CN112064053B - Stirring type fluorination electrolytic tank - Google Patents
Stirring type fluorination electrolytic tank Download PDFInfo
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- CN112064053B CN112064053B CN202010978562.9A CN202010978562A CN112064053B CN 112064053 B CN112064053 B CN 112064053B CN 202010978562 A CN202010978562 A CN 202010978562A CN 112064053 B CN112064053 B CN 112064053B
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/245—Fluorine; Compounds thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
- B01F27/72—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with helices or sections of helices
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
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- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
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- Engineering & Computer Science (AREA)
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- Materials Engineering (AREA)
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
Abstract
The invention relates to the technical field of fluorination electrolysis, and discloses an agitating type fluorination electrolytic cell which comprises a fluorination electrolytic cell, wherein an air adding box is fixedly arranged at the top of the fluorination electrolytic cell, a transmission box is fixedly arranged on the left side surface of the fluorination electrolytic cell, a quantitative box is fixedly arranged in the air adding box, a supporting plate is fixedly arranged in the quantitative box, a sliding groove is formed in the outer side surface of the supporting plate, a sliding plate is movably connected to the outer side surface of the supporting plate, a connecting plate is fixedly connected to the back surface of the sliding plate, and one end of the connecting plate extends to the inside of the sliding groove. This stirring formula electrolytic cell that fluoridizes drives the rotary rod through the inside motor of transmission case and can rotate, and the driven gear that drives both sides through the driving gear of its lateral surface can rotate to drive the inside stirring turbine of bearing and rotate, avoid the fluorine gas to enter into the inside of electrolytic cell and carry out the speed of fluoridizing and reduce, thereby realize stirring the chemical substance of electrolytic cell inside, realize the effect of quick fluoridizing.
Description
Technical Field
The invention relates to the technical field of fluorination electrolysis, in particular to a stirring type fluorination electrolytic tank.
Background
The electrolytic bath is composed of a bath body, an anode and a cathode, wherein most of the electrolytic bath is divided into an aqueous solution electrolytic bath, a fused salt electrolytic bath and a non-aqueous solution electrolytic bath by a diaphragm, when direct current passes through the electrolytic bath, an oxidation reaction occurs at the interface of the anode and the solution, a reduction reaction occurs at the interface of the cathode and the solution, so as to prepare a required product, the structure of the electrolytic bath is optimally designed, and the electrode and the diaphragm are reasonably selected, so that the key points of improving the current efficiency, reducing the voltage of the bath and saving the energy consumption are achieved.
The existing fluorination electrolytic cell adds fluoride into the inside of the electrolytic cell, carries out fluorination electrolytic reaction on compounds, and fluoride is continuously added into the inside of the electrolytic cell, so that the efficiency of the reaction is limited, and the fluoride continuously enters the inside of the electrolytic cell to cause the waste of the fluoride, thereby causing the loss of cost by fluorination electrolysis.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the stirring type fluorination electrolytic tank which has the advantages that the fluorine gas can be quantitatively added into the electrolytic tank for fluorination, and the like, and the problem that a large amount of fluoride continuously enters the electrolytic tank to cause the waste of a large amount of fluoride is solved.
(II) technical scheme
In order to realize the aim that the fluorine gas can be quantitatively added into the electrolytic cell for fluorination, the invention provides the following technical scheme: an agitation type fluorination electrolytic tank comprises a fluorination electrolytic tank, wherein an air adding box is fixedly arranged at the top of the fluorination electrolytic tank, a transmission box is fixedly arranged on the left side surface of the fluorination electrolytic tank, a quantitative box is fixedly arranged in the air adding box, a supporting plate is fixedly arranged in the quantitative box, a sliding groove is formed in the outer side surface of the supporting plate, a sliding plate is movably connected to the outer side surface of the supporting plate, a connecting plate is fixedly connected to the back surface of the sliding plate, one end of the connecting plate extends into the sliding groove, connecting plates are fixedly arranged on the outer side surface of the sliding plate, the number of the connecting plates is two, the two connecting plates are symmetrically distributed by taking the axis of the sliding plate as the center, a rotating support rod is fixedly arranged on the outer side surface of the sliding plate, a connecting rod is movably sleeved on the outer side surface of the rotating support rod, the number of the connecting rods is two, and a cam is fixedly arranged in the quantitative box through a rotating shaft, one end of the connecting rod is movably connected with the outer side surface of the cam, a movable sleeve is fixedly arranged in the quantitative box, a loop bar is movably connected in the movable sleeve, the top end of the loop bar penetrates through the movable sleeve and extends to the outer side surface of the movable sleeve, an extension bar is fixedly arranged at the bottom of the loop bar, the bottom end of the extension bar penetrates through the movable sleeve and extends to the bottom of the quantitative box, a supporting spring is movably sleeved on the outer side surface of the extension bar, a supporting frame is fixedly arranged at the top of the loop bar, a rubber wheel is movably connected in the supporting frame, the bottom of the cam is contacted with the outer side surface of the rubber wheel, a fixed plate is fixedly arranged at the top of the sliding plate, a driving wheel is fixedly arranged in the quantitative box, the driving wheel is eccentrically connected with one end of the driving rod, the other end of the driving rod is movably connected with the fixed plate, and a bearing is fixedly arranged in the fluorination electrolytic tank, the quantity of the bearings is four, two bearings are a group, a stirring turbine is fixedly connected between every two bearings, a transmission rod is fixedly connected inside each bearing, a driven gear is fixedly sleeved on the outer side surface of the transmission rod, a bearing block is fixedly installed inside the transmission box, transmission grooves are formed in the fluorination electrolytic cell and the bearing block, a rotary rod is movably connected inside each transmission groove, a driving gear is fixedly sleeved on the outer side surface of the rotary rod, an outlet pipe is fixedly installed at the bottom of the fluorination electrolytic cell, a flange is fixedly installed at the bottom of the outlet pipe, a sliding rod is fixedly installed on the outer side surface of the outlet pipe, a sliding sleeve plate is movably sleeved on the outer side surface of the sliding rod, a limiting spring is fixedly installed at the bottom of the sliding sleeve plate, and a limiting rod is fixedly installed at the bottom of the limiting spring, the inside fixedly connected with connecting rod of gag lever post, the gag lever post is all run through at the both ends of connecting rod, the lateral surface activity of gag lever post has cup jointed the plugboard.
Preferably, the motor is fixedly installed in the quantitative box, and the output end of the motor is movably connected with the driving wheel.
Preferably, the fixed cover of lateral surface of rotary rod has connect the restriction board, the quantity of restriction board is two, two the restriction board is the inside that has the drive groove, driven gear and driving gear mesh mutually.
Preferably, the motor is fixedly installed in the transmission case, the driving belt is movably sleeved on the outer side surface of the rotating rod, and the rotating rod is connected with the output end of the motor through the driving belt.
Preferably, the shape of slide bar is L type shape, fixedly connected with peg graft pole between slide bar and the outlet pipe, the slip lagging pegs graft mutually with the peg graft pole, the internal thread of slide bar is connected with the screw rod, the right-hand member of screw rod runs through the slide bar and extends to the lateral surface of slip lagging, the fixed cover of lateral surface of screw rod has connect the baffle, the quantity of baffle is two, two the baffle is located the both sides of slip lagging respectively.
Preferably, the top of the gas filling box is provided with two gas inlets, and the two gas inlets are symmetrically distributed by taking the axis of the gas filling box as a center.
Preferably, a feeding port is formed in the top of the fluorination electrolytic tank and located on the right side face of the gas adding box, and a fixing frame is fixedly mounted at the bottom of the fluorination electrolytic tank.
Preferably, the top end of the supporting spring is fixedly connected with the bottom of the loop bar, the bottom end of the supporting spring is fixedly connected with the bottom of the movable sleeve, and the width value of the supporting spring is larger than that of the outlet of the movable sleeve.
Preferably, a quantitative gas outlet is formed in the fluorination electrolytic cell, a gas baffle is movably connected in the quantitative gas outlet, the outer side surface of the gas baffle is in contact with the inner wall of the quantitative gas outlet, and the top of the gas baffle is fixedly connected with the bottom end of the extension rod.
(III) advantageous effects
Compared with the prior art, the invention provides a stirring type fluorination electrolytic cell, which has the following beneficial effects:
1. this stirring formula electrolytic cell that fluoridizes drives the rotary rod through the inside motor of transmission case and can rotate, and the driven gear that drives both sides through the driving gear of its lateral surface can rotate to drive the inside stirring turbine of bearing and rotate, avoid the fluorine gas to enter into the inside of electrolytic cell and carry out the speed of fluoridizing and reduce, thereby realize stirring the chemical substance of electrolytic cell inside, realize the effect of quick fluoridizing.
2. This stirring formula fluorination electrolysis trough enters into the inside of air entrainment case with fluorine gas through the air inlet, and the motor of cooperation air entrainment incasement portion is slowed down and is rotated and make the driving wheel can rotate, drives the inside of slide at backup pad lateral surface sliding tray through the drive pole and can stretch to the horizontal rotation of drive cam drives the choke plate and carries out the removal of repeated upper and lower position, realizes the inside of fluorine gas ration entering into the fluorination electrolysis trough, avoids the inside that fluorine gas directly enters into the electrolysis trough in a large amount to fluorinate, thereby causes the waste.
3. This electrolysis trough is fluoridized to stirring formula makes the slip lagging slide at the lateral surface of slide bar through rotatory screw rod to be convenient for adjust the position of slip lagging, the restriction spring of cooperation slip lagging bottom is connected with the plugboard, thereby realizes carrying out the high-speed joint to the connecting pipe of flange bottom fast, avoids connection speed slow, causes work efficiency to reduce.
Drawings
FIG. 1 is a schematic front view of the present invention;
FIG. 2 is a schematic cross-sectional front view of the present invention;
FIG. 3 is an enlarged schematic view of the structure at A in FIG. 1 according to the present invention;
fig. 4 is an enlarged schematic view of the structure at B in fig. 2 according to the present invention.
In the figure: 1. a fluorination electrolytic cell; 2. a transmission case; 3. an air-adding box; 4. a feeding port; 5. an air inlet; 6. an outlet pipe; 7. a flange; 8. a transmission rod; 9. a bearing block; 10. rotating the rod; 11. a driving gear; 12. a driven gear; 13. an air outlet; 14. a choke plate; 15. a bearing; 16. a stirring turbine; 17. a limiting plate; 18. a transmission groove; 19. a support plate; 20. an extension rod; 21. a movable sleeve; 22. a support spring; 23. a loop bar; 24. a support frame; 25. a rubber wheel; 26. a slide plate; 27. a fixing plate; 28. driving the wheel; 29. driving the rod; 30. a connector tile; 31. a rotating shaft; 32. a cam; 33. a connecting rod; 34. a sliding groove; 35. a plug rod; 36. a sliding sleeve plate; 37. a baffle plate; 38. a screw; 39. a slide bar; 40. a restraining spring; 41. a connecting rod; 42. a limiting rod; 43. a plugboard.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, an agitation type fluorination electrolytic cell comprises a fluorination electrolytic cell 1, a feed inlet 4 is arranged at the top of the fluorination electrolytic cell 1, the feed inlet 4 is arranged at the right side surface of an air adding box 3, a fixing frame is fixedly arranged at the bottom of the fluorination electrolytic cell 1, the air adding box 3 is fixedly arranged at the top of the fluorination electrolytic cell 1, two air inlets 5 are arranged at the top of the air adding box 3, the two air inlets 5 are symmetrically distributed by taking the axis of the air adding box 3 as the center, a transmission box 2 is fixedly arranged at the left side surface of the fluorination electrolytic cell 1, a quantitative box is fixedly arranged inside the air adding box 3, a support plate 19 is fixedly arranged inside the quantitative box, a sliding groove 34 is arranged at the outer side surface of the support plate 19, a sliding plate 26 is movably connected to the outer side surface of the support plate 19, a connecting plate is fixedly connected to the back surface of the sliding plate 26, and one end of the connecting plate extends to the inside of the sliding groove 34, the outer side surface of the sliding plate 26 is fixedly provided with connecting plates 30, the connecting rods 33 are limited by arranging the connecting plates 30, the number of the connecting plates 30 is two, the two connecting plates 30 are symmetrically distributed by taking the axis of the sliding plate 26 as the center, the outer side surface of the sliding plate 26 is fixedly provided with a rotary supporting rod, the outer side surface of the rotary supporting rod is movably sleeved with the connecting rods 33, the number of the connecting rods 33 is two, the quantitative box is internally and fixedly provided with a cam 32 through a rotating shaft 31, one end of the connecting rod 33 is movably connected with the outer side surface of the cam 32, the quantitative box is internally and fixedly provided with a movable sleeve 21, the movable sleeve 21 is movably connected with a sleeve rod 23, the top end of the sleeve rod 23 penetrates through the movable sleeve 21 and extends to the outer side surface of the movable sleeve 21, the bottom of the sleeve rod 23 is fixedly provided with an extension rod 20, and the bottom end of the extension rod 20 penetrates through the movable sleeve 21 and extends to the bottom of the quantitative box, supporting spring 22 is sleeved on the outer side face of extension rod 20, the top end of supporting spring 22 is fixedly connected with the bottom of loop bar 23, the bottom end of supporting spring 22 is fixedly connected with the bottom of movable sleeve 21, the width of supporting spring 22 is larger than the width of movable sleeve 21, support frame 24 is fixedly mounted at the top of loop bar 23, the inside of support frame 24 is movably connected with rubber wheel 25, the bottom of cam 32 is contacted with the outer side face of rubber wheel 25, fixed plate 27 is fixedly mounted at the top of sliding plate 26, driving wheel 28 is fixedly mounted in the inside of quantitative box, motor is fixedly mounted in the inside of quantitative box, the output end of motor is movably connected with driving wheel 28, driving wheel 28 is eccentrically connected with one end of driving rod 29, the other end of driving rod 29 is movably connected with fixed plate 27, bearing 15 is fixedly mounted in the inside of fluorination electrolytic tank 1, the number of the bearings 15 is four, two bearings 15 are a group, a stirring turbine 16 is fixedly connected between each group of bearings 15, a transmission rod 8 is fixedly connected inside each bearing 15, a driven gear 12 is fixedly sleeved on the outer side surface of the transmission rod 8, a bearing block 9 is fixedly installed inside the transmission case 2, transmission grooves 18 are formed in the fluorination electrolytic tank 1 and the bearing block 9, a rotary rod 10 is movably connected inside each transmission groove 18, a motor is fixedly installed inside the transmission case 2, a transmission belt is movably sleeved on the outer side surface of the rotary rod 10, the rotary rod 10 is connected with the output end of the motor through the transmission belt, limiting plates 17 are fixedly sleeved on the outer side surface of the rotary rod 10, the number of the limiting plates 17 is two, the two limiting plates 17 are both inside the transmission grooves 18, the driven gear 12 is meshed with the driving gear 11, the outer side surface of the rotary rod 10 is fixedly sleeved with the driving gear 11, an outlet pipe 6 is fixedly installed at the bottom of the fluorination electrolytic tank 1, a flange 7 is fixedly installed at the bottom of the outlet pipe 6, a sliding rod 39 is fixedly installed on the outer side surface of the outlet pipe 6, the sliding rod 39 is L-shaped, an inserting rod 35 is fixedly connected between the sliding rod 39 and the outlet pipe 6, the sliding sleeve plate 36 can be supported in an auxiliary mode when moving by arranging the inserting rod 35, the sliding sleeve plate 36 is prevented from being overturned when sliding, the sliding sleeve plate 36 is inserted into the inserting rod 35, a screw rod 38 is connected with the inner thread of the sliding rod 39, the right end of the screw rod 38 penetrates through the sliding rod and extends to the outer side surface of the sliding sleeve plate 36, two baffles 37 are fixedly sleeved on the outer side surface of the screw rod 38, the two baffles 37 are respectively positioned on two sides of the sliding sleeve plate 36, the sliding sleeve plate 36 is movably sleeved on the outer side surface of the sliding rod 39, a limiting spring 40 is fixedly installed at the bottom of the sliding sleeve plate 36, make pinboard 43 can stretch through setting up restriction spring 40, the one end of the connecting pipe of being convenient for can insert, thereby realize the fixed connection to the connecting pipe, restriction spring 40's bottom fixed mounting has gag lever post 42, gag lever post 42's inside fixedly connected with connecting rod 41, gag lever post 42 has all been run through at connecting rod 41's both ends, pegboard 43 has been cup jointed in gag lever post 42's lateral surface activity, ration gas outlet 13 has been seted up to the inside of fluoridizing electrolysis trough 1, the inside swing joint of ration gas outlet 13 has choke plate 14, choke plate 14's lateral surface contacts with the inner wall of ration gas outlet 13, choke plate 14's top and extension rod 20's bottom fixed connection.
During operation, fluorine gas enters the interior of the gas adding box 3 through the gas inlet 5, the driving wheel 28 is rotated by matching with the slow rotation of the motor in the gas adding box 3, the driving rod 29 drives the sliding plate 26 to be stretched in the sliding groove 34 on the outer side surface of the supporting plate 19, so that the cam 32 is driven to rotate left and right, the gas baffle plate 14 is driven to repeatedly move in the vertical direction, the fluorine gas quantitatively enters the interior of the fluorination electrolytic tank 1, the motor in the transmission box 2 is matched to drive the rotating rod 10 to rotate, the driven gears 12 on two sides are driven to rotate through the driving gear 11 on the outer side surface, so that the stirring turbine 16 in the bearing 15 is driven to rotate, the chemical substances in the electrolytic tank are stirred, and the rapid fluorination effect is realized.
In summary, in the stirring type fluorination electrolytic cell, the motor inside the transmission case 2 drives the rotating rod 10 to rotate, and the driving gear 11 on the outer side surface drives the driven gears 12 on the two sides to rotate, so as to drive the stirring turbine 16 inside the bearing 15 to rotate, and prevent the fluorine gas from entering the inside of the electrolytic cell to be fluorinated, so that the chemical substances inside the electrolytic cell are stirred, and the rapid fluorination effect is realized; fluorine gas enters the interior of the gas adding box 3 through the gas inlet 5, the driving wheel 28 is rotated by matching with the slow rotation of a motor in the gas adding box 3, the driving rod 29 drives the sliding plate 26 to be stretched in the sliding groove 34 on the outer side surface of the supporting plate 19, so that the cam 32 is driven to rotate left and right, the gas baffle plate 14 is driven to move in the vertical direction repeatedly, the fluorine gas quantitatively enters the interior of the fluorination electrolytic tank 1, and the fluorine gas is prevented from directly entering the interior of the electrolytic tank in a large amount to be fluorinated, so that waste is caused; make slip lagging 36 slide at the lateral surface of slide bar 39 through rotatory screw rod 38 to be convenient for adjust the position of slip lagging 36, the restriction spring 40 that cooperates the slip lagging 36 bottom is connected with plugboard 43, thereby realizes carrying out the high-speed joint to the connecting pipe of flange 7 bottom fast, avoids connection speed slow, causes work efficiency to reduce.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. An agitated fluorination cell comprising a fluorination cell (1), characterized in that: fluoridize electrolysis trough (1) top fixed mounting have air entrainment case (3), the left surface fixed mounting who fluoridizes electrolysis trough (1) has transmission case (2), the inside fixed mounting of air entrainment case (3) has quantitative case, and the inside fixed mounting of quantitative case has backup pad (19), sliding tray (34) have been seted up to the lateral surface of backup pad (19), the lateral surface swing joint of backup pad (19) has slide (26), the inside fixedly connected with connecting plate of back of slide (26), the one end of connecting plate extend to the inside of sliding tray (34), the lateral surface fixed mounting of slide (26) has linkage plate (30), the quantity of linkage plate (30) is two, two the axle center that uses slide (26) linkage plate (30) is central symmetric distribution, the lateral surface fixed mounting of slide (26) has the rotation support pole, connecting rod (33) has been cup jointed in the lateral surface activity of rotatory bracing piece, the quantity of connecting rod (33) is two, and there are cam (32) inside the ration case through axis of rotation (31) fixed mounting, the one end of connecting rod (33) and the lateral surface swing joint of cam (32), and the inside fixed mounting of ration case has movable sleeve (21), the inside swing joint of movable sleeve (21) has loop bar (23), the top of loop bar (23) runs through movable sleeve (21) and extends to the lateral surface of movable sleeve (21), the bottom fixed mounting of loop bar (23) has extension rod (20), the bottom of extension rod (20) runs through movable sleeve (21) and extends to the bottom of ration case, supporting spring (22) have been cup jointed in the lateral surface activity of extension rod (20), the top fixed mounting of loop bar (23) has support frame (24), the inside swing joint of support frame (24) has rubber wheel (25), the bottom of cam (32) contacts with the lateral surface of rubber wheel (25), the top fixed mounting of slide (26) has fixed plate (27), and the inside fixed mounting of ration case has driving wheel (28), driving wheel (28) and driving rod (29) one end eccentric connection, driving rod (29) other end and fixed plate (27) swing joint, the inside fixed mounting of fluoridizing electrolysis trough (1) has bearing (15), the quantity of bearing (15) is four, two bearing (15) are a set of, and every group equal fixedly connected with stirring turbine (16) between bearing (15), the inside fixedly connected with transfer line (8) of bearing (15), the lateral surface fixed cover of transfer line (8) has connect passive gear (12), the inner fixed mounting of transmission case (2) has bearing block (9), transmission groove (18) have all been seted up with the inside of bearing block (9) to fluoridize electrolysis trough (1), the inside swing joint of transmission groove (18) has rotary rod (10), driving gear (11) have been cup jointed to the lateral surface of rotary rod (10), the bottom fixed mounting of fluoridizing electrolysis trough (1) has outlet pipe (6), the bottom fixed mounting of outlet pipe (6) has flange (7), the lateral surface fixed mounting of outlet pipe (6) has slide bar (39), the lateral surface activity of slide bar (39) has been cup jointed slip lagging (36), the bottom fixed mounting of slip lagging (36) has limiting spring (40), the bottom fixed mounting of limiting spring (40) has gag lever post (42), the inside fixedly connected with connecting rod (41) of gag lever post (42), the two ends of the connecting rod (41) penetrate through the limiting rod (42), and the outer side surface of the limiting rod (42) is movably sleeved with the insertion plate (43).
2. An agitated fluorination cell as claimed in claim 1 in which: the inside of the quantitative box is fixedly provided with a motor, and the output end of the motor is movably connected with a driving wheel (28).
3. An agitated fluorination cell as claimed in claim 1 in which: the lateral surface of rotary rod (10) is fixed cup joints limiting plate (17), limiting plate (17)'s quantity is two, two limiting plate (17) are the inside that has drive groove (18), driven gear (12) and driving gear (11) mesh mutually.
4. An agitated fluorination cell as claimed in claim 1 in which: the inside fixed mounting of transmission case (2) has the motor, the drive belt has been cup jointed in the lateral surface activity of rotary rod (10), rotary rod (10) are connected with the output of motor through the drive belt.
5. An agitated fluorination cell as claimed in claim 1 in which: the shape of slide bar (39) is L type shape, fixedly connected with peg graft pole (35) between slide bar (39) and outlet pipe (6), slip lagging (36) are pegged graft mutually with peg graft pole (35), the inside threaded connection of slide bar (39) has screw rod (38), the right-hand member of screw rod (38) runs through the slide bar and extends to the lateral surface of slip lagging (36), the lateral surface of screw rod (38) is fixed cup jointed baffle (37), the quantity of baffle (37) is two, two baffle (37) are located the both sides of slip lagging (36) respectively.
6. An agitated fluorination cell as claimed in claim 1 in which: air inlet (5) have been seted up at the top of air entrainment case (3), the quantity of air inlet (5) is two, two air inlet (5) use the axle center of air entrainment case (3) as central symmetry distribution.
7. An agitated fluorination cell as claimed in claim 1 in which: a feeding port (4) is formed in the top of the fluorination electrolytic tank (1), the feeding port (4) is located on the right side face of the gas adding box (3), and a fixing frame is fixedly mounted at the bottom of the fluorination electrolytic tank (1).
8. An agitated fluorination cell as claimed in claim 1 in which: the top end of the supporting spring (22) is fixedly connected with the bottom of the loop bar (23), the bottom end of the supporting spring (22) is fixedly connected with the bottom of the movable sleeve (21), and the width value of the supporting spring (22) is larger than the outlet width value of the movable sleeve (21).
9. An agitated fluorination cell as claimed in claim 1 in which: the quantitative gas outlet (13) is formed in the fluorination electrolytic cell (1), the gas baffle plate (14) is movably connected in the quantitative gas outlet (13), the outer side surface of the gas baffle plate (14) is in contact with the inner wall of the quantitative gas outlet (13), and the top of the gas baffle plate (14) is fixedly connected with the bottom end of the extension rod (20).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010978562.9A CN112064053B (en) | 2020-09-17 | 2020-09-17 | Stirring type fluorination electrolytic tank |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010978562.9A CN112064053B (en) | 2020-09-17 | 2020-09-17 | Stirring type fluorination electrolytic tank |
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| Publication Number | Publication Date |
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| CN112064053A CN112064053A (en) | 2020-12-11 |
| CN112064053B true CN112064053B (en) | 2021-10-12 |
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| US6691640B1 (en) * | 2002-04-22 | 2004-02-17 | Tom Huckabee | Animal feeder insert with desiccant cavity |
| WO2012039024A1 (en) * | 2010-09-21 | 2012-03-29 | 三菱マテリアル株式会社 | Method and device for recovering perfluoroalkanesulfonyl fluoride |
| CN203270046U (en) * | 2013-04-23 | 2013-11-06 | 湖北诺邦化学有限公司 | Stirring type fluorinated electrolytic bath |
| CN107118074A (en) * | 2017-04-11 | 2017-09-01 | 黎明化工研究设计院有限责任公司 | A kind of method for purifying perfluoromethylcyclohexane (PFMCH) |
| CN209065058U (en) * | 2018-10-23 | 2019-07-05 | 安徽辰控智能科技有限公司 | A kind of quantitative filler equipment of high-precision gas monitoring instrument shell |
| CN209428615U (en) * | 2019-01-26 | 2019-09-24 | 北京潮兴科技发展有限公司 | A kind of sodium hypochlorite electrolytic preparation device convenient for exhaust |
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