CN112537793B - Three-dimensional polymer and preparation method thereof - Google Patents
Three-dimensional polymer and preparation method thereof Download PDFInfo
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- CN112537793B CN112537793B CN202011611987.2A CN202011611987A CN112537793B CN 112537793 B CN112537793 B CN 112537793B CN 202011611987 A CN202011611987 A CN 202011611987A CN 112537793 B CN112537793 B CN 112537793B
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G3/00—Compounds of copper
- C01G3/006—Compounds containing, besides copper, two or more other elements, with the exception of oxygen or hydrogen
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/56—Mixers with shaking, oscillating, or vibrating mechanisms having a vibrating receptacle provided with stirring elements, e.g. independent stirring elements
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/70—Mixers specially adapted for working at sub- or super-atmospheric pressure, e.g. combined with de-foaming
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
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Abstract
The invention discloses a three-dimensional polymer and a preparation method thereof, belonging to the technical field of inorganic chemistry. The invention discloses a three-dimensional polymer, which has a chemical formula of C30H22N4O8Cu2, and is a monoclinic system; and a preparation method of the three-dimensional polymer, wherein a single-mode stirring effect of the traditional preparation equipment is changed into a multi-mode stirring effect through the design of a first stirring module, a second stirring module, a third stirring module and a fourth stirring module in the material mixing assembly, and during stirring, multiple stirring effects can be repeatedly and circularly performed.
Description
Technical Field
The invention belongs to the technical field of inorganic chemistry, and particularly relates to a three-dimensional polymer and a preparation method thereof.
Background
Inorganic macromolecules, also known as inorganic polymers, belong to the interdiscipline between inorganic chemistry and polymer chemistry; due to small size effect, surface and interface effect, quantum size effect and quantum tunneling effect, the material has unique performance, thereby being focused by people and being one of the important directions of the current material science research; the heterochain inorganic polymer polyaluminium sulfate and polyferric sulfate are currently recognized as high-efficiency inorganic polymer flocculants and are widely applied to the field of domestic and industrial sewage treatment, manganese sulfate, ferrocenecarboxylic acid, bipyridine and potassium hydroxide are required to be added into a mixed solution of ethanol and distilled water in the preparation process of the polymer, the mixture is fully stirred and then filtered, a special preparation device is required to be used for realizing the preparation process, the device in the prior art can only stir materials in a single mode in the preparation process, so that the mixing rate of the materials is low, and a novel preparation device of a three-dimensional polymer is urgently needed in the market to solve the technical problems.
Disclosure of Invention
The object of the present invention is to provide a three-dimensional polymer and a method for preparing the same, which solves the problems mentioned in the background above by the design of the compounding assembly.
In order to achieve the purpose, the invention provides the following technical scheme: a three-dimensional polymer of formula C 30 H 22 N 4 O 8 Cu 2 The polymer is monoclinic. A preparation method of a three-dimensional polymer comprises two symmetrically arranged bases; the top surfaces of the two bases are fixedly connected with a group of damping shock absorption pieces which are mutually connected through a connecting rod, the top ends of the two groups of damping shock absorption pieces are fixedly connected with connecting angle seats, and the bottom surfaces of the two connecting angle seats are fixedly connected with vibrating motors;
the top surfaces of the two connecting angle seats are fixedly connected with an outer shell, a heating outer cavity and a mixing cavity which are mutually isolated are formed in the outer shell from outside to inside, the inner wall of the outer shell and the position corresponding to the mixing cavity are rotatably connected with a mixing assembly through a bearing, the end surface of the outer shell is fixedly connected with a main driving motor, and one end of an output shaft of the main driving motor is in transmission connection with the mixing assembly through a gear;
the mixing component comprises a rotary drum, the peripheral side surface of the rotary drum is rotationally connected with the outer shell through a bearing, the peripheral side surface of the rotary drum is fixedly connected with a driven gear ring, one end of an output shaft of a main driving motor is meshed with the driven gear ring through a driving gear, a mixing cavity is fixedly formed in the rotary drum, a plurality of groups of sieve meshes distributed in a circumferential array are formed in the peripheral side surface of the rotary drum, the peripheral side surface of the mixing cavity is fixedly communicated with the mixing cavity through the sieve meshes, and two symmetrically-arranged material blocking ring pieces are fixedly connected to the outer wall of the rotary drum;
a group of first stirring modules distributed in a circumferential array, a group of second stirring modules distributed in a circumferential array and a group of third stirring modules distributed in a circumferential array are arranged on the inner wall of the stirring cavity, a group of fourth stirring modules distributed in a circumferential array are arranged between the opposite surfaces of the two material blocking ring pieces, a fixed tooth ring is fixedly connected to the inner wall of the outer shell, and the peripheral side surfaces of the first stirring modules, the second stirring modules, the third stirring modules and the fourth stirring modules are all meshed with the fixed tooth ring;
the end face axis position of the outer shell is rotationally connected with a liquid distribution fixed pipe, one end of the liquid distribution fixed pipe is fixedly communicated with a liquid distribution outer seat, one ends of a group of first stirring modules and a group of second stirring modules are rotationally communicated with the liquid distribution outer seat, one surface of the liquid distribution outer seat is rotationally communicated with a connecting pipe, the peripheral side surface of the connecting pipe is rotationally connected with a rotary cylinder, the other end of the connecting pipe is fixedly communicated with a liquid distribution inner seat, the peripheral side surface of the connecting pipe is fixedly connected with a driven inner gear, and one surface of the liquid distribution inner seat is fixedly communicated with a group of stirring inner pipes distributed in a circumferential array;
a heating liquid inlet pipe is fixedly mounted on the surface of the outer shell through a connecting piece, the tail end of the heating liquid inlet pipe is rotatably communicated with the liquid distribution fixed pipe, one surface of the heating liquid inlet pipe is fixedly communicated with the heating outer cavity through a branch pipe, a feeding pipe is fixedly mounted on the surface of the outer shell, a material guide nozzle communicated with the mixing cavity is fixedly mounted on the surface of the rotary cylinder, and one end of the feeding pipe extends into the outer shell and is communicated with the material guide nozzle;
and a liquid discharge pipe communicated with the mixing cavity is fixedly arranged on the bottom surface of the outer shell.
The scheme is as follows:
the main driving motor, the vibrating motor, the second temperature sensor and the first temperature sensor are common parts in the prior art, and the adopted models and the like can be customized according to actual use requirements;
as a preferred embodiment, the maintenance closing cap is installed through the connecting piece to the shell body top surface, overhaul closing cap surface fixed mounting respectively has first temperature sensor, relief valve, vacuum generating pipe and pressure gauge, first temperature sensor, pressure gauge monitoring end all extend to the material mixing intracavity portion, vacuum generating pipe and relief valve one end all with the fixed intercommunication in material mixing chamber.
As a preferred embodiment, first stirring module, second stirring module, third stirring module are two liang of interval settings in the intracavity that mixes, fourth stirring module sets up in the intracavity that mixes, the equal fixed mounting in all sides of inlet pipe and fluid-discharge tube week has the valve, shell body terminal surface fixed mounting has well accuse panel.
As a preferred embodiment, first stirring module and second stirring module all include the cloth liquid central siphon, cloth liquid central siphon week side is rotated with the section of thick bamboo and is connected, cloth liquid central siphon week side just corresponds the first driven external gear of the fixed gear's of fixedly connected with in position of fixed ring gear, first driven external gear week side meshes with fixed ring gear and driven internal gear respectively mutually, cloth liquid central siphon tip with divide the outer seat rotation of liquid and communicate.
As a preferred embodiment, the liquid distribution shaft tube is a hollow tubular structure with openings at two ends, the circumferential side surface of the liquid distribution shaft tube at the first stirring module is fixedly connected with a helical blade a, the circumferential side surface of the liquid distribution shaft tube at the second stirring module is fixedly connected with a helical blade b, heating inner cavities communicated with the liquid distribution shaft tube are fixedly formed in the helical blade a and the helical blade b, the shape of each heating inner cavity is matched with that of the helical blade a, and the helical directions of the helical blades a and the helical blades b are opposite and have the same other structural characteristics.
As a preferred embodiment, the third stirring module and the fourth stirring module both include driven shafts, the circumferential side of the driven shaft at the third stirring module is rotatably connected to the rotary drum, the circumferential side of the driven shaft at the fourth stirring module is rotatably connected to the two material blocking ring pieces, the circumferential side of the driven shaft and corresponding to the fixed gear ring are fixedly connected to a second driven external gear, the circumferential side of the second driven external gear is engaged with the fixed gear ring, the circumferential side of the driven shaft is fixedly connected to a group of stirring blades distributed in a circumferential array, and the surfaces of the stirring blades are uniformly provided with stirring teeth.
As a preferred embodiment, a heating liquid discharge pipe and a second temperature sensor are respectively and fixedly mounted on the bottom surface of the outer shell, one end of the heating liquid discharge pipe is fixedly communicated with the heating outer cavity, one end of the second temperature sensor extends into the heating outer cavity, and the bottom shape of the outer shell is matched with the shape of the rotary cylinder.
As a preferred embodiment, the rotary cylinder is a hollow cylindrical structure with two closed ends, the inner wall and the outer wall of the fixed tooth ring are both provided with teeth distributed in a circular array, and the stirring inner tube is a hollow tubular structure with one open end and one closed end.
Compared with the prior art, the preparation method of the three-dimensional polymer provided by the invention at least comprises the following beneficial effects:
(1) According to the invention, through the design of the first stirring module, the second stirring module, the third stirring module and the fourth stirring module in the mixing component, a single-mode stirring effect of the traditional preparation equipment is changed into a multi-mode stirring effect, and during stirring, multiple stirring effects can be repeatedly and circularly carried out, through the realization of the technical effects, the processing strength and the processing efficiency of the device on materials are effectively improved, meanwhile, through the realization of the multi-mode stirring effect, the collision and agitation degree of the materials during mixing can be effectively improved, the uniformity of the materials during mixing can be effectively enhanced, and through the design of the filter cartridge, the filtering process of the materials can be automatically realized.
(2) According to the invention, through the vibration arrangement of the vibration motor, on one hand, the liquid to be processed can be agitated, so that the fusion and mixing effects among materials are enhanced, on the other hand, impurities adhered to the inner wall of the rotary cylinder or impurities blocked in sieve pores can be quickly dropped, and then the cleanliness of the inner wall of the rotary cylinder and the anti-blocking effect of the rotary cylinder are ensured to a certain extent.
(3) According to the invention, through the design of the heating outer cavity, the heating inner cavity and the stirring inner tube, the traditional single external heating mode is changed into a multi-point and multi-directional heating mode, and the multi-point and multi-directional heating mode is realized, so that the rapid temperature rise in the material processing process and the constant temperature state maintenance in the material processing process are facilitated.
Drawings
FIG. 1 is a schematic structural view of a process for preparing a three-dimensional polymer;
FIG. 2 is a schematic cross-sectional view of FIG. 1;
FIG. 3 is a schematic view of the mixing chamber, the liquid-separating outer seat, and the mixing chamber;
FIG. 4 is a schematic view of a portion of the enlarged structure at A in FIG. 3;
FIG. 5 is a schematic view of a portion of the enlarged structure at B in FIG. 3;
FIG. 6 is a schematic view of a portion of the enlarged structure at C in FIG. 3;
FIG. 7 is a schematic structural view of a compounding assembly;
FIG. 8 is a schematic structural view of a first stirring module;
FIG. 9 is a schematic structural view of a third stirring module;
FIG. 10 is a schematic view showing the structure of the liquid-separating inner base and the stirring inner tube.
In the figure: 1. a base; 2. a damping shock absorbing member; 3. connecting the corner seats; 4. a vibration motor; 5. an outer housing; 6. heating the outer chamber; 7. a mixing chamber; 8. a mixing assembly; 9. a main drive motor; 10. rotating the cylinder; 11. a driven gear ring; 12. a mixing cavity; 13. screening holes; 14. a material blocking ring sheet; 15. a first stirring module; 16. a second stirring module; 17. a third stirring module; 18. a fourth stirring module; 19. a fixed gear ring; 20. liquid distribution and pipe fixing; 21. a liquid separating outer seat; 22. a liquid separating inner seat; 23. a driven internal gear; 24. stirring the inner pipe; 25. heating liquid enters the pipe; 26. a feed pipe; 27. a material guiding nozzle; 28. a second temperature sensor; 29. a liquid discharge pipe; 30. overhauling the seal cover; 31. a first temperature sensor; 32. a vacuum generating tube; 33. a liquid distribution shaft tube; 34. a first driven external gear; 35. heating the inner cavity; 36. a driven shaft lever; 37. a second driven external gear; 38. the liquid discharge pipe is heated.
Detailed Description
The present invention will be further described with reference to the following examples.
The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention. The conditions in the embodiments may be further adjusted according to specific conditions, and simple modifications of the method of the present invention based on the concept of the present invention are all within the scope of the present invention as claimed.
A three-dimensional polymer characterized by: has a chemical formula of C 30 H 22 N 4 O 8 Cu 2 The polymer is monoclinic.
Referring to fig. 1-10, the present invention provides a method for preparing a three-dimensional polymer, comprising two symmetrically disposed bases 1; the top surfaces of the two bases 1 are fixedly connected with a group of damping shock absorption pieces 2 which are mutually connected through a connecting rod, the top ends of the two groups of damping shock absorption pieces 2 are fixedly connected with connecting angle seats 3, the bottom surfaces of the two connecting angle seats 3 are fixedly connected with vibrating motors 4, when the device works, the two vibrating motors 4 work at a set vibration frequency, through the vibration setting of the vibrating motors 4, on one hand, liquid to be processed can be enabled to be agitated, and then the fusion and mixing effect among materials is enhanced, on the other hand, impurities adhered to the inner wall of the rotary cylinder 10 or impurities blocked in the sieve pores 13 can be enabled to quickly fall off, and then the cleanliness of the inner wall of the rotary cylinder 10 and the anti-blocking effect of the rotary cylinder 10 are ensured to a certain degree;
the top surfaces of the two connecting angle seats 3 are fixedly connected with an outer shell 5, a heating outer cavity 6 and a mixing cavity 7 which are mutually isolated are arranged in the outer shell 5 from outside to inside, the inner wall of the outer shell 5 and the position corresponding to the mixing cavity 7 are rotatably connected with a mixing component 8 through a bearing, the end surface of the outer shell 5 is fixedly connected with a main driving motor 9, and one end of an output shaft of the main driving motor 9 is in transmission connection with the mixing component 8 through a gear;
the mixing component 8 comprises a rotary drum 10, the peripheral side surface of the rotary drum 10 is rotationally connected with the outer shell 5 through a bearing, the peripheral side surface of the rotary drum 10 is fixedly connected with a driven gear ring 11, one end of an output shaft of a main driving motor 9 is meshed with the driven gear ring 11 through a driving gear, a mixing cavity 12 is fixedly arranged inside the rotary drum 10, a plurality of groups of sieve holes 13 distributed in a circumferential array are arranged on the peripheral side surface of the rotary drum 10, the peripheral side surface of the mixing cavity 12 is fixedly communicated with the mixing cavity 7 through the sieve holes 13, and two symmetrically arranged material blocking ring pieces 14 are fixedly connected to the outer wall of the rotary drum 10;
a group of first stirring modules 15 distributed in a circumferential array manner, a group of second stirring modules 16 distributed in a circumferential array manner and a group of third stirring modules 17 distributed in a circumferential array manner are installed on the inner wall of the stirring cavity 12, a group of fourth stirring modules 18 distributed in a circumferential array manner are installed between the opposite surfaces of the two material blocking ring pieces 14, a fixed tooth ring 19 is fixedly connected to the inner wall of the outer shell 5, the circumferential side surfaces of the first stirring modules 15, the second stirring modules 16, the third stirring modules 17 and the fourth stirring modules 18 are all meshed with the fixed tooth ring 19, and when the rotary cylinder 10 performs revolution movement under the action of the main driving motor 9, due to the meshed connection design of the first stirring modules 15, the second stirring modules 16, the third stirring modules 17 and the fourth stirring modules 18, the first stirring modules 15, the second stirring modules 16, the third stirring modules 17 and the fourth stirring modules 18 rotate to form multiple stirring effects on materials;
a liquid distribution fixed pipe 20 is rotationally connected to the axial center position of the end face of the outer shell 5, one end of the liquid distribution fixed pipe 20 is fixedly communicated with a liquid distribution outer seat 21, one ends of a group of first stirring modules 15 and a group of second stirring modules 16 are rotationally communicated with the liquid distribution outer seat 21, one surface of the liquid distribution outer seat 21 is rotationally communicated with a connecting pipe, the peripheral side face of the connecting pipe is rotationally connected with the rotary cylinder 10, the other end of the connecting pipe is fixedly communicated with a liquid distribution inner seat 22, the peripheral side face of the connecting pipe is fixedly connected with a driven inner gear 23, and one surface of the liquid distribution inner seat 22 is fixedly communicated with a group of stirring inner pipes 24 distributed in a circumferential array;
a heating liquid inlet pipe 25 is fixedly arranged on the surface of the outer shell 5 through a connecting piece, the tail end of the heating liquid inlet pipe 25 is rotatably communicated with the liquid distribution fixed pipe 20, one surface of the heating liquid inlet pipe 25 is fixedly communicated with the heating outer cavity 6 through a branch pipe, a feeding pipe 26 is fixedly arranged on the surface of the outer shell 5, a material guide nozzle 27 communicated with the mixing cavity 12 is fixedly arranged on the surface of the rotary cylinder 10, and one end of the feeding pipe 26 extends into the outer shell 5 and is communicated with the material guide nozzle 27;
a liquid discharge pipe 29 communicated with the mixing cavity 7 is fixedly arranged on the bottom surface of the outer shell 5.
The scheme is as follows:
the main driving motor 9, the vibration motor 4, the second temperature sensor 28 and the first temperature sensor 31 are common components in the prior art, and the adopted models and the like can be customized according to actual use requirements;
5 top surfaces of shell body are installed through the connecting piece and are overhauld closing cap 30, it has first temperature sensor 31 to overhaul closing cap 30 surface difference fixed mounting, the relief valve, vacuum generating pipe 32 and pressure gauge, first temperature sensor 31, pressure gauge monitoring end all extends to material mixing chamber 7 insidely, vacuum generating pipe 32 and relief valve one end all with material mixing chamber 7 fixed intercommunication, during the use, vacuum generating pipe 32 and outside vacuum generating equipment intercommunication, and then build vacuum environment for the device is inside.
First stirring module 15, second stirring module 16, third stirring module 17 are two liang of intervals setting inside mixing chamber 12, and fourth stirring module 18 sets up inside material mixing chamber 7, and the equal fixed mounting in inlet pipe 26 and 29 week sides of fluid-discharge tube has the valve, and outer shell 5 terminal surface fixed mounting has well accuse panel, and well accuse panel inside fixed mounting has the PLC controller that is used for controlling this mechanism moving ordinary model.
First stirring module 15 and second stirring module 16 all include cloth liquid central siphon 33, and cloth liquid central siphon 33 week side rotates with a section of thick bamboo 10 and is connected, and the first driven external gear 34 of the fixed tooth ring 19's of the fixed position fixedly connected with of cloth liquid central siphon 33 week side and corresponding, first driven external gear 34 week side meshes with fixed tooth ring 19 and driven internal gear 23 mutually respectively, and cloth liquid central siphon 33 tip with divide liquid outer seat 21 to rotate the intercommunication.
Cloth liquid central siphon 33 is both ends open-ended hollow tubular structure, 33 all side fixedly connected with helical blade a on the cloth liquid central siphon of 15 departments of first stirring module, 33 all side fixedly connected with helical blade b on the cloth liquid central siphon of 16 departments of second stirring module, helical blade a and helical blade b are inside all fixed set up with the heating inner chamber 35 of cloth liquid central siphon 33 intercommunication, the shape of heating inner chamber 35 and helical blade a's shape adaptation, other opposite structural feature of helical blade an and helical blade b's spiral direction are the same, through the design of the opposite formula of spiral direction, thereby play the stirring effect of two directions to the material, and the stirring effect repetition of two directions goes on in turn.
The bottom surface of the outer shell 5 is fixedly provided with a heating liquid discharge pipe 38 and a second temperature sensor 28, one end of the heating liquid discharge pipe 38 is fixedly communicated with the heating outer cavity 6, one end of the second temperature sensor 28 extends into the heating outer cavity 6, and the bottom of the outer shell 5 is matched with the rotary cylinder 10 in shape.
The rotary cylinder 10 is a hollow cylindrical structure with two closed ends, the inner wall and the outer wall of the fixed tooth ring 19 are both provided with teeth distributed in a circular array, and the stirring inner tube 24 is a hollow tubular structure with one open end and one closed end.
When in use, the raw material to be processed is injected into the mixing cavity 7 from the feeding pipe 26, the heating liquid inlet pipe 25 and the heating liquid discharge pipe 38 are communicated with the external circulating heating liquid feeding device, the heating liquid is heat conducting oil, the external circulating heating liquid feeding device is matched with the first temperature sensor 31, so that the internal temperature of the mixing cavity 7 is kept at a set temperature, after the raw material enters, the corresponding valve is sealed, the internal state of the device is kept at a sealed state, after the sealing, the vacuum generating pipe 32 is communicated with the external vacuum creating device, so that the internal state of the device is kept at a vacuum environment, after the vacuum environment is created, the main driving motor 9 works, after the main driving motor 9 works, the rotary cylinder 10 is driven to perform revolution movement, during the revolution movement of the rotary cylinder 10, due to the meshing connection design of the first stirring module 15, the second stirring module 16, the third stirring module 17 and the fourth stirring module 18 and the fixed gear ring 19, the first stirring module 15, the second stirring module 16, the third stirring module 17 and the fourth stirring module 18 rotate, multiple stirring effects are formed on materials, after the rotary cylinder 10 revolves, the driven inner gear 23 rotates under the action of the first driven outer gear 34 and the second driven outer gear 37, the three stirring inner tubes 24 move circularly through the rotation of the driven inner gear 23, and stirring operation is performed, when the stirring operation is performed, the heating outer cavity 6 is matched with the heating inner cavity 35 and the stirring inner tubes 24, so that all-directional heating of the materials in the device is realized, after the material mixing is finished, the normal pressure in the device is recovered, after the recovery, the liquid discharge tube 29 is opened, and the processed materials are quickly discharged.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (3)
1. A method of making a three-dimensional polymer, comprising: the chemical formula of the three-dimensional polymer is C 30 H 22 N 4 O 8 Cu 2 The three-dimensional polymer is a monoclinic system, the device comprises two symmetrically arranged bases (1), a group of damping shock absorption pieces (2) which are mutually connected through a connecting rod are fixedly connected to the top surfaces of the two bases (1), connecting angle seats (3) are fixedly connected to the top ends of the two groups of damping shock absorption pieces (2), and vibrating motors (4) are fixedly connected to the bottom surfaces of the two connecting angle seats (3); the top surfaces of the two connecting angle seats (3) are fixedly connected with outer shells (5), heating outer cavities (6) and material mixing cavities (7) which are mutually isolated are formed in the outer shells (5) from outside to inside, the positions, corresponding to the material mixing cavities (7), of the inner walls of the outer shells (5) are rotatably connected with material mixing components (8) through bearings, the end surfaces of the outer shells (5) are fixedly connected with main driving motors (9), and one ends of output shafts of the main driving motors (9) are in transmission connection with the material mixing components (8) through gears; the mixing component (8) comprises a rotary cylinder (10), the peripheral side surface of the rotary cylinder (10) is rotatably connected with the outer shell (5) through a bearing, a driven toothed ring (11) is fixedly connected to the peripheral side surface of the rotary cylinder (10), one end of an output shaft of a main driving motor (9) is meshed with the driven toothed ring (11) through a driving gear, a mixing cavity (12) is fixedly formed in the rotary cylinder (10), a plurality of groups of sieve pores (13) distributed in a circumferential array are formed in the peripheral side surface of the rotary cylinder (10), the peripheral side surface of the mixing cavity (12) is fixedly communicated with a mixing cavity (7) through the sieve pores (13), and two symmetrically-arranged material blocking ring pieces (14) are fixedly connected to the outer wall of the rotary cylinder (10); the inner wall of the mixing cavity (12) is provided with a group of first stirring modules (15) distributed in a circumferential array, a group of second stirring modules (16) distributed in a circumferential array and a group of third stirring modules (17) distributed in a circumferential array, and the two material blocking ring sheets (14)A group of fourth stirring modules (18) distributed in a circumferential array are arranged between the opposite surfaces, a fixed gear ring (19) is fixedly connected to the inner wall of the outer shell (5), and the circumferential side surfaces of the first stirring module (15), the second stirring module (16), the third stirring module (17) and the fourth stirring module (18) are all meshed with the fixed gear ring (19); the end face axis position of the outer shell (5) is rotationally connected with a liquid distribution fixed pipe (20), one end of the liquid distribution fixed pipe (20) is fixedly communicated with a liquid distribution outer seat (21), one ends of a group of first stirring modules (15) and a group of second stirring modules (16) are rotationally communicated with the liquid distribution outer seat (21), one surface of the liquid distribution outer seat (21) is rotationally communicated with a connecting pipe, the circumferential side surface of the connecting pipe is rotationally connected with a rotary cylinder (10), the other end of the connecting pipe is fixedly communicated with a liquid distribution inner seat (22), the circumferential side surface of the connecting pipe is fixedly connected with a driven inner gear (23), and one surface of the liquid distribution inner seat (22) is fixedly communicated with a group of stirring inner pipes (24) distributed in a circumferential array; the device comprises an outer shell (5), a heating liquid inlet pipe (25) is fixedly mounted on the surface of the outer shell (5) through a connecting piece, the tail end of the heating liquid inlet pipe (25) is rotationally communicated with a liquid distribution fixed pipe (20), one surface of the heating liquid inlet pipe (25) is fixedly communicated with a heating outer cavity (6) through a branch pipe, a feeding pipe (26) is fixedly mounted on the surface of the outer shell (5), a material guide nozzle (27) communicated with a mixing cavity (12) is fixedly mounted on the surface of a rotary cylinder (10), and one end of the feeding pipe (26) extends into the outer shell (5) and is communicated with the material guide nozzle (27); a liquid discharge pipe (29) communicated with the mixing cavity (7) is fixedly arranged on the bottom surface of the outer shell (5); the first stirring module (15) and the second stirring module (16) both comprise a liquid distribution shaft tube (33), the peripheral side surface of the liquid distribution shaft tube (33) is rotationally connected with the rotary drum (10), the peripheral side surface of the liquid distribution shaft tube (33) corresponds to a first driven outer gear (34) in fixed connection with the fixed gear ring (19), the peripheral side surface of the first driven outer gear (34) is respectively meshed with the fixed gear ring (19) and the driven inner gear (23), and the end part of the liquid distribution shaft tube (33) is rotationally communicated with the liquid distribution outer seat (21); the liquid distribution shaft tube (33) is of a hollow tubular structure with openings at two ends; the first stirring module(15) The circumferential side surface of the liquid distribution shaft tube (33) at the position is fixedly connected with a helical blade a, the circumferential side surface of the liquid distribution shaft tube (33) at the position of the second stirring module (16) is fixedly connected with a helical blade b, heating inner cavities (35) communicated with the liquid distribution shaft tube (33) are fixedly formed in the helical blade a and the helical blade b, the shape of each heating inner cavity (35) is matched with that of the helical blade a, and the helical directions of the helical blades a and the helical blades b are opposite and have the same other structural characteristics; the third stirring module (17) and the fourth stirring module (18) both comprise driven shaft levers (36), the peripheral side surface of each driven shaft lever (36) at the third stirring module (17) is rotationally connected with the rotary drum (10), the peripheral side surface of each driven shaft lever (36) at the fourth stirring module (18) is rotationally connected with the two material blocking ring pieces (14), the peripheral side surface of each driven shaft lever (36) is fixedly connected with a second driven outer gear (37) corresponding to the position of the fixed tooth ring (19), the peripheral side surface of each second driven outer gear (37) is meshed with the fixed tooth ring (19), the peripheral side surface of each driven shaft lever (36) is fixedly connected with a group of stirring blades distributed in a circumferential array manner, the surfaces of the stirring blades are uniformly distributed with stirring teeth, the top surface of the outer shell (5) is provided with an overhauling sealing cover (30) through a connecting piece, the surface of the overhauling sealing cover (30) is respectively and fixedly provided with a first temperature sensor (31), a pressure release valve, a vacuum generating pipe (32) and a pressure gauge (31) and a pressure gauge end of the first temperature sensor (7) are respectively extended to the interior of the material mixing chamber (7), and one end of the mixing chamber (7) is communicated with the mixing chamber; the first stirring module (15), the second stirring module (16) and the third stirring module (17) are arranged in the stirring cavity (12) at intervals, the fourth stirring module (18) is arranged in the mixing cavity (7), valves are fixedly arranged on the peripheral side surfaces of the feeding pipe (26) and the liquid discharge pipe (29), and a central control panel is fixedly arranged on the end surface of the outer shell (5); the method comprises the following steps: raw materials to be processed are injected into the mixing cavity from the feeding pipe, the heating liquid inlet pipe and the heating liquid discharge pipe are communicated with external circulating heating liquid feeding equipment, the heating liquid is heat conduction oil, and the external circulating heating liquid feeding equipment transmits the heat conduction oil to the mixing cavity through the first temperatureThe matching of the sensor, thus the inner part of the mixing cavity is kept at a set temperature, after the raw material enters, the corresponding valve is sealed, and then the inner part of the device is kept in a sealed state, after the sealing, the vacuum generating pipe is communicated with the external vacuum creating equipment, and then the inner part of the device is kept in a vacuum environment, after the vacuum environment is created, the main driving motor works, and after the main driving motor works, the main driving motor then drives the rotary cylinder to perform revolution motion, and in the process of the revolution motion of the rotary cylinder, due to the meshing connection design of the first stirring module, the second stirring module, the third stirring module and the fourth stirring module and the fixed tooth ring, first stirring module, the second stirring module, the third stirring module, the rotation takes place for the fourth stirring module, then form multiple stirring effect to the material, and revolve a section of thick bamboo revolution back, the rotation motion takes place for driven internal gear under the effect of first driven external gear and the driven external gear of second, rotation through driven internal gear, thereby make three stirring inner tube circular motion, and then stir the operation, and when stirring the operation goes on, the heating exocoel is through cooperating with heating inner chamber and stirring inner tube, and then realize the all-round heating to the inside material of the device, the compounding finishes the back, make the inside ordinary pressure that resumes of the device, resume the back, open the fluid-discharge tube, then with the material quick discharge after finishing processing.
2. The method for preparing the three-dimensional polymer according to claim 1, wherein a heating liquid discharge pipe (38) and a second temperature sensor (28) are respectively fixedly installed on the bottom surface of the outer shell (5), one end of the heating liquid discharge pipe (38) is fixedly communicated with the heating outer cavity (6), one end of the second temperature sensor (28) extends into the heating outer cavity (6), and the shape of the bottom of the outer shell (5) is matched with the shape of the rotary drum (10).
3. The method for preparing the three-dimensional polymer according to claim 1, wherein the rotary cylinder (10) is a hollow cylindrical structure with two closed ends, the inner wall and the outer wall of the fixed-tooth ring (19) are provided with teeth distributed in a circular array, and the stirring inner tube (24) is a hollow tubular structure with one open end and one closed end.
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