CN112317724B - Method for fixing ceramic shell for directional solidification - Google Patents

Method for fixing ceramic shell for directional solidification Download PDF

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CN112317724B
CN112317724B CN202011220088.XA CN202011220088A CN112317724B CN 112317724 B CN112317724 B CN 112317724B CN 202011220088 A CN202011220088 A CN 202011220088A CN 112317724 B CN112317724 B CN 112317724B
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shell
chassis
mold
wax
directional solidification
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CN112317724A (en
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卢玉章
郑伟
申健
张功
王栋
谢光
王迪
王莉
张少华
董加胜
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Institute of Metal Research of CAS
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D27/00Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
    • B22D27/04Influencing the temperature of the metal, e.g. by heating or cooling the mould
    • B22D27/045Directionally solidified castings

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Abstract

本发明公开了一种定向凝固用陶瓷型壳的固定方法,属于陶瓷型壳制备技术领域。该方法首先在蜡模底盘边缘设置环形凹槽;并在蜡模底盘侧部设置凸起锁紧结构Ⅰ;利用该蜡模底盘模具制备型壳底部具有环形凸起、侧面具有4个凹陷锁紧结构;然后在激冷底盘上表面设置与环形凸起相配合的阻流槽,在激冷底盘的侧面设置4个梯形凸起锁紧结构Ⅱ;将型壳四周凹陷结构的开口对准激冷盘上的凸起锁紧结构Ⅱ,将型壳向下推进紧密贴近激冷盘表面后,沿着顺时针旋转型壳,直至型壳与激冷盘紧密配合。该方法能够提高型壳底部与激冷盘的接触紧密程度,杜绝从型壳底部与激冷盘之间缝隙处产生的跑钢现象。

Figure 202011220088

The invention discloses a fixing method of a ceramic mold shell for directional solidification, and belongs to the technical field of ceramic mold shell preparation. In the method, an annular groove is firstly arranged on the edge of the wax mold chassis; a convex locking structure I is arranged on the side of the wax mold chassis; the wax mold chassis mold is used to prepare an annular protrusion at the bottom of the shell and four depressions on the side for locking Then, set the choke groove matching the annular protrusion on the upper surface of the chilled chassis, and set up four trapezoidal protrusion locking structures II on the side of the chilled chassis; align the opening of the concave structure around the mold shell with the chilled pan The convex locking structure II on the top, after pushing the mold shell down and close to the surface of the chiller plate, rotate the mold shell clockwise until the mold shell and the chiller plate are tightly matched. The method can improve the tightness of the contact between the bottom of the mold shell and the chilling plate, and prevent the phenomenon of steel running from the gap between the bottom of the mold shell and the chilling plate.

Figure 202011220088

Description

Method for fixing ceramic shell for directional solidification
Technical Field
The invention relates to the technical field of ceramic shell preparation, in particular to a method for fixing a ceramic shell for directional solidification, which is suitable for preparing single crystal and directional casting ceramic shells.
Background
With the continuous increase of inlet temperature of aero-engines and gas turbines, higher temperature bearing capacity requirements are put forward on hot end parts of cast high-temperature alloys. Cast superalloys have undergone a progression from equiaxed to oriented, single crystal. The directional solidification technology is that a mould shell is placed on a chilling plate, the mould shell is heated to about 1500 ℃ in a heat preservation furnace, then molten high-temperature alloy is poured into the mould shell, and the pouring temperature is generally 1500-. After the molten high-temperature alloy is poured, the shell needs to be continuously heated in a heat-preserving furnace, after standing for a period of time (generally 10min), the shell is drawn at a certain speed (generally 3-10mm/min) to a water-cooling (HRS process) sleeve at the bottom of the heat-preserving furnace or a low-melting-point cooling medium (LMC process), so that the directional solidification of the casting is realized.
Unlike the shells of isometric crystal castings, the greatest feature of the oriented and single crystal shells is that, except for the area where the gates are open, the lower part of the shell, i.e. the bottom of the seed-taking section or spiral seed selector of the casting, must be open: when the shell is placed on the chilling plate and molten high-temperature alloy is poured into the shell, the high-temperature alloy can be in contact with the chilling plate at the opening at the lower part of the shell and is rapidly solidified, and a layer of chilling grains is generated. In addition, because the chilling plate has low temperature, longitudinal temperature gradient is generated for the high-temperature alloy, and the crystal grains of the chilling layer compete for growth, so that a directional columnar crystal structure is generated, or a single crystal structure is formed by passing through a spiral crystal selector.
Although the chilling plate has low temperature (the upper surface temperature is about 400-1600 ℃), the poured molten high-temperature alloy liquid (1500-1600 ℃) cannot be instantly solidified. When the bottom of the shell and the chilling disc cannot be in close contact with each other, molten high-temperature alloy liquid can completely flow out from a gap between the bottom of the shell and the chilling disc, and cannot fill the inner cavity of the shell, so that the steel leakage phenomenon is caused, castings are scrapped, serious economic loss is caused, and equipment is damaged. Therefore, a new shell fixing process is urgently needed to be explored, the close contact degree between the shell and the chilling chassis is enhanced, and the steel leakage phenomenon generated from a gap between the bottom of the shell and the chilling chassis is avoided.
Disclosure of Invention
The invention aims to provide a method for fixing a ceramic shell for directional solidification, which can improve the contact tightness between the bottom of the shell and a chilling disc and avoid the steel running phenomenon generated at a gap between the bottom of the shell and the chilling disc.
In order to achieve the purpose, the technical scheme adopted by the invention is as follows:
a method of fixing a ceramic shell for directional solidification, the method comprising the steps of:
(1) designing a wax mould chassis mould:
when a wax mold of a casting chassis is designed, an annular groove is arranged at a position (which cannot interfere with a crystallization section of a casting) which is 1-20mm away from the inner side of the edge of the wax mold chassis; a convex locking structure I is arranged on the side part of the wax mould chassis;
(2) preparing a shell:
carrying out directional or single crystal ceramic shell preparation by using the wax mould chassis mould designed in the step (1), wherein the bottom of the prepared ceramic shell is provided with an annular bulge (flow blocking structure), and the side surface of the prepared ceramic shell is provided with 4 concave locking structures;
(3) preparing a chilling chassis:
the outline dimension of the chilling chassis is phi 100-300mm, and the height is 10-200 mm; the upper surface of the chilling chassis is provided with a groove structure (a choke groove) matched with the annular bulge at the bottom of the shell, and when the shell is placed on the chilling chassis, the annular bulge on the shell is matched and clamped with the choke groove on the upper surface of the chilling chassis; 4 trapezoidal convex locking structures II are arranged on the side surface of the chilling chassis and at positions corresponding to the concave structures on the side surface of the ceramic shell chassis;
(4) assembling the shell and the chilling plate:
and (3) aligning the openings of the peripheral concave structures of the shell with the convex locking structures II on the chilling plate, pushing the shell downwards to be tightly close to the surface of the chilling plate, and then rotating the shell clockwise until the shell is tightly matched with the chilling plate.
In the step (1), the wax mold of the casting bottom plate is a cylindrical structure with the thickness of phi 100-; the radial longitudinal section of the annular groove along the wax pattern chassis is of a semicircular structure with the radius R being 1mm-5mm, and the annular groove takes a chassis wax pattern dot as the center. The design of the wax mould chassis can form a convex flow resisting structure on the casting shell.
In the step (1), the protrusion locking structures I are uniformly provided with 4 inverted L-shaped protrusions on the side surface of the wax mould chassis in the circumferential direction with the distance of more than or equal to 10mm from the surface with the annular groove; the dimensions of the inverted-L-shaped protrusion are as follows: the height h1 of one side is more than or equal to 10mm, the height h2 of the other side is 3mm to (h1-5) mm, the width w1 of the upper part is more than or equal to 10mm, the width w2 of the lower part is 5mm to (w1-3) mm, and the thickness t of the bulge is 5-10 mm. The convex locking structure on the side surface of the wax mould chassis can form a concave locking structure on the casting shell.
In the step (3), the size of the trapezoidal convex locking structure II is as follows: the shorter side length h4 is more than or equal to h2, the upper side length w3 is more than or equal to w2 and w3 is more than or equal to w1-w2, the longer side length h3 is more than or equal to h2, and the plane L1 is more than or equal to the plane L3. The design aims to enable the trapezoidal convex locking structure on the periphery of the chilling chassis to smoothly pass through w2 and achieve the purpose of tight fit with the locking mechanism of the shell after the shell is rotated clockwise.
And (4) assembling the shell and the chilling disc and performing directional solidification, rotating the shell along the anticlockwise direction after the directional solidification is finished, and then pulling the shell upwards until the shell is taken out, so that the shell can be cleaned.
The design principle and the beneficial effects of the invention are as follows:
in the invention, the flow resistance groove is additionally arranged on the upper surface of the chilling disc, and in the preparation process of the shell, the flow resistance protrusion additionally arranged on the bottom surface of the shell is matched with the flow resistance groove on the upper surface of the chilling disc; and locking mechanisms are additionally arranged on the periphery of the shell chassis and the chilling plate, so that the trapezoidal convex locking structures on the periphery of the chilling chassis can smoothly pass through the concave structures on the side surface of the shell during directional solidification, and after the shell is rotated clockwise, the locking mechanisms are tightly matched with the locking mechanisms of the shell to prevent steel from running.
Drawings
FIG. 1 shows the design of flow-resisting grooves on the bottom plate of a wax mold in the fixing method of the present invention.
FIG. 2 shows the dimension of the locking structure on the side of the wax pattern chassis in the fixing method of the present invention.
FIG. 3 is a graph of the locking mechanism dimensions around the chill plate in the present method of securing.
Detailed Description
For a further understanding of the present invention, the following description is given in conjunction with the examples which are set forth to illustrate, but are not to be construed to limit the present invention, features and advantages.
The invention provides a method for fixing a ceramic shell for directional solidification, which comprises the following steps:
1. designing a wax mould chassis mould:
(1.1) wax mould chassis flow-blocking groove: according to the size and the shape of the prepared casting crystallization section, a casting chassis wax mold (the commonly used size is phi 100 and 300mm) mold is designed: and a semicircular groove with the radius R of 1mm-5mm is arranged at a position 1-20mm away from the inner side of the edge of the wax mould chassis (the semicircular groove cannot interfere with a crystal growing section of a casting), and the groove is distributed in a circumferential manner by taking a chassis wax mould dot as a center. As shown in fig. 1. The design of the wax mould chassis can form a convex flow resisting structure on the casting shell. When the chassis wax pattern mould is designed, a light metal or nonmetal reinforcing plate can be added in the chassis wax pattern to prevent the wax pattern from deforming. The reinforcing plate can be automatically removed after dewaxing.
(1.2) a wax mould chassis side locking mechanism: the thickness of the wax mould chassis is 10-80mm, the circumferential direction with the distance between the surface of the groove and the circumferential surface of the wax mould chassis being more than or equal to 10mm is uniformly distributed with 4 inverted L-shaped bulges, and the size of the L-shaped bulges is shown in figure 2. Wherein h1 is more than or equal to 10mm, h2 is more than or equal to 3mm, w1 is more than or equal to 10mm, w2 is more than or equal to 5mm, and the protrusion thickness is 5-10 mm. The convex locking structure on the side surface of the wax mould chassis can form a concave locking structure on the casting shell.
2. Preparing a shell:
and (3) carrying out directional and single crystal wax tree combination according to the designed wax mould base plate, and carrying out slurry dipping and sanding processes. And determining the number of different shell preparation layers according to the shape and the size of the casting. The design of the shell fixing mode is suitable for the directional and single crystal shell preparation processes of different silica sol and molding sand.
3. Designing and processing a chilling chassis:
the external dimension of the chilling chassis is phi 100-300mm, the height is 10-200mm, and the chilling chassis can be matched with the size of the prepared shell.
(3.1) designing a corresponding concave structure on the upper surface of the chilling chassis at the position corresponding to the convex choke groove at the bottom of the shell, wherein when the shell is placed on the chilling chassis, the convex choke groove and the concave choke groove can be matched together.
And (3.2) designing 4 trapezoidal convex locking mechanisms at the corresponding positions of the concave locking structures on the side surface of the shell chassis on the side surface of the chilling plate. The size is shown in figure 3, wherein h4 is more than or equal to h2, w3 is more than or equal to w2, w3 is more than or equal to w1-w2, h3 is more than or equal to h2, and a plane L1 is/a plane L3. The design aims to enable the trapezoidal convex locking mechanism on the periphery of the chilling chassis to smoothly pass through w2 and achieve the purpose of tight fit with the locking mechanism of the shell after the shell is rotated clockwise.
4. Matching the shell with the chilling plate:
and aligning the openings of the concave locking mechanisms on the periphery of the shell with the convex locking mechanisms on the chilling plate, tightly pressing the shell downwards to the surface of the chilling plate, and then rotating the shell clockwise until the shell is tightly matched with the chilling plate.
5. Releasing the shell locking mechanism:
after the directional solidification is finished, the shell is rotated along the anticlockwise direction, then the shell is pulled upwards, and the shell can be cleaned until the shell is taken out.
Example 1:
the embodiment is a locking mechanism design applied to an LMC directional solidification process:
1. designing a wax mould chassis mould:
and (1.1) a wax mold chassis flow-blocking groove. The chassis wax pattern size of the shell is designed to be phi 180mm, a semicircular groove with the radius R being 3mm is arranged at a position 10mm away from the inner side of the edge of the shell chassis, and the groove is distributed in a circumferential manner by taking a chassis wax pattern dot as a center. When wax is pressed, a thin aluminum sheet reinforcing plate is added in the wax mould of the chassis to prevent the wax mould from deforming. The reinforcing plate comes out by itself after dewaxing.
And (1.2) a wax mould chassis side locking mechanism. The thickness of the wax mould base plate is 50mm, 4 inverted L-shaped bulges are uniformly distributed on the circumferential surface of the circumference of the cylindrical surface of the wax mould base plate, which is 20mm away from the surface with the groove, and the size of each L-shaped bulge is shown in figure 2. Wherein h 1-30 mm, h 2-5 mm, w 1-20mm, w 2-10 mm, and t-5 mm. The convex locking structure on the side surface of the wax mould chassis can form a concave locking structure on the casting shell.
2. Preparing a shell:
and (3) carrying out directional and single crystal wax tree combination according to the designed wax mould base plate, and carrying out slurry dipping and sanding processes. The number of shell preparation layers was 10.
3. Designing and processing a chilling chassis:
the material of the chilling plate is stainless steel, the overall dimension of the chilling chassis is phi 180mm, the height of the chilling chassis is 50mm, and the chilling chassis can be matched with the size of the prepared shell for use.
(3.1) a semicircular groove with the radius R of 3mm is designed and arranged on the upper surface of the chilling chassis at a position which is 10mm away from the edge of the chassis, and the groove is distributed in a circumferential shape by taking a wax pattern dot of the chassis as a center. When the shell is placed on the chilling plate, the convex and the concave flow resisting grooves can be matched together.
And (3.2) designing 4 trapezoidal convex locking mechanisms at the corresponding positions of the convex locking structures on the side surface of the wax mould chassis on the side surface of the chilling plate. The dimensions are shown in fig. 3, where h 4-6 mm, w 3-8 mm, h 3-10, and plane L1 is parallel to plane L3. The design can ensure that the trapezoidal convex locking mechanism on the periphery of the chilling chassis passes through w2 and is tightly matched with the locking mechanism of the shell after the shell is rotated clockwise.
4. Matching the shell with the chilling plate:
and aligning the openings of the concave locking mechanisms on the periphery of the shell with the convex locking mechanisms on the chilling plate, tightly pressing the shell downwards to the surface of the chilling plate, and then rotating the shell clockwise until the shell is tightly matched with the chilling plate.
5. Releasing the shell locking mechanism:
after the directional solidification is finished, the shell is rotated along the anticlockwise direction, then the shell is pulled upwards, and the shell can be cleaned until the shell is taken out.

Claims (5)

1.一种定向凝固用陶瓷型壳的固定方法,其特征在于:该方法包括如下步骤:1. a fixing method of a ceramic shell for directional solidification, is characterized in that: the method comprises the steps: (1)蜡模底盘模具的设计:(1) Design of wax mold chassis mold: 设计铸件底盘蜡模模具时,在距离蜡模底盘边缘内侧1-20mm的位置设置环形凹槽;并在蜡模底盘侧部设置凸起锁紧结构Ⅰ;When designing the wax mold mold of the casting chassis, set an annular groove at a position 1-20mm from the inner side of the edge of the wax mold chassis; and set a raised locking structure I on the side of the wax mold chassis; (2)型壳制备:(2) Shell preparation: 利用步骤(1)设计的蜡模底盘模具进行定向或单晶陶瓷型壳的制备,所制备陶瓷型壳的底部具有环形凸起的阻流结构、侧面具有4个凹陷锁紧结构;Use the wax mold chassis mold designed in step (1) to prepare the directional or single crystal ceramic shell, and the prepared ceramic shell has a ring-shaped convex blocking structure at the bottom and four concave locking structures on the side; (3)激冷底盘的制备:(3) Preparation of chilled chassis: 激冷底盘的外形尺寸为Φ100-300mm,高度为10-200mm;在激冷底盘的上表面,设置与型壳底部环形凸起相配合的凹槽结构作为阻流槽,当型壳放置于激冷盘之上时,型壳上的环形凸起与激冷底盘上表面上的阻流槽相配合卡接在一起;在激冷底盘的侧面、在与陶瓷型壳底盘侧面凹陷结构相对应位置设置4个梯形凸起锁紧结构Ⅱ;The external dimension of the chilled chassis is Φ100-300mm, and the height is 10-200mm; on the upper surface of the chilled chassis, a groove structure matched with the annular protrusion at the bottom of the shell is set as a choke groove. When it is above the cold plate, the annular protrusion on the mold shell is matched with the choke groove on the upper surface of the chilled chassis. 4 trapezoidal protrusion locking structures II; (4)型壳与激冷盘的装配:(4) Assembly of the shell and the chill plate: 将型壳四周凹陷结构的开口对准激冷盘上的凸起锁紧结构Ⅱ,将型壳向下推进紧密贴近激冷盘表面后,沿着顺时针旋转型壳,直至型壳与激冷盘紧密配合。Align the opening of the concave structure around the mold shell with the raised locking structure II on the chill plate, push the mold shell down and close to the surface of the chill plate, and then rotate the mold shell clockwise until the mold shell and the chill plate are tightly fitted . 2.根据权利要求1所述的定向凝固用陶瓷型壳的固定方法,其特征在于:步骤(1)中,铸件底盘蜡模为Φ100-300mm、厚度10-80mm的圆柱状结构;所述环形凹槽沿蜡模底盘径向的纵截面为半径R=1mm-5mm的半圆形结构,所述环形凹槽以底盘蜡模圆点为中心;蜡模底盘上这种设计可以在铸件型壳上形成凸出的阻流结构。2. The method for fixing a ceramic shell for directional solidification according to claim 1, characterized in that: in step (1), the casting chassis wax mold is a cylindrical structure with a thickness of Φ100-300mm and a thickness of 10-80mm; The longitudinal section of the groove along the radial direction of the wax mold chassis is a semicircular structure with a radius of R=1mm-5mm, and the annular groove is centered on the wax mold dot of the chassis; this design on the wax mold chassis can be used in the casting shell. A protruding blocking structure is formed on it. 3.根据权利要求1所述的定向凝固用陶瓷型壳的固定方法,其特征在于:步骤(1)中,所述凸起锁紧结构Ⅰ是在蜡模底盘的侧表面上,距离具有环形凹槽的表面≥10mm的周向,均匀设置4个倒L型凸起;倒L型凸起的尺寸为:一侧高度h1≥10mm,另一侧高度h2=3mm~(h1-5)mm,上部宽度w1≥10mm,下部宽度w2=5mm~(w1-3)mm,凸起厚度t=5-10mm;蜡模底盘侧面这种凸起的锁紧结构,可以在铸件型壳上形成凹陷的锁紧结构。3. The method for fixing a ceramic shell for directional solidification according to claim 1, wherein in step (1), the convex locking structure I is on the side surface of the wax mold chassis, and the distance has a ring-shaped distance. The surface of the groove is ≥10mm in the circumferential direction, and 4 inverted L-shaped protrusions are evenly arranged; the size of the inverted L-shaped protrusions is: the height of one side is h1≥10mm, and the height of the other side is h2=3mm~(h1-5)mm , the upper width w1≥10mm, the lower width w2=5mm~(w1-3)mm, the convex thickness t=5-10mm; the convex locking structure on the side of the wax mold chassis can form a depression on the casting shell locking structure. 4.根据权利要求3所述的定向凝固用陶瓷型壳的固定方法,其特征在于:步骤(3)中,所述梯形凸起锁紧结构Ⅱ的尺寸为:较短的一个侧边长度h4≥h2,上边的长度w3≤w2且w3≤w1-w2,较长的一个侧边长度h3≥h2,平面L1∥平面L3;所述平面L3是指梯形凸起锁紧结构的下底面,所述平面L1是指倒L型凸起的突出端的下表面。4. The method for fixing a ceramic shell for directional solidification according to claim 3, wherein in step (3), the size of the trapezoidal protrusion locking structure II is: a shorter side length h4 ≥h2, the length of the upper side w3≤w2 and w3≤w1-w2, the length of the longer side h3≥h2, the plane L1∥ plane L3; the plane L3 refers to the lower bottom surface of the trapezoidal convex locking structure, so The plane L1 refers to the lower surface of the protruding end of the inverted L-shaped protrusion. 5.根据权利要求1所述的定向凝固用陶瓷型壳的固定方法,其特征在于:经步骤(4)型壳与激冷盘装配并进行定向凝固,定向凝固结束后,沿着逆时针方向旋转型壳,然后向上提拉型壳,直至型壳取出后,方可清理。5. The method for fixing a ceramic shell for directional solidification according to claim 1, characterized in that: through step (4), the shell is assembled with the chill plate and directional solidification is carried out, and after the directional solidification is completed, rotate counterclockwise. The mold case, and then pull the mold case upwards, until the mold case is taken out, then it can be cleaned.
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CN106825410A (en) * 2017-01-16 2017-06-13 沈阳工业大学 Prepare the device and method of orientation magnesium alloy
CN111590056A (en) * 2020-05-22 2020-08-28 东方电气集团东方汽轮机有限公司 Casting structure and casting method for directional solidification of high-temperature alloy

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