CN112267033B - Automatic temperature control device for titanium sponge production - Google Patents
Automatic temperature control device for titanium sponge production Download PDFInfo
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- CN112267033B CN112267033B CN202011224609.9A CN202011224609A CN112267033B CN 112267033 B CN112267033 B CN 112267033B CN 202011224609 A CN202011224609 A CN 202011224609A CN 112267033 B CN112267033 B CN 112267033B
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/02—Halides of titanium
- C01G23/022—Titanium tetrachloride
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- Manufacture And Refinement Of Metals (AREA)
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Abstract
The invention provides an automatic temperature control device for titanium sponge production, wherein a rack is meshed on the upper surface of a gear, the rack is slidably mounted inside a sleeve, a magnet is arranged inside the rack, a corresponding coil is arranged on the opposite surface of the magnet and inside the sleeve, a movable rod is movably mounted on the front surface of the inner end of the rack, a connecting rod is movably mounted at the top end of the movable rod, and wind shields are fixedly mounted on the opposite surfaces of the adjacent connecting rods. According to the invention, when the speed of mixed gas passing through the air inlet pipe is faster, the fan blades are driven to rotate, and current generated by cutting a magnetic induction line through the magnetic block and the metal bar is introduced into the coil, so that the magnetic field generated by the coil is ensured to push the magnet, the rack is pushed to move inwards at the same time, the movable rod is driven to swing, the top end of the movable rod drives the connecting rod to pull outwards, the connecting rod drives the wind shield to pull open, the air outlet is enlarged, the air flow in the exothermic reaction is increased, and the automatic temperature control effect of the interior is achieved.
Description
Technical Field
The invention belongs to the technical field of titanium sponge, and particularly relates to an automatic temperature control device for titanium sponge production.
Background
The titanium sponge is prepared by adding magnesium metal into a reduction reactor, continuously adding titanium tetrachloride to react with the magnesium metal to obtain spongy titanium metal and magnesium chloride, wherein the titanium tetrachloride in the slurry is required to be recovered in the production process of the titanium sponge at present, and the titanium tetrachloride in the chlorinated slurry is fully contacted with mixed gas from a dust collector to cool the titanium tetrachloride gas into liquid, so that the purpose of recovering the titanium tetrachloride is achieved.
In the recycling process, the proportion of the chloridized slurry cannot be automatically adjusted according to the flow velocity of the mixed gas, meanwhile, when the reaction rate is faster, the internal exothermic reaction is more violent, the internal automatic temperature control cannot be carried out, the absorption efficiency is influenced, meanwhile, solid particles are contained in the leaching process, the filter plate is blocked, and the internal heat exchange is influenced.
Disclosure of Invention
In order to solve the technical problems, the invention provides an automatic temperature control device for titanium sponge production, which is achieved by the following specific technical means:
the utility model provides an automatic temperature control device for titanium sponge production, includes condensation drip washing tower, the bottom fixed mounting of condensation drip washing tower has cold spiral bin outlet, and the top fixed mounting of condensation drip washing tower has the gas outlet, the inside slidable mounting of condensation drip washing tower has the filter plate, the inside movable mounting of filter plate has the stress pole, and is provided with the clamp plate above the filter plate, the outer end fixed mounting of clamp plate has the sill bar, and is provided with the shower pipe above the clamp plate, the left and right sides fixed connection of shower pipe has flexible bag, the bottom of flexible bag is provided with the push pedal, the lower surface swing joint of push pedal has the support, the bottom swing joint of support has the rotor plate, the terminal movable mounting of rotor plate is between adjacent sector plate, and the bottom rear surface movable mounting of rotor plate has the auxiliary rod, the auxiliary rod slidable mounting is in the inside of regulating plate, and the inside of auxiliary rod runs through there is the pendulum rod, the top fixed mounting of pendulum rod is on the surface of gear, the last surface toothing of gear has the rack, rack slidable mounting is in telescopic inside, and the inside of rack is provided with magnet, the opposite face of magnet and be provided with corresponding coil in telescopic inside, the inner front surface movable mounting of rack has the movable rod, the top movable mounting of movable rod has the connecting rod, and is adjacent the equal fixed mounting of opposite face of connecting rod has the deep bead, the right side fixed surface of condensation drip washing tower installs the intake pipe, the inside of intake pipe is rotated and is installed the flabellum, the surface of flabellum is provided with the metal rod, the outside of metal rod is provided with corresponding magnetic path.
Further, the magnetic field magnetic pole that the coil produced is the same with the magnetic pole of opposite face magnet, electric connection between coil and the metal rod, the magnetic path is the U-shaped structure, the outside fixedly connected with spring of rack gets into the intake pipe through the mist after, drives the flabellum rotatory, and when the flabellum drove the metal rod rotatory, the electric current that produces through magnetic path and metal rod cutting magnetic induction line lets in inside the coil to guarantee the magnetic field that the coil produced and promote magnet, promote the rack and move to the inboard simultaneously.
Further, the inside of regulating plate and the top of auxiliary rod are provided with corresponding arc hole and slider respectively, the junction at support and commentaries on classics board is connected to the bottom of auxiliary rod, and when the pendulum rod drove the auxiliary rod and moved in the inside of regulating plate to the outside, the junction downstream that the bottom of auxiliary rod drove support and commentaries on classics board to the range that the push pedal reciprocated has been changed.
Furthermore, the interior of the flexible bag is provided with chlorinated slurry, the wind shield and the air outlet are arranged in an up-down corresponding mode, and the movable rod is rotatably installed on the outer side of the condensation leaching tower.
Furthermore, the rear surface of the sector plate is fixedly arranged at the output end of the motor, and the joint of the bracket and the rotating plate is vertically and correspondingly arranged with the bottom rod.
Furthermore, the outer surface of the bottom rod is sleeved with a spring, the pressing plate is of an L-shaped structure, the stress rod is obliquely arranged on the basis of the inner wall of the condensation leaching tower, when the joint of the support and the rotating plate moves to the bottom end, the bottom rod is pressed when the fan-shaped plate belt rotates, the bottom rod drives the pressing plate to move downwards, so that the filtering plate at the bottom of the stress rod is subjected to intermittent shock, and the influence of solid particles on heat exchange caused by the internal blockage of the filtering plate is avoided.
Compared with the prior art, the invention has the following beneficial effects:
1. when the sponge titanium is produced, after mixed gas enters the gas inlet pipe, the fan-shaped plate is driven to rotate by the motor, the fan-shaped plate drives the rotating plate to rotate when rotating, the rotating plate drives the push plate at the top end of the support to move up and down, so that chlorinated slurry in the flexible bag is extruded, the chlorinated slurry is discharged through the leaching pipe and contacts with the mixed gas, then the titanium tetrachloride gas is cooled into liquid, the whole process is in an exothermic reaction, meanwhile, when the exothermic reaction is carried out, the bottom end of the auxiliary rod drives the connecting part of the support and the rotating plate to move to the bottommost end, the internal reaction is violent, after the fan-shaped plate rotates, the bottom rod is pressed, the bottom rod drives the pressing plate to move downwards, so that the intermittent shock is carried out on the filter plate at the bottom of the stress rod, and the influence of solid particles on heat exchange due to internal blockage of the filter plate is avoided.
2. According to the invention, when the speed of mixed gas passing through the gas inlet pipe is faster, the fan blades are driven to rotate, and current generated by cutting a magnetic induction line through the magnetic block and the metal bar is introduced into the coil, so that the magnetic field generated by the coil pushes the magnet to push the rack to move inwards at the same time, the rack is meshed with the gear to drive the swing rod to swing, and when the auxiliary rod is driven to move outwards by utilizing the corresponding arc hole and the sliding block between the adjusting plate and the auxiliary rod, the bottom end of the auxiliary rod drives the connecting part of the bracket and the rotating plate to move downwards, the vertical movement amplitude of the push plate is changed, and the purpose of automatically adjusting the specific gravity of the chlorinated slurry according to the flow rate of the mixed gas is realized.
3. According to the invention, when the flow rate of the mixed gas is faster, the reaction rate of the chlorinated slurry and the mixed gas is more violent, the temperature of the condensation leaching tower is excessively increased, the rack moves inwards and drives the movable rod to swing, the top end of the movable rod drives the connecting rod to pull outwards, and the connecting rod drives the wind shield to pull open, so that the air outlet is enlarged, the air flow in the exothermic reaction is increased, and the internal automatic temperature control effect is achieved.
Drawings
FIG. 1 is a schematic view of the internal structure of the present invention;
FIG. 2 is a schematic view of the internal structure of the condensing elution column of the present invention;
FIG. 3 is a schematic view showing the structure of the joint between the adjustment plate and the auxiliary rod according to the present invention;
FIG. 4 is an enlarged view of portion A of FIG. 3 according to the present invention;
fig. 5 is a schematic view of the internal structure of the intake pipe of the present invention.
In the figure: 1. a condensing and leaching tower; 2. a spiral discharge outlet; 3. an air outlet; 4. filtering the plate; 5. a stress beam; 6. pressing a plate; 7. a bottom bar; 8. a shower pipe; 9. a flexible bladder; 10. pushing the plate; 11. a support; 12. rotating the plate; 13. a sector plate; 14. an auxiliary lever; 15. an adjusting plate; 16. a swing rod; 17. a gear; 18. a rack; 19. a sleeve; 1901. a coil; 1902. a magnet; 20. a movable rod; 21. a connecting rod; 22. a wind deflector; 23. an air inlet pipe; 2301. a fan blade; 2302. a metal rod; 2303. a magnetic block.
Detailed Description
The invention is further described below with reference to the accompanying drawings:
the invention provides an automatic temperature control device for titanium sponge production, which is shown in the attached drawings 1 to 5: the device comprises a condensation leaching tower 1, wherein a cold spiral discharge port 2 is fixedly arranged at the bottom of the condensation leaching tower 1, a gas outlet 3 is fixedly arranged at the top of the condensation leaching tower 1, a filter plate 4 is slidably arranged in the condensation leaching tower 1, a stress rod 5 is movably arranged in the filter plate 4, a press plate 6 is arranged above the filter plate 4, a bottom rod 7 is fixedly arranged at the outer end of the press plate 6, a spring is sleeved on the outer surface of the bottom rod 7, the press plate 6 is of an L-shaped structure, the stress rod 5 is obliquely arranged by taking the inner wall of the condensation leaching tower 1 as a reference, a leaching pipe 8 is arranged above the press plate 6, flexible bags 9 are fixedly connected to the left side and the right side of the leaching pipe 8, chlorinated slurry is arranged in the flexible bags 9, a push plate 10 is arranged at the bottom of the flexible bags 9, a support 11 is movably connected to the lower surface of the push plate 10, a rotating plate 12 is movably connected to the bottom end of the support 11, and the rotating plate 12 is movably arranged between adjacent fan-shaped plates 13, the rear surface of the sector plate 13 is fixedly arranged at the output end of the motor, the joint of the support 11 and the rotating plate 12 and the bottom rod 7 are arranged up and down correspondingly, when the joint of the support 11 and the rotating plate 12 moves to the bottommost end, the sector plate 13 rotates to press the bottom rod 7, the bottom rod 7 drives the pressing plate 6 to move downwards, so that the filtering plate 4 at the bottom of the stressed rod 5 is subjected to intermittent jarring, the influence of solid particles on heat exchange due to blockage in the filtering plate 4 is avoided, the auxiliary rod 14 is movably arranged on the rear surface at the bottom end of the rotating plate 12, the auxiliary rod 14 is slidably arranged in the adjusting plate 15, corresponding arc holes and sliding blocks are respectively arranged in the adjusting plate 15 and at the top end of the auxiliary rod 14, when the oscillating rod 16 drives the auxiliary rod 14 to move outwards in the adjusting plate 15, the bottom end of the auxiliary rod 14 drives the joint of the support 11 and the rotating plate 12 to move downwards, so that the up and down movement amplitude of the pushing plate 10 is changed, the bottom end of the auxiliary rod 14 is connected to the joint of the bracket 11 and the rotating plate 12, the swing rod 16 penetrates through the auxiliary rod 14, the top end of the swing rod 16 is fixedly mounted on the surface of the gear 17, the upper surface of the gear 17 is meshed with the rack 18, the rack 18 is slidably mounted inside the sleeve 19, the magnet 1902 is arranged inside the rack 18, and the corresponding coil 1901 is arranged on the opposite surface of the magnet 1902 and inside the sleeve 19.
A movable rod 20 is movably installed on the front surface of the inner end of the rack 18, the movable rod 20 is rotatably installed on the outer side of the condensation leaching tower 1, a connecting rod 21 is movably installed at the top end of the movable rod 20, wind shields 22 are fixedly installed on opposite surfaces of adjacent connecting rods 21, the wind shields 22 and the air outlet 3 are arranged in an up-and-down corresponding mode, an air inlet pipe 23 is fixedly installed on the right side surface of the condensation leaching tower 1, a fan blade 2301 is rotatably installed inside the air inlet pipe 23, a metal bar 2302 is arranged on the surface of the fan blade 2301, corresponding magnetic blocks 2303 are arranged on the outer side of the metal bar 2302, magnetic poles of a magnetic field generated by the coil 1901 are the same as those of the magnet 1902 on the opposite surfaces, the coil 1901 is electrically connected with the metal bar 2302, the magnetic blocks 2303 are of a U-shaped structure, a spring is fixedly connected on the outer side of the rack 18, after mixed gas enters the air inlet pipe 23, the fan blade 2301 is driven to rotate, when the metal bar 2302 is driven by the fan blade 2301, current generated by cutting a magnetic induction line through the magnet 2303 and the metal bar 2302 is introduced into the coil 1901, thereby ensuring that the magnetic field generated by the coil 1901 pushes the magnet 1902, pushing the rack 18 while moving inwardly.
The specific use mode and function of the embodiment are as follows:
in the invention, when the sponge titanium is produced, after mixed gas enters the air inlet pipe 23, the fan-shaped plate 13 is driven to rotate by the motor, the fan-shaped plate 13 drives the rotating plate 12 to rotate when rotating, the rotating plate 12 drives the push plate 10 at the top end of the bracket 11 to move up and down, thereby the chloridized mud in the flexible bag 9 is extruded, titanium tetrachloride gas is cooled into liquid after being discharged through the showering pipe 8 and being contacted with the mixed gas, the whole process is in exothermic reaction, when the speed of the mixed gas passing through the air inlet pipe 23 is higher, the fan blade 2301 is driven to rotate, current generated by cutting a magnetic induction line by the magnet 2303 and the metal rod 2302 is led into the coil 1901, thereby ensuring that the magnetic field generated by the coil 1901 pushes the magnet 1902 to push the rack 18 to move inwards at the same time, after the rack 18 is meshed with the gear 17, the swing rod 16 is driven to swing, and when the auxiliary rod 14 is driven to move outwards by utilizing the corresponding arc hole and the slide block between the adjusting plate 15 and the auxiliary rod 14, the bottom end of the auxiliary rod 14 drives the connecting part of the bracket 11 and the rotating plate 12 to move downwards, the amplitude of the up-and-down movement of the push plate 10 is changed, the automatic adjustment of the specific gravity of the chloridized slurry according to the flow velocity of the mixed gas is realized, the reaction rate of the chloridized slurry and the mixed gas is accelerated, at the moment, the temperature of the condensation leaching tower 1 is raised too much, the rack 18 moves inwards, the movable rod 20 is driven to swing, the top end of the movable rod 20 drives the connecting rod 21 to pull outwards, the connecting rod 21 drives the wind shield 22 to pull open, the gas outlet 3 is enlarged, the air flow in the exothermic reaction is increased, the automatic temperature control effect of the interior is achieved, meanwhile, when the exothermic reaction is carried out, the bottom end of the auxiliary rod 14 drives the connecting part of the bracket 11 and the rotating plate 12 to move to the bottom end, the interior reaction is violent, the sector plate 13 rotates to press the bottom rod 7, the bottom rod 7 drives the pressing plate 6 to move downwards, therefore, the filter plate 4 at the bottom of the stress rod 5 is subjected to intermittent shock, and the influence of solid particles on heat exchange due to blockage in the filter plate 4 is avoided.
The technical solutions of the present invention or similar technical solutions designed by those skilled in the art based on the teachings of the technical solutions of the present invention are all within the scope of the present invention to achieve the above technical effects.
Claims (5)
1. The utility model provides an automatic temperature control device for titanium sponge production, includes condensation drip washing tower (1), its characterized in that: the device comprises a condensation leaching tower (1), a cold spiral discharge port (2) is fixedly arranged at the bottom of the condensation leaching tower (1), a gas outlet (3) is fixedly arranged at the top of the condensation leaching tower (1), a filter plate (4) is slidably arranged inside the condensation leaching tower (1), a stress rod (5) is movably arranged inside the filter plate (4), a pressing plate (6) is arranged above the filter plate (4), a bottom rod (7) is fixedly arranged at the outer end of the pressing plate (6), a leaching pipe (8) is arranged above the pressing plate (6), flexible bags (9) are fixedly connected to the left side and the right side of the leaching pipe (8), a push plate (10) is arranged at the bottom of each flexible bag (9), a support (11) is movably connected to the lower surface of the push plate (10), a rotating plate (12) is movably connected to the bottom end of the support (11), and the rotating plate (12) is movably arranged between adjacent fan-shaped plates (13), and the bottom rear surface movable mounting of commentaries on classics board (12) has auxiliary rod (14), auxiliary rod (14) slidable mounting has in the inside of regulating plate (15), and the inside of auxiliary rod (14) runs through has pendulum rod (16), the top fixed mounting of pendulum rod (16) is on the surface of gear (17), the last surface toothing of gear (17) has rack (18), rack (18) slidable mounting has in the inside of sleeve (19), and the inside of rack (18) is provided with magnet (1902), the opposite face of magnet (1902) just is provided with corresponding coil (1901) in the inside of sleeve (19), the inner front surface movable mounting of rack (18) has movable rod (20), the top movable mounting of movable rod (20) has connecting rod (21), the opposite face adjacent connecting rod (21) all fixed mounting have deep bead (22), the right side surface fixed mounting of condensation leaching tower (1) has intake pipe (23), a fan blade (2301) is rotatably mounted in the air inlet pipe (23), a metal rod (2302) is arranged on the surface of the fan blade (2301), and a corresponding magnetic block (2303) is arranged on the outer side of the metal rod (2302);
the coil (1901) is electrically connected with the metal rod (2302), the inner portion of the adjusting plate (15) and the top end of the auxiliary rod (14) are respectively provided with a corresponding arc hole and a corresponding sliding block, and the bottom end of the auxiliary rod (14) is connected to the connecting position of the support (11) and the rotating plate (12).
2. The automatic temperature control device for titanium sponge production as claimed in claim 1, wherein: the magnetic pole of the magnetic field generated by the coil (1901) is the same as that of the magnet (1902) opposite to the magnetic pole, the magnetic block (2303) is of a U-shaped structure, and the outer side of the rack (18) is fixedly connected with a spring.
3. The automatic temperature control device for titanium sponge production as claimed in claim 1, wherein: the interior of the flexible bag (9) is provided with chlorinated slurry, the wind shield (22) and the air outlet (3) are arranged up and down correspondingly, and the movable rod (20) is rotatably arranged on the outer side of the condensation leaching tower (1).
4. The automatic temperature control device for titanium sponge production as claimed in claim 1, wherein: the rear surface of the sector plate (13) is fixedly arranged at the output end of the motor, and the joint of the bracket (11) and the rotating plate (12) is vertically and correspondingly arranged with the bottom rod (7).
5. The automatic temperature control device for titanium sponge production as claimed in claim 1, wherein: the outer surface of the bottom rod (7) is sleeved with a spring, the pressing plate (6) is of an L-shaped structure, and the stress rod (5) is obliquely arranged on the basis of the inner wall of the condensation leaching tower (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011224609.9A CN112267033B (en) | 2020-11-05 | 2020-11-05 | Automatic temperature control device for titanium sponge production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011224609.9A CN112267033B (en) | 2020-11-05 | 2020-11-05 | Automatic temperature control device for titanium sponge production |
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| Publication Number | Publication Date |
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| CN112267033A CN112267033A (en) | 2021-01-26 |
| CN112267033B true CN112267033B (en) | 2022-04-29 |
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| CN202011224609.9A Active CN112267033B (en) | 2020-11-05 | 2020-11-05 | Automatic temperature control device for titanium sponge production |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN113774235B (en) * | 2021-08-25 | 2022-06-21 | 西安交通大学 | Method and device for intermittently and continuously extracting crystallized magnesium in Pidgeon magnesium smelting |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101464098A (en) * | 2007-12-17 | 2009-06-24 | 贵阳铝镁设计研究院 | Eluting column with folded plate |
| KR20110075770A (en) * | 2009-12-29 | 2011-07-06 | 주식회사 포스코 | Device for manufacturing sponge titanium |
| CN204211799U (en) * | 2014-10-31 | 2015-03-18 | 云南新立有色金属有限公司 | For pressure control device and the titanium sponge conversion unit of titanium sponge conversion unit |
| CN107475539A (en) * | 2017-08-18 | 2017-12-15 | 中南大学 | A kind of method that gaseous state electrochemistry prepares Titanium |
| CN209957879U (en) * | 2019-03-28 | 2020-01-17 | 朝阳金达钛业股份有限公司 | Be used for titanium sponge circulation production distillation process to go up reactor cooling system |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2014148687A1 (en) * | 2013-03-18 | 2014-09-25 | 한국생산기술연구원 | Refining device and refining method for titanium scraps and sponge titanium using deoxidising gas |
-
2020
- 2020-11-05 CN CN202011224609.9A patent/CN112267033B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101464098A (en) * | 2007-12-17 | 2009-06-24 | 贵阳铝镁设计研究院 | Eluting column with folded plate |
| KR20110075770A (en) * | 2009-12-29 | 2011-07-06 | 주식회사 포스코 | Device for manufacturing sponge titanium |
| CN204211799U (en) * | 2014-10-31 | 2015-03-18 | 云南新立有色金属有限公司 | For pressure control device and the titanium sponge conversion unit of titanium sponge conversion unit |
| CN107475539A (en) * | 2017-08-18 | 2017-12-15 | 中南大学 | A kind of method that gaseous state electrochemistry prepares Titanium |
| CN209957879U (en) * | 2019-03-28 | 2020-01-17 | 朝阳金达钛业股份有限公司 | Be used for titanium sponge circulation production distillation process to go up reactor cooling system |
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