CN112229763B - Method for detecting water absorption and water retention capacity of soybean dietary fiber - Google Patents
Method for detecting water absorption and water retention capacity of soybean dietary fiber Download PDFInfo
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- 235000010469 Glycine max Nutrition 0.000 title claims abstract description 81
- 244000068988 Glycine max Species 0.000 title claims abstract description 81
- 235000013325 dietary fiber Nutrition 0.000 title claims abstract description 80
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 66
- 238000010521 absorption reaction Methods 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 22
- 230000014759 maintenance of location Effects 0.000 claims abstract description 31
- 239000000843 powder Substances 0.000 claims abstract description 25
- 238000003756 stirring Methods 0.000 claims abstract description 19
- 239000000203 mixture Substances 0.000 claims abstract description 12
- 239000002002 slurry Substances 0.000 claims abstract description 12
- 239000012530 fluid Substances 0.000 claims abstract description 8
- 238000004364 calculation method Methods 0.000 claims abstract description 6
- 238000005303 weighing Methods 0.000 claims abstract description 6
- 238000012797 qualification Methods 0.000 claims description 6
- 238000003825 pressing Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 2
- 238000012216 screening Methods 0.000 claims description 2
- 238000001514 detection method Methods 0.000 abstract description 6
- 235000013305 food Nutrition 0.000 description 9
- 239000000835 fiber Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 4
- 235000013622 meat product Nutrition 0.000 description 4
- 238000012545 processing Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 241000227653 Lycopersicon Species 0.000 description 2
- 235000007688 Lycopersicon esculentum Nutrition 0.000 description 2
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- 235000015097 nutrients Nutrition 0.000 description 2
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- 230000001105 regulatory effect Effects 0.000 description 2
- 235000015067 sauces Nutrition 0.000 description 2
- WQZGKKKJIJFFOK-QTVWNMPRSA-N D-mannopyranose Chemical compound OC[C@H]1OC(O)[C@@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-QTVWNMPRSA-N 0.000 description 1
- 102000004877 Insulin Human genes 0.000 description 1
- 108090001061 Insulin Proteins 0.000 description 1
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- 238000004458 analytical method Methods 0.000 description 1
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- 229920002678 cellulose Polymers 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 102000038379 digestive enzymes Human genes 0.000 description 1
- 108091007734 digestive enzymes Proteins 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000007661 gastrointestinal function Effects 0.000 description 1
- 229940125396 insulin Drugs 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 235000015094 jam Nutrition 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000001814 pectin Substances 0.000 description 1
- 229920001277 pectin Polymers 0.000 description 1
- 235000010987 pectin Nutrition 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 235000013324 preserved food Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
- 238000010257 thawing Methods 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
- 229920001221 xylan Polymers 0.000 description 1
- 150000004823 xylans Chemical class 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N11/00—Investigating flow properties of materials, e.g. viscosity, plasticity; Analysing materials by determining flow properties
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Abstract
The invention discloses a method for detecting water absorption and retention capacity of soybean dietary fiber, which relates to the field of soybean dietary fiber detection methods, and comprises the steps of selecting uniformly-powdered soybean dietary fiber powder, accurately weighing the selected soybean dietary fiber powder, mixing the weighed soybean dietary fiber powder with water, adding the mixture into a stirring container, uniformly stirring the mixture in the stirring container to form slurry, correcting levelness of a Bostwick consistometer by using a leveling level screw and a level meter, pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer, measuring the flow rate of fluid in the instrument through precision scales on a bottom plate of the Bostwick consistometer, and calculating the water absorption and retention rate of the soybean dietary fiber according to a calculation formula V = 30/L. The method has the advantages of extremely simple process steps, easy operation, convenient implementation and strong practicability, can quickly, conveniently and accurately measure the water absorption and retention capacity of the soybean dietary fiber, and solves the problem of detecting the water absorption and retention capacity of the soybean dietary fiber in the current industry.
Description
Technical Field
The invention relates to the field of soybean dietary fiber detection methods, in particular to a method for detecting water absorption and water retention capacity of soybean dietary fiber.
Background
The soybean dietary fiber is a general term for macromolecular saccharides which cannot be digested by human digestive enzymes, and mainly comprises cellulose, pectin, xylan, mannose and the like. Dietary fiber, although not providing any nutrients to the human body, has important physiological functions to the human body. The dietary fiber has the functions of obviously reducing plasma cholesterol, regulating gastrointestinal function, regulating insulin level and the like. Dietary fiber is recognized as the seventh major nutrient in the medical and nutritional communities. The soybean dietary fiber has the characteristics of rich nutrition, unique flavor, safety and convenience in eating and the like, and is superior in the dietary fiber;
soybean dregs generated by processing soybeans contain abundant dietary fibers, the structure of the soybean fibers can be changed by alkaline hydrogen peroxide treatment, hydrophilic groups in the soybean fibers are exposed, so that the water absorption and swelling property of the soybean fibers are increased, and when the addition amount is low, the soybean fibers show good water retention when applied to emulsified minced meat products. When added to flour, can improve some of the rheological properties of the dough. The soybean dietary fiber absorbs water and expands in intestines and stomach to form high-viscosity gel or sol, so that people can feel full and can inhibit eating, the soybean dietary fiber has a good diet and weight-losing effect on obese people, and also has good water retention and expansibility, and when the soybean dietary fiber is added into food, the water content of the product can be increased, and the aging of the product can be delayed; the product has good emulsifying property, suspension property and thickening property, and can improve water retention and shape retention of food and improve freezing and thawing stability when added into food and beverage. The product can be widely applied to the fields of meat products, quick-frozen foods, seasoning foods, baked foods and the like and health-care products, and can also be used for preparing weight-losing foods, low-fat and low-sugar foods, high-fiber foods and the like;
in the processing application of meat products, jam and tomato sauce, the water absorption and retention capacity of the soybean dietary fiber plays a very key role in the final quality of the products, and the soybean dietary fiber product has good water absorption and retention capacity, so that the soybean dietary fiber product is suitable for being matched with protein isolate to process meat products, tomato sauce, canned foods and baked products;
at present, the method for judging the water absorption and water retention capacity of the soybean dietary fiber is mostly based on the practical application effect, and if the water absorption and water retention capacity of the soybean dietary fiber can be digitalized, the soybean dietary fiber can be better served for production enterprises. For the product control work of production enterprises and the production of application type terminal enterprises, the detection of the water absorption and retention capacity of the soybean dietary fiber needs to shorten the detection time and simplify the detection program, and methods with too long analysis time, complicated programs or inaccurate judgment results generally cause great troubles to the enterprises in practical application. Therefore, a detection method is needed, which can rapidly, conveniently and accurately determine the water absorption performance of the soybean dietary fiber, so as to judge whether the water absorption and retention capacity of the soybean dietary fiber meets the processing application of terminal products, and better serve enterprise production.
Disclosure of Invention
The invention aims to provide a detection method for the water absorption and retention capacity of soybean dietary fibers, which is used for quickly and accurately judging the water absorption and retention capacity of the soybean dietary fibers so as to judge whether the soybean dietary fibers can meet the application and processing requirements of terminal enterprises.
The invention achieves the above purpose through the following technical scheme:
a method for detecting water absorption and water retention capacity of soybean dietary fiber comprises the following steps:
firstly, selecting soybean dietary fiber powder, accurately weighing 5g +/-0.1 g of the selected soybean dietary fiber powder and 75g +/-0.1 g of water, mixing and adding into a stirring container;
step two, uniformly stirring the mixture in the stirring container to form slurry, wherein the stirring time is 60-80 seconds;
correcting levelness of the Bostwick consistometer by using a leveling level screw and a level meter, and then pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer;
step four, preparing an electronic stopwatch, pressing a lock catch on a spring door of the Bostwick consistency meter to enable the spring door to bounce instantly and start timing at the same time;
measuring the flow progress of the fluid in the instrument through a precision scale on a bottom plate of the Bostwick consistency meter, and recording and measuring the flow distance L (cm) in a specific time period (30 seconds);
and step six, calculating the water absorption and retention rate of the soybean dietary fiber according to a calculation formula V =30/L, comparing the water absorption and retention rate with qualified water absorption rate corresponding to the mesh number of the selected soybean dietary fiber powder, and judging whether the soybean dietary fiber is qualified or not, wherein V represents the water absorption and retention rate of the soybean dietary fiber.
Further, the soybean dietary fiber powder in the step one is screened by a sieve to realize uniform powder screening, and the water and the soybean dietary fiber powder are subjected to bearing by an electronic balance.
Further, in the second step, the stirring container is a 200ml plastic beaker, and the mixture is stirred by a handheld rapid stirrer.
Furthermore, in the sixth step, the qualification standard of the water absorption and retention rate of 80-mesh soybean dietary fiber powder is more than 3.60, the qualification standard of the water absorption and retention rate of 100-mesh soybean dietary fiber powder is more than 2.70, and the qualification standard of the water absorption and retention rate of 120-mesh soybean dietary fiber particles is more than 1.90.
In the invention, the lock catch on the spring door can make the spring door bounce instantly, and the instant opening door can prevent the sample from flowing too early.
The method for detecting the water absorption and retention capacity of the soybean dietary fiber provided by the invention has the beneficial effects that: the method has the advantages of extremely simple steps, easy operation, convenient implementation and strong practicability, can quickly, conveniently and accurately determine the water absorption and retention capacity of the soybean dietary fiber, and solves the problem of detecting the water absorption and retention capacity of the soybean dietary fiber in the current industry.
Detailed Description
The invention is further illustrated by the following examples and comparative examples:
example 1
A method for detecting water absorption and water retention capacity of soybean dietary fiber mainly aims at 80-mesh soybean dietary fiber powder, and comprises the following steps:
step one, weighing 5g of 80-mesh soybean dietary fiber powder and 75g of water, mixing and adding the mixture into a 200mL plastic beaker;
step two, uniformly stirring the mixture in a 200mL plastic beaker by using a handheld rapid stirrer to form slurry, wherein the stirring time is 75 seconds;
thirdly, correcting the levelness of the Bostwick consistometer by using a leveling level screw and a level meter, and then pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer;
step four, preparing an electronic stopwatch, pressing a lock catch on a spring door of the Bostwick consistency meter to enable the spring door to bounce instantly and start timing at the same time;
measuring the flow progress of the fluid in the instrument through a precision scale on a bottom plate of the Bostwick consistency meter, and recording and measuring the flow distance L (cm) within a specific time period (30 seconds) to be 7.8cm;
and step six, calculating the water absorption and retention rate of the soybean dietary fibers according to the calculation formula V =30/L to obtain 30/7.8=3.85.
In this example, the water absorption and retention rate of the 80 mesh fiber reached 3.60 or more, and the water absorption and retention rate of the target product was 3.85 at this time, and it was judged as being acceptable.
Example 2
A method for detecting water absorption and water retention capacity of soybean dietary fiber mainly aims at 100-mesh soybean dietary fiber powder, and comprises the following steps:
step one, weighing 5g of 100-mesh soybean dietary fiber powder and 75g of water, mixing and adding the mixture into a 200mL plastic beaker;
step two, uniformly stirring the mixture in a 200mL plastic beaker by using a handheld rapid stirrer to form slurry, wherein the stirring time is 75 seconds;
thirdly, correcting the levelness of the Bostwick consistometer by using a leveling level screw and a level meter, and then pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer;
step four, preparing an electronic stopwatch, pressing a lock catch on a spring door of the Bostwick consistency meter to enable the spring door to bounce instantly and start timing at the same time;
measuring the flow progress of the fluid in the instrument through the precision scales on the bottom plate of the Bostwick consistency meter, and recording and measuring the flow distance L (cm) within a specific time period (30 seconds) to be 10.6cm;
and step six, calculating the water absorption water holding rate of the soybean dietary fiber according to the calculation formula V =30/L to obtain 30/10.6=2.83.
In this example, the water absorption and retention rate of the 100 mesh fiber was 2.70 or more, and the water absorption and retention rate of the target product was 2.83 at this time, and it was judged as being acceptable.
Example 3
A method for detecting water absorption and water retention capacity of soybean dietary fiber mainly aims at 120-mesh soybean dietary fiber powder, and comprises the following steps:
step one, weighing 5g of 120-mesh soybean dietary fiber powder and 75g of water, mixing and adding the mixture into a 200mL plastic beaker;
step two, uniformly stirring the mixture in a 200mL plastic beaker by using a handheld rapid stirrer to form slurry, wherein the stirring time is 75 seconds;
correcting levelness of the Bostwick consistometer by using a leveling level screw and a level meter, and then pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer;
step four, preparing an electronic stopwatch, pressing a lock catch on a spring door of the Bostwick consistency meter to enable the spring door to bounce instantly and start timing at the same time;
measuring the flow progress of the fluid in the instrument through the precision scales on the bottom plate of the Bostwick consistency meter, and recording and measuring the flow distance L (cm) within a specific time period (30 seconds) to be 14.5cm;
and step six, calculating the water absorption water holding rate of the soybean dietary fiber according to the calculation formula V =30/L to obtain 30/14.5=2.10.
In this example, the water absorption capacity of the 100 mesh fiber reached 1.90 or more, and the water absorption capacity of the target product at this time was 2.10, which was judged to be acceptable.
In the three embodiments, the Bostwick consistometer is used for measuring the water absorbing and holding capacity of the soybean dietary fiber, the strength of the water absorbing and holding capacity of the soybean dietary fiber is reflected from the side according to the flow progress of the fluid in the instrument, and the shorter the flow progress of the fluid in the instrument is, the better the water absorbing and holding effect of the soybean dietary fiber is, and of course, the soybean dietary fiber can also be visually expressed in numerical value.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (4)
1. A method for detecting the water absorption and water retention capacity of soybean dietary fiber is characterized by comprising the following steps:
firstly, selecting soybean dietary fiber powder, accurately weighing 5g +/-0.1 g of the selected soybean dietary fiber powder and 75g +/-0.1 g of water, mixing and adding into a stirring container;
step two, uniformly stirring the mixture in the stirring container to form slurry, wherein the stirring time is 60-80 seconds;
correcting levelness of the Bostwick consistometer by using a leveling level screw and a level meter, and then pouring all the stirred slurry into a sample tank behind a spring door of the Bostwick consistometer;
step four, preparing an electronic stopwatch, pressing a lock catch on a spring door of the Bostwick consistency meter to enable the spring door to bounce instantly and start timing at the same time;
measuring the flow progress of the fluid in the instrument through the precision scales on the bottom plate of the Bostwick consistency meter, and recording and measuring the flow distance L (cm) in a specific time period (30 seconds);
and step six, calculating the water absorption and retention rate of the soybean dietary fiber according to a calculation formula V =30/L, comparing the water absorption and retention rate with qualified water absorption rate corresponding to the mesh number of the selected soybean dietary fiber powder, and judging whether the soybean dietary fiber is qualified or not, wherein V represents the water absorption and retention rate of the soybean dietary fiber.
2. The method for detecting the water absorbing and holding capacity of the soybean dietary fiber according to claim 1, wherein the method comprises the following steps: and (3) screening the uniform powder from the soybean dietary fiber powder in the step one through a sieve, and carrying out bearing on the water and the soybean dietary fiber powder through an electronic balance.
3. The method for detecting the water absorbing and holding capacity of the soybean dietary fiber according to claim 1, wherein the method comprises the following steps: in the second step, the stirring container is a 200ml plastic beaker, and the mixture is stirred by a handheld rapid stirrer.
4. The method for detecting the water absorbing and holding capacity of the soybean dietary fiber according to claim 1, wherein the method comprises the following steps: in the sixth step, the qualification standard of the water absorption and retention rate of 80-mesh soybean dietary fiber powder is more than 3.60, the qualification standard of the water absorption and retention rate of 100-mesh soybean dietary fiber powder is more than 2.70, and the qualification standard of the water absorption and retention rate of 120-mesh soybean dietary fiber particles is more than 1.90.
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4495798A (en) * | 1982-12-12 | 1985-01-29 | Chesebrough-Pond's Inc. | Method and apparatus for measuring consistency of non-Newtonian fluids |
| CN104602537A (en) * | 2012-08-31 | 2015-05-06 | 尤妮佳股份有限公司 | Pet food |
| CN107543905A (en) * | 2017-10-23 | 2018-01-05 | 临邑禹王植物蛋白有限公司 | A kind of soy protein gel sexuality official's decision method |
| CN108132201A (en) * | 2017-10-30 | 2018-06-08 | 甘肃达利食品有限公司 | A kind of detection method of potato full-powder water imbibition |
| CN108871998A (en) * | 2018-03-28 | 2018-11-23 | 湖北葛店人福药用辅料有限责任公司 | Powder water absorbing properties detection method and device |
-
2020
- 2020-08-23 CN CN202010853496.2A patent/CN112229763B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4495798A (en) * | 1982-12-12 | 1985-01-29 | Chesebrough-Pond's Inc. | Method and apparatus for measuring consistency of non-Newtonian fluids |
| CN104602537A (en) * | 2012-08-31 | 2015-05-06 | 尤妮佳股份有限公司 | Pet food |
| CN107543905A (en) * | 2017-10-23 | 2018-01-05 | 临邑禹王植物蛋白有限公司 | A kind of soy protein gel sexuality official's decision method |
| CN108132201A (en) * | 2017-10-30 | 2018-06-08 | 甘肃达利食品有限公司 | A kind of detection method of potato full-powder water imbibition |
| CN108871998A (en) * | 2018-03-28 | 2018-11-23 | 湖北葛店人福药用辅料有限责任公司 | Powder water absorbing properties detection method and device |
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Denomination of invention: A test method for water absorption and holding capacity of soybean dietary fiber Effective date of registration: 20230302 Granted publication date: 20221101 Pledgee: Qilu bank Limited by Share Ltd. Liaocheng Shenxian branch Pledgor: Shandong Jiahua Biotechnology Co.,Ltd. Registration number: Y2023980033858 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20221101 Pledgee: Qilu bank Limited by Share Ltd. Liaocheng Shenxian branch Pledgor: Shandong Jiahua Biotechnology Co.,Ltd. Registration number: Y2023980033858 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A testing method for the water absorption and holding capacity of soybean dietary fiber Granted publication date: 20221101 Pledgee: Industrial and Commercial Bank of China Limited Xinxian sub branch Pledgor: Shandong Jiahua Biotechnology Co.,Ltd. Registration number: Y2024980014705 |