CN112301506A - Preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric - Google Patents
Preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric Download PDFInfo
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- CN112301506A CN112301506A CN202011260228.6A CN202011260228A CN112301506A CN 112301506 A CN112301506 A CN 112301506A CN 202011260228 A CN202011260228 A CN 202011260228A CN 112301506 A CN112301506 A CN 112301506A
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- polyester
- moisture
- absorbing sweat
- proof
- polyester fabric
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/08—Melt spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/12—Stretch-spinning methods
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/22—Formation of filaments, threads, or the like with a crimped or curled structure; with a special structure to simulate wool
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/24—Formation of filaments, threads, or the like with a hollow structure; Spinnerette packs therefor
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01D—MECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
- D01D5/00—Formation of filaments, threads, or the like
- D01D5/253—Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
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- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2101/00—Inorganic fibres
- D10B2101/20—Metallic fibres
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
- D10B2331/04—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
-
- D—TEXTILES; PAPER
- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2401/00—Physical properties
- D10B2401/22—Physical properties protective against sunlight or UV radiation
Abstract
The invention discloses a preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric, which comprises the following steps: drying polyester powder and micro-nano calcium carbonate; then carrying out double-screw mixing, cooling and granulating to obtain master batches; uniformly mixing the moisture-absorbing polyester fiber master batch and the polyester chips, and spinning through a C-shaped hollow spinneret plate to obtain nascent fibers; then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber; the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric. According to the moisture-absorbing sweat-releasing radiation-proof polyester fabric, the polyester fibers are modified by the micro-nano calcium carbonate and are spun by the C-shaped hollow spinneret plate, so that the obtained polyester fibers are good in moisture-absorbing sweat-releasing effect; and the radiation-proof fabric is obtained by adopting a mode of coating the stainless steel wires with the polyester fibers and blending.
Description
Technical Field
The invention relates to the technical field of polyester fabric preparation, in particular to a preparation method of a moisture-absorbing sweat-releasing radiation-proof polyester fabric.
Background
The polyester fiber is the fiber with the fastest development, the highest yield and the largest consumption in various synthetic fibers, and is the first large variety of the current synthetic fibers. It has excellent performance and low cost, and has great use in national defense, industrial cloth, civil clothing, etc. Particularly in the field of fibers, polyester chips prepared by polycondensation are prepared into polyester fibers through melt spinning, and the fibers have the advantages of high breaking strength and elastic modulus, moderate rebound resilience, light resistance, heat resistance, corrosion resistance and the like, so that the rapid development is realized since the appearance of the polyester fibers.
The existing electromagnetic wave shielding fabrics comprise metal wire fabrics, metal wire and textile yarn interweaving or embedding fabrics, metal fiber or carbon fiber and conventional textile fiber blended yarn fabrics, and electroplating, chemical plating and vacuum plating metal film fabrics. The electromagnetic wave shielding fabrics have the advantages and the disadvantages, but basically have the disadvantages of poor moisture absorption and sweat releasing effects of the fabric, so the invention provides the preparation method of the moisture absorption and sweat releasing radiation protection polyester fabric.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of a moisture-absorbing sweat-releasing radiation-proof polyester fabric.
The technical scheme of the invention is as follows:
a preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric comprises the following steps:
A. grinding the PET slices, sieving the ground PET slices with a 80-mesh sieve, and taking undersize products to obtain polyester powder;
B. carrying out vacuum pre-crystallization drying treatment on polyester powder and micro-nano calcium carbonate;
C. mixing the dried polyester powder and the micro-nano calcium carbonate by a double screw, cooling and granulating to obtain moisture-absorbing polyester fiber master batches;
D. uniformly mixing 3-8% of moisture-absorbing polyester fiber master batch with polyester chips by weight ratio, melting by a screw extruder, statically mixing, filtering, metering by a box metering pump, extruding by a C-shaped hollow spinneret plate, and quenching by asymmetric ring blowing strong wind to obtain nascent fiber;
E. then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber;
F. the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric.
Preferably, in the step B, the particle size of the micro-nano calcium carbonate is 800-1500 nm.
Preferably, in the step B, the mass ratio of the polyester powder to the micro-nano calcium carbonate is (50-120): 1.
preferably, in the step B, the process conditions of the vacuum pre-crystallization drying treatment are as follows: the vacuum degree is less than 0.1-0.3MPa, the temperature is 85-95 ℃, the temperature is kept for 2-3h, and then the temperature is raised by 8-10 ℃ in turn every hour until 130-;
preferably, in the step D, the spinning temperature is 265-.
Preferably, in the step E, the draft ratio after the draft is 4 to 5 times.
Preferably, in the step F, the weight percentage of the stainless steel wires in the moisture-absorbing sweat-releasing radiation-proof polyester fabric is 15-30%.
The invention has the advantages that: the preparation method of the moisture-absorbing sweat-releasing radiation-proof polyester fabric comprises the following steps: grinding and sieving the PET slices to obtain polyester powder; carrying out vacuum pre-crystallization drying on polyester powder and micro-nano calcium carbonate; then carrying out double-screw mixing, cooling and granulating to obtain moisture-absorbing polyester fiber master batches; uniformly mixing the moisture-absorbing polyester fiber master batch and polyester chips, and spinning through a C-shaped hollow spinneret plate to obtain nascent fiber; then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber; the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric. According to the moisture-absorbing sweat-releasing radiation-proof polyester fabric, the polyester fibers are modified by adopting the micro-nano calcium carbonate and are spun by adopting the C-shaped hollow spinneret plate, so that the obtained three-dimensional spiral curled hollow polyester fibers are good in moisture-absorbing sweat-releasing effect; and the radiation-proof fabric is obtained by adopting a mode of coating the stainless steel wires with the polyester fibers and blending.
Detailed Description
Example 1
A preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric comprises the following steps:
A. grinding the PET slices, sieving the ground PET slices with a 80-mesh sieve, and taking undersize products to obtain polyester powder;
B. carrying out vacuum pre-crystallization drying treatment on polyester powder and micro-nano calcium carbonate;
C. mixing the dried polyester powder and the micro-nano calcium carbonate by a double screw, cooling and granulating to obtain moisture-absorbing polyester fiber master batches;
D. uniformly mixing 6% of moisture-absorbing polyester fiber master batch with polyester chips by weight ratio, melting by a screw extruder, statically mixing, filtering, metering by a box metering pump, extruding by a C-shaped hollow spinneret plate, and quenching by asymmetric circular blowing strong wind to obtain nascent fiber;
E. then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber;
F. the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric.
In the step B, the particle size of the micro-nano calcium carbonate is 800-1500 nm; the mass ratio of the polyester powder to the micro-nano calcium carbonate is 75: 1.
in the step B, the process conditions of the vacuum pre-crystallization drying treatment are as follows: keeping the temperature at 87 ℃ for 2.5h under the vacuum degree of less than 0.2MPa, and then sequentially increasing the temperature by 8.5 ℃ per hour until the temperature reaches 131 ℃;
in the step D, the spinning temperature is 270 ℃.
In the step E, the draft ratio after the draft is 4.5 times.
In the step F, the weight percentage of the stainless steel wires in the moisture absorption and sweat releasing radiation protection terylene fabric is 23%.
Example 2
A preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric comprises the following steps:
A. grinding the PET slices, sieving the ground PET slices with a 80-mesh sieve, and taking undersize products to obtain polyester powder;
B. carrying out vacuum pre-crystallization drying treatment on polyester powder and micro-nano calcium carbonate;
C. mixing the dried polyester powder and the micro-nano calcium carbonate by a double screw, cooling and granulating to obtain moisture-absorbing polyester fiber master batches;
D. uniformly mixing moisture-absorbing polyester fiber master batches and polyester slices according to the weight ratio of 3%, melting by a screw extruder, statically mixing, filtering, metering by a box metering pump, extruding by a C-shaped hollow spinneret plate, and quenching by asymmetric circular blowing strong wind to obtain nascent fiber;
E. then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber;
F. the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric.
In the step B, the particle size of the micro-nano calcium carbonate is 800-1500 nm; the mass ratio of the polyester powder to the micro-nano calcium carbonate is 120: 1.
in the step B, the process conditions of the vacuum pre-crystallization drying treatment are as follows: keeping the temperature at 95 ℃ for 2h under the vacuum degree of less than 0.1MPa, and then sequentially increasing the temperature by 10 ℃ per hour until the temperature reaches 130 ℃;
in the step D, the spinning temperature is 285 ℃.
In the step E, the draft ratio after the draft is 4 times.
In the step F, the weight percentage of the stainless steel wires in the moisture absorption and sweat releasing radiation protection terylene fabric is 30%.
Example 3
A preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric comprises the following steps:
A. grinding the PET slices, sieving the ground PET slices with a 80-mesh sieve, and taking undersize products to obtain polyester powder;
B. carrying out vacuum pre-crystallization drying treatment on polyester powder and micro-nano calcium carbonate;
C. mixing the dried polyester powder and the micro-nano calcium carbonate by a double screw, cooling and granulating to obtain moisture-absorbing polyester fiber master batches;
D. uniformly mixing 8% of moisture-absorbing polyester fiber master batch with polyester chips by weight ratio, melting by a screw extruder, statically mixing, filtering, metering by a box metering pump, extruding by a C-shaped hollow spinneret plate, and quenching by asymmetric circular blowing strong wind to obtain nascent fiber;
E. then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber;
F. the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric.
In the step B, the particle size of the micro-nano calcium carbonate is 800-1500 nm; the mass ratio of the polyester powder to the micro-nano calcium carbonate is 50: 1.
in the step B, the process conditions of the vacuum pre-crystallization drying treatment are as follows: keeping the temperature for 3h at the vacuum degree of less than 0.3MPa and the temperature of 85 ℃, and then sequentially increasing the temperature by 8 ℃ per hour until the temperature reaches 135 ℃;
in the step D, the spinning temperature is 265 ℃.
In the step E, the draft ratio after the draft is 5 times.
In the step F, the weight percentage of the stainless steel wires in the moisture absorption and sweat releasing radiation protection terylene fabric is 15%.
The following test results were obtained by testing the moisture absorption properties of the polyester fabrics spun from the polyester fibers prepared in examples 1 to 3 by the methods of JISL1907-2010, respectively, and the specific results are shown in table 1.
Table 1: examples 1 to 3 results of moisture absorption property measurement;
| example 1 | Example 2 | Example 3 | |
| Longitudinal wicking height (10 min) | 96 | 96 | 96 |
| Transverse wicking height (10 min) | 98 | 98 | 98 |
| Residual water content of 45 minutes% | 7.2 | 7.1 | 7.0 |
The test data show that the moisture absorption polyester fiber prepared by the invention has very good moisture absorption performance.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (7)
1. A preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric is characterized by comprising the following steps:
A. grinding the PET slices, sieving the ground PET slices with a 80-mesh sieve, and taking undersize products to obtain polyester powder;
B. carrying out vacuum pre-crystallization drying treatment on polyester powder and micro-nano calcium carbonate;
C. mixing the dried polyester powder and the micro-nano calcium carbonate by a double screw, cooling and granulating to obtain moisture-absorbing polyester fiber master batches;
D. uniformly mixing 3-8% of moisture-absorbing polyester fiber master batch with polyester chips by weight ratio, melting by a screw extruder, statically mixing, filtering, metering by a box metering pump, extruding by a C-shaped hollow spinneret plate, and quenching by asymmetric ring blowing strong wind to obtain nascent fiber;
E. then drawing, heat setting, washing, drying and winding the nascent fiber to obtain the moisture absorption polyester fiber;
F. the stainless steel wires are wrapped and wound on the moisture absorption polyester fibers to serve as warps, the weft stainless steel wires serve as wefts, and the warps and the wefts are interwoven to form the moisture absorption and sweat releasing radiation protection polyester fabric.
2. The method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric as claimed in claim 1, wherein in the step B, the particle size of the micro-nano calcium carbonate is 800-1500 nm.
3. The method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric according to claim 1, wherein in the step B, the mass ratio of the polyester powder to the micro-nano calcium carbonate is (50-120): 1.
4. the method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric according to claim 1, wherein in the step B, the process conditions of the vacuum pre-crystallization drying treatment are as follows: the vacuum degree is less than 0.1-0.3MPa, the temperature is 85-95 ℃, the temperature is kept for 2-3h, and then the temperature is raised by 8-10 ℃ in turn every hour until the temperature reaches 130-135 ℃.
5. The method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric as claimed in claim 1, wherein in the step D, the spinning temperature is 265-285 ℃.
6. The method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric according to claim 1, wherein in the step E, the drafting ratio after drafting is 4-5 times.
7. The method for preparing moisture-absorbing sweat-releasing radiation-proof polyester fabric according to claim 1, wherein in the step F, the weight percentage of the stainless steel wires in the moisture-absorbing sweat-releasing radiation-proof polyester fabric is 15-30%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011260228.6A CN112301506A (en) | 2020-11-12 | 2020-11-12 | Preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202011260228.6A CN112301506A (en) | 2020-11-12 | 2020-11-12 | Preparation method of moisture-absorbing sweat-releasing radiation-proof polyester fabric |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113930860A (en) * | 2021-09-22 | 2022-01-14 | 暖博士新材料（无锡）有限公司 | Shellfish nanofiber |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08291462A (en) * | 1995-04-20 | 1996-11-05 | Mitsubishi Rayon Co Ltd | Polyester hollow thick and thin yarn and its production |
| CN101275329A (en) * | 2008-04-30 | 2008-10-01 | 江苏新民纺织科技股份有限公司 | Radiation-proof fabric and production process thereof |
| CN102330191A (en) * | 2011-08-09 | 2012-01-25 | 上海贵达科技有限公司 | Hollow heat insulation fiber being warm in winter and cool in summer |
| CN102586908A (en) * | 2012-03-04 | 2012-07-18 | 江苏德赛化纤有限公司 | Multifunctional hollow polyester fiber production method |
| CN103320889A (en) * | 2013-06-27 | 2013-09-25 | 上海贵达科技有限公司 | Hydrophilic hygroscopic and sweat-releasing polyester fiber and preparation method thereof |
| CN106948030A (en) * | 2017-03-30 | 2017-07-14 | 厦门安踏体育用品有限公司 | A kind of high hydrophilic moisture absorption terylene and preparation method thereof |
| CN208324446U (en) * | 2018-05-08 | 2019-01-04 | 上海凰艮服饰科技有限公司 | A kind of radiation proof function fabric |
-
2020
- 2020-11-12 CN CN202011260228.6A patent/CN112301506A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08291462A (en) * | 1995-04-20 | 1996-11-05 | Mitsubishi Rayon Co Ltd | Polyester hollow thick and thin yarn and its production |
| CN101275329A (en) * | 2008-04-30 | 2008-10-01 | 江苏新民纺织科技股份有限公司 | Radiation-proof fabric and production process thereof |
| CN102330191A (en) * | 2011-08-09 | 2012-01-25 | 上海贵达科技有限公司 | Hollow heat insulation fiber being warm in winter and cool in summer |
| CN102586908A (en) * | 2012-03-04 | 2012-07-18 | 江苏德赛化纤有限公司 | Multifunctional hollow polyester fiber production method |
| CN103320889A (en) * | 2013-06-27 | 2013-09-25 | 上海贵达科技有限公司 | Hydrophilic hygroscopic and sweat-releasing polyester fiber and preparation method thereof |
| CN106948030A (en) * | 2017-03-30 | 2017-07-14 | 厦门安踏体育用品有限公司 | A kind of high hydrophilic moisture absorption terylene and preparation method thereof |
| CN208324446U (en) * | 2018-05-08 | 2019-01-04 | 上海凰艮服饰科技有限公司 | A kind of radiation proof function fabric |
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| Title |
|---|
| 刘吉平: "《纺织科学中的纳米技术》", 31 May 2003, 中国纺织出版社 * |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113930860A (en) * | 2021-09-22 | 2022-01-14 | 暖博士新材料（无锡）有限公司 | Shellfish nanofiber |
| CN113930860B (en) * | 2021-09-22 | 2023-09-01 | 暖博士新材料（无锡）有限公司 | shellfish nanofiber |
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Application publication date: 20210202 |