CN112408927A - Chemically foamed low-density alkali slag foam concrete and preparation method thereof - Google Patents
Chemically foamed low-density alkali slag foam concrete and preparation method thereof Download PDFInfo
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- CN112408927A CN112408927A CN202011355982.8A CN202011355982A CN112408927A CN 112408927 A CN112408927 A CN 112408927A CN 202011355982 A CN202011355982 A CN 202011355982A CN 112408927 A CN112408927 A CN 112408927A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
- C04B28/08—Slag cements
- C04B28/082—Steelmaking slags; Converter slags
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B38/00—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
- C04B38/02—Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof by adding chemical blowing agents
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/40—Surface-active agents, dispersants
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
- C04B2103/48—Foam stabilisers
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/52—Sound-insulating materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/20—Mortars, concrete or artificial stone characterised by specific physical values for the density
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Abstract
The invention discloses a chemical foaming low-density alkali slag foam concrete and a preparation method thereof, relating to the technical field of building materials, and the key points of the technical scheme are as follows: the composite material comprises the following components in percentage by mass: slag: 56-58 percent; water glass: 16 to 20 percent; sodium hydroxide: 2 to 4 percent; chemical foaming agent: 1 to 2 percent; foam stabilizer: 0.057-0.082%; water: 12 to 18 percent; surfactant (b): 1.0-1.2 percent. The density of the alkali slag foam concrete provided by the invention is as low as 250kg/m3Has the advantages of short condensation time, fast strength development and good heat preservationThe sound performance can effectively utilize slag which is an industrial byproduct, is a lightweight low-carbon environment-friendly concrete material, and accords with the development trend of 'green and environment-friendly' of building materials.
Description
Technical Field
The invention relates to the technical field of building materials, relates to foam concrete, and particularly relates to chemically foamed low-density alkali slag foam concrete and a preparation method thereof.
Background
Cement is a common building material used in industry. However, the cement production process consumes a lot of energy and discharges carbon dioxide, and there are data showing: carbon dioxide gas discharged in the process of producing ordinary portland cement accounts for 5% of the global carbon dioxide release amount. This aggravates the greenhouse effect and does not meet the national strategy of low energy and low carbon consumption. The alkali slag cement is a novel cementitious material comprising an alkali metal compound and finely ground water-quenched blast furnace slag as main components, and is an industrial byproduct. The alkali slag cement is named as a cementing material with the greatest development potential in the twenty-first century, and has the advantages of quick setting, quick strength development, excellent fire resistance and chemical corrosion resistance and better freezing resistance than a portland cement system. Compared with portland cement, the energy required for producing the same amount of slag powder is nearly 90% lower, so that the alkali slag concrete is a low-carbon, environment-friendly and low-energy-consumption building material.
At present, because organic heat-insulating materials have the problems of fire hazard, poor durability, easy generation of a large amount of garbage after service and the like, the exit of the building heat-insulating materials represented by polystyrene boards is only a time problem, and under the condition, the research and preparation of inorganic heat-insulating materials will cause the revolution in the field of heat-insulating materials. The alkali slag foam concrete is probably the main force of the inorganic heat-insulating material due to a series of advantages. The existing alkali slag foam concrete is mainly prepared by a chemical foaming method, and the preparation process comprises the steps of uniformly mixing raw materials such as slag, an alkali activator, a foam stabilizer, a foaming agent and the like in a stirring pot; then pouring the mixture into a mould, and utilizing a chemical foaming agent to perform chemical reaction in the slag slurry to generate bubbles so as to expand the slag slurry; after the forming, the light porous heat insulation material is obtained through standard maintenance.
The density of the existing alkali slag foam concrete is generally 300kg/m3In the building structure such as the inner wall, the outer wall, the layer surface, the floor surface, the upright post and the like of the building, the low-density foamed concrete can reduce the dead weight of the building and improve the bearing capacity of the building construction. However, at present, the national concern is lowThe density chemical foaming alkali slag foam concrete is only reported, so how to research and design the chemical foaming low-density alkali slag foam concrete and the preparation method are the problems which need to be solved urgently at present.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention aims to provide a chemically foamed low-density alkali slag foam concrete and a preparation method thereof.
The technical purpose of the invention is realized by the following technical scheme:
in a first aspect, the chemically foamed low-density alkali slag foam concrete is provided, which comprises the following components in percentage by mass:
slag: 56-58 percent;
water glass: 16 to 20 percent;
sodium hydroxide: 2 to 4 percent;
chemical foaming agent: 1 to 2 percent;
foam stabilizer: 0.057-0.082%;
water: 12 to 18 percent;
surfactant (b): 1.0-1.2 percent.
Preferably, the alkali slag foam concrete consists of the following components in percentage by mass:
slag: 57-58%;
water glass: 18 to 20 percent;
sodium hydroxide: 3 to 4 percent;
chemical foaming agent: 1.3 to 1.5 percent;
foam stabilizer: 0.057-0.082%;
water: 12 to 15 percent;
surfactant (b): 1.1-1.2%.
Preferably, the alkali slag foam concrete consists of the following components in percentage by mass:
slag: 57 percent;
water glass: 18 percent;
sodium hydroxide: 3 percent;
chemical foaming agent: 1.3 percent;
foam stabilizer: 0.057-0.082%;
water: 15 percent;
surfactant (b): 1.1 percent.
Preferably, the water glass has a modulus of 3.08, a water content of 57.1%, and Na2O content 9.1%, SiO2The content was 27.19%.
Preferably, the chemical foaming agent is aluminum powder, and is prepared into an aluminum powder-water-surfactant suspension when in use.
Preferably, the foam stabilizer is tea saponin.
Preferably, the surfactant is water-based calcium stearate, and the mass fraction of the surfactant is 50%.
Preferably, the slag is ground water-quenched blast furnace slag.
In a second aspect, there is provided a method of producing a chemically foamed low-density alkali slag foamed concrete according to any one of the first aspects, comprising the steps of:
s1: mixing and stirring aluminum powder, water and a surfactant to prepare an aluminum powder-water-surfactant suspension;
s2: adding the slag and the foam stabilizer into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
Preferably, the preparation of the water glass-sodium hydroxide composite alkali activator specifically comprises the following steps: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use.
Compared with the prior art, the invention has the following beneficial effects:
the density of the alkali slag foam concrete provided by the invention is as low as 250kg/m3Has short coagulation time and high strengthThe concrete has the advantages of fast development, good heat preservation and sound insulation performance, can effectively utilize slag which is an industrial byproduct, is a light low-carbon environment-friendly concrete material, and accords with the development trend of 'green and environment-friendly' building materials.
Detailed Description
In order to make the technical problems, technical solutions and advantageous effects to be solved by the present invention more apparent, the present invention is further described in detail below with reference to the following embodiments.
Example 1: the chemical foaming low-density alkali slag foam concrete comprises the following components in percentage by mass: slag: 56 percent; water glass: 16 percent; sodium hydroxide: 2 percent; chemical foaming agent: 1 percent; foam stabilizer: 0.057%; water: 12 percent; surfactant (b): 1.0 percent.
Wherein the water glass has a modulus of 3.08, a water content of 57.1%, and Na2O content 9.1%, SiO2The content was 27.19%. The chemical foaming agent is aluminum powder, and is prepared into an aluminum powder-water-surfactant suspension when in use. The foam stabilizer is tea saponin. The surfactant is water-based calcium stearate with the mass fraction of 50%. The slag is ground water-quenched blast furnace slag.
The preparation method comprises the following steps:
s1: dispersing aluminum powder in water, stirring for 5min, adding water-based calcium stearate, mixing and stirring for 5min to obtain a water-aluminum powder-water-based calcium stearate suspension;
s2: adding the slag and the tea saponin into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use. Adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
Example 2: the chemical foaming low-density alkali slag foam concrete comprises the following components in percentage by mass: slag: 58 percent; water glass: 20 percent; sodium hydroxide: 4 percent; chemical foaming agent: 2 percent; foam stabilizer: 0.082%; water: 18 percent; surfactant (b): 1.2 percent.
Wherein the water glass has a modulus of 3.08, a water content of 57.1%, and Na2O content 9.1%, SiO2The content was 27.19%. The chemical foaming agent is aluminum powder, and is prepared into an aluminum powder-water-surfactant suspension when in use. The foam stabilizer is tea saponin. The surfactant is water-based calcium stearate with the mass fraction of 50%. The slag is ground water-quenched blast furnace slag.
The preparation method comprises the following steps:
s1: dispersing aluminum powder in water, stirring for 5min, adding water-based calcium stearate, mixing and stirring for 5min to obtain a water-aluminum powder-water-based calcium stearate suspension;
s2: adding the slag and the tea saponin into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use. Adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
Example 3: the chemical foaming low-density alkali slag foam concrete comprises the following components in percentage by mass: slag: 57 percent; water glass: 18 percent; sodium hydroxide: 3 percent; chemical foaming agent: 1.3 percent; foam stabilizer: 0.057%; water: 15 percent; surfactant (b): 1.1 percent.
Wherein the water glass has a modulus of 3.08, a water content of 57.1%, and Na2O content 9.1%, SiO2The content was 27.19%. The chemical foaming agent is aluminum powder, and is prepared into an aluminum powder-water-surfactant suspension when in use. The foam stabilizer is tea saponin. Watch (A)The surfactant is water-based calcium stearate with the mass fraction of 50%. The slag is ground water-quenched blast furnace slag.
The preparation method comprises the following steps:
s1: dispersing aluminum powder in water, stirring for 5min, adding water-based calcium stearate, mixing and stirring for 5min to obtain a water-aluminum powder-water-based calcium stearate suspension;
s2: adding the slag and the tea saponin into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use. Adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
Example 4: the chemical foaming low-density alkali slag foam concrete comprises the following components in percentage by mass: slag: 57 percent; water glass: 18 percent; sodium hydroxide: 3 percent; chemical foaming agent: 1.3 percent; foam stabilizer: 0.082%; water: 15 percent; surfactant (b): 1.1 percent.
Wherein the water glass has a modulus of 3.08, a water content of 57.1%, and Na2O content 9.1%, SiO2The content was 27.19%. The chemical foaming agent is aluminum powder, and is prepared into an aluminum powder-water-surfactant suspension when in use. The foam stabilizer is tea saponin. The surfactant is water-based calcium stearate with the mass fraction of 50%. The slag is ground water-quenched blast furnace slag.
The preparation method comprises the following steps:
s1: dispersing aluminum powder in water, stirring for 5min, adding water-based calcium stearate, mixing and stirring for 5min to obtain a water-aluminum powder-water-based calcium stearate suspension;
s2: adding the slag and the tea saponin into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use. Adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
Experimental verification and analysis:
(1) based on the alkali slag foam concrete and the preparation method provided in examples 3 and 4, the compressive strength and density of the alkali slag foam concrete 28d were measured at different tea saponin contents, and the experimental data are shown in table 1:
TABLE 1 ratio, strength and density of alkali slag foam concrete under different tea saponin contents
(2) The content of the water-based calcium stearate is changed, the compressive strength and the density of the alkali slag foam concrete 28d are measured under different tea saponin mixing amounts, and the experimental data are shown in the table 2:
TABLE 2 ratio, strength and density of alkali slag foam concrete under different tea saponin contents
As can be seen from tables 1 and 2, the density of the alkali slag foamed concrete provided by the present invention is as low as 250kg/m3The concrete has the advantages of short condensation time and fast strength development, has good heat preservation and sound insulation performance, can effectively utilize slag which is an industrial byproduct, is a light, low-carbon and environment-friendly concrete material, and accords with the development trend of 'green and environment-friendly' building materials.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.
Claims (10)
1. The chemically foamed low-density alkali slag foam concrete is characterized by comprising the following components in percentage by mass:
slag: 56-58 percent;
water glass: 16 to 20 percent;
sodium hydroxide: 2 to 4 percent;
chemical foaming agent: 1 to 2 percent;
foam stabilizer: 0.057-0.082%;
water: 12 to 18 percent;
surfactant (b): 1.0-1.2 percent.
2. The chemically foamed low-density alkali slag foam concrete according to claim 1, wherein the alkali slag foam concrete consists of the following components in percentage by mass:
slag: 57-58%;
water glass: 18 to 20 percent;
sodium hydroxide: 3 to 4 percent;
chemical foaming agent: 1.3 to 1.5 percent;
foam stabilizer: 0.057-0.082%;
water: 12 to 15 percent;
surfactant (b): 1.1-1.2%.
3. The chemically foamed low-density alkali slag foam concrete according to claim 1, wherein the alkali slag foam concrete consists of the following components in percentage by mass:
slag: 57 percent;
water glass: 18 percent;
sodium hydroxide: 3 percent;
chemical foaming agent: 1.3 percent;
foam stabilizer: 0.057-0.082%;
water: 15 percent;
surfactant (b): 1.1 percent.
4. The chemically expanded low-density alkali slag foamed concrete as set forth in claim 1, wherein said water glass has a modulus of 3.08, a water content of 57.1%, Na2O content 9.1%, SiO2The content was 27.19%.
5. The chemically expanded low-density alkaline slag foamed concrete according to claim 1, wherein said chemical foaming agent is aluminum powder and is formulated into an aluminum powder-water-surfactant suspension in use.
6. The chemically foamed low density alkali slag foamed concrete according to claim 1 wherein the foam stabilizer is tea saponin.
7. The chemically expanded low-density alkaline slag foamed concrete according to claim 1, wherein said surfactant is aqueous calcium stearate in a mass fraction of 50%.
8. The chemically expanded low-density alkali slag foamed concrete according to claim 1, wherein said slag is ground water-quenched blast furnace slag.
9. A method of producing a chemically expanded low density alkali slag foamed concrete according to any one of claims 1 to 8, comprising the steps of:
s1: mixing and stirring aluminum powder, water and a surfactant to prepare an aluminum powder-water-surfactant suspension;
s2: adding the slag and the foam stabilizer into a stirring pot for mixing, and stirring for 2-3min at a low speed by using a cement mortar stirrer;
s3: adding a water glass-sodium hydroxide composite alkali activator into S2, and rapidly stirring for 1 min;
s4: and adding the aluminum powder-water-surfactant suspension prepared in the step S1 into the step S3, quickly stirring for 15S, pouring into a mold for molding, and performing standard curing to obtain the alkali slag foam concrete.
10. The preparation method of claim 9, wherein the water glass-sodium hydroxide composite alkali activator is prepared by: firstly, mixing sodium hydroxide and water according to the proportion of 1: 1, cooling to room temperature, adding the sodium hydroxide solution into a certain amount of water glass, adjusting the modulus of the water glass to be 1.2, and cooling to room temperature for later use.
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Cited By (1)
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CN113603386A (en) * | 2021-08-24 | 2021-11-05 | 重庆大学 | Low-density alkali slag cement foam concrete chemical foaming agent and preparation method thereof |
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Application publication date: 20210226 |