CN112479645A - Preparation method of multifunctional permeable tile glue with strong binding power - Google Patents
Preparation method of multifunctional permeable tile glue with strong binding power Download PDFInfo
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- CN112479645A CN112479645A CN202011543277.0A CN202011543277A CN112479645A CN 112479645 A CN112479645 A CN 112479645A CN 202011543277 A CN202011543277 A CN 202011543277A CN 112479645 A CN112479645 A CN 112479645A
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- strong binding
- binding power
- tile glue
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00637—Uses not provided for elsewhere in C04B2111/00 as glue or binder for uniting building or structural materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Finishing Walls (AREA)
Abstract
The invention provides a preparation method of multifunctional permeable tile glue with strong binding power, which is prepared by stirring and mixing the following raw materials by weight percentage, 30-50% of cement, 50-70% of quartz sand, 0.3-2.5% of dispersible latex powder, 0.1-2.5% of cellulose, 0.05-1.5% of starch ether, 0.05-3.5% of industrial salt and 0.3-2.5% of calcium formate. The tile adhesive prepared by the formula overcomes and solves various problems of the tile adhesives in the market at present, develops from single performance to multiple functions, has strong cohesive force, can solve the problems of quick drying, long airing time, frost resistance, droop, slippage, low water absorption rate, easiness in hollowing, falling and the like, can also increase the adjustment time, reduce shrinkage and prolong the opening time, has a permeability function, plays a role in mechanical anchoring similar to a key inserted into a lock hole, and easily solves the problem of sticking tiles on various walls with different interfaces.
Description
Technical Field
The invention relates to the field of building material industry, in particular to a preparation method of multifunctional permeable tile glue with strong binding power.
Background
1. The ceramic tile is a decorative building material widely used, along with the rapid development of the building industry, the ceramic tile building material is continuously updated and developed, the ceramic tile adhesive product types correspond to different types of ceramic tiles, and the ceramic tile adhesive product types are carried forward, so that various problems of ceramic tile laying in the building are solved, the ceramic tile adhesive has multiple types and varieties, and consumers and constructors feel puzzled.
2. Because the texture and the technology of the ceramic tile are continuously updated, the performance requirement on ceramic tile glue is higher and higher, the ceramic tile with the large size is more and more popular with consumers in recent years and occupies the market main body, meanwhile, the ceramic tile with the functions of stain resistance and low permeability is gradually increased, the water absorption rate of the ceramic tile is lower and lower, the back of the ceramic tile is more and more compact and smooth, the bonding difficulty is increased, and the ceramic tile cannot be instantly stuck, dropped and hollowed after being paved. These characteristics put higher demands on the adhesive property of the tile adhesive, such as fast drying, sagging resistance, slip resistance, strong adhesion force and certain flexibility.
At present, the problem of large bricks and low water absorption rate is solved in the market, and the ceramic tile glue of the water agent is pushed out, namely the ceramic tile back glue. The main components of the product are acrylic emulsion and some high polymers, the product is a synthetic organic glue substance, the problem of time durability exists, the durability of a cement inorganic substance material is not long, the product is expensive, the painting area is small, one more procedure is needed for construction, the construction cost is increased, and the construction cost is high.
3. In modern decoration engineering, the novel thin-layer tile pasting technology is increasingly applied due to the advantages of environmental protection, space saving and the like. Therefore, the ceramic tile adhesive has the requirements of good construction performance and tensile bonding strength, small shrinkage rate and long airing time.
4. The weather environment also has certain influence to the ceramic tile glue, and anti stability of melting, in winter the outer wall construction, the ceramic tile of outer wall exposes in addition outdoors, and the change in weather, season will lead to the change of ceramic tile surface temperature, and this kind of change will produce great shear stress in the binder, leads to the destruction that ceramic tile and wall body bonded. Therefore, the requirement on the bonding strength of the ceramic tile adhesive is simultaneously required on the freeze-thaw cycle strength and the heat deformation resistance.
5. The variety of wall body also is the problem that ceramic tile glue needs to be solved in recent years, and many wall bodies adopt light partition walls such as dampproofing gypsum board, cement board, calcium silicate board, and this type of panel has certain wet expansibility, can take place the flexible deformation of panel under the wet change futilely, also can take place the side direction bending under the effect of external force, so under this condition, the ceramic tile drops, accidents such as fracture just take place more easily. In addition, the problem of tiling on the external thermal insulation of the external wall frequently occurs, for the external thermal insulation wall, the related factors are more, wherein the most important factor is the stability of the external thermal insulation system of the external wall and the characteristics of different external thermal insulation systems of the external wall, the current tile glue hardly plays a role in bonding, and one of the reasons is that the water content of the tile glue is excessively absorbed by the base layer during tiling, so that hollowing is caused. Such problems also occur in indoor lightweight partition panels.
Aiming at the various problems, at present, the tile glue on the market has uneven quality and mixed fish and dragon, has single functionality and various types, fails to solve various problems simultaneously by one formula, cannot further improve the bonding strength on the basis of quick drying, cannot combine the rigid bonding strength with the flexibility, ensures the sagging resistance and the slippage resistance, is difficult to ensure the hollowing condition of the tile with low water absorption rate and smooth bottom, and is difficult to ensure the airing time and the adjusting time for quick drying.
Disclosure of Invention
The invention aims to solve the problems that: the technical scheme is that the defects of a tile adhesive product are greatly improved, the tile adhesive is developed from single performance to multiple functions, not only has strong cohesive force, but also can solve the problems of quick drying, long airing time, frost resistance, droop, slippage, low water absorption, easiness in hollowing, falling and the like, can prolong the adjustment time, reduce the contraction and prolong the opening time, has the permeability function which is the main breakthrough at this time, uses industrial salt as an additive, is matched with starch ether and calcium formate, has cohesive force strength and certain permeability function, has the permeability function, can permeate into the pores of the tiles before the initial setting of the tile adhesive, is coagulated and hardened, and has the mechanical anchoring function similar to the insertion of a key into a lock hole, the method well solves the problems of low water absorption of large bricks and large difficulty in dense and smooth bonding of the back surfaces of the tiles, and easily solves the problem of sticking the tiles on various walls, and the addition of the industrial salt is the main research direction of the formula and also the main purpose of the invention.
In order to achieve the purpose, the invention adopts the technical scheme that: a preparation method of multifunctional permeable ceramic tile glue with strong binding power. The multifunctional permeable tile glue with strong binding power is characterized by being prepared by stirring and mixing 30-50% of cement, 50-70% of quartz sand, 0.3-2.5% of dispersible latex powder, 0.1-2.5% of cellulose, 0.05-1.5% of starch ether, 0.05-3.5% of industrial salt and 0.3-2.5% of calcium formate.
Through a large number of experimental researches, the inventor adds a formula to the tile adhesive on the basis of main materials of cement and quartz sand, mainly selects industrial salt, calcium formate and starch ether as formula auxiliaries, and the calcium formate is used as a quick setting agent, a lubricating agent and an early strength agent of the cement, so that the hardening speed of the cement is accelerated, the setting time is shortened, the bonding strength is improved, and particularly in winter construction, the phenomenon that the setting speed is too low at low temperature is avoided, so that the strength of the tile adhesive is improved as early as possible. The starch ether can be used for thickening the tile glue, so that the sagging resistance, the sagging resistance and the rheological property of the tile glue are improved, and the slip resistance of the tile glue can be obviously improved by adding the starch ether. The main components of the industrial salt are sodium chloride and sodium nitrite, experiments prove that the industrial salt is also a ceramic tile adhesive early strength agent, a coagulant and a coagulant, the ceramic tile adhesive can be used as an antifreeze by adding the industrial salt, so that the ceramic tile adhesive is normally hydrated at a low temperature of 0-15 ℃, the freezing point is reduced, the early strength of the ceramic tile adhesive is improved, the freeze-thaw stability of the wall strength ceramic tile adhesive is enhanced, the ceramic tile adhesive is used outdoors, the temperature change of weather and seasons reduces the generation of shear stress, the ceramic tile adhesive can ensure quick drying, the airing time and the adjusting time are prolonged, freezing resistance is realized, shrinkage is reduced, the opening time is prolonged, and particularly, the ceramic tile adhesive has certain permeability, cement can permeate ceramic tile pores before initial setting, is coagulated and hardened, the mechanical anchoring effect similar to inserting a key is realized, and the problems of large tiles and low water absorption rate are well solved.
Preferably, the industrial salt is a fine salt.
Preferably, the cement is of a Huarun 42.5 type or a 52.5 type.
Preferably, the dispersible latex powder is soft rubber powder, and German Wake 5010 rubber powder is used
Preferably, the cellulose is selected from 15-20 ten thousand model of high temperature resistant, hydroxypropyl methyl cellulose HPMC
Preferably, the starch ether is hydroxypropyl starch ether (HPS).
Preferably, the quartz sand is 60-120 meshes. River sand is not recommended, so that the impurities are too much, and the formula effect is difficult to control.
The invention also provides a preparation method of the multifunctional permeable tile glue with strong binding power, which comprises the following steps:
(1) adding cement and quartz sand into a stirrer through a spiral feeding machine according to the weight ratio for stirring
(2) And (3) stopping stirring after the step (1) is added, respectively pouring the ingredients with the weight ratio of the formula except the industrial salt into the opening of the horizontal stirrer, and stirring for about 10 minutes in a sealed manner.
(3) And (3) stopping stirring after the step (2) is finished, and directly pouring the industrial salt in a weight ratio into the opening of the horizontal stirrer.
(4) And after all the ingredients in the formula are added, continuously stirring for 10-20 minutes by using a sealed stirrer, and uniformly mixing.
(5) Stopping stirring, completely producing, and canning and bagging.
(6) The stirring time depends on the size of the stirrer and the stirring amount, the larger the stirring amount of the stirrer is, the longer the stirring time is, and the stirring and mixing time is 1-3 tons of the stirrer.
The invention has the beneficial effects that: the invention provides a preparation method of a multifunctional permeable tile adhesive with strong bonding force, which overcomes various problems of the tile adhesives in the existing market, enables the tile adhesives to develop from single characteristic to multiple functionality, enables the tile adhesives to have strong bonding force, and solves the problems of quick drying, increased airing time, adjustment time, frost resistance, droop, slippage, low water absorption rate, easiness in hollowing, falling and the like, enables the tile adhesives to have a permeable function, uses industrial salt as an additive, is matched with starch ether and calcium formate, has adhesive strength by using the tile adhesives, has a certain permeable function, easily solves the problem that various walls with different interfaces are stuck with tiles, and solves the problems that large tiles are difficult to be put on walls, low water absorption rate and large difficulty in smooth and compact sticking of the back of the tiles, and can solve various problems by using a product formula, the quick-drying anti-freezing ceramic tile has the advantages that the quick-drying anti-freezing ceramic tile is quick-drying, anti-sagging and anti-sliding, strong adhesion is achieved, the airing time is prolonged, the opening time is prolonged, a certain permeability function is achieved, cement mortar can penetrate into pores of the ceramic tile before initial setting, the ceramic tile is condensed and hardened, a mechanical anchoring effect similar to that of inserting a key into a lock hole is achieved, the problems of large tiles and low water absorption rate are well solved, even the ceramic tile back gluing can be abandoned during construction, the construction process is simple, the labor cost and the engineering cost are reduced, the main beneficial effect of the invention is also achieved, the economic benefit is obvious, and the popularization is easy.
Detailed Description
To better illustrate the objects, aspects and advantages of the present invention, the present invention will be further described with reference to specific examples.
Example 1
The invention provides a preparation method of a multifunctional permeable tile adhesive with strong binding power, which is prepared by stirring and mixing 35% of cement, 62.92% of quartz sand, 0.8% of dispersible latex powder, 0.2% of cellulose, 0.08% of starch ether, 0.5% of industrial salt and 0.5% of calcium formate by weight percentage through a stirrer.
The invention also provides a preparation method of the multifunctional permeable tile glue with strong binding power, which comprises the following steps:
(1) adding cement and quartz sand into a stirrer through a spiral feeding machine according to the weight ratio for stirring
(2) And (3) stopping stirring after the step (1) is added, respectively pouring the ingredients with the weight ratio of the formula except the industrial salt into the opening of the horizontal stirrer, and stirring for about 10 minutes in a sealed manner.
(3) And (3) stopping stirring after the step (2) is finished, and directly pouring the industrial salt in a weight ratio into the opening of the horizontal stirrer.
(4) And after all the ingredients in the formula are added, continuously stirring for 10-20 minutes by using a sealed stirrer, and uniformly mixing.
(5) Stopping stirring, completely producing, and canning and bagging.
(6) The stirring time depends on the size of the stirrer and the stirring amount, the larger the stirring amount of the stirrer is, the longer the stirring time is, and the stirring and mixing time is 1-3 tons of the stirrer.
Example 2
The difference between the embodiment of the invention and the embodiment 1 is that the quick-drying anti-freezing anti-sagging anti-slip permeation ceramic tile glue provided by the embodiment of the invention is prepared by mixing and stirring 40% of cement, 57.1% of quartz sand, 1% of dispersible latex powder, 0.3% of cellulose, 0.1% of starch ether, 0.8% of industrial salt and 0.7% of calcium formate.
Example 3
The multifunctional permeable tile glue with strong binding power in the embodiment of the present invention is different from the tile glue in embodiment 1 in that the multifunctional permeable tile glue with strong binding power is obtained by mixing and stirring 45% of cement, 51% of quartz sand, 1.5% of dispersible latex powder, 0.3% of cellulose, 0.2% of starch ether, 1% of industrial salt and 1% of calcium formate.
Example 4
The multifunctional permeable tile glue with strong binding power is obtained by mixing and stirring 50% of cement, 45.4% of quartz sand, 1.5% of dispersible latex powder, 0.3% of cellulose, 0.4% of starch ether, 1.2% of industrial salt and 1.2% of calcium formate.
Comparative example
The multifunctional permeable tile glue with strong binding power in the embodiment of the present invention is different from the tile glue in embodiment 3 in that the multifunctional permeable tile glue with strong binding power is obtained by mixing and stirring 45% of cement, 48.8% of quartz sand, 1.5% of dispersible latex powder, 0.3% of cellulose, 0.2% of starch ether, 2.5% of industrial salt and 1% of calcium formate. .
1. The tile glues of examples 1 to 4 and comparative example, which are of the multifunctional penetration type having strong adhesive force, were examined.
2. The test is carried out according to the requirements specified in JC/T547-2017 ceramic tile adhesive in the standards of the building materials industry of the people's republic of China.
The results are shown in Table 1.
As can be seen from Table 1, the tensile bonding strength after soaking, the tensile bonding strength after heat aging, the air-drying time of 20MIN, the bonding strength after freeze-thaw cycling, the air-drying time and the adjusting time of the multifunctional permeable tile adhesive prepared by the invention are all obviously higher than the standard requirements of JC/T547-, in the comparative example, under the condition that the cement proportion is not changed by 45 percent, when the proportion of the industrial salt is increased, the tensile bonding strength of various types is obviously improved, and the airing time and the adjusting time are also increased.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (14)
1. The multifunctional permeable ceramic tile glue with strong binding power is prepared with cement 30-50 wt%, quartz sand 50-70 wt%, dispersible latex powder 0.3-2.5 wt%, cellulose 0.1-2.5 wt%, starch ether 0.05-1.5 wt%, industrial salt 0.05-3.5 wt% and calcium formate 0.3-2.5 wt% and through mixing in stirrer.
2. The multifunctional permeable tile glue with strong binding power of claim 1, wherein 0.05-3.5% of industrial salt is added to the mixer at the end of all ingredients.
3. The multifunctional permeable tile glue with strong binding power according to claim 2, wherein the other ingredients except the main material aggregate (i.e. cement and quartz sand) are directly poured into the opening of the horizontal mixer during the addition.
4. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the cement is 30-50%.
5. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the dispersible latex powder accounts for 0.3-2.5% of the total weight of the tile glue.
6. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the cellulose is hydroxypropyl methyl cellulose HPMC in a ratio of 0.1-2.5%.
7. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the starch ether is 0.05-1.5% by weight.
8. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the calcium formate is 0.3-2.5%.
9. The multifunctional permeable tile glue with strong binding power of claim 1, wherein the quartz sand accounts for 50-70%.
10. A process for preparing a multifunctional permeable tile glue with strong binding power according to any one of claims 1-10, characterized in that it comprises the following sequential steps:
(1) adding cement and quartz sand into a stirrer through a spiral feeding machine according to the weight ratio for stirring
(2) And (3) stopping stirring after the step (1) is finished, respectively pouring the ingredients (dispersible emulsion powder, cellulose, starch ether and calcium formate) with the weight ratio of other formulas except the industrial salt into the opening of the horizontal stirrer, and sealing and stirring for about 10-15 minutes.
And 11, (3) stopping stirring after the step (2) is finished, and directly pouring the industrial salt in a weight ratio into an opening of the horizontal stirrer.
And 12, (4) after all the ingredients in the formula are added, continuously stirring for 10-20 minutes by using a sealed stirrer, and uniformly mixing.
(5) stopping stirring, completing the production process, and canning and bagging the materials to be prepared.
(6) the stirring time depends on the size of the stirrer and the amount of the stirred material, and the larger the stirring amount of the stirrer is, the longer the stirring time is, the more the stirrer needs to stir and mix, and the time is 1-3 tons of the size of the stirrer.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011543277.0A CN112479645A (en) | 2020-12-24 | 2020-12-24 | Preparation method of multifunctional permeable tile glue with strong binding power |
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| CN202011543277.0A CN112479645A (en) | 2020-12-24 | 2020-12-24 | Preparation method of multifunctional permeable tile glue with strong binding power |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115340326A (en) * | 2022-07-06 | 2022-11-15 | 宿州市焜燿环保建材有限公司 | Environment-friendly ceramic tile glue and production method thereof |
| CN116332598A (en) * | 2023-03-15 | 2023-06-27 | 江苏顺丽成建筑新材料有限公司 | Ceramic tile adhesive for adhering ceramic tile, face brick and floor tile and preparation method thereof |
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| US4065319A (en) * | 1975-11-18 | 1977-12-27 | Hercules Incorporated | Tile cements |
| US20050241539A1 (en) * | 2004-04-27 | 2005-11-03 | Wolfgang Hagen | Tile cement mortars using water retention agents |
| CN103466996A (en) * | 2013-09-12 | 2013-12-25 | 德高（广州）建材有限公司 | Neutral mosaic back gum with high flexibility |
| CN104310910A (en) * | 2014-10-21 | 2015-01-28 | 李金平 | Tile adhesive |
| CN105503106A (en) * | 2015-12-28 | 2016-04-20 | 上海亚瓦新型建筑材料有限公司 | Quickly-hardened high-strength ceramic tile adhesive |
| CN105837125A (en) * | 2016-04-28 | 2016-08-10 | 佛山市恒学科技服务有限公司 | Efficient tile adhesive |
| CN106348688A (en) * | 2016-08-26 | 2017-01-25 | 派丽(上海)管理有限公司 | Low-elasticity tile adhesive |
| CN107117908A (en) * | 2017-06-21 | 2017-09-01 | 江世妹 | A kind of ceramic tile adhesive of exterior wall retrofit |
| CN109095866A (en) * | 2018-10-30 | 2018-12-28 | 辽宁壹立方砂业有限责任公司 | A kind of glue for tile and preparation method thereof |
| CN110510951A (en) * | 2019-09-12 | 2019-11-29 | 佛山市卓仕高新型材料有限公司 | A kind of novel HHT higher high tensile bonding glue for tile |
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2020
- 2020-12-24 CN CN202011543277.0A patent/CN112479645A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4065319A (en) * | 1975-11-18 | 1977-12-27 | Hercules Incorporated | Tile cements |
| US20050241539A1 (en) * | 2004-04-27 | 2005-11-03 | Wolfgang Hagen | Tile cement mortars using water retention agents |
| CN103466996A (en) * | 2013-09-12 | 2013-12-25 | 德高（广州）建材有限公司 | Neutral mosaic back gum with high flexibility |
| CN104310910A (en) * | 2014-10-21 | 2015-01-28 | 李金平 | Tile adhesive |
| CN105503106A (en) * | 2015-12-28 | 2016-04-20 | 上海亚瓦新型建筑材料有限公司 | Quickly-hardened high-strength ceramic tile adhesive |
| CN105837125A (en) * | 2016-04-28 | 2016-08-10 | 佛山市恒学科技服务有限公司 | Efficient tile adhesive |
| CN106348688A (en) * | 2016-08-26 | 2017-01-25 | 派丽(上海)管理有限公司 | Low-elasticity tile adhesive |
| CN107117908A (en) * | 2017-06-21 | 2017-09-01 | 江世妹 | A kind of ceramic tile adhesive of exterior wall retrofit |
| CN109095866A (en) * | 2018-10-30 | 2018-12-28 | 辽宁壹立方砂业有限责任公司 | A kind of glue for tile and preparation method thereof |
| CN110510951A (en) * | 2019-09-12 | 2019-11-29 | 佛山市卓仕高新型材料有限公司 | A kind of novel HHT higher high tensile bonding glue for tile |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115340326A (en) * | 2022-07-06 | 2022-11-15 | 宿州市焜燿环保建材有限公司 | Environment-friendly ceramic tile glue and production method thereof |
| CN116332598A (en) * | 2023-03-15 | 2023-06-27 | 江苏顺丽成建筑新材料有限公司 | Ceramic tile adhesive for adhering ceramic tile, face brick and floor tile and preparation method thereof |
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