CN112516624A - Liquid separation process and equipment for drug synthesis - Google Patents

Liquid separation process and equipment for drug synthesis Download PDF

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Publication number
CN112516624A
CN112516624A CN202011393418.5A CN202011393418A CN112516624A CN 112516624 A CN112516624 A CN 112516624A CN 202011393418 A CN202011393418 A CN 202011393418A CN 112516624 A CN112516624 A CN 112516624A
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China
Prior art keywords
liquid
shell
sides
pipe
liquid separation
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CN202011393418.5A
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Chinese (zh)
Inventor
庞学民
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Shandong Laopangjia Biotechnology Co ltd
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Shandong Laopangjia Biotechnology Co ltd
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Priority to CN202011393418.5A priority Critical patent/CN112516624A/en
Publication of CN112516624A publication Critical patent/CN112516624A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • B01D17/0217Separation of non-miscible liquids by centrifugal force
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D17/00Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02Separation of non-miscible liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D36/00Filter circuits or combinations of filters with other separating devices
    • B01D36/04Combinations of filters with settling tanks
    • B01D36/045Combination of filters with centrifugal separation devices

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Centrifugal Separators (AREA)

Abstract

The invention discloses a liquid separation process for drug synthesis and equipment thereof, belonging to the field of medical devices. According to the invention, separated liquid is slowly immersed into the filter plate and the bottom shell through the liquid suction hopper, internal water liquid can enter the liquid collection pipe through the liquid inlet hole on one side of the liquid collection pipe during centrifugation, and flows into the liquid outlet groove through the through hole after being filtered by the second filter element at the bottom, and double-effect liquid separation is performed on the separated liquid at the centrifugal vortex during liquid separation, and the separated liquid is not contacted with external air during liquid separation, so that the oxidation degree of the liquid medicine during processing is reduced, the separated liquid can be directly subjected to filtrate during centrifugal filtration, the liquid separation effect is obviously improved, the liquid separation efficiency of liquid medicine production is improved, and the liquid outlet.

Description

Liquid separation process and equipment for drug synthesis
Technical Field
The invention relates to the field of medical devices, in particular to a liquid separation process and liquid separation equipment for drug synthesis.
Background
The medicine is a substance or preparation for preventing or treating or diagnosing diseases of human beings and livestock, and the medicine is divided into natural medicine and synthetic medicine according to the source. The medicine can also prevent diseases, treat diseases, reduce pain, promote health, or enhance the resistance of the body to diseases or help diagnose the diseases, and liquid separation is carried out on the mixed and catalyzed liquid medicine to obtain liquid medicines with different pharmacologies for use when the medicine is synthesized;
chinese patent document publication No. CN210121241U discloses a liquid separating device for drug synthesis, specifically a liquid separating device for drug synthesis, which comprises a liquid separating bottle, a main liquid inlet pipe is provided on one side of the upper surface of the liquid separating bottle, a main sealing ring is provided at one end of the liquid separating bottle close to the main liquid inlet pipe, a main conveying pipe is fixedly connected to one side of the main sealing ring far away from the main liquid inlet pipe, and a cavity is provided at the inner bottom wall of the liquid separating bottle. This a divide liquid device for medicine is synthetic, and the surface of cavity is provided with the apron, can take out the apron from the spacing inslot, clean the cavity, nevertheless the liquid medicine is stood after passing centrifuge separation and is got liquid, need wait for the time of standing of a long time, and need filter outside the cauldron when getting liquid, lead to the oxidation by air contact easily, it is more inconvenient to divide liquid equipment inner chamber clearance simultaneously, many can simply wash, the liquid medicine influences next minute liquid precision on attached to the inner wall, and the discharge opening aperture can't be adjusted, can not satisfy the user demand.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide a liquid separation process for drug synthesis and equipment thereof, which can meet the characteristics of no need of filtering liquid taking, reduced standing time and the like.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a liquid separating device for drug synthesis, which comprises a liquid taking mechanism, wherein a plurality of liquid separating mechanisms are arranged in an inner cavity of the liquid taking mechanism, a fixing mechanism is arranged on one side of the liquid taking mechanism, and the liquid separating mechanisms and the liquid taking mechanism are both communicated with the fixing mechanism.
In a preferred technical scheme of the invention, the liquid taking mechanism comprises a shell, a feeding pipe is arranged at the top of the shell, the bottom of the shell is movably connected with a bottom shell, the bottom of the bottom shell is fixedly connected with a base, a first bearing is embedded at the top of the base, a first rotating shaft is sleeved in the first bearing, the top end of the first rotating shaft is fixedly connected with a liquid separating mechanism, the bottom end of the first rotating shaft is fixedly provided with a motor, the bottom of the motor is fixedly connected with a mounting seat, the liquid separating mechanism is arranged in the shell, filter cells are arranged on both sides of the top of the shell, a liquid suction hopper is movably connected with one side of the inner cavity of each filter cell, the liquid suction hopper is communicated with one side of the external liquid separating mechanism, a first filter element is arranged in the filter tank, a filter plate is arranged at the top of the first filter element, and the filter plate is attached to the liquid suction hopper on one side, the top of the filter plate is fixedly connected with a conical plug, and the conical plug is arranged on the top of the inner cavity of the filter tank.
In a preferred technical scheme of the invention, the liquid separating mechanism comprises a liquid separating box, the liquid separating box is arranged in an inner cavity of the shell, two sides of the top of the inner cavity of the liquid separating box are respectively embedded with a threaded cap, the threaded cap is internally threaded with a threaded column, the top of the threaded column is fixedly connected with a handle, the bottom of the threaded column is fixedly connected with a second rotating shaft, the outer side wall of the second rotating shaft is sleeved with a second bearing, the outer side wall of the second bearing is embedded with a baffle, one side of the baffle is attached to one side of the inner cavity of the liquid separating box, one side of the baffle is provided with a plurality of first liquid outlet holes, corresponding positions of the liquid separating box and one side of the inner cavity of the filter tank are respectively provided with a second liquid outlet hole, and.
In a preferred technical scheme of the invention, the liquid separation mechanism further comprises a liquid collection seat, a second filter element is placed in an inner cavity of the liquid collection seat, the top of the liquid collection seat is communicated with a liquid collection pipe, a sealing ring is sleeved on the outer side wall of the liquid collection pipe, a plurality of liquid inlet holes are formed in two sides of the liquid collection pipe, a through hole is formed in the bottom of the liquid collection seat, liquid outlet grooves are formed in two sides of the bottom of the liquid separation box and communicated with the bottom of the liquid collection seat, a liquid collection hopper is embedded in the bottom of the inner cavity of the shell and communicated with the liquid outlet grooves, the liquid collection hopper is communicated with a filter tank on one side, the liquid inlet holes and the liquid collection pipe are formed at an inclined angle, and.
In a preferred technical scheme of the invention, the cross section of the second liquid outlet hole is inclined, the top of the liquid separating box is provided with an opening, and the opening is positioned at the bottom of the top feeding pipe.
In a preferred technical scheme of the invention, rollers are fixedly connected to both sides of the bottom of the liquid separation box, and the rollers are attached to the top of the base.
In a preferred technical scheme of the invention, the fixing mechanism comprises two fixing seats, connecting blocks are fixedly connected to two sides of the outer walls of the fixing seats on two sides, the connecting blocks on two sides are fixedly connected through fixing bolts, the fixing seats on two sides are communicated with one side of the shell, a discharge sleeve is sleeved between the fixing seats on two sides, the other side of the discharge sleeve is communicated with a discharge pipe, and the discharge pipe is communicated with an external storage tank.
In a preferred technical scheme of the invention, one side of the fixed seat is fixedly connected with a sealing gasket, and the sealing gaskets on the two sides are attached to each other.
In a preferred technical scheme of the invention, the cross section of the fixing seat is in an L shape, and the width of the inner cavity of the fixing seat is larger than the diameter of the discharging sleeve.
The liquid separation process for drug synthesis specifically comprises the following steps:
s1, during liquid separation, injecting liquid medicine to be separated into the feed pipe, wherein the liquid medicine enters the liquid separation box through the top opening of the liquid separation box;
s2, the output shaft of the motor rotates to drive the liquid separation box to rotate in the shell through the bottom roller, and the liquid separation box rotates to centrifuge the liquid medicine in the liquid separation box;
s3, after the liquid medicine is centrifuged, the separation liquid with light gravity is moved into second liquid outlet holes from a plurality of first liquid outlet holes on two sides, the separated liquid is slowly immersed into the filter plate through the liquid suction hopper and flows into the first filter element at the bottom after being filtered by the filter plate, the first filter element further filters the separation liquid and then enters the bottom shell, and meanwhile, a discharge pipe on one side extracts the separated liquid medicine in the bottom shell;
s4, the internal water liquid can enter the liquid collecting pipe through the liquid inlet hole on one side of the liquid collecting pipe during centrifugation, and flows into the liquid outlet groove through the through hole after being filtered by the second filter element at the bottom, and enters the bottom shell through the liquid collecting hoppers at two sides, and the separation of the filtrate is completed.
The invention has the beneficial effects that:
1. according to the invention, through the designed liquid medicine box and the liquid collecting pipe, liquid medicine to be separated is injected into the feeding pipe, the liquid medicine enters the liquid separating box through the opening at the top of the liquid separating box, the liquid separating box rotates to centrifuge the internal liquid medicine, the separation liquid with light gravity is moved into the second liquid outlet holes from the first liquid outlet holes at two sides after the liquid medicine is centrifuged, the separated liquid is slowly immersed into the filter plate and the bottom shell through the liquid suction hopper, the internal liquid water can enter the liquid collecting pipe through the liquid inlet hole at one side of the liquid collecting pipe during centrifugation and flows into the liquid outlet groove through the through hole after being filtered by the second filter element at the bottom, double-effect liquid separation is carried out on the vortex separation liquid at the centrifugation part during liquid separation, and the liquid separation is not contacted with external air during liquid separation, the oxidation degree of the liquid medicine during processing is reduced, the separation liquid medicine can be directly filtered during, effectively improving the liquid outlet effect.
2. According to the invention, the handle is rotated to drive the threaded column to rotate in the threaded cap, the threaded column rotates in the threaded cap to move upwards, the threaded column pulls the baffle to move upwards, the baffle moves to drive the first liquid outlet on one side to shield the second liquid outlet on one side, so that the liquid outlet flow can be adjusted through the cross configuration of the second liquid outlet and the second liquid outlet, the liquid outlet liquid separating amount can be effectively controlled, the liquid medicine can be separated after centrifugation, the centrifugation effect is ensured, and the use requirement is met.
3. According to the invention, after the liquid medicine is separated to the fixing seat, the separated liquid medicine in the fixing seat can be moved into the discharging pipe through the discharging sleeve, and when the liquid medicine is adhered to the inner cavity of the fixing seat, the connecting block on one side and the fixing seat can be screwed and separated through the fixing bolt, so that the inner cavity of the bottom shell can be conveniently cleaned, the inner cleanness of the shell is ensured, and the cleaning and maintenance difficulty is reduced.
Drawings
FIG. 1 is a schematic view of the front cross-sectional structure of the present invention;
FIG. 2 is a schematic front view of the present invention;
FIG. 3 is an enlarged schematic view of portion A of FIG. 1 according to the present invention;
FIG. 4 is an enlarged schematic view of portion B of FIG. 1 in accordance with the present invention;
FIG. 5 is a schematic perspective view of a dispensing mechanism according to the present invention;
FIG. 6 is a schematic perspective view of the header of the present invention.
In the figure:
1. a liquid taking mechanism; 101. a housing; 102. a feed pipe; 103. a bottom case; 104. a base; 105. a first bearing; 106. a motor; 107. a first rotating shaft; 108. a mounting seat; 109. a roller; 110. a conical plug; 111. filtering the plate; 112. a liquid suction hopper; 113. a first filter element; 2. a liquid separating mechanism; 201. a liquid separation box; 202. a first liquid outlet hole; 203. a baffle plate; 204. a second bearing; 205. a second rotating shaft; 206. a threaded post; 207. a threaded cap; 208. a liquid collecting seat; 209. a liquid collecting pipe; 210. a liquid inlet hole; 211. a second filter element; 212. a through hole; 213. a liquid outlet groove; 214. a liquid collecting hopper; 215. a second liquid outlet hole; 3. a fixing mechanism; 301. a fixed seat; 302. connecting blocks; 303. fixing the bolt; 304. a gasket; 305. a discharging sleeve; 306. and (4) discharging the pipe.
Detailed Description
The technical scheme of the invention is further explained by the specific implementation mode in combination with the attached drawings.
As shown in fig. 1, the embodiment provides a liquid separating device for drug synthesis, which includes a liquid taking mechanism 1, a plurality of liquid separating mechanisms 2 are arranged in an inner cavity of the liquid taking mechanism 1, a fixing mechanism 3 is arranged on one side of the liquid taking mechanism 1, and both the liquid separating mechanisms 2 and the liquid taking mechanism 1 are communicated with the fixing mechanism 3.
Further, the liquid taking mechanism 1 comprises a shell 101, the top of the shell 101 is provided with an inlet pipe 102, the bottom of the shell 101 is movably connected with a bottom shell 103, the bottom of the bottom shell 103 is fixedly connected with a base 104, a first bearing 105 is embedded at the top of the base 104, a first rotating shaft 107 is sleeved in the first bearing 105, a liquid separating mechanism 2 is fixedly connected to the top end of the first rotating shaft 107, a motor 106 is fixedly mounted at the bottom end of the first rotating shaft 107, a mounting seat 108 is fixedly connected to the bottom of the motor 106, the liquid separating mechanism 2 is arranged in the shell 101, filter grooves are respectively formed in two sides of the top of the shell 101, a liquid sucking hopper 112 is movably connected to one side of an inner cavity of each filter groove, the liquid sucking hopper 112 is communicated with one side of the external liquid separating mechanism 2, a first filter element 113 is arranged in each filter groove, a filter plate 111 is placed at the top of the first, the top of the filter plate 111 is fixedly connected with a conical plug 110, and the conical plug 110 is arranged at the top of the inner cavity of the filter tank.
Further, liquid separating mechanism 2 is including dividing liquid box 201, divide liquid box 201 to arrange the shell 101 inner chamber in, divide liquid box 201 inner chamber top both sides all to inlay and be equipped with screw cap 207, screw cap 207 female connection has screw post 206, screw post 206 top fixedly connected with handle, screw post 206 bottom fixedly connected with second pivot 205, the 205 lateral wall cover of second pivot is equipped with second bearing 204, the second bearing 204 lateral wall inlays and is equipped with baffle 203, baffle 203 one side is laminated mutually with minute liquid box 201 inner chamber one side, a plurality of first liquid holes 202 have been seted up to baffle 203 one side, and divides liquid box 201 and filter cell inner chamber one side to correspond the position and all seted up second liquid hole 215, and filter cell one side second liquid hole 215 is laminated mutually with imbibition fill 112 one side.
Further, liquid separating mechanism 2 still includes liquid collecting seat 208, second filter core 211 has been placed to liquid collecting seat 208 inner chamber, liquid collecting seat 208 top intercommunication has liquid collecting pipe 209, liquid collecting pipe 209 lateral wall cover is equipped with the sealing washer, a plurality of feed liquor holes 210 have all been seted up to liquid collecting pipe 209 both sides, through-hole 212 has been seted up to liquid collecting seat 208 bottom, liquid outlet tank 213 has all been seted up to branch liquid case 201 bottom both sides, liquid outlet tank 213 communicates with liquid collecting seat 208 bottom, shell 101 inner chamber bottom is inlayed and is equipped with liquid collecting bucket 214, liquid collecting bucket 214 is linked together with liquid outlet tank 213, liquid collecting bucket 214 is linked together with one side filter cell, feed liquor hole 210 is the inclination with liquid collecting pipe 209 and offers, and liquid collecting pipe 209 is the plastic pipe.
Further, the cross sectional shape of second liquid outlet 215 is the slope form, the opening has been seted up at branch liquid case 201 top, and the opening is located top inlet pipe 102 bottom, divide the equal fixedly connected with gyro wheel 109 in liquid case 201 bottom both sides, gyro wheel 109 and base 104 top laminating mutually.
The liquid separation process for drug synthesis specifically comprises the following steps:
s1, during liquid separation, liquid medicine to be separated is injected into the feed pipe 102, and the liquid medicine enters the liquid separation box 201 through the opening at the top of the liquid separation box 201;
s2, the output shaft of the motor 106 rotates to drive the liquid separation box 201 to rotate in the shell 101 through the bottom roller 109, and the liquid separation box 201 rotates to centrifuge the internal liquid medicine;
s3, after the liquid medicine is centrifuged, the separation liquid with light gravity is moved into the second liquid outlet holes 215 from the first liquid outlet holes 202 on the two sides, the separated liquid slowly immerses into the filter plate 111 through the liquid suction hopper 112, is filtered through the filter plate 111 and flows into the first filter element 113 at the bottom, the first filter element 113 further filters the separation liquid and then enters the bottom shell 103, and meanwhile, the discharge pipe 306 on one side extracts the separated liquid medicine in the bottom shell 103;
s4, the internal water liquid can enter the liquid collecting pipe 209 through the liquid inlet hole 210 on one side of the liquid collecting pipe 209 during centrifugation, and flows into the liquid outlet groove 213 through the through hole 212 after being filtered by the second filter element 211 at the bottom, and enters the bottom shell 103 through the liquid collecting hoppers 214 on the two sides, and the separation of the filtrate is completed.
The implementation mode is specifically as follows: during liquid separation, liquid medicine to be separated is injected into the feeding pipe 102, the liquid medicine enters the liquid separation box 201 through the opening at the top of the liquid separation box 201, meanwhile, the output shaft of the motor 106 rotates to drive the liquid separation box 201 to rotate in the shell 101 through the bottom roller 109, the liquid separation box 201 rotates more stably at the top of the base 104 through the bottom roller 109, the liquid separation box 201 rotates to centrifuge the internal liquid medicine, separated liquid with light gravity after the liquid medicine is centrifuged moves into the second liquid outlet holes 215 from the first liquid outlet holes 202 at two sides, the separated liquid slowly immerses into the filter plate 111 through the liquid suction hopper 112 and flows into the first filter element 113 at the bottom after being filtered through the filter plate 111, the separated liquid enters the bottom shell 103 after being further filtered by the first filter element 113, meanwhile, the separated liquid medicine in the bottom shell 103 is extracted through the discharging pipe 306 at one side, and the internal liquid medicine can enter the liquid collection pipe 209 through the liquid inlet hole 210 at, and flow into play liquid groove 213 through-hole 212 after filtering through bottom second filter core 211 to in getting into drain pan 103 through both sides collecting hopper 214, carry out the double-effect to centrifugal vortex department parting liquid when dividing liquid, showing and improving and divide the liquid effect, thereby can directly carry out the filtrating to the parting liquid when centrifugal filtration, and adjust liquid medicine liquid outlet volume according to the rotational speed, improve liquid medicine production and divide liquid efficiency, effectively improve out the liquid effect.
Divide 201 inner chamber top both sides of liquid box to all inlay and be equipped with screw cap 207, screw cap 207 female connection has screw thread post 206, screw thread post 206 top fixedly connected with handle, screw thread post 206 bottom fixedly connected with second pivot 205, second pivot 205 lateral wall cover is equipped with second bearing 204, second bearing 204 lateral wall inlays and is equipped with baffle 203, baffle 203 one side is laminated mutually with branch 201 inner chamber one side of liquid box, a plurality of first liquid holes 202 have been seted up to baffle 203 one side, and divides liquid box 201 and filter bowl inner chamber one side to correspond the position and have all seted up second liquid hole 215, and filter bowl one side second liquid hole 215 laminates mutually with imbibition fill 112 one side.
The implementation mode is specifically as follows: the handle is rotated to drive the threaded column 206 to rotate in the threaded cap 207, the threaded column 206 rotates in the threaded cap 207 to move upwards, the threaded column 206 rotates in the second bearing 204 more stably through the second rotating shaft 205 at the bottom, the baffle 203 is prevented from being shifted when the threaded column 206 rotates, the moving stability of the baffle 203 is improved, the threaded column 206 pulls the baffle 203 to move upwards, the baffle 203 moves to drive the first liquid outlet hole 202 at one side to shield the second liquid outlet hole 215 at one side, and the first liquid outlet 202 and the second liquid outlet 215 are obliquely arranged, so that the centrifugal liquid can be discharged conveniently, the residue of the liquid medicine in the first liquid outlet 202 and the second liquid outlet 215 during the centrifugation can be effectively reduced, so that the liquid flow rate can be adjusted by the cross arrangement of the second liquid outlet holes 215 and the second liquid outlet holes 215, therefore, the liquid separating amount can be effectively controlled, the liquid medicine is ensured to be separated after centrifugation, the centrifugation effect is ensured, and the use requirement is met.
Fixing mechanism 3 includes two fixing bases 301, and the equal fixedly connected with connecting block 302 in both sides fixing base 301 outer wall both sides, and through fixing bolt 303 fixed connection between the connecting block 302 of both sides, and both sides fixing base 301 is linked together with shell 101 one side, and has cup jointed ejection of compact sleeve pipe 305 between the fixing base 301 of both sides, ejection of compact sleeve pipe 305 opposite side intercommunication has discharging pipe 306, discharging pipe 306 is linked together with outside storage tank, the sealed pad 304 of fixing base 301 one side fixedly connected with, and the sealed pad 304 laminating of both sides mutually, the shape of cross section of fixing base 301 is L shape, and the width of fixing base 301 inner chamber is greater than the diameter of ejection of compact sleeve pipe 305.
The implementation mode is specifically as follows: after liquid medicine separation to fixing base 301, the liquid medicine after the separation can move to in discharging pipe 306 through discharging sleeve 305 in fixing base 301, and fixing base 301 cup joints at discharging sleeve 305 outer wall, fixing base 301 assembly stability has been guaranteed, when the liquid medicine adhesion is when fixing base 301 inner chamber, can twist the separation through fixing bolt 303 with one side connecting block 302 and fixing base 301, the convenience is cleared up drain pan 103 inner chamber this moment, the sealed pad 304 of fixing base 301 one side can guarantee the water proof effect simultaneously, avoid clean and tidy liquid medicine to leak, guarantee that shell 101 is inside, reduce the clearance and maintain the degree of difficulty.
While the invention has been described with reference to a preferred embodiment, it will be understood by those skilled in the art that various changes may be made and equivalents may be substituted for elements thereof without departing from the spirit and scope of the invention. The present invention is not to be limited by the specific embodiments disclosed herein, and other embodiments that fall within the scope of the claims of the present application are intended to be within the scope of the present invention.

Claims (10)

1. A divide liquid equipment for pharmaceutical synthesis which characterized in that:
the device comprises a liquid taking mechanism (1), wherein a plurality of liquid separating mechanisms (2) are arranged in the inner cavity of the liquid taking mechanism (1);
and one side of the liquid taking mechanism (1) is provided with a fixing mechanism (3);
the liquid separating mechanism (2) and the liquid taking mechanism (1) are both communicated with the fixing mechanism (3).
2. A device for dispensing liquids for use in drug synthesis as claimed in claim 1, wherein:
the liquid taking mechanism (1) comprises a shell (101), a feeding pipe (102) is arranged at the top of the shell (101), a bottom shell (103) is movably connected to the bottom of the shell (101), and a base (104) is fixedly connected to the bottom of the bottom shell (103);
a first bearing (105) is embedded in the top of the base (104), a first rotating shaft (107) is sleeved in the first bearing (105), a liquid separating mechanism (2) is fixedly connected to the top end of the first rotating shaft (107), a motor (106) is fixedly mounted at the bottom end of the first rotating shaft (107), a mounting seat (108) is fixedly connected to the bottom of the motor (106), the liquid separating mechanism (2) is arranged in the shell (101), filter cells are respectively arranged on two sides of the top of the shell (101), and a liquid suction hopper (112) is movably connected to one side of an inner cavity of each filter cell;
the liquid suction hopper (112) is communicated with one side of the external liquid separating mechanism (2), a first filter element (113) is placed in the filter tank, a filter plate (111) is placed at the top of the first filter element (113), and the filter plate (111) is attached to the liquid suction hopper (112) on one side;
the top of the filter plate (111) is fixedly connected with a conical plug (110), and the conical plug (110) is arranged at the top of the inner cavity of the filter tank.
3. A device for dispensing liquids for use in drug synthesis as claimed in claim 2, wherein:
the liquid separation mechanism (2) comprises a liquid separation box (201), the liquid separation box (201) is arranged in an inner cavity of the shell (101), two sides of the top of the inner cavity of the liquid separation box (201) are respectively embedded with a threaded cap (207), and a threaded column (206) is connected with the threaded cap (207) in an internal thread manner;
the top end of the threaded column (206) is fixedly connected with a handle, the bottom end of the threaded column (206) is fixedly connected with a second rotating shaft (205), a second bearing (204) is sleeved on the outer side wall of the second rotating shaft (205), a baffle (203) is embedded in the outer side wall of the second bearing (204), and one side of the baffle (203) is attached to one side of the inner cavity of the liquid distribution box (201);
a plurality of first liquid holes (202) have been seted up to baffle (203) one side, and divide liquid case (201) and filter cell inner chamber one side corresponding position and all seted up second and go out liquid hole (215), and filter cell one side second goes out liquid hole (215) and attaches to each other with inhale liquid fill (112) one side.
4. A device for dispensing liquids for use in drug synthesis as claimed in claim 3, wherein:
the liquid separation mechanism (2) further comprises a liquid collection seat (208), a second filter element (211) is arranged in an inner cavity of the liquid collection seat (208), the top of the liquid collection seat (208) is communicated with a liquid collection pipe (209), and a sealing ring is sleeved on the outer side wall of the liquid collection pipe (209);
both sides of the liquid collecting pipe (209) are provided with a plurality of liquid inlet holes (210), the bottom of the liquid collecting seat (208) is provided with a through hole (212), both sides of the bottom of the liquid separating box (201) are provided with liquid outlet grooves (213), and the liquid outlet grooves (213) are communicated with the bottom of the liquid collecting seat (208);
the bottom of the inner cavity of the shell (101) is embedded with a liquid collecting hopper (214), the liquid collecting hopper (214) is communicated with the liquid outlet tank (213), the liquid collecting hopper (214) is communicated with a filter tank on one side, the liquid inlet hole (210) and the liquid collecting pipe (209) are arranged at an inclined angle, and the liquid collecting pipe (209) is a plastic pipe.
5. A liquid separation device for drug synthesis according to claim 4, wherein:
the cross section of the second liquid outlet hole (215) is inclined, the top of the liquid distribution box (201) is provided with an opening, and the opening is positioned at the bottom of the top feeding pipe (102).
6. A device for dispensing liquids for use in drug synthesis as claimed in claim 3, wherein:
divide liquid case (201) bottom both sides equal fixedly connected with gyro wheel (109), gyro wheel (109) and base (104) top are laminated mutually.
7. A device for dispensing liquids for use in drug synthesis as claimed in claim 1, wherein:
the fixing mechanism (3) comprises two fixing seats (301), and connecting blocks (302) are fixedly connected to two sides of the outer wall of the fixing seats (301) at two sides;
the connecting blocks (302) on the two sides are fixedly connected through a fixing bolt (303), and the fixing seats (301) on the two sides are communicated with one side of the shell (101);
and a discharge sleeve (305) is sleeved between the fixed seats (301) at the two sides, the other side of the discharge sleeve (305) is communicated with a discharge pipe (306), and the discharge pipe (306) is communicated with an external storage tank.
8. A liquid separation device for drug synthesis according to claim 6, wherein:
fixing base (301) one side fixedly connected with sealed pad (304), and sealed pad (304) of both sides laminate mutually.
9. A device for dispensing liquids for use in drug synthesis as claimed in claim 7, wherein:
the cross section of the fixed seat (301) is L-shaped, and the width of the inner cavity of the fixed seat (301) is larger than the diameter of the discharging sleeve (305).
10. A device for dispensing liquids for use in drug synthesis according to any of claims 1 to 9, characterized in that: the liquid separation process for drug synthesis by using the liquid separation equipment comprises the following steps:
s1, during liquid separation, liquid medicine to be separated is injected into the feed pipe (102), and the liquid medicine enters the liquid separation box (201) through the opening at the top of the liquid separation box (201);
s2, an output shaft of a motor (106) rotates to drive a liquid separation box (201) to rotate in a shell (101) through a bottom roller (109), and the liquid separation box (201) rotates to centrifuge the liquid medicine inside;
s3, after liquid medicine centrifugation, separating liquid with light gravity is moved into second liquid outlet holes (215) from a plurality of first liquid outlet holes (202) on two sides, the separated liquid slowly immerses into the filter plate (111) through the liquid suction hopper (112), flows into the first filter element (113) at the bottom after being filtered through the filter plate (111), the first filter element (113) further filters the separating liquid and then enters the bottom shell (103), and meanwhile, a discharge pipe (306) on one side extracts the separated liquid medicine in the bottom shell (103);
s4, the internal water liquid can enter the liquid collecting pipe (209) through the liquid inlet hole (210) on one side of the liquid collecting pipe (209) during centrifugation, and flows into the liquid outlet groove (213) through the through hole (212) after being filtered by the second filter element (211) at the bottom, and enters the bottom shell (103) through the liquid collecting hoppers (214) on the two sides, and the separation of the filtrate is completed.
CN202011393418.5A 2020-12-03 2020-12-03 Liquid separation process and equipment for drug synthesis Pending CN112516624A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202011393418.5A CN112516624A (en) 2020-12-03 2020-12-03 Liquid separation process and equipment for drug synthesis

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Application Number Priority Date Filing Date Title
CN202011393418.5A CN112516624A (en) 2020-12-03 2020-12-03 Liquid separation process and equipment for drug synthesis

Publications (1)

Publication Number Publication Date
CN112516624A true CN112516624A (en) 2021-03-19

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CN202011393418.5A Pending CN112516624A (en) 2020-12-03 2020-12-03 Liquid separation process and equipment for drug synthesis

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CN101306264A (en) * 2008-01-25 2008-11-19 天津同仁汇智科技开发有限公司 Rotational liquid separation pot for continuously separating and discharging liquid and solid
CN105797434A (en) * 2016-03-14 2016-07-27 浙江理工大学 Separation and collection device
CN206530791U (en) * 2017-02-24 2017-09-29 沧州华意科技有限公司 A kind of fast disassembly type connecting pipe
CN108499269A (en) * 2018-05-03 2018-09-07 高威 A kind of machinery oily-water seperating equipment
CN208465247U (en) * 2018-06-06 2019-02-05 四川森科制药有限公司 A kind of centrifugal extractor

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CN101306264A (en) * 2008-01-25 2008-11-19 天津同仁汇智科技开发有限公司 Rotational liquid separation pot for continuously separating and discharging liquid and solid
CN105797434A (en) * 2016-03-14 2016-07-27 浙江理工大学 Separation and collection device
CN206530791U (en) * 2017-02-24 2017-09-29 沧州华意科技有限公司 A kind of fast disassembly type connecting pipe
CN108499269A (en) * 2018-05-03 2018-09-07 高威 A kind of machinery oily-water seperating equipment
CN208465247U (en) * 2018-06-06 2019-02-05 四川森科制药有限公司 A kind of centrifugal extractor

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Application publication date: 20210319