CN112169575A - Device and method for measuring pH and density of slurry in absorption tower - Google Patents
Device and method for measuring pH and density of slurry in absorption tower Download PDFInfo
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- CN112169575A CN112169575A CN202011056489.6A CN202011056489A CN112169575A CN 112169575 A CN112169575 A CN 112169575A CN 202011056489 A CN202011056489 A CN 202011056489A CN 112169575 A CN112169575 A CN 112169575A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
- B01D53/80—Semi-solid phase processes, i.e. by using slurries
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/501—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound
- B01D53/502—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound characterised by a specific solution or suspension
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/501—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound
- B01D53/504—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound characterised by a specific device
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/96—Regeneration, reactivation or recycling of reactants
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01D—MEASURING NOT SPECIALLY ADAPTED FOR A SPECIFIC VARIABLE; ARRANGEMENTS FOR MEASURING TWO OR MORE VARIABLES NOT COVERED IN A SINGLE OTHER SUBCLASS; TARIFF METERING APPARATUS; MEASURING OR TESTING NOT OTHERWISE PROVIDED FOR
- G01D21/00—Measuring or testing not otherwise provided for
- G01D21/02—Measuring two or more variables by means not covered by a single other subclass
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/40—Alkaline earth metal or magnesium compounds
- B01D2251/404—Alkaline earth metal or magnesium compounds of calcium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/60—Inorganic bases or salts
- B01D2251/606—Carbonates
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Abstract
The invention discloses a device for measuring the PH and density of slurry in an absorption tower, which comprises a gravity flow pipe connected with the bottom of the absorption tower, a first storage tank connected with the gravity flow pipe, and a second storage tank connected with the first storage tank; a slurry switch valve, a PH detector and a density detector are sequentially arranged on the detection pipe; the bottom of the first storage tank is connected with the top of the second storage tank through a connecting pipe, and an electric switch valve is installed on the connecting pipe; a liquid outlet at the bottom of the second storage tank is connected with a liquid inlet at the top of the absorption tower through a return pipe; install pressure pipe and pressure release pipe at the top of second holding vessel, install the force (forcing) pump on the pressure pipe, install electronic relief pressure valve on the pressure release pipe, install level detection sensor on the well upper portion of second holding vessel, level detection sensor under the bottom installation of second holding vessel. The invention has no slurry pump, avoids the slurry pump from being washed by slurry, does not need frequent shutdown for replacing the slurry pump, ensures the working efficiency and ensures the normal operation.
Description
Technical Field
The invention relates to the technical field of environmental protection, in particular to a device and a method for measuring pH and density of slurry in an absorption tower.
Background
The electric power structure of China is mainly thermal power, and a thermal power plant is a sulfur dioxide emission amplifying household. In order to reduce the emission of a large amount of sulfur dioxide, most of domestic coal-fired units are provided with flue gas desulfurization systems at present, and a limestone-gypsum wet desulfurization process is taken as a main process, namely, a large amount of limestone is added into an absorption tower to absorb the sulfur dioxide, so that the aim of removing the sulfur dioxide is fulfilled.
The pH value and density of the slurry in the absorption tower are important monitoring indexes for the operation of the desulfurization system. If the pH value of the slurry is too low, the sulfur dioxide absorption effect is poor, and the desulfurization efficiency is low; if the pH value is too high, the utilization rate of limestone and the purity of gypsum are low, which is not beneficial to the desulfurization reaction. If the density of the slurry is too low, the content of limestone and gypsum in the slurry is low, the desulfurization efficiency is low, and the water content of the gypsum is high; if the slurry density is too high, the equipment abrasion and the system operation power consumption are large, and the problems of reduction of the desulfurization efficiency, high water content of gypsum and the like are caused. Present pH value and density's measurement is generally taken out the thick liquid from the absorption tower bottom through the thick liquid pump, then the pump returns to absorption tower top, installation PH measuring apparatu and density measuring apparatu on the pipeline, carry out PH measurement and density measurement through PH measuring apparatu and density measuring apparatu, when measuring through this kind of mode, the thick liquid erodees the thick liquid pump seriously, the life of thick liquid pump is very short, need frequent shut down to change the thick liquid pump, influence work efficiency, PH measurement and density measurement accuracy are lower simultaneously.
Disclosure of Invention
Aiming at the prior art, the invention aims to provide a device and a method for measuring the PH and the density of slurry in an absorption tower, and the invention has no slurry pump, avoids the slurry pump from being washed by the slurry, does not need to be frequently stopped and replaced, ensures the working efficiency and ensures the normal work; the arrangement of the inverted U-shaped pipe ensures that the pulp in the detection pipe is full, and the preparation of PH measurement and density measurement is ensured.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a device for measuring the PH and density of slurry in an absorption tower, which comprises a gravity flow pipe connected with the bottom of the absorption tower, a first storage tank connected with the gravity flow pipe, and a second storage tank connected with the first storage tank; the gravity flow pipe comprises a detection pipe and an inverted U-shaped pipe connected with the detection pipe, the upper end of the detection pipe is connected with a liquid outlet at the bottom of the absorption tower, the lower end of the detection pipe is connected with an inlet of the inverted U-shaped pipe, and an outlet at the lower end of the inverted U-shaped pipe is connected with a liquid inlet at the top of the first storage tank; a slurry switch valve, a PH detector and a density detector are sequentially arranged on the detection pipe; the bottom of the first storage tank is connected with the top of the second storage tank through a connecting pipe, and an electric switch valve is installed on the connecting pipe; a liquid outlet at the bottom of the second storage tank is connected with a liquid inlet at the top of the absorption tower through a return pipe; install pressure pipe and pressure release pipe at the top of second holding vessel, install the force (forcing) pump on the pressure pipe, install electronic relief pressure valve on the pressure release pipe, install level detection sensor on the well upper portion of second holding vessel, level detection sensor under the bottom installation of second holding vessel, installation manometer on the second holding vessel.
Preferably, the highest position of the inverted U-shaped pipe is higher than the installation position of the PH detector. The slurry filling at the positions of the PH detector and the density detector can be ensured, and the detection accuracy is ensured.
Preferably, the height difference between the first storage tank and the liquid outlet at the bottom of the absorption tower is 3-4 m. The slurry flows out from the bottom of the absorption tower in a self-flowing mode, flows through the PH detector and the density detector and then enters the first storage tank for storage.
Preferably, the connecting pipe is provided with a plurality of connecting pipes, and each connecting pipe is provided with an electric switch valve.
Preferably, the second storage tank is located lower than the first storage tank.
Preferably, the upper liquid level detection sensor, the lower liquid level detection sensor and the pressure gauge are connected with the input end of the controller, and the pressure pump, the electric pressure reducing valve and the electric switch valve are respectively connected with the output end circuit of the controller.
In a second aspect of the present invention, there is provided a method for measuring PH and density of slurry in an absorption tower by using the above-mentioned measuring apparatus, comprising the steps of: firstly, opening a slurry switch valve on a detection pipe and an electric switch valve on a connecting pipe, enabling slurry to enter a first storage tank through a self-flowing pipe and then to automatically flow to a second storage tank through the connecting pipe, closing the electric switch valve when the slurry reaches the position of an upper liquid level detection sensor, pressurizing the second storage tank by a pressurizing pump, and enabling the slurry in the second storage tank to flow back to an absorption tower under the action of pressure; when the slurry reaches below the lower liquid level detection sensor, the electric pressure reducing valve is opened to relieve pressure of the second storage tank, after pressure relief is completed, the electric switch valve is opened, and the slurry enters the second storage tank again from the first storage tank.
The invention has the beneficial effects that:
the slurry pump is not needed, so that the slurry pump is prevented from being washed by slurry, the slurry pump does not need to be frequently stopped and replaced, the working efficiency is ensured, and the normal operation is ensured; the arrangement of the inverted U-shaped pipe ensures that the pulp in the detection pipe is full, and the preparation of PH measurement and density measurement is ensured.
Drawings
FIG. 1 is a schematic structural diagram of the present invention.
In the figure: 1. absorption tower, 2, first holding vessel, 3, second holding vessel, 4, test tube, 5, fall U type pipe, 6, thick liquid ooff valve, 7, PH detector, 8, density detector, 9, connecting pipe, 10, electronic ooff valve, 11, force (forcing) pump, 12, electronic relief pressure valve, 13, go up liquid level detection sensor, 14, lower liquid level detection sensor, 15, manometer, 16, back flow.
Detailed Description
It should be noted that the following detailed description is exemplary and is intended to provide further explanation of the disclosure. Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this application belongs.
In order to make the technical solutions of the present application more clearly understood by those skilled in the art, the technical solutions of the present application will be described in detail below with reference to specific embodiments.
The test materials used in the examples of the present invention are all conventional in the art and commercially available.
As shown in fig. 1, the apparatus for measuring PH and density of slurry in an absorption tower according to the present invention comprises a gravity pipe connected to the bottom of an absorption tower 1, a first storage tank 2 connected to the gravity pipe, and a second storage tank 3 connected to the first storage tank 2.
The gravity flow pipe comprises a detection pipe 4 and an inverted U-shaped pipe 5 connected with the detection pipe 4, the upper end of the detection pipe 4 is connected with a liquid outlet at the bottom of the absorption tower 1, the lower end of the detection pipe 4 is connected with an inlet of the inverted U-shaped pipe 5, and a lower end outlet of the inverted U-shaped pipe 5 is connected with a liquid inlet at the top of the first storage tank 2. A slurry switch valve 6, a pH detector 7 and a density detector 8 are sequentially installed on the detection pipe 4.
In this embodiment, in order to ensure that the slurry at the positions of the PH detector 7 and the density detector 8 is full and the detection accuracy is ensured, the highest position of the inverted U-shaped pipe 5 is higher than the installation position of the PH detector 7. The slurry flows out from the bottom of the absorption tower 1 in a self-flowing mode, flows through a PH detector 7 and a density detector 8, and then enters a first storage tank 2 for storage. In this embodiment, the height difference between the first storage tank 2 and the liquid outlet at the bottom of the absorption tower 1 is 3-4 m.
The bottom of first holding vessel 2 is passed through connecting pipe 9 and is connected with 3 tops of second holding vessel, installs electronic ooff valve on connecting pipe 9, the position of second holding vessel 3 is less than first holding vessel 2, and the thick liquid gets into second holding vessel 3 by first holding vessel 2 through the mode of flowing certainly. The liquid outlet at the bottom of the second storage tank 3 is connected with the liquid inlet at the top of the absorption tower 1 through a return pipe 16. The connecting pipes 9 are multiple, and each connecting pipe 9 is provided with an electric switch valve 10.
Install pressure pipe and pressure release pipe at the top of second holding vessel 3, install force (forcing) pump 11 on the pressure pipe, install electronic relief pressure valve 12 on the pressure release pipe, install level detection sensor 13 on the well upper portion of second holding vessel 3, level detection sensor 14 under the bottom installation of second holding vessel 3, install manometer 15 on second holding vessel 3. The upper liquid level detection sensor 13, the lower liquid level detection sensor 14 and the pressure gauge 15 are connected with the input end of the controller, and the pressure pump 11, the electric pressure reducing valve 12 and the electric switch valve 10 are respectively connected with the output end circuit of the controller. The structural principles and circuit connection parts of the upper liquid level detection sensor 13, the lower liquid level detection sensor 14, the pressure gauge 15, the pressure pump 11, the electric pressure reducing valve 12, the electric switch valve 10 and the controller are known to those skilled in the art, and are also explicitly described in related patent documents, so detailed description of the connection relationship and structure of the circuit is omitted.
When the slurry reaches the position of the upper liquid level detection sensor 13, the upper liquid level detection sensor 13 transmits a signal to the controller, the controller controls the electric switch valve 10 to be closed and controls the pressure pump 11 to pressurize the second storage tank 3, the slurry in the second storage tank 3 flows back to the absorption tower 1 under the action of pressure, when the slurry reaches the position below the lower liquid level detection sensor 14, the lower liquid level detection sensor 14 transmits a signal to the controller, the controller controls the electric pressure reducing valve 12 to be decompressed and opens the electric switch valve 10, so that the slurry enters the second storage tank 3 again from the first storage tank 2, and the working process is circulated.
The method for measuring the PH and the density of the slurry in the absorption tower 1 by using the measuring device comprises the following steps: firstly, opening a slurry switch valve 6 on a detection pipe 4 and an electric switch valve 10 on a connecting pipe 9, enabling the slurry to enter a first storage tank 2 through a self-flowing pipe, then enabling the slurry to automatically flow to a second storage tank 3 through the connecting pipe 9, closing the electric switch valve 10 when the slurry reaches the position of an upper liquid level detection sensor 13, pressurizing the second storage tank 3 by a pressurizing pump 11, and enabling the slurry in the second storage tank 3 to flow back to an absorption tower 1 under the action of pressure; when the slurry reaches the position below the lower liquid level detection sensor 14, the electric pressure reducing valve 12 is opened to relieve the pressure of the second storage tank 3, after the pressure relief is completed, the electric switch valve 10 is opened, and the slurry enters the second storage tank 3 again from the first storage tank 2.
The above description is only a preferred embodiment of the present application and is not intended to limit the present application, and various modifications and changes may be made by those skilled in the art. Any modification, equivalent replacement, improvement and the like made within the spirit and principle of the present application shall be included in the protection scope of the present application.
Claims (7)
1. The device for measuring the PH and the density of the slurry in the absorption tower is characterized by comprising a self-flowing pipe connected with the bottom of the absorption tower, a first storage tank connected with the self-flowing pipe and a second storage tank connected with the first storage tank; the gravity flow pipe comprises a detection pipe and an inverted U-shaped pipe connected with the detection pipe, the upper end of the detection pipe is connected with a liquid outlet at the bottom of the absorption tower, the lower end of the detection pipe is connected with an inlet of the inverted U-shaped pipe, and an outlet at the lower end of the inverted U-shaped pipe is connected with a liquid inlet at the top of the first storage tank; a slurry switch valve, a PH detector and a density detector are sequentially arranged on the detection pipe; the bottom of the first storage tank is connected with the top of the second storage tank through a connecting pipe, and an electric switch valve is installed on the connecting pipe; a liquid outlet at the bottom of the second storage tank is connected with a liquid inlet at the top of the absorption tower through a return pipe; install pressure pipe and pressure release pipe at the top of second holding vessel, install the force (forcing) pump on the pressure pipe, install electronic relief pressure valve on the pressure release pipe, install level detection sensor on the well upper portion of second holding vessel, level detection sensor under the bottom installation of second holding vessel, installation manometer on the second holding vessel.
2. The apparatus for measuring pH and density of slurry in an absorption tower according to claim 1, wherein: the highest position of the inverted U-shaped pipe is higher than the installation position of the PH detector.
3. The apparatus for measuring pH and density of slurry in an absorption tower according to claim 1, wherein: the height difference between the first storage tank and the liquid outlet at the bottom of the absorption tower is 3-4 m.
4. The apparatus for measuring pH and density of slurry in an absorption tower according to claim 1, wherein: the connecting pipe is a plurality of, all installs electric switch valve on every connecting pipe.
5. The apparatus for measuring pH and density of slurry in an absorption tower according to claim 1, wherein: the second storage tank is positioned lower than the first storage tank.
6. The apparatus for measuring pH and density of slurry in an absorption tower according to claim 1, wherein: the upper liquid level detection sensor, the lower liquid level detection sensor and the pressure gauge are connected with the input end of the controller, and the pressure pump, the electric pressure reducing valve and the electric switch valve are respectively connected with the output end circuit of the controller.
7. The method for measuring pH and density of slurry in an absorption tower by using a measuring device as set forth in any one of claims 1 to 6, comprising the steps of: firstly, opening a slurry switch valve on a detection pipe and an electric switch valve on a connecting pipe, enabling slurry to enter a first storage tank through a self-flowing pipe and then to automatically flow to a second storage tank through the connecting pipe, closing the electric switch valve when the slurry reaches the position of an upper liquid level detection sensor, pressurizing the second storage tank by a pressurizing pump, and enabling the slurry in the second storage tank to flow back to an absorption tower under the action of pressure; when the slurry reaches below the lower liquid level detection sensor, the electric pressure reducing valve is opened to relieve pressure of the second storage tank, after pressure relief is completed, the electric switch valve is opened, and the slurry enters the second storage tank again from the first storage tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011056489.6A CN112169575A (en) | 2020-09-30 | 2020-09-30 | Device and method for measuring pH and density of slurry in absorption tower |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011056489.6A CN112169575A (en) | 2020-09-30 | 2020-09-30 | Device and method for measuring pH and density of slurry in absorption tower |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112169575A true CN112169575A (en) | 2021-01-05 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011056489.6A Pending CN112169575A (en) | 2020-09-30 | 2020-09-30 | Device and method for measuring pH and density of slurry in absorption tower |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN112169575A (en) |
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2020
- 2020-09-30 CN CN202011056489.6A patent/CN112169575A/en active Pending
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