil pipe, includes the barrel, the both ends of barrel are sealed through the apron, it has heat-conducting medium to fill in the barrel, heat-conducting medium be provided with built-in coil pipe in the barrel, the one end and the import union coupling of built-in coil pipe, the other end is connected with the outlet pipe, the outer wall of barrel is provided with electric heating tape, electric heating tape links to each other with temperature controller.
2. The heating/vaporizing device of claim 1, wherein the top of the cylinder is provided with a heat conducting medium expansion tank and the bottom is provided with a conductive shower.
3. The heating/vaporizing device of claim 1, wherein an outer wall of the cylinder is provided with a cylinder wall thermometer, the cylinder wall thermometer being connected to the temperature controller; preferably, a heat-conducting medium thermometer is arranged on the cylinder and used for detecting the temperature of the heat-conducting medium.
4. The heating/vaporizing device comprises a barrel, wherein two ends of the barrel are sealed through cover plates, a heat-conducting medium is filled in the barrel, the barrel is internally provided with the built-in coil, one end of the built-in coil is connected with an inlet pipe, the other end of the built-in coil is connected with an outlet pipe, and the barrel is connected with a heat-conducting medium circulating heating unit.
5. The heating/vaporizing device according to claim 4, wherein a heat transfer medium thermometer is provided on the cylinder, and the heat transfer medium thermometer is connected to the heat transfer medium circulation heating unit.
6. The heating/vaporizing apparatus according to any one of claims 1 to 5, wherein the heat transfer medium is a heat transfer oil; preferably, the outlet tube is provided with an outlet thermometer.
7. The heating/vaporizing device of any one of claims 1 to 5, wherein the cover plate and the cylinder are connected by means of a clip connection, a screw connection or a flange connection for easy disassembly, preferably a clip connection.
8. The heating/vaporizing device of any one of claims 1 to 5, wherein the built-in coil and the cover plate are connected in a manner of a bayonet connection, a threaded connection or a flanged connection for easy disassembly, preferably a bayonet connection.
9. The heating/vaporizing device of any one of claims 1 to 5, wherein the built-in coil is connected to the inlet and outlet pipes in a manner of easy-to-detach snap-fit connection, screw-fit connection or flange connection, preferably a snap-fit connection.
10. The heating/vaporizing apparatus of any one of claims 1-5, wherein the material of the internal coil is carbon steel, stainless steel, alloy steel, copper or aluminum; preferably, the diameter of the built-in coil is 1/20-1/10 of the inner diameter of the cylinder, such as 1/18, 1/15 or 1/12, and preferably, the diameter of the coil spiral structure is 1/5-4/5 of the inner diameter of the cylinder, such as 2/5 or 3/5.
CN201910908761.XA 2019-09-24 2019-09-24 Heating/vaporizing device comprising built-in coil Pending CN112629287A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201910908761.XA CN112629287A (en) 2019-09-24 2019-09-24 Heating/vaporizing device comprising built-in coil

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Application Number Priority Date Filing Date Title
CN201910908761.XA CN112629287A (en) 2019-09-24 2019-09-24 Heating/vaporizing device comprising built-in coil

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CN112629287A true CN112629287A (en) 2021-04-09

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN200986297Y (en) * 2006-10-26 2007-12-05 赵放 Pipecoil heating medium electric heater
US20110041781A1 (en) * 2009-08-18 2011-02-24 Sridhar Deivasigamani Coil tube heat exchanger for a tankless hot water system
CN104531173A (en) * 2014-12-22 2015-04-22 杭州锅炉集团股份有限公司 Coke oven crude gas riser pipe sensible heat recovery device and coke oven crude gas riser pipe sensible heat recovery method
CN205536540U (en) * 2016-01-28 2016-08-31 广东华特气体股份有限公司 High -efficient gaseous heating device
CN207649417U (en) * 2017-11-17 2018-07-24 广东米特拉电器科技有限公司 A kind of novel heat exchange water tank
CN208398186U (en) * 2018-06-08 2019-01-18 河北国鼎新能源科技有限公司 Energy storage electric heating equipment
US20190048781A1 (en) * 2017-08-09 2019-02-14 Hyundai Motor Company Coolant heating apparatus for electric vehicle
CN209069055U (en) * 2018-11-05 2019-07-05 故城县渤海化工有限公司 A kind of coiled chlorine gasifier for trichloroacetone production

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN200986297Y (en) * 2006-10-26 2007-12-05 赵放 Pipecoil heating medium electric heater
US20110041781A1 (en) * 2009-08-18 2011-02-24 Sridhar Deivasigamani Coil tube heat exchanger for a tankless hot water system
CN104531173A (en) * 2014-12-22 2015-04-22 杭州锅炉集团股份有限公司 Coke oven crude gas riser pipe sensible heat recovery device and coke oven crude gas riser pipe sensible heat recovery method
CN205536540U (en) * 2016-01-28 2016-08-31 广东华特气体股份有限公司 High -efficient gaseous heating device
US20190048781A1 (en) * 2017-08-09 2019-02-14 Hyundai Motor Company Coolant heating apparatus for electric vehicle
CN207649417U (en) * 2017-11-17 2018-07-24 广东米特拉电器科技有限公司 A kind of novel heat exchange water tank
CN208398186U (en) * 2018-06-08 2019-01-18 河北国鼎新能源科技有限公司 Energy storage electric heating equipment
CN209069055U (en) * 2018-11-05 2019-07-05 故城县渤海化工有限公司 A kind of coiled chlorine gasifier for trichloroacetone production

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