CN112593149A - Production process for controlling surface cracks of microalloyed hot-rolled round steel - Google Patents

Production process for controlling surface cracks of microalloyed hot-rolled round steel Download PDF

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Publication number
CN112593149A
CN112593149A CN202011344548.XA CN202011344548A CN112593149A CN 112593149 A CN112593149 A CN 112593149A CN 202011344548 A CN202011344548 A CN 202011344548A CN 112593149 A CN112593149 A CN 112593149A
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CN
China
Prior art keywords
rolling
steel
temperature
normalizing
surface cracks
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Pending
Application number
CN202011344548.XA
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Chinese (zh)
Inventor
张新文
江宏亮
轩康乐
孙智伟
孟祥岩
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Jiangsu Lianfeng Energy Equipment Co Ltd
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Jiangsu Lianfeng Energy Equipment Co Ltd
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Priority to CN202011344548.XA priority Critical patent/CN112593149A/en
Publication of CN112593149A publication Critical patent/CN112593149A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B3/00Rolling materials of special alloys so far as the composition of the alloy requires or permits special rolling methods or sequences ; Rolling of aluminium, copper, zinc or other non-ferrous metals
    • B21B3/02Rolling special iron alloys, e.g. stainless steel
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B37/00Control devices or methods specially adapted for metal-rolling mills or the work produced thereby
    • B21B37/74Temperature control, e.g. by cooling or heating the rolls or the product
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/28Normalising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/06Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
    • C21D8/065Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires of ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/001Ferrous alloys, e.g. steel alloys containing N
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/08Ferrous alloys, e.g. steel alloys containing nickel
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/12Ferrous alloys, e.g. steel alloys containing tungsten, tantalum, molybdenum, vanadium, or niobium

Abstract

The invention belongs to the technical field of ferrous metallurgy and steel rolling, and particularly relates to a production process for controlling surface cracks of microalloyed hot-rolled round steel. The method comprises the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet. The main process parameters are as follows: the initial rolling temperature of the finish rolling is 800-850 ℃, and the final rolling temperature is 750-770 ℃; normalizing heat treatment: because of adopting micro-alloying, in order to ensure that the alloy elements are fully dissolved in solution, normalizing heat treatment is carried out at the temperature of 620-650 ℃. The method has the advantages that the technological parameters in the rolling process are controlled to enable the grain boundary to be precipitated to play a role in precipitation strengthening, the strength is improved, and the qualified mechanical properties are ensured; and through normalizing treatment, the cracking tendency of the component is reduced, the surface cracks of the casting blank are effectively reduced, and the quality of the casting blank product is improved.

Description

Production process for controlling surface cracks of microalloyed hot-rolled round steel
Technical Field
The invention belongs to the technical field of ferrous metallurgy and steel rolling, and particularly relates to a production process for controlling surface cracks of microalloyed hot-rolled round steel.
Background
The steel bar is the steel variety with the largest output and sale amount in China at present, the quality level of the steel bar is close to the international advanced level, but the use strength of the steel bar has a certain gap with that of the steel bar in developed countries. The hot rolled ribbed steel bars in China are divided into three strength grades of 400, 500 and 600 according to the strength grade. Through years of popularization and application, the HRB500(E) is generally applied to key engineering projects such as nuclear power, landmark buildings and the like. With the implementation of the issuing of GB 1499.2-2018, higher requirements are put forward for the internal organization of the national standard steel bar in the new standard, and the national standard steel bar products are produced by processes such as water penetration and the like.
With the rapid development of building industry, the requirements of engineering structures such as urban municipal engineering, high-rise buildings and the like on the performance of reinforcing steel bars are higher and higher, the safety and the earthquake resistance of the building structures attract general attention, and the key for improving the safety and the earthquake resistance of the buildings is to improve the strength and the comprehensive performance of the reinforcing steel bars. However, while improving the strength and the overall performance, the problem of cracking is inevitable. In the traditional formula, when the Nb content is too high, the alloy cost is increased, the quality of a casting blank is reduced due to the increase of the Nb, the defects of transverse cracks and the like on the surface of the casting blank are easily caused under the stress action in continuous casting production, and the defects of warping, folding and the like on the surface of a steel bar are caused.
Disclosure of Invention
In view of the problems in the prior art, the invention aims to provide a production process for controlling surface cracks of micro-alloyed hot-rolled round steel, the internal structure of the obtained steel bar is bainite, the mechanical property is stable, and the requirement of industrial batch stable production is met.
The present invention achieves the above-described object by the following technical means.
A production process for controlling surface cracks of microalloyed hot rolled round steel comprises the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet; the method specifically comprises the following steps:
the steel billet comprises the following components by weight: 0.11 to 0.13 wt% of C, 0.10 to 0.20 wt% of Si, 1.75 to 1.85 wt% of Mn, 0.03 to 0.06 wt% of V, 0.01 to 0.02 wt% of Mo, 0.01 to 0.013 wt% of N, 0.03 to 0.06 wt% of Ni, and the balance of Fe and inevitable impurities.
When the billet is reheated, the billet is heated to 950-1100 ℃.
The initial rolling temperature of the rough rolling is 900-950 ℃, and the final rolling temperature of the rough rolling is 870-890 ℃.
The initial rolling temperature of the finish rolling is 800-850 ℃, and the final rolling temperature of the finish rolling is 750-770 ℃.
Normalizing heat treatment: because microalloying is adopted, in order to ensure that alloy elements are fully dissolved in solution, normalizing heat treatment is carried out at the temperature of 620-650 ℃.
The cooling speed is 20-30 ℃/s.
Further, the air conditioner is provided with a fan,
the initial rolling temperature of the finish rolling is 820-830 ℃; the finish rolling temperature of the finish rolling is 760-770 ℃.
The temperature of the normalizing treatment was 620 ℃.
The cooling rate was 30 ℃/s.
The C plays a role in solid solution strengthening, so that the strength of the steel can be improved, the yield ratio can be improved, but the welding performance is affected and the plasticity is reduced due to the excessively high content of the C, so that the content of the C element is 0.22-0.25%, and preferably 0.23-0.25%.
Si plays a role in solid solution strengthening and can improve the strength of the steel, but the toughness and plasticity of the steel are reduced when the content is too high, so that the content of the Si element is 0.40-0.60%, preferably 0.46-0.48% in the invention.
Mn plays a role in solid solution strengthening, so that the strength and hardenability of the steel are obviously improved, the pearlite content is increased, and the yield ratio is improved, but the increase of Mn element can cause the increase of production cost, and meanwhile, the coarseness of crystal grains is promoted; therefore, in the present invention, the content of the Mn element is 1.45 to 1.55%, preferably 1.29 to 1.31%.
V is an important microalloy strengthening element, and the austenite grain refining effect of V is weaker. The element V can separate out nano-scale V (C, N) compounds in the rolling process, increases ferrite nucleation points, prevents ferrite grains from growing, has strong precipitation strengthening effect, and can obviously improve the yield strength of the steel bar.
Both Ni and Mo can play a certain role in solid solution strengthening, the yield strength of the steel is improved, the plasticity and the formability of the steel are reduced, and the recrystallization temperature of the steel can be increased by Mo; therefore, the Ni content is limited to not more than 0.07%, and the Mo content is limited to not more than 0.02%.
The invention has the beneficial effects that:
the method has the advantages that the technological parameters in the rolling process are controlled to enable the grain boundary to be precipitated to play a role in precipitation strengthening, the strength is improved, and the qualified mechanical properties are ensured; and through normalizing treatment, the cracking tendency of the component is reduced, the surface cracks of the casting blank are effectively reduced, and the quality of the casting blank product is improved.
Drawings
FIG. 1 is a photograph of a steel surface prepared by a conventional process.
FIG. 2 is a photograph of a steel surface prepared by the process of the present invention.
Detailed Description
The invention will be further described with reference to the following figures and specific examples, but the scope of the invention is not limited thereto.
Example 1
A production process for controlling surface cracks of microalloyed hot rolled round steel comprises the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet; the method specifically comprises the following steps:
the steel billet comprises the following components by weight: 0.11 to 0.13 wt% of C, 0.10 to 0.20 wt% of Si, 1.75 to 1.85 wt% of Mn, 0.03 to 0.06 wt% of V, 0.01 to 0.02 wt% of Mo, 0.01 to 0.013 wt% of N, 0.03 to 0.06 wt% of Ni, and the balance of Fe and inevitable impurities.
When the billet is reheated, the billet is heated to 950 ℃.
The initial rolling temperature of the rough rolling is 900 ℃, and the final rolling temperature of the rough rolling is 870 ℃.
The initial rolling temperature of the finish rolling is 800 ℃, and the final rolling temperature of the finish rolling is 750 ℃.
Normalizing heat treatment: because of adopting micro-alloying, in order to ensure the alloy elements to be fully dissolved in solution, the normalizing heat treatment is carried out at the temperature of 620 ℃.
The cooling rate was 20 ℃/s.
Example 2
A production process for controlling surface cracks of microalloyed hot rolled round steel comprises the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet; the method specifically comprises the following steps:
the steel billet comprises the following components by weight: 0.11 to 0.13 wt% of C, 0.10 to 0.20 wt% of Si, 1.75 to 1.85 wt% of Mn, 0.03 to 0.06 wt% of V, 0.01 to 0.02 wt% of Mo, 0.01 to 0.013 wt% of N, 0.03 to 0.06 wt% of Ni, and the balance of Fe and inevitable impurities.
When the billet is reheated, the billet is heated to 1000 ℃.
The initial rolling temperature of the rough rolling is 920 ℃, and the final rolling temperature of the rough rolling is 880 ℃.
The initial rolling temperature of the finish rolling is 820 ℃, and the final rolling temperature of the finish rolling is 760 ℃.
Normalizing heat treatment: because of adopting micro-alloying, in order to ensure the alloy elements to be fully dissolved in solution, the normalizing heat treatment is carried out at the temperature of 630 ℃.
The cooling rate was 25 ℃/s.
Example 3
A production process for controlling surface cracks of microalloyed hot rolled round steel comprises the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet; the method specifically comprises the following steps:
the steel billet comprises the following components by weight: 0.11 to 0.13 wt% of C, 0.10 to 0.20 wt% of Si, 1.75 to 1.85 wt% of Mn, 0.03 to 0.06 wt% of V, 0.01 to 0.02 wt% of Mo, 0.01 to 0.013 wt% of N, 0.03 to 0.06 wt% of Ni, and the balance of Fe and inevitable impurities.
When the billet is reheated, the billet is heated to 1100 ℃.
The initial rolling temperature of the rough rolling is 950 ℃, and the final rolling temperature of the rough rolling is 890 ℃.
The initial rolling temperature of the finish rolling is 850 ℃, and the final rolling temperature of the finish rolling is 770 ℃.
Normalizing heat treatment: because of adopting micro-alloying, in order to ensure the alloy elements to be fully dissolved in solution, the normalizing heat treatment is carried out at the temperature of 650 ℃.
The cooling rate was 30 ℃/s.
The present invention is not limited to the above-described embodiments, and any obvious improvements, substitutions or modifications can be made by those skilled in the art without departing from the spirit of the present invention.

Claims (5)

1. A production process for controlling surface cracks of microalloyed hot rolled round steel is characterized by comprising the following steps: continuously casting the molten steel to obtain a steel billet, and sequentially reheating, roughly rolling, finely rolling, normalizing and cooling the steel billet; the method specifically comprises the following steps:
when the steel billet is reheated, heating the steel billet to 950-1100 ℃;
the initial rolling temperature of the rough rolling is 900-950 ℃, and the final rolling temperature of the rough rolling is 870-890 ℃;
the initial rolling temperature of the finish rolling is 800-850 ℃, and the final rolling temperature of the finish rolling is 750-770 ℃;
normalizing heat treatment: because microalloying is adopted, in order to ensure that alloy elements are fully dissolved in solution, normalizing heat treatment is carried out at the temperature of 620-650 ℃;
the cooling speed is 20-30 ℃/s.
2. The process of claim 1, wherein the steel slab comprises, based on the total weight of the steel slab: 0.11 to 0.13 wt% of C, 0.10 to 0.20 wt% of Si, 1.75 to 1.85 wt% of Mn, 0.03 to 0.06 wt% of V, 0.01 to 0.02 wt% of Mo, 0.01 to 0.013 wt% of N, 0.03 to 0.06 wt% of Ni, and the balance of Fe and inevitable impurities.
3. The production process for controlling the surface cracks of the microalloyed hot-rolled round steel as claimed in claim 1, wherein the start rolling temperature of finish rolling is 820-830 ℃; the finish rolling temperature of the finish rolling is 760-770 ℃.
4. The process of claim 1, wherein the normalizing temperature is 620 ℃.
5. The process of claim 1, wherein the cooling rate is 30 ℃/s.
CN202011344548.XA 2020-11-26 2020-11-26 Production process for controlling surface cracks of microalloyed hot-rolled round steel Pending CN112593149A (en)

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Citations (14)

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Publication number Priority date Publication date Assignee Title
CN101367094A (en) * 2008-08-22 2009-02-18 马鞍山钢铁股份有限公司 Combined control rolling process for hot-rolled steel bar with rib
CN101798654A (en) * 2010-04-09 2010-08-11 中国石油天然气集团公司 Steel used for straight seam electric resistance welding petroleum casing and casing manufacturing method
CN101805871A (en) * 2010-04-09 2010-08-18 中国石油天然气集团公司 Steel used for solid expandable casing of oil and gas well and manufacturing method of expandable casing
CN101871077A (en) * 2010-06-08 2010-10-27 武汉钢铁(集团)公司 Normalizing type high-strength pressure vessel steel and manufacturing method thereof
CN101942978A (en) * 2010-08-12 2011-01-12 中国石油天然气集团公司 Preparation method of continuous expansion pipe with high strength and high plastic elasticity
CN102367538A (en) * 2011-12-21 2012-03-07 南阳汉冶特钢有限公司 Super-thick low alloy high strength Q345C steel plate and production method thereof
CN102653844A (en) * 2011-03-03 2012-09-05 中国石油天然气集团公司 Electric-resistance-welded steel pipe resisting acidic environment corrosion and preparation method thereof
CN104862614A (en) * 2015-06-03 2015-08-26 南京钢铁股份有限公司 X60N normalizing pipeline steel and production method thereof
CN105018861A (en) * 2015-08-10 2015-11-04 山东钢铁股份有限公司 Low-cost normalizing rolling hot rolling H type steel and preparation method thereof
CN105603311A (en) * 2016-01-20 2016-05-25 广西丛欣实业有限公司 Production method of high-strength rebars excellent in weldability
CN108624813A (en) * 2018-04-23 2018-10-09 舞阳钢铁有限责任公司 With it is resistance to long when die welding hydrogen sulfide corrosion resistant tank plate and its production method
CN109022708A (en) * 2018-09-19 2018-12-18 江阴兴澄特种钢铁有限公司 The low-carbon used under a kind of condition of ultralow temperature easily welds normalizing acid-resistant pipeline steel plate
CN110184530A (en) * 2018-07-14 2019-08-30 江阴兴澄特种钢铁有限公司 The pipe fitting used under low temperature and acid condition normalizing state steel plate and its manufacturing method
CN111440930A (en) * 2020-03-18 2020-07-24 江阴兴澄特种钢铁有限公司 AS NZS 3678-350L 15Z15-Z35 normalized steel plate and manufacturing method thereof

Patent Citations (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101367094A (en) * 2008-08-22 2009-02-18 马鞍山钢铁股份有限公司 Combined control rolling process for hot-rolled steel bar with rib
CN101798654A (en) * 2010-04-09 2010-08-11 中国石油天然气集团公司 Steel used for straight seam electric resistance welding petroleum casing and casing manufacturing method
CN101805871A (en) * 2010-04-09 2010-08-18 中国石油天然气集团公司 Steel used for solid expandable casing of oil and gas well and manufacturing method of expandable casing
CN101871077A (en) * 2010-06-08 2010-10-27 武汉钢铁(集团)公司 Normalizing type high-strength pressure vessel steel and manufacturing method thereof
CN101942978A (en) * 2010-08-12 2011-01-12 中国石油天然气集团公司 Preparation method of continuous expansion pipe with high strength and high plastic elasticity
CN102653844A (en) * 2011-03-03 2012-09-05 中国石油天然气集团公司 Electric-resistance-welded steel pipe resisting acidic environment corrosion and preparation method thereof
CN102367538A (en) * 2011-12-21 2012-03-07 南阳汉冶特钢有限公司 Super-thick low alloy high strength Q345C steel plate and production method thereof
CN104862614A (en) * 2015-06-03 2015-08-26 南京钢铁股份有限公司 X60N normalizing pipeline steel and production method thereof
CN105018861A (en) * 2015-08-10 2015-11-04 山东钢铁股份有限公司 Low-cost normalizing rolling hot rolling H type steel and preparation method thereof
CN105603311A (en) * 2016-01-20 2016-05-25 广西丛欣实业有限公司 Production method of high-strength rebars excellent in weldability
CN108624813A (en) * 2018-04-23 2018-10-09 舞阳钢铁有限责任公司 With it is resistance to long when die welding hydrogen sulfide corrosion resistant tank plate and its production method
CN110184530A (en) * 2018-07-14 2019-08-30 江阴兴澄特种钢铁有限公司 The pipe fitting used under low temperature and acid condition normalizing state steel plate and its manufacturing method
CN109022708A (en) * 2018-09-19 2018-12-18 江阴兴澄特种钢铁有限公司 The low-carbon used under a kind of condition of ultralow temperature easily welds normalizing acid-resistant pipeline steel plate
CN111440930A (en) * 2020-03-18 2020-07-24 江阴兴澄特种钢铁有限公司 AS NZS 3678-350L 15Z15-Z35 normalized steel plate and manufacturing method thereof

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CN112593149A (en) Production process for controlling surface cracks of microalloyed hot-rolled round steel

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