CN112352994A - Additive for improving mouthfeel of cut stems and preparation method and application thereof - Google Patents

Additive for improving mouthfeel of cut stems and preparation method and application thereof Download PDF

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Publication number
CN112352994A
CN112352994A CN202011455595.1A CN202011455595A CN112352994A CN 112352994 A CN112352994 A CN 112352994A CN 202011455595 A CN202011455595 A CN 202011455595A CN 112352994 A CN112352994 A CN 112352994A
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CN
China
Prior art keywords
additive
mouthfeel
improving
cut
stems
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011455595.1A
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Chinese (zh)
Inventor
孙九喆
王鹏飞
张晓兵
颜权平
马波波
赵森森
王宝林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Henan Industrial Co Ltd
Zhengzhou Tobacco Research Institute of CNTC
Original Assignee
China Tobacco Henan Industrial Co Ltd
Zhengzhou Tobacco Research Institute of CNTC
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Publication date
Application filed by China Tobacco Henan Industrial Co Ltd, Zhengzhou Tobacco Research Institute of CNTC filed Critical China Tobacco Henan Industrial Co Ltd
Priority to CN202011455595.1A priority Critical patent/CN112352994A/en
Publication of CN112352994A publication Critical patent/CN112352994A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Confectionery (AREA)

Abstract

The invention discloses an additive for improving the mouthfeel of cut stems, and a preparation method and application thereof, wherein the additive for improving the mouthfeel of the cut stems comprises citric acid, strong ammonia water, cocoa extracts, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin. The additive for improving the mouthfeel of the cut stems can improve the fragrance and the smoke taste, reduce the miscellaneous gas and the burning feeling and improve the aftertaste. Moreover, the additive for improving the mouthfeel of the cut stems has low raw material cost, and is beneficial to popularization and application.

Description

Additive for improving mouthfeel of cut stems and preparation method and application thereof
Technical Field
The invention relates to the field of cigarette manufacturing, in particular to an additive for improving the mouthfeel of cut stems and a preparation method and application thereof.
Background
The tobacco stem is the coarse and hard veins in the tobacco leaf, and the weight of the tobacco stem accounts for about 25 to 30 percent of the weight of the leaf. The tobacco stems contain a large amount of macromolecular substances such as cellulose, pectin, lignin, polysaccharide and the like, so that the cut stems obtained after the tobacco stems are cut into shreds have the defects of large stimulation, high concentration, obvious miscellaneous gas and the like.
However, the cut stems have the advantages of low content of tar and nicotine, good filling performance and the like, are one of main filling materials of the cigarette leaf formula, and play an important role in the cigarette formula. Under the condition that the design of cigarette products allows, the use amount of cut stems is properly increased, so that the method is one of important means for reducing tar and harm and is a good method for saving cost.
Therefore, how to provide an additive capable of effectively improving the mouthfeel of cut rolled stems becomes a technical problem to be solved urgently in the field.
Disclosure of Invention
An object of the present invention is to provide a new technical solution of an additive which can effectively improve the mouthfeel of cut rolled stems.
According to a first aspect of the present invention, there is provided an additive for improving the mouthfeel of cut rolled stems.
The additive for improving the mouthfeel of cut stems comprises citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin.
Optionally, the mass ratio of citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin is (20-40): 10-30): 0.5-1.5): 0.05-0.25): 0.05-0.15): 0.01-0.05.
Optionally, the citric acid is citric acid monohydrate.
Optionally, the mass fraction of the concentrated ammonia water is greater than 28%.
Optionally, the content of theobromine in the cocoa extract is 1-3% by mass.
Optionally, the nutmeg oil has a relative density of 30.883-0.917 and a refractive index of 1.475-1.488.
Optionally, the relative density of the cardamom oil is 0.919-0.940, the refractive index is 1.460-1.470, the optical rotation is +22 ° -44 °, the mass percentage of the cineole in the cardamom oil is 20% -35%, and the mass percentage of the terpinyl acetate is 30% -45%.
Optionally, the linalool in the coriander seed oil accounts for 60-72% by mass.
According to a second aspect of the present invention, there is provided a method of preparing the additive for improving mouthfeel of cut rolled stems of the present disclosure.
The preparation method of the additive for improving the mouthfeel of the cut rolled stems comprises the following steps:
step (1): mixing citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, fructus Amomi rotundus oil, coriander seed oil and vanillin uniformly to obtain mixture;
step (2): adding a diluent with the temperature of 30-45 ℃ into the mixture according to the mass ratio of 1 (3-9), and uniformly stirring to obtain the additive for improving the mouthfeel of the cut stems.
According to a third aspect of the invention, the application of the additive for improving the mouthfeel of the cut rolled stems disclosed in the invention is provided, wherein the mass ratio of the additive for improving the mouthfeel of the cut rolled stems to the cut rolled stems is (0.1-1): 50.
The additive for improving the mouthfeel of the cut stems can improve the fragrance and the smoke taste, reduce the miscellaneous gas and the burning feeling and improve the aftertaste. Moreover, the additive for improving the mouthfeel of the cut stems has low raw material cost, and is beneficial to popularization and application.
Detailed Description
Various exemplary embodiments of the present invention will now be described in detail. It should be noted that: the relative arrangement of the components and steps, the numerical expressions and numerical values set forth in these embodiments do not limit the scope of the present invention unless specifically stated otherwise.
The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses.
Techniques, methods, and apparatus known to those of ordinary skill in the relevant art may not be discussed in detail but are intended to be part of the specification where appropriate.
In all examples shown and discussed herein, any particular value should be construed as merely illustrative, and not limiting. Thus, other examples of the exemplary embodiments may have different values.
The present disclosure provides an additive for improving the mouthfeel of cut rolled stems, comprising citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil, and vanillin.
In one embodiment of the cut rolled stem mouthfeel improving additive of the present disclosure, the mass ratio of citric acid, concentrated ammonia water, cocoa extract, glycerin, nutmeg oil, cardamom oil, coriander seed oil, and vanillin is (20-40): 10-30): 0.5-1.5): 0.05-0.25): 0.05-0.15): 0.01-0.05.
In order to more effectively improve the mouthfeel of the cut rolled stems, the citric acid is citric acid monohydrate.
In order to effectively improve the mouthfeel of the cut stems, the mass fraction of the strong ammonia water is more than 28 percent.
In order to improve the mouthfeel of the cut stems more effectively, the content of theobromine in the cocoa extract is 1 to 3 percent by mass.
In order to improve the mouthfeel of cut rolled stems more effectively, the relative density of nutmeg oil is 30.883-0.917 (20/20 ℃ C. relative to water), and the refractive index is 1.475-1.488.
In order to effectively improve the mouthfeel of cut stems, the relative density of the cardamom oil is 0.919-0.940 (relative to water, 20/20 ℃), the refractive index is 1.460-1.470, the optical rotation is +22 DEG to +44 DEG, the mass percentage content of eucalyptol in the cardamom oil is 20-35%, and the mass percentage content of terpinyl acetate is 30-45%.
In order to effectively improve the mouthfeel of the cut stems, the linalool in the coriander seed oil accounts for 60-72% by mass.
Through carrying out thermal cracking experimental analysis on the additive for improving the cut stem mouthfeel, a detection result shows that a cracking final product mainly comprises acetic acid, alpha-pinene, beta-phellandrene, myristic acid, vanillin, trimethyl pyrazine, caffeine, linalool and capric acid. The cracking products are all components which can be coordinated with the natural essence of tobacco, and are beneficial to the aroma, taste and mouthfeel of cigarettes.
After the additive for improving the mouthfeel of the cut stems is added into the cut stems, the additive is beneficial to reducing aldehydes such as formaldehyde, acetaldehyde, acrolein, butanedial and the like in combustion cracking products of the cut stems, and the aldehydes can cause smoke to generate rough feeling and incongruous feeling, and belong to substances which are not beneficial to the taste of tobacco.
The present disclosure also provides a method for preparing an additive for improving the mouthfeel of cut rolled stems, comprising the steps of:
step (1): mixing citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, fructus Amomi rotundus oil, coriander seed oil and vanillin uniformly to obtain mixture.
Step (2): adding a diluent with the temperature of 30-45 ℃ into the mixture according to the mass ratio of 1 (3-9), and uniformly stirring to obtain the additive for improving the mouthfeel of the cut stems. The diluent may be water.
The disclosure also provides an application of the additive for improving the mouthfeel of the cut rolled stems, and particularly, the mass ratio of the additive for improving the mouthfeel of the cut rolled stems to the cut rolled stems is (0.1-1): 50.
In practical application, the additive for improving the mouthfeel of the cut stems can be uniformly applied to the cut stems in a spraying manner.
In order to ensure the effect of the additive for improving the mouthfeel of the cut rolled stems, the cut rolled stems to which the additive for improving the mouthfeel of the cut rolled stems is applied may be left in a leaf storage cabinet for 2 to 4 hours.
The experimental procedures used in the examples below are conventional unless otherwise specified, the materials and reagents used therein are commercially available, and the equipment used in the experiments are well known to those skilled in the art without otherwise specified.
Example 1
Weighing the raw materials of citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin according to the mass ratio of 25:35:20:20:1:0.2:0.1:0.05, and uniformly mixing to obtain the mixture. Adding water of 45 ℃ into the mixture according to the mass ratio of 1:5, and uniformly stirring to obtain the additive S1 for improving the mouthfeel of the cut rolled stems.
Weighing additive S1 for improving mouthfeel of the cut stems according to a proportion of 0.5% of the weight of the cut stems, and uniformly spraying the additive S1 on the cut stems through a feeding device. And (3) placing the cut stems sprayed with the additive S1 for improving the mouthfeel of the cut stems in a leaf storage cabinet for 3 hours to obtain the No. 1 modulated cut stems.
Example 2
Weighing the raw materials of citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin according to the mass ratio of 20:30:15:15:1:0.2:0.1:0.05, and uniformly mixing to obtain the mixture. Adding water of 45 ℃ into the mixture according to the mass ratio of 1:3, and uniformly stirring to obtain the additive S2 for improving the mouthfeel of the cut rolled stems.
Weighing additive S2 for improving mouthfeel of the cut stems according to a proportion of 0.5% of the weight of the cut stems, and uniformly spraying the additive S2 on the cut stems through a feeding device. And (3) placing the cut stems sprayed with the additive S2 for improving the mouthfeel of the cut stems in a leaf storage cabinet for 3 hours to obtain the 2# modulated cut stems.
Comparative example 1
Uniformly spraying water on the cut stems by a feeding device according to the proportion of 0.5 percent of the weight of the cut stems, and placing the cut stems in a leaf storage cabinet for 3 hours to obtain blank cut stems.
Preparing the No. 1 modulated cut stems, the No. 2 modulated cut stems and the blank cut stems into cut stem cigarette samples, and performing smoking evaluation on the cut stem cigarette samples, wherein the smoking evaluation results are shown in Table 1. As can be seen from table 1, the additive for improving the mouthfeel of cut rolled stems of the present disclosure can improve the aroma and the smoke flavor, reduce the offensive odor and the burning sensation, and improve the aftertaste.
TABLE 1 results of the test
Numbering Fragrance Smell of tobacco Miscellaneous qi Irritation property Aftertaste Burning sensation Feeling of dryness
Blank space 6 5 5 6 4 6 6
1# 7 6 4 6 6 4 6
2# 8 6 4 5 5 5 5
Although some specific embodiments of the present invention have been described in detail by way of examples, it should be understood by those skilled in the art that the above examples are for illustrative purposes only and are not intended to limit the scope of the present invention. It will be appreciated by those skilled in the art that modifications may be made to the above embodiments without departing from the scope and spirit of the invention. The scope of the invention is defined by the appended claims.

Claims (10)

1. An additive for improving the mouthfeel of cut rolled stems is characterized by comprising citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, cardamom oil, coriander seed oil and vanillin.
2. The additive for improving the mouthfeel of cut rolled stems according to claim 1, wherein the mass ratio of citric acid, concentrated ammonia water, cocoa extract, glycerin, nutmeg oil, cardamom oil, coriander seed oil and vanillin is (20-40): 10-30): 0.5-1.5): 0.05-0.25): 0.05-0.15): 0.01-0.05.
3. Additive for improving the mouthfeel of rolled stems according to claim 1, wherein the citric acid is citric acid monohydrate.
4. Additive for improving the mouthfeel of rolled stems according to claim 1, wherein the mass fraction of concentrated ammonia water is more than 28%.
5. The additive for improving the mouthfeel of cut rolled stems according to claim 1, wherein the content of theobromine in the cocoa extract is 1 to 3 percent by mass.
6. The additive for improving the mouthfeel of rolled cut stems according to claim 1, wherein the nutmeg oil has a relative density of 30.883-0.917 and a refractive index of 1.475-1.488.
7. The additive for improving the mouthfeel of cut rolled stems according to claim 1, wherein the relative density of the cardamom oil is 0.919-0.940, the refractive index is 1.460-1.470, the optical rotation is +22 ° - +44 °, the mass percentage of the cineole in the cardamom oil is 20% -35%, and the mass percentage of the terpinyl acetate is 30% -45%.
8. The additive for improving the cut rolled stem mouthfeel according to claim 1, wherein the linalool content in the coriander seed oil is 60-72% by mass.
9. A method for preparing an additive for improving the mouthfeel of cut rolled stems according to any one of claims 1 to 8, comprising the steps of:
step (1): mixing citric acid, strong ammonia water, cocoa extract, glycerol, nutmeg oil, fructus Amomi rotundus oil, coriander seed oil and vanillin uniformly to obtain mixture;
step (2): adding a diluent with the temperature of 30-45 ℃ into the mixture according to the mass ratio of 1 (3-9), and uniformly stirring to obtain the additive for improving the mouthfeel of the cut stems.
10. Use of the additive for improving the mouthfeel of rolled stems according to any one of claims 1 to 8, wherein the mass ratio of the additive for improving the mouthfeel of rolled stems to the rolled stems is (0.1-1): 50.
CN202011455595.1A 2020-12-10 2020-12-10 Additive for improving mouthfeel of cut stems and preparation method and application thereof Pending CN112352994A (en)

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CN202011455595.1A CN112352994A (en) 2020-12-10 2020-12-10 Additive for improving mouthfeel of cut stems and preparation method and application thereof

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5103843A (en) * 1988-10-31 1992-04-14 Naarden International N.V. Process for improving the taste and aroma of tobacco
CN102972859A (en) * 2012-12-27 2013-03-20 云南瑞升烟草技术(集团)有限公司 Method for preparing burley tobacco stems into stem particles or strip-shaped stem threads
CN104705779A (en) * 2015-01-28 2015-06-17 中国烟草总公司郑州烟草研究院 Processing method for improving cut stem quality
CN110934320A (en) * 2020-01-20 2020-03-31 中国烟草总公司郑州烟草研究院 Preparation and application of additive capable of reducing wood gas and irritation of cut stems
CN111184248A (en) * 2020-03-19 2020-05-22 中国烟草总公司郑州烟草研究院 Preparation and application of additive capable of improving sensory quality of cut stems

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5103843A (en) * 1988-10-31 1992-04-14 Naarden International N.V. Process for improving the taste and aroma of tobacco
CN102972859A (en) * 2012-12-27 2013-03-20 云南瑞升烟草技术(集团)有限公司 Method for preparing burley tobacco stems into stem particles or strip-shaped stem threads
CN104705779A (en) * 2015-01-28 2015-06-17 中国烟草总公司郑州烟草研究院 Processing method for improving cut stem quality
CN110934320A (en) * 2020-01-20 2020-03-31 中国烟草总公司郑州烟草研究院 Preparation and application of additive capable of reducing wood gas and irritation of cut stems
CN111184248A (en) * 2020-03-19 2020-05-22 中国烟草总公司郑州烟草研究院 Preparation and application of additive capable of improving sensory quality of cut stems

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
黄嘉礽 主编: "《烟草工业手册》", 30 April 1999, 中国轻工业出版社 *

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Application publication date: 20210212