CN112090358A - Production equipment and production method of composite nano calcium - Google Patents
Production equipment and production method of composite nano calcium Download PDFInfo
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- CN112090358A CN112090358A CN202010888328.7A CN202010888328A CN112090358A CN 112090358 A CN112090358 A CN 112090358A CN 202010888328 A CN202010888328 A CN 202010888328A CN 112090358 A CN112090358 A CN 112090358A
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- Prior art keywords
- calcium
- nano calcium
- motor
- composite nano
- agitator
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- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 title claims abstract description 47
- 239000011575 calcium Substances 0.000 title claims abstract description 47
- 229910052791 calcium Inorganic materials 0.000 title claims abstract description 47
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 34
- 239000002131 composite material Substances 0.000 title claims abstract description 23
- 238000003756 stirring Methods 0.000 claims abstract description 52
- 239000000463 material Substances 0.000 claims abstract description 33
- 238000002156 mixing Methods 0.000 claims abstract description 24
- 230000009471 action Effects 0.000 claims abstract description 10
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 40
- 239000000843 powder Substances 0.000 claims description 23
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 20
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 18
- 239000000292 calcium oxide Substances 0.000 claims description 18
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 18
- 239000005018 casein Substances 0.000 claims description 16
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims description 16
- 235000021240 caseins Nutrition 0.000 claims description 16
- 238000006243 chemical reaction Methods 0.000 claims description 13
- 239000002245 particle Substances 0.000 claims description 13
- 239000000725 suspension Substances 0.000 claims description 12
- 230000029087 digestion Effects 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 9
- 238000004945 emulsification Methods 0.000 claims description 9
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 claims description 8
- OPSXJNAGCGVGOG-DKWTVANSSA-L Calcium L-aspartate Chemical compound [Ca+2].[O-]C(=O)[C@@H](N)CC([O-])=O OPSXJNAGCGVGOG-DKWTVANSSA-L 0.000 claims description 8
- 229920001287 Chondroitin sulfate Polymers 0.000 claims description 8
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 8
- 239000005715 Fructose Substances 0.000 claims description 8
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims description 8
- 229930091371 Fructose Natural products 0.000 claims description 8
- 241000237502 Ostreidae Species 0.000 claims description 8
- 108010001441 Phosphopeptides Proteins 0.000 claims description 8
- 229940034055 calcium aspartate Drugs 0.000 claims description 8
- 229940059329 chondroitin sulfate Drugs 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 8
- 235000020636 oyster Nutrition 0.000 claims description 8
- 108090000765 processed proteins & peptides Proteins 0.000 claims description 8
- NRHMKIHPTBHXPF-TUJRSCDTSA-M sodium cholate Chemical compound [Na+].C([C@H]1C[C@H]2O)[C@H](O)CC[C@]1(C)[C@@H]1[C@@H]2[C@@H]2CC[C@H]([C@@H](CCC([O-])=O)C)[C@@]2(C)[C@@H](O)C1 NRHMKIHPTBHXPF-TUJRSCDTSA-M 0.000 claims description 8
- 239000000600 sorbitol Substances 0.000 claims description 8
- 238000003763 carbonization Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 3
- 239000000920 calcium hydroxide Substances 0.000 claims description 3
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 3
- 230000018044 dehydration Effects 0.000 claims description 3
- 238000006297 dehydration reaction Methods 0.000 claims description 3
- 230000001804 emulsifying effect Effects 0.000 claims description 3
- 239000008213 purified water Substances 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 238000005979 thermal decomposition reaction Methods 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 2
- 238000010008 shearing Methods 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 14
- 210000000988 bone and bone Anatomy 0.000 description 6
- 238000000034 method Methods 0.000 description 5
- 238000010521 absorption reaction Methods 0.000 description 4
- 238000012216 screening Methods 0.000 description 4
- 210000004369 blood Anatomy 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
- 206010006956 Calcium deficiency Diseases 0.000 description 2
- 229940069978 calcium supplement Drugs 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000011812 mixed powder Substances 0.000 description 2
- 210000005036 nerve Anatomy 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 206010005963 Bone formation increased Diseases 0.000 description 1
- 206010009944 Colon cancer Diseases 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 208000001132 Osteoporosis Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000023555 blood coagulation Effects 0.000 description 1
- 230000037180 bone health Effects 0.000 description 1
- 239000004566 building material Substances 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 208000029742 colonic neoplasm Diseases 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 230000002124 endocrine Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 230000005484 gravity Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000003387 muscular Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 210000002990 parathyroid gland Anatomy 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 230000035790 physiological processes and functions Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 208000007442 rickets Diseases 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/181—Preventing generation of dust or dirt; Sieves; Filters
- B01F35/187—Preventing generation of dust or dirt; Sieves; Filters using filters in mixers, e.g. during venting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
- B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/22—Mixing of ingredients for pharmaceutical or medical compositions
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses production equipment of composite nano calcium, which belongs to the technical field of composite nano calcium production and comprises an equipment main body, wherein one end of the equipment main body is provided with a stirring barrel, two sides of the stirring barrel are respectively provided with a support frame, the top of the stirring barrel is rotatably connected with a rotating assembly, the top of the rotating assembly is provided with a top cover, the top of one end of the stirring barrel is provided with a driving assembly, and one end of the stirring barrel is provided with a motor. According to the invention, the rotating shaft and the gear are driven to rotate under the action of electric power by the motor, and the gear ring is driven to rotate under the action of the clamping teeth, so that the gear ring is rotatably connected with the top cover and the stirring barrel under the mutual matching of the sliding block and the sliding groove, and the supporting plate and the filter screen are driven to rotate on the adjacent end surfaces of the top cover and the stirring barrel, so that the rotating scattering of materials on the top of the gear ring is realized, the uniform blanking of the materials is realized, the mixing effect of the materials is better, the full mixing is realized, and the utilization rate is improved to a certain extent.
Description
Technical Field
The invention relates to the technical field of composite nano calcium production, in particular to production equipment and a production method of composite nano calcium.
Background
Calcium is an inorganic element with the largest content in human bodies, is not only a building material necessary for the growth and development of human bones and keeping the bones firm, but also an essential element for maintaining and regulating the normal physiological functions of nerves, muscles, blood, cell membranes and various enzyme activities, has important effects on bone health, cardiovascular, nerves, endocrine, muscular systems and blood coagulation, is not only influenced by calcium deficiency to normal development of children and cause rickets, but also has effects on various diseases such as hyperosteogeny of middle-aged and old people, colon cancer, hypertension and the like, and has important therapeutic effects on diseases caused by calcium deficiency.
Calcium is a threshold nutrient, when the calcium intake is lower than a threshold value, the reserve volume of the calcium in the body is positively correlated with the intake volume, when the calcium intake is higher than the threshold value, the reserve volume of the calcium in the body is irrelevant to the intake volume, the apparent absorption rate and the reserve rate of the calcium can reflect the absorption and utilization state of the calcium by the body, when the calcium absorption is low, the low blood calcium stimulates parathyroid glands to secrete PTH (PTH) to increase, so that the bone absorption process is enhanced, the bone calcium is mobilized to maintain the blood calcium, and if the calcium is persistently deficient, the bone calcium is continuously lost to form osteoporosis and the content of the bone calcium is reduced.
There are diversified calcium supplement products among the prior art, and calcium supplement product generally need use stirring mixing arrangement to stir each composition at the in-process of production and mix, however at the in-process of using, stirring mixing arrangement's feed end generally makes each composition pile and drops in the inside of agitator, stir it using the (mixing) shaft, however this kind of method makes its effect of mixing poor, unable intensive mixing, the rate of utilization has been reduced to a certain extent, and current stirring mixing arrangement is when using, lack the screening structure to each composition in advance, thereby make the powder fine and smooth nature of mixing poor, the effect of later stage mixture has been reduced.
Disclosure of Invention
The invention aims to: in order to solve the problem that the stirring and mixing device is used, the feeding end of the stirring and mixing device generally enables each component to fall in a pile in the stirring barrel, the stirring shaft is used for stirring the components, however, the method is poor in mixing effect and incapable of fully mixing, the utilization rate is reduced to a certain extent, and the existing stirring and mixing device is lack of a screening structure for each component in advance when being used, so that the mixed powder is poor in fineness, and the later-stage mixing effect is reduced, and the production equipment and the production method of the composite nano calcium are provided.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a production facility of compound nanometer calcium, includes the equipment principal, the one end of equipment principal is provided with the agitator, the both sides of agitator all are provided with the support frame, the top of agitator is rotated and is connected with the runner assembly, the top of runner assembly is provided with the top cap, the top of agitator one end is provided with drive assembly, the motor is installed to the one end of agitator, the output of motor is provided with the (mixing) shaft that runs through to the inside one end of agitator, the outside of (mixing) shaft evenly is provided with multiunit stirring vane, the bottom of agitator is provided with the discharging pipe, the top of top cap evenly is provided with the multiunit inlet pipe.
Preferably, the rotating assembly includes the backup pad, the top and the bottom of backup pad all are provided with the spacing ring, the four corners department in the spacing ring outside all is provided with the slider, the top of backup pad is provided with the filter screen, the outside of backup pad is provided with the ring gear, and is two sets of the terminal surface that the backup pad was kept away from to the inside of spacing ring all leans out.
Preferably, the top of agitator inner wall and the bottom of top cap inner wall all are provided with slider assorted spout, and the spout all is the loop configuration, the spacing ring all through mutually supporting of slider and spout respectively with agitator and top cap sliding connection.
Preferably, drive assembly's bottom is provided with the mounting panel, the motor is installed at the top of mounting panel, the output of motor is provided with the axis of rotation, the outside cover of axis of rotation is equipped with the gear, the one end that the top cap is close to the motor is provided with the roof, the bottom of roof is provided with the bearing frame, the axis of rotation passes through the bearing frame and is connected with the roof rotation.
Preferably, the outside of ring gear evenly is provided with the multiunit and the gear assorted latch, the ring gear all passes through latch and gear intermeshing.
Preferably, two sets of the one end of support frame all is provided with first fixed block and second fixed block respectively, and two sets of the support frame is all through first fixed block and top cap fixed connection, and is two sets of the support frame is all through second fixed block and 3 fixed connection of agitator.
Preferably, the specific production method comprises the following steps:
preparing the following raw materials, namely 10-20 parts of nano calcium carbonate powder, 15-25 parts of pearl powder, 20-35 parts of oyster powder, 30-50 parts of calcium aspartate, 15-20 parts of casein calcium peptide, 5-10 parts of sodium cholate, 5-10 parts of casein phosphopeptide, 10-15 parts of chondroitin sulfate, 3-5 parts of sorbitol and 5-10 parts of fructose;
secondly, deep processing is carried out on the nano calcium carbonate, thermal decomposition treatment is carried out on the calcium carbonate powder with the purity of more than 98 percent by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes, and digestion reaction, emulsification reaction and drying treatment are sequentially carried out to obtain the nano calcium carbonate with the average particle size of 1-10 nanometers;
opening a valve on a feeding pipe, then sequentially guiding nano calcium carbonate, pearl powder, oyster powder, calcium aspartate, casein calcium peptide, sodium cholate, casein phosphopeptide, chondroitin sulfate, sorbitol and fructose into the inner side of the top cover through the feeding pipe 11, enabling the nano calcium carbonate, the pearl powder, the oyster powder, the calcium aspartate, the casein calcium peptide, the sodium cholate, the casein phosphopeptide, the chondroitin sulfate, the sorbitol and the fructose to fall into the limiting ring and drop onto the top of the filter screen;
step four, a power supply is switched on, the motor and the motor operate under the action of electric power, the output end of the motor is rotated, the output end of the motor drives the rotating shaft and drives a gear outside the rotating shaft to rotate, then the gear ring is driven to rotate under the coordination of the clamping teeth, so that the gear ring is rotatably connected with the top cover and the stirring barrel under the mutual coordination of the sliding block and the sliding groove, the supporting plate and the filter screen are driven to rotate on the adjacent end surfaces of the top cover and the stirring barrel, the rotating scattering of materials on the top of the gear ring is realized, the uniform blanking of the materials is realized, then the output end of the motor drives the stirring shaft and the stirring blades to rotate, the materials in the stirring barrel are stirred until the materials are uniformly stirred, and the composite nano calcium is obtained;
and step five, opening a valve on the discharge pipe for leading out the composite nano calcium.
Preferably, according to the second step, in the digestion reaction, the particulate calcium oxide is sent into a groove type continuous digester, meanwhile, purified water with the weight being five times that of the particulate calcium oxide is added, and the mixture is stirred for 10 minutes to 5 minutes by a stirring device in the digester, so that the digestion reaction is finished, and meanwhile, calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet, and calcium oxide suspension is obtained.
Preferably, according to the second step, in the emulsification reaction, the generated calcium oxide suspension is put into a high-shear emulsifying machine, and is subjected to shear emulsification for 20 to 30 minutes, so that the calcium oxide suspension is fully refined and uniform; and then dehydrating, drying and surface treating are carried out, and H202 in the second stage carbonization liquid is discharged along with the second stage carbonization liquid during dehydration and drying, so that the nano calcium carbonate with the average grain diameter of 1-10 nanometers is obtained.
Preferably, according to the fourth step, the material is spirally discharged in an annular radial manner by taking the middle position of the filter screen as a base point.
Compared with the prior art, the invention has the beneficial effects that:
1. according to the invention, through the arrangement of the supporting plate, the filter screen, the gear ring, the latch, the motor, the gear and the rotating shaft, the motor drives the rotating shaft and the gear to rotate under the action of electric power, and drives the gear ring to rotate under the action of the latch, so that the gear ring is rotatably connected with the top cover and the stirring barrel under the mutual matching of the slide block and the chute, and drives the supporting plate and the filter screen to rotate on the adjacent end surfaces of the top cover and the stirring barrel, thereby realizing the rotary material scattering of materials on the top of the gear ring, realizing the uniform material blanking of the materials, further realizing the better mixing effect of the materials, realizing the sufficient mixing and improving the utilization rate to a certain extent;
2. according to the invention, through the arranged filter screen, the support plate is rotated under the action of the motor, the rotating shaft, the gear and the toothed ring, so that materials are discharged spirally in an annular radial manner by taking the middle position of the filter screen as a base point, and meanwhile, as a plurality of groups of filter holes are formed in the filter screen, the filter screen plays a role in vibrating and screening the materials when rotating, so that the materials are filtered, more fine and smooth materials fall down, the screening of the materials with various components is realized, the mixed powder has better fineness, and the later mixing effect is improved.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a partial schematic view of the present invention;
FIG. 3 is a schematic view of the rotating assembly of the present invention;
FIG. 4 is a front view of the rotating assembly of the present invention;
fig. 5 is an enlarged view of the present invention a.
In the figure: 1. an apparatus main body; 2. a support frame; 3. a stirring barrel; 4. a rotating assembly; 401. a support plate; 402. a limiting ring; 403. a filter screen; 404. a slider; 405. a chute; 406. a toothed ring; 5. a top cover; 6. a drive assembly; 601. a motor; 602. a rotating shaft; 603. a gear; 604. mounting a plate; 605. A top plate; 606. clamping teeth; 7. a motor; 8. a stirring shaft; 9. a stirring blade; 10. a discharge pipe; 11. A feed pipe; 12. a first fixed block; 13. and a second fixed block.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "center", "upper", "lower", "left", "right", "vertical", "horizontal", "inner", "outer", etc., indicate orientations or positional relationships based on the orientations or positional relationships shown in the drawings, and are only for convenience of description and simplicity of description, but do not indicate or imply that the device or element being referred to must have a particular orientation, be constructed and operated in a particular orientation, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance. In the description of the present invention, it should be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "connected," and "disposed" are to be construed broadly, e.g., as meaning either a fixed connection, a removable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art. The following describes an embodiment of the present invention based on its overall structure.
The electric machine (model number 90YYJJ) and the motor (model number Y90S-6-1.1) mentioned in the present invention can be obtained in the market or by private order.
Referring to fig. 1-5, a production device of composite nano calcium comprises a device main body 1, one end of the device main body 1 is provided with an agitator 3, both sides of the agitator 3 are provided with support frames 2, the top of the agitator 3 is rotatably connected with a rotating assembly 4, the top of the rotating assembly 4 is provided with a top cover 5, the top of one end of the agitator 3 is provided with a driving assembly 6, one end of the agitator 3 is provided with a motor 7, the output end of the motor 7 is provided with a stirring shaft 8 penetrating through one end inside the agitator 3, the outer side of the stirring shaft 8 is uniformly provided with a plurality of groups of stirring blades 9, the bottom of the agitator 3 is provided with a discharge pipe 10, and the top of the top cover 5 is uniformly provided.
According to the invention, through the arrangement of the supporting plate 401, the filter screen 403, the gear ring 406, the latch 606, the motor 601, the gear 603 and the rotating shaft 602, the motor 601 drives the rotating shaft 602 and the gear 603 to rotate under the action of electric power, and drives the gear ring 406 to rotate under the action of the latch 606, so that the gear ring 406 is rotatably connected with the top cover 5 and the stirring barrel 3 under the mutual matching of the sliding block 404 and the sliding groove 405, and the supporting plate 401 and the filter screen 403 are driven to rotate on the adjacent end faces of the top cover 5 and the stirring barrel 3, so that the rotary scattering of materials on the top of the gear ring is realized, the uniform blanking of the materials is realized, the mixing effect of the materials is better, the sufficient mixing is realized, and the utilization rate is improved to a certain extent.
Please refer to fig. 1, 2, 3, 4 and 5, the rotating assembly 4 includes a supporting plate 401, the top and the bottom of the supporting plate 401 are provided with limiting rings 402, four corners of the outer side of the limiting rings 402 are provided with sliding blocks 404, the top of the supporting plate 401 is provided with a filtering net 403, the outer side of the supporting plate 401 is provided with a toothed ring 406, the end surfaces of the two sets of limiting rings 402 far away from the supporting plate 401 are inclined outwards, and the end surfaces of the supporting plate 401 are inclined outwards, so that the top end section of the inner side of the limiting rings 402 is in a slope shape, the falling effect of the material is better, and the material is prevented from being accumulated at the contact position of the limiting rings 402.
Please refer to fig. 1, 2, 3 and 5, the top end of the inner wall of the stirring barrel 3 and the bottom end of the inner wall of the top cover 5 are both provided with a sliding groove 405 matched with the sliding block 404, and the sliding grooves 405 are both in an annular structure, the limit ring 402 is respectively connected with the stirring barrel 3 and the top cover 5 in a sliding manner through the mutual matching of the sliding block 404 and the sliding groove 405, the bottom end of the driving component 6 is provided with a mounting plate 604, the top of the mounting plate 604 is provided with a motor 601, the output end of the motor 601 is provided with a rotating shaft 602, the outer side of the rotating shaft 602 is sleeved with a gear 603, one end of the top cover 5 close to the motor 601 is provided with a top plate 605, the bottom of the top plate 605 is provided with a bearing seat, the rotating shaft 602 is rotatably connected with the top plate 605 through the bearing seat, and the limit ring 402 is slidably connected, the rotating effect of the motor is better, the motor 601 is conveniently supported through the top plate 605 and the mounting plate 604, the top of the rotating shaft 602 is supported, and the rotating position of the rotating shaft is more stable.
Please refer to fig. 1, 2, 3, 4 and 5, the outer side of the gear ring 406 is uniformly provided with a plurality of sets of latches 606 matching with the gear 603, the gear ring 406 is engaged with the gear 603 through the latches 606, one end of each of the two sets of supporting frames 2 is respectively provided with a first fixing block 12 and a second fixing block 13, and the two groups of supporting frames 2 are fixedly connected with the top cover 5 through the first fixing block 12, the two groups of supporting frames 2 are fixedly connected with the stirring barrel 3 through the second fixing block 13, the gear ring 406 is meshed with the gear 603 through the latch 606, so that the gear 603 can drive the gear ring 406 to rotate when rotating, thereby the rotating effect of the gear ring 406 is better, the rotation is more labor-saving, and the top cover 5 and the stirring barrel 3 are convenient to fix through the arranged first fixing block 12 and the second fixing block 13, so that the stability of the top cover is better, and the influence of the gravity of the top cover 5 on the rotation of the rotating assembly 4 is avoided.
Referring to fig. 1, 2, 3, 4 and 5, the specific manufacturing method comprises the following steps:
preparing the following raw materials, namely 10-20 parts of nano calcium carbonate powder, 15-25 parts of pearl powder, 20-35 parts of oyster powder, 30-50 parts of calcium aspartate, 15-20 parts of casein calcium peptide, 5-10 parts of sodium cholate, 5-10 parts of casein phosphopeptide, 10-15 parts of chondroitin sulfate, 3-5 parts of sorbitol and 5-10 parts of fructose;
secondly, deep processing is carried out on the nano calcium carbonate, thermal decomposition treatment is carried out on the calcium carbonate powder with the purity of more than 98 percent by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes, and digestion reaction, emulsification reaction and drying treatment are sequentially carried out to obtain the nano calcium carbonate with the average particle size of 1-10 nanometers;
opening a valve on the feeding pipe 11, then sequentially guiding the nano calcium carbonate, the pearl powder, the oyster powder, the calcium aspartate, the casein calcium peptide, the sodium cholate, the casein phosphopeptide, the chondroitin sulfate, the sorbitol and the fructose into the inner side of the top cover 5 through the feeding pipe 11, and dropping into the limiting ring 402 and the top of the filter screen 403;
step four, a power supply is switched on, the motor 601 and the motor 7 run under the action of electric power, and the output ends of the motor 601 and the motor 7 rotate, so that the output end of the motor 601 drives the rotating shaft 602 and drives the gear 603 outside the rotating shaft 602 to rotate, then the gear ring 406 is driven to rotate under the matching of the clamping teeth 606, so that the gear ring 406 is rotatably connected with the top cover 5 and the stirring barrel 3 under the mutual matching of the sliding block 404 and the sliding groove 405, and the support plate 401 and the filter screen 403 are driven to rotate on the adjacent end faces of the top cover 5 and the stirring barrel 3, so that the rotating scattering of materials on the top of the gear ring is realized, the uniform blanking of the materials is realized, then the output end of the motor 7 drives the stirring shaft 8 and the stirring blades 9 to rotate, the materials in the stirring barrel 3 are stirred until the materials are uniformly stirred;
and step five, opening a valve on the discharge pipe 10 for leading out the composite nano calcium.
In this example, according to the second step, the fine calcium oxide particles are fed into the continuous tank digester, and at the same time, purified water in an amount five times the weight of the fine calcium oxide particles is added, and the mixture is stirred for 10 to 5 minutes by a stirring device in the digester, so that the digestion reaction is completed, and simultaneously, the calcium hydroxide suspension produced by digestion flows out from the slurry overflow outlet, and the calcium oxide suspension is obtained.
In this embodiment, according to the second step, in which emulsification reaction, the generated calcium oxide suspension is put into a high shear emulsifying machine, and shearing emulsification is carried out for 20 to 30 minutes, so as to fully refine and homogenize the calcium oxide suspension; and then dehydrating, drying and surface treating are carried out, H202 in the second stage of carbonization liquid is discharged along with the second stage of carbonization liquid during dehydration and drying, so that nano calcium carbonate with the average grain diameter of 1-10 nanometers is obtained, and according to the fourth step, the material is spirally fed in an annular radial manner by taking the middle position of the filter screen 403 as a base point.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (10)
1. A production device of composite nano calcium comprises a device main body (1), and is characterized in that: the one end of equipment main part (1) is provided with agitator (3), the both sides of agitator (3) all are provided with support frame (2), the top of agitator (3) is rotated and is connected with runner assembly (4), the top of runner assembly (4) is provided with top cap (5), the top of agitator (3) one end is provided with drive assembly (6), motor (7) are installed to the one end of agitator (3), the output of motor (7) is provided with (mixing) shaft (8) that run through to the inside one end of agitator (3), the outside of (mixing) shaft (8) evenly is provided with multiunit stirring vane (9), the bottom of agitator (3) is provided with discharging pipe (10), the top of top cap (5) evenly is provided with multiunit inlet pipe (11).
2. The production equipment of composite nano calcium as claimed in claim 1, wherein: rotating assembly (4) are including backup pad (401), the top and the bottom of backup pad (401) all are provided with spacing ring (402), the four corners department in spacing ring (402) outside all is provided with slider (404), the top of backup pad (401) is provided with filter screen (403), the outside of backup pad (401) is provided with ring gear (406), and is two sets of the terminal surface that backup pad (401) was kept away from to the inside of spacing ring (402) all leans out.
3. The production equipment of composite nano calcium as claimed in claim 2, wherein: the top of agitator (3) inner wall and the bottom of top cap (5) inner wall all are provided with slider (404) assorted spout (405), and spout (405) all are the loop configuration, spacing ring (402) all cooperate each other through slider (404) and spout (405) respectively with agitator (3) and top cap (5) sliding connection.
4. The production equipment of composite nano calcium as claimed in claim 1, wherein: the bottom of drive assembly (6) is provided with mounting panel (604), motor (601) are installed at the top of mounting panel (604), the output of motor (601) is provided with axis of rotation (602), the outside cover of axis of rotation (602) is equipped with gear (603), top cap (5) are close to the one end of motor (601) and are provided with roof (605), the bottom of roof (605) is provided with the bearing frame, axis of rotation (602) are connected with roof (605) through the bearing frame rotation.
5. The production equipment of composite nano calcium as claimed in claim 2, wherein: the outer side of the gear ring (406) is uniformly provided with a plurality of groups of clamping teeth (606) matched with the gear (603), and the gear ring (406) is meshed with the gear (603) through the clamping teeth (606).
6. The production equipment of composite nano calcium as claimed in claim 1, wherein: two sets of the one end of support frame (2) all is provided with first fixed block (12) and second fixed block (13) respectively, and is two sets of support frame (2) all are through first fixed block (12) and top cap (5) fixed connection, and are two sets of support frame (2) all are through second fixed block (13) and agitator (3) fixed connection.
7. The production equipment and the production method of the composite nano calcium are characterized in that: the specific production method comprises the following steps:
preparing the following raw materials, namely 10-20 parts of nano calcium carbonate powder, 15-25 parts of pearl powder, 20-35 parts of oyster powder, 30-50 parts of calcium aspartate, 15-20 parts of casein calcium peptide, 5-10 parts of sodium cholate, 5-10 parts of casein phosphopeptide, 10-15 parts of chondroitin sulfate, 3-5 parts of sorbitol and 5-10 parts of fructose;
secondly, deep processing is carried out on the nano calcium carbonate, thermal decomposition treatment is carried out on the calcium carbonate powder with the purity of more than 98 percent by adopting plasma flame to prepare particle calcium oxide with the particle size of 2500 meshes, and digestion reaction, emulsification reaction and drying treatment are sequentially carried out to obtain the nano calcium carbonate with the average particle size of 1-10 nanometers;
opening a valve on the feeding pipe (11), then sequentially guiding the nano calcium carbonate, the pearl powder, the oyster powder, the calcium aspartate, the casein calcium peptide, the sodium cholate, the casein phosphopeptide, the chondroitin sulfate, the sorbitol and the fructose into the inner side of the top cover (5) through the feeding pipe (11), enabling the nano calcium carbonate, the pearl powder, the oyster powder, the calcium aspartate, the casein calcium peptide, the sodium cholate, the casein phosphopeptide, the chondroitin sulfate, the sorbitol and the fructose to fall into the inner part of the limiting ring (402), and enabling the;
step four, a power supply is switched on, the motor (601) and the motor (7) run under the action of electric power, and the output end of the motor is rotated, so that the output end of the motor (601) drives the rotating shaft (602) and the gear (603) outside the rotating shaft (602) to rotate, then the gear ring (406) is driven to rotate under the matching of the clamping teeth (606), so that the gear ring (406) is driven to rotate under the mutual matching of the sliding block (404) and the sliding groove (405) to be connected with the top cover (5) and the stirring barrel (3) in a rotating way, and the support plate (401) and the filter screen (403) are driven to rotate on the adjacent end faces of the top cover (5) and the stirring barrel (3), so that the rotating scattering of the top material is realized, the uniform blanking of the material is realized, then the output end of the motor (7) drives the stirring shaft (8) and the stirring blades (9) to rotate, and the material in the stirring barrel (3, until the materials are evenly stirred, thereby obtaining the composite nano calcium;
and step five, opening a valve on the discharge pipe (10) for leading out the composite nano calcium.
8. The production equipment and the production method of the composite nano calcium as claimed in claim 7, wherein the production equipment comprises: according to the second step, the fine calcium oxide particles are sent into a groove type continuous digester, meanwhile, purified water with the weight being five times that of the fine calcium oxide particles is added, the mixture is stirred for 10 minutes to 5 minutes through a stirring device in the digester, so that the digestion reaction is finished, and meanwhile, the calcium hydroxide suspension produced by digestion flows out from a slurry overflow outlet, and therefore the calcium oxide suspension is obtained.
9. The production equipment and the production method of the composite nano calcium as claimed in claim 8, wherein the production equipment comprises: according to the second step, the emulsification reaction is carried out, the generated calcium oxide suspension is put into a high-shear emulsifying machine, and shearing emulsification is carried out for 20 to 30 minutes, so that the calcium oxide suspension is fully refined and uniform; and then dehydrating, drying and surface treating are carried out, and H202 in the second stage carbonization liquid is discharged along with the second stage carbonization liquid during dehydration and drying, so that the nano calcium carbonate with the average grain diameter of 1-10 nanometers is obtained.
10. The production equipment and the production method of the composite nano calcium as claimed in claim 7, wherein the production equipment comprises: according to the fourth step, the materials are spirally discharged in an annular radial mode by taking the middle position of the filter screen (403) as a base point.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010888328.7A CN112090358A (en) | 2020-08-28 | 2020-08-28 | Production equipment and production method of composite nano calcium |
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| CN202010888328.7A CN112090358A (en) | 2020-08-28 | 2020-08-28 | Production equipment and production method of composite nano calcium |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023224397A1 (en) * | 2022-05-20 | 2023-11-23 | 주식회사 엘지에너지솔루션 | Raw material mixing apparatus for producing slurry |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2023224397A1 (en) * | 2022-05-20 | 2023-11-23 | 주식회사 엘지에너지솔루션 | Raw material mixing apparatus for producing slurry |
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Application publication date: 20201218 |