CN112452280B - Device for monitoring racemization of glufosinate-ammonium big data cluster - Google Patents
Device for monitoring racemization of glufosinate-ammonium big data cluster Download PDFInfo
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- CN112452280B CN112452280B CN202011471613.5A CN202011471613A CN112452280B CN 112452280 B CN112452280 B CN 112452280B CN 202011471613 A CN202011471613 A CN 202011471613A CN 112452280 B CN112452280 B CN 112452280B
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- ammonium
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- 230000006340 racemization Effects 0.000 title claims abstract description 20
- 238000012544 monitoring process Methods 0.000 title claims abstract description 17
- IAJOBQBIJHVGMQ-UHFFFAOYSA-N 2-amino-4-[hydroxy(methyl)phosphoryl]butanoic acid Chemical compound CP(O)(=O)CCC(N)C(O)=O IAJOBQBIJHVGMQ-UHFFFAOYSA-N 0.000 title claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 claims abstract description 49
- 238000003756 stirring Methods 0.000 claims abstract description 34
- 239000003054 catalyst Substances 0.000 claims abstract description 24
- 238000007789 sealing Methods 0.000 claims description 73
- 239000007788 liquid Substances 0.000 claims description 5
- 239000003814 drug Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 6
- 229940079593 drug Drugs 0.000 abstract description 3
- ZBMRKNMTMPPMMK-UHFFFAOYSA-N 2-amino-4-[hydroxy(methyl)phosphoryl]butanoic acid;azane Chemical compound [NH4+].CP(O)(=O)CCC(N)C([O-])=O ZBMRKNMTMPPMMK-UHFFFAOYSA-N 0.000 description 19
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000005561 Glufosinate Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 102000005396 glutamine synthetase Human genes 0.000 description 3
- 108020002326 glutamine synthetase Proteins 0.000 description 3
- 230000002363 herbicidal effect Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- LOUPRKONTZGTKE-WZBLMQSHSA-N Quinine Chemical compound C([C@H]([C@H](C1)C=C)C2)C[N@@]1[C@@H]2[C@H](O)C1=CC=NC2=CC=C(OC)C=C21 LOUPRKONTZGTKE-WZBLMQSHSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000001258 Cinchona calisaya Nutrition 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 231100000674 Phytotoxicity Toxicity 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000002210 biocatalytic effect Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 210000003763 chloroplast Anatomy 0.000 description 1
- LOUPRKONTZGTKE-UHFFFAOYSA-N cinchonine Natural products C1C(C(C2)C=C)CCN2C1C(O)C1=CC=NC2=CC=C(OC)C=C21 LOUPRKONTZGTKE-UHFFFAOYSA-N 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 239000004009 herbicide Substances 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000029553 photosynthesis Effects 0.000 description 1
- 238000010672 photosynthesis Methods 0.000 description 1
- 230000005080 plant death Effects 0.000 description 1
- 229960000948 quinine Drugs 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 230000009261 transgenic effect Effects 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/08—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles
- B01J8/10—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with moving particles moved by stirrers or by rotary drums or rotary receptacles or endless belts
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/30—Phosphinic acids [R2P(=O)(OH)]; Thiophosphinic acids ; [R2P(=X1)(X2H) (X1, X2 are each independently O, S or Se)]
- C07F9/301—Acyclic saturated acids which can have further substituents on alkyl
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/584—Recycling of catalysts
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- Chemical Kinetics & Catalysis (AREA)
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Abstract
The invention discloses a device for despinning a large data cluster of supervisory glufosinate-ammonium, which belongs to the technical field of despinning and comprises a spiral elevator, a support frame and a lifting frame, wherein the spiral elevator is obliquely arranged on the lifting frame, the inlet of the spiral elevator is connected with a funnel, the outlet of the spiral elevator is provided with a discharge pipe, the bottom end of the discharge pipe is inserted into a reaction box, the side wall of the reaction box is fixedly provided with a catalyst quantitative discharge mechanism, and the reaction box is provided with a stirring mechanism. According to the device for monitoring racemization of the glufosinate-ammonium big data cluster, when the quantitative telescopic mechanism works, the racemized glufosinate-ammonium materials are quantitatively conveyed into the reaction box through one stroke of movement, each reaction is monitored in real time, the racemized glufosinate-ammonium materials are collected into the big data to establish a cluster, data of the cluster are observed, an effective monitoring system is established, the racemized drug amount is quantified, and the racemization effect is improved.
Description
Technical Field
The invention relates to the technical field of racemization, in particular to a device for monitoring racemization of a glufosinate-ammonium big data cluster.
Background
Glufosinate (Glufosinate), developed by Hoechst (Hoechst) in germany, is a Glutamine Synthetase (GS) inhibitor that inhibits all known forms of GS, resulting in disturbed nitrogen metabolism, excessive accumulation of ammonia, chloroplast disintegration in plants, and thus inhibited photosynthesis, ultimately leading to plant death. The glufosinate-ammonium has strong herbicidal activity, can almost effectively prevent and kill off various weeds to be tested, is safe to crops, has high activity, wide herbicidal spectrum and small phytotoxicity, and is an ideal herbicide for transgenic resistant crops at present. Glufosinate is also an excellent fungicide.
The existing methods for resolving racemic mixtures are mainly divided into chemical chiral resolution and biocatalytic chiral resolution.
The chemical chiral resolution method is to chemically synthesize racemic D, L-glufosinate-ammonium or derivatives thereof, and then separate D-type and L-type isomers by using a chiral resolution reagent, so as to prepare the optically pure L-glufosinate-ammonium. Salifying glufosinate-ammonium racemate and quinine, crystallizing, filtering and washing to obtain high-purity L-glufosinate-ammonium quinine salt, and neutralizing with ammonia to obtain L-glufosinate-ammonium. The yield is 86% at most, and the e.e. value is 99% at most. The resolution process has obvious defects: firstly, glufosinate-ammonium derivatives need to be synthesized, and then enzyme catalysis reaction is carried out, so that the technical process is complex, the product yield is low, racemization is not supported by big data, and the reaction effect and the accuracy of the ratio need to be improved.
Disclosure of Invention
The invention aims to provide a despinning device for monitoring large glufosinate-ammonium data clusters, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a supervision glufosinate-ammonium big data cluster rotation eliminating device, includes screw elevator, support frame and hoisting frame, the slope of screw elevator is installed on the hoisting frame, and screw elevator's import meets with the funnel, and screw elevator's export installation discharging pipe, in the reaction box was inserted to the bottom of discharging pipe, fixed catalyst ration discharge mechanism on the lateral wall of reaction box installed rabbling mechanism on the reaction box.
Further, the stirring mechanism comprises a motor, a motor base, a stirring shaft and stirring blades, the bottom end of the motor base is fixed on the reaction box, the motor is fixed on the motor base, a motor shaft at the output end of the motor is connected with one end of the stirring shaft through a shaft key, the other end of the stirring shaft penetrates into the reaction box, and the stirring blades are distributed on the stirring shaft at equal intervals.
Further, the catalyst quantitative discharge mechanism comprises an upper supporting plate, a lower supporting plate, a catalyst storage tank and a quantitative telescopic mechanism, wherein the upper supporting plate and the lower supporting plate are fixed on the same side of the reaction box, and are fixed through a support;
the catalyst storage tank is arranged on the upper supporting plate, the quantitative telescopic mechanism is arranged on the lower supporting plate, the side wall of the catalyst storage tank is connected with the feeding pipe, a display screen for monitoring the content of glufosinate ammonium is fixed above the catalyst storage tank, a measuring cylinder connected to the bottom of the catalyst storage tank is sleeved with a discharge pipe, one end of the discharge pipe is communicated with the reaction box, and the other end of the discharge pipe is inserted into the quantitative telescopic mechanism.
Further, the discharge pipe and the measuring cylinder are perpendicular to each other, the inner diameters of the discharge pipe and the measuring cylinder are the same, and the discharge pipe is provided with a U-shaped hole communicated with the reaction box.
Furthermore, the quantitative telescopic mechanism comprises an outer cylinder, a shell, a cross rod, a front sealing plate, an inner cylinder and a rear sealing plate, wherein the outer cylinder is arranged on the lower supporting plate, a piston rod of the outer cylinder is connected with the shell, the shell is connected with the discharge pipe in a sealing manner, the other end of the shell, which is symmetrical to the piston rod, is fixed with the port of the cross rod, and the front sealing plate which is sealed with the discharge pipe is fixed at the other end of the cross rod;
the inner cylinder is arranged in the shell, and a piston rod of the inner cylinder penetrates out of the shell to be connected with the rear sealing plate.
Further, the outer cylinder is in an initial state, the bottom end of the measuring cylinder is positioned between the front sealing plate and the rear sealing plate, and the volume of a cavity formed by the front sealing plate, the rear sealing plate and the discharge pipe is the volume of quantitative discharge;
the outer cylinder is in a middle state, the outer cylinder works to drive the shell to slide and seal the bottom of the measuring cylinder, the front sealing plate slides to the outside of the U-shaped hole, and the cavity is communicated with the U-shaped hole;
the inner cylinder is in a tail end state, the rear sealing plate is driven to slide towards the front sealing plate in a working mode, and the rear sealing plate pushes liquid to flow into the reaction box through the U-shaped hole.
Further, when the rear sealing plate contacts with the front sealing plate, the rear sealing plate seals the U-shaped hole, the outer cylinder drives the shell to move reversely, the rear sealing plate and the front sealing plate synchronously move to the initial position of the outer cylinder, the inner cylinder works again, and the rear sealing plate moves to the initial position.
Compared with the prior art, the invention has the beneficial effects that: according to the monitoring glufosinate-ammonium big data cluster racemization device, an outer air cylinder is in an initial state, the bottom end of a measuring cylinder is located between a front sealing plate and a rear sealing plate, and the volume of a cavity formed by the front sealing plate, the rear sealing plate and a discharge pipe is the volume of quantitative discharge; the outer cylinder is in a middle state, the outer shell is driven to slide and seal the bottom of the measuring cylinder in a working mode, the front sealing plate slides to the outside of the U-shaped hole, and the cavity is communicated with the U-shaped hole; the inner cylinder is in a tail end state, the rear sealing plate is driven to slide towards the front sealing plate in a working mode, and the rear sealing plate pushes liquid to flow into the reaction box through the U-shaped hole. The stirring blade stirs the glufosinate-ammonium in the reaction box to improve the mixing with the medicine during working, racemization is promoted, the arranged quantitative telescopic mechanism quantitatively sends the glufosinate-ammonium racemized material into the reaction box through movement of one stroke during working, reaction is monitored in real time each time, the material is collected into big data to establish a cluster, data of the cluster is observed, an effective monitoring system is established, the racemized medicine amount is quantified, and the racemization effect is improved.
Drawings
FIG. 1 is an overall block diagram of the present invention;
FIG. 2 is a partial block diagram of the present invention;
FIG. 3 is a perspective view of a reaction tank of the present invention;
FIG. 4 is an initial state diagram of the quantitative retraction device of the present invention;
FIG. 5 is a middle view of the quantitative retraction device of the present invention;
FIG. 6 is a view showing the end state of the quantitative retraction device according to the present invention;
fig. 7 is a partial perspective view of the quantitative retraction device of the present invention.
In the figure: 1. a screw elevator; 11. a funnel; 12. a discharge pipe; 2. a support frame; 3. a lifting frame; 4. a reaction box; 5. a catalyst quantitative discharge mechanism; 51. an upper supporting plate; 52. a lower supporting plate; 53. a catalyst storage tank; 531. a measuring cylinder; 532. a feed pipe; 54. a quantitative telescopic mechanism; 541. an outer cylinder; 542. a housing; 543. a cross bar; 544. a front sealing plate; 545. an inner cylinder; 546. a rear sealing plate; 6. a stirring mechanism; 61. a motor; 62. a motor base; 63. a stirring shaft; 64. stirring blades; 7. a discharge pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Please refer to fig. 1, a device for monitoring racemization of a glufosinate-ammonium big data cluster comprises a spiral elevator 1, a support frame 2 and a lifting frame 3, wherein the spiral elevator 1 is obliquely installed on the lifting frame 3, an inlet of the spiral elevator 1 is connected with a funnel 11, an outlet of the spiral elevator 1 is provided with a discharge pipe 12, the bottom end of the discharge pipe 12 is inserted into a reaction box 4, the spiral elevator 1 conveys glufosinate-ammonium to the reaction box 4, a catalyst quantitative discharge mechanism 5 is fixed on the side wall of the reaction box 4, and a stirring mechanism 6 is installed on the reaction box 4.
Referring to fig. 2-3, the stirring mechanism 6 includes a motor 61, a motor base 62, a stirring shaft 63 and a stirring blade 64, the bottom end of the motor base 62 is fixed on the reaction box 4, the motor 61 is fixed on the motor base 62, a motor shaft at an output end of the motor 61 is connected with one end of the stirring shaft 63 through a shaft key, the other end of the stirring shaft 63 penetrates into the reaction box 4, the stirring blades 64 are distributed on the stirring shaft 63 at equal intervals, the stirring blade 64 is driven to rotate by the arranged motor 61, and the stirring blade 64 stirs glufosinate ammonium in the reaction box 4 during operation to improve the mixing with the medicine, so as to promote racemization.
Referring to fig. 4-7, the catalyst quantitative discharge mechanism 5 includes an upper support plate 51, a lower support plate 52, a catalyst storage tank 53 and a quantitative telescopic mechanism 54, the upper support plate 51 and the lower support plate 52 are fixed on the same side of the reaction chamber 4, the upper support plate 51 and the lower support plate 52 are fixed by a support, and the upper support plate 51 and the lower support plate 52 play a role of support.
The catalyst storage tank 53 is arranged on the upper supporting plate 51, the quantitative telescopic mechanism 54 is arranged on the lower supporting plate 52, the side wall of the catalyst storage tank 53 is connected with the feeding pipe 532, a display screen for monitoring the content of glufosinate ammonium is fixed above the catalyst storage tank 53, the measuring cylinder 531 connected to the bottom of the catalyst storage tank 53 is sleeved with the discharge pipe 7, one end of the discharge pipe 7 is communicated with the reaction box 4, and the other end of the discharge pipe 7 is inserted by the quantitative telescopic mechanism 54.
The discharge pipe 7 and the measuring cylinder 531 are perpendicular to each other, and the discharge pipe 7 and the measuring cylinder 531 have the same inner diameter, and the discharge pipe 7 is provided with a U-shaped hole communicated with the reaction chamber 4.
The quantitative telescopic mechanism 54 comprises an outer cylinder 541, a casing 542, a cross rod 543, a front sealing plate 544, an inner cylinder 545 and a rear sealing plate 546, wherein the outer cylinder 541 is installed on the lower support plate 52, a piston rod of the outer cylinder 541 is connected with the casing 542, the casing 542 is connected with the discharge pipe 7 in a sealing manner, the other end of the casing 542, which is symmetrical to the piston rod, is fixed with the port of the cross rod 543, the front sealing plate 544 which is sealed with the discharge pipe 7 is fixed at the other end of the cross rod 543, the inner cylinder 545 is installed in the casing 542, and a piston rod of the inner cylinder 545 penetrates through the casing 542 to be connected with the rear sealing plate 546.
The outer cylinder 541 is in an initial state, the bottom end of the measuring cylinder 531 is located between the front sealing plate 544 and the rear sealing plate 546, and the cavity volume formed by the front sealing plate 544, the rear sealing plate 546 and the discharge pipe 7 is the volume of the metered discharge.
When the rear sealing plate 546 contacts the front sealing plate 544, the rear sealing plate 546 seals the U-shaped hole, the outer cylinder 541 drives the housing 542 to move in the reverse direction, the rear sealing plate 546 moves to the initial position of the outer cylinder 541 in synchronization with the front sealing plate 544, the inner cylinder 545 operates again, and the rear sealing plate 546 moves to the initial position.
When the quantitative telescopic mechanism 54 is in operation, the material racemized by glufosinate-ammonium is quantitatively conveyed into the reaction box 4 through one stroke of movement, each reaction is monitored in real time, the reaction is collected into big data to establish a cluster, the data of the cluster is observed, an effective monitoring system is established, the amount of racemized drug is quantified, and the racemization effect is improved.
In conclusion; in the device for monitoring racemization of the glufosinate-ammonium big data cluster, the outer cylinder 541 is in an initial state, the bottom end of the measuring cylinder 531 is positioned between the front sealing plate 544 and the rear sealing plate 546, and the volume of a cavity formed by the front sealing plate 544, the rear sealing plate 546 and the discharge pipe 7 is the volume of quantitative discharge. With the outer cylinder 541 in the intermediate position, the operating drive housing 542 slides to seal the bottom of the cylinder 531, the front seal plate 544 slides to the exterior of the U-shaped aperture, and the cavity communicates with the U-shaped aperture. Inner cylinder 545 is in the end position and operates to slide rear sealing plate 546 toward front sealing plate 544, and rear sealing plate 546 pushes liquid through the U-shaped holes into reaction chamber 4. The stirring blade 64 stirs glufosinate-ammonium in the reaction box 4 during operation to improve mixing with medicines and promote racemization, the quantitative telescopic mechanism 54 is arranged to quantitatively convey glufosinate-ammonium racemized materials into the reaction box 4 through movement of one stroke during operation, reaction is monitored in real time each time, the materials are collected into big data to establish a cluster, data of the clusters are observed, an effective monitoring system and quantitative racemization medicine amount are established, and the racemization effect is improved.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be able to cover the technical solutions and the inventive concepts of the present invention within the technical scope of the present invention.
Claims (3)
1. A device for monitoring racemization of a glufosinate-ammonium big data cluster comprises a spiral elevator (1), a support frame (2) and a lifting frame (3), wherein the spiral elevator (1) is obliquely arranged on the lifting frame (3), an inlet of the spiral elevator (1) is connected with a funnel (11), and an outlet of the spiral elevator (1) is provided with a discharge pipe (12), and is characterized in that; the bottom end of the discharge pipe (12) is inserted into the reaction box (4), the side wall of the reaction box (4) is fixed with a catalyst quantitative discharge mechanism (5), and the reaction box (4) is provided with a stirring mechanism (6);
the catalyst quantitative discharge mechanism (5) comprises an upper supporting plate (51), a lower supporting plate (52), a catalyst storage tank (53) and a quantitative telescopic mechanism (54), wherein the upper supporting plate (51) and the lower supporting plate (52) are fixed on the same side of the reaction box (4), and the upper supporting plate (51) and the lower supporting plate (52) are fixed through a support;
the catalyst storage tank (53) is arranged on the upper supporting plate (51), the quantitative telescopic mechanism (54) is arranged on the lower supporting plate (52), the side wall of the catalyst storage tank (53) is connected with the feeding pipe (532), a display screen for monitoring the content of glufosinate ammonium is fixed above the catalyst storage tank (53), a measuring cylinder (531) connected to the bottom of the catalyst storage tank (53) is sleeved with a discharge pipe (7), one end of the discharge pipe (7) is communicated with the reaction box (4), and the other end of the discharge pipe (7) is inserted by the quantitative telescopic mechanism (54);
the discharge pipe (7) and the measuring cylinder (531) are perpendicular to each other, the inner diameters of the discharge pipe (7) and the measuring cylinder (531) are the same, and a U-shaped hole communicated with the reaction box (4) is formed in the discharge pipe (7);
the quantitative telescopic mechanism (54) comprises an outer cylinder (541), a shell (542), a cross bar (543), a front sealing plate (544), an inner cylinder (545) and a rear sealing plate (546), the outer cylinder (541) is installed on the lower supporting plate (52), a piston rod of the outer cylinder (541) is connected with the shell (542), the shell (542) is connected with the discharge pipe (7) in a sealing manner, the other end of the shell (542) which is symmetrical to the piston rod is fixed with the port of the cross bar (543), and the other end of the cross bar (543) is fixed with the front sealing plate (544) which is sealed with the discharge pipe (7);
an inner cylinder (545) is arranged in the outer shell (542), and a piston rod of the inner cylinder (545) penetrates out of the outer shell (542) to be connected with the rear sealing plate (546);
the outer cylinder (541) is in an initial state, the bottom end of the measuring cylinder (531) is positioned between the front sealing plate (544) and the rear sealing plate (546), and the cavity formed by the front sealing plate (544), the rear sealing plate (546) and the discharge pipe (7) is a quantitative discharge volume;
the outer cylinder (541) is in a middle state, the working driving shell (542) slides to seal the bottom of the measuring cylinder (531), the front sealing plate (544) slides to the outside of the U-shaped hole, and the cavity is communicated with the U-shaped hole;
the inner cylinder (545) is in a tail end state, the rear sealing plate (546) is driven to slide towards the front sealing plate (544) in an operating mode, and the rear sealing plate (546) pushes liquid to flow into the reaction box (4) through the U-shaped hole.
2. The device for monitoring racemization of glufosinate-ammonium big data clusters as claimed in claim 1, wherein the stirring mechanism (6) comprises a motor (61), a motor base (62), a stirring shaft (63) and stirring blades (64), the bottom end of the motor base (62) is fixed on the reaction box (4), the motor (61) is fixed on the motor base (62), a motor shaft at the output end of the motor (61) is connected with one end of the stirring shaft (63) through a shaft key, the other end of the stirring shaft (63) penetrates into the reaction box (4), and the stirring blades (64) are distributed on the stirring shaft (63) at equal intervals.
3. The apparatus for despinning a glufosinate-ammonium big data cluster racemization device according to claim 1, wherein when the rear sealing plate (546) is in contact with the front sealing plate (544), the rear sealing plate (546) seals the U-shaped hole, the outer cylinder (541) drives the outer shell (542) to move in a reverse direction, the rear sealing plate (546) and the front sealing plate (544) move synchronously to an initial position of the outer cylinder (541), the inner cylinder (545) operates again, and the rear sealing plate (546) moves to the initial position.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011471613.5A CN112452280B (en) | 2020-12-14 | 2020-12-14 | Device for monitoring racemization of glufosinate-ammonium big data cluster |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011471613.5A CN112452280B (en) | 2020-12-14 | 2020-12-14 | Device for monitoring racemization of glufosinate-ammonium big data cluster |
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| Publication Number | Publication Date |
|---|---|
| CN112452280A CN112452280A (en) | 2021-03-09 |
| CN112452280B true CN112452280B (en) | 2022-09-02 |
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| CN202011471613.5A Active CN112452280B (en) | 2020-12-14 | 2020-12-14 | Device for monitoring racemization of glufosinate-ammonium big data cluster |
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| DE10122491A1 (en) * | 2001-05-10 | 2002-11-14 | Bayer Ag | Device and method for carrying out experiments in parallel |
| CN107983194A (en) * | 2017-11-13 | 2018-05-04 | 深圳润丰投资咨询有限公司 | It is a kind of quantitative fixed than chemical fertilizer aqueous solution device for formulating |
| CN209663269U (en) * | 2019-02-14 | 2019-11-22 | 江苏长青农化南通有限公司 | Reaction kettle is used in a kind of production of glufosinate-ammonium |
| CN209646346U (en) * | 2019-03-18 | 2019-11-19 | 山东宾利环保科技有限公司 | A kind of SNCR denitration agent automatic assembly line dosages distribution reaction unit |
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