CN112063270A - Enameled wire insulation impregnating varnish and preparation method and application thereof - Google Patents

Enameled wire insulation impregnating varnish and preparation method and application thereof Download PDF

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Publication number
CN112063270A
CN112063270A CN202011013224.8A CN202011013224A CN112063270A CN 112063270 A CN112063270 A CN 112063270A CN 202011013224 A CN202011013224 A CN 202011013224A CN 112063270 A CN112063270 A CN 112063270A
Authority
CN
China
Prior art keywords
component
wire
impregnating varnish
enameled wire
diluent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202011013224.8A
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Chinese (zh)
Inventor
潘勤
李如福
赵广智
韩谋智
高洁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Anhui Hengci Magnetoelectric Co ltd
Original Assignee
Anhui Hengci Magnetoelectric Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Anhui Hengci Magnetoelectric Co ltd filed Critical Anhui Hengci Magnetoelectric Co ltd
Priority to CN202011013224.8A priority Critical patent/CN112063270A/en
Publication of CN112063270A publication Critical patent/CN112063270A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/08Anti-corrosive paints
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18Fireproof paints including high temperature resistant paints
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01BCABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • H01B3/308Wires with resins

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Manufacture Of Motors, Generators (AREA)
  • Organic Insulating Materials (AREA)

Abstract

The invention discloses an enameled wire insulating impregnating varnish and a preparation method and application thereof, wherein the enameled wire insulating impregnating varnish comprises a component A and a component B, and the weight ratio of the component A to the component B is 1: 0.32-1: 0.35; the component A is prepared from the following raw materials in parts by weight: 98 parts of epoxy resin, 1 part of defoaming agent and 1 part of flatting agent; the component B is a curing agent. The enameled wire insulating impregnating varnish provided by the invention has excellent insulativity, heat resistance, freezing resistance and chemical corrosion resistance; the enameled wire insulating impregnating varnish is applied to a magnetizing clamp coil, and the coating is complete and does not fall off after long-time use.

Description

Enameled wire insulation impregnating varnish and preparation method and application thereof
Technical Field
The invention belongs to the technical field of wire enamel, and particularly relates to an insulated impregnating varnish for an enameled wire, and a preparation method and application thereof.
Background
The insulating enamel paint for enameled wire has the effect of generating a good insulating layer between the wires in the winding to prevent the current from flowing, and the insulating layer can keep the original performance under the conditions of long-time moisture, heat, mechanical action, chemical attack and the like.
The varieties of the wire enamel comprise oil-based wire enamel, polyurethane wire enamel, polyester wire enamel, epoxy wire enamel and the like, but the existing wire enamel has complex component structure, complex preparation process, poor performance and large application limitation. The magnetizing fixture coil for magnetizing magnetic material is generally coated with PPG electrophoretic paint, but in practical application, the electrophoretic coating has poor insulation, poor adhesion and poor flexibility, and after repeated winding and electrification magnetizing of the electric wire in practical use, the coating on the copper wire falls off.
Disclosure of Invention
The purpose of the invention is as follows: the invention aims to provide the enameled wire insulating impregnating varnish, and the preparation method and application thereof, aiming at the defects of the prior art, wherein the enameled wire insulating impregnating varnish has excellent insulativity, heat resistance and freezing resistance, and is suitable for occasions such as magnetizing clamp coils.
The technical scheme is as follows: the enameled wire insulation impregnating varnish comprises a component A and a component B, wherein the weight ratio of the component A to the component B is 1: 0.32-1: 0.35; the component A is prepared from the following raw materials in parts by weight: 98 parts of epoxy resin, 1 part of defoaming agent and 1 part of flatting agent; the component B is a curing agent.
Further perfecting the technical scheme, the curing agent is polyamide.
Further, the weight ratio of the component A to the component B is 1: 0.33.
Further, a diluent is also included.
Further, after the diluent is added, a paint-4 cup is adopted to carry out a viscosity test on the insulated wire impregnating varnish for the enameled wire, and the viscosity test reaches 150 seconds at 25 ℃.
Further, the diluent is xylene and isobutanol which are prepared according to the weight ratio of 7: 3.
The preparation method of the enameled wire insulation impregnating varnish comprises the following steps:
(1) mixing the component A and the component B according to the weight ratio of 1:0.33, and the component A is prepared from the following raw materials in parts by weight: 98 parts of epoxy resin, 1 part of defoaming agent and 1 part of flatting agent, wherein the component B is a curing agent;
(2) adding a diluent, and uniformly stirring to obtain the enameled wire insulating impregnating varnish;
(3) and (3) adopting a coating-4 cup to carry out viscosity on the enameled wire insulation impregnating varnish obtained in the step (2) until the viscosity reaches 150 seconds at 25 ℃, otherwise, repeating the step (2).
The invention also provides the application of the enameled wire insulating impregnating varnish in the magnetizing clamp coil.
The application of the enameled wire insulating impregnating varnish in the magnetizing clamp coil comprises the following steps: and (3) soaking the copper wire of the magnetizing clamp coil in enameled wire insulating impregnating varnish, vertically hanging the soaked copper wire, air-drying for 24 hours, and then sending the copper wire into an oven for drying at 150 ℃ for 30min for use.
Has the advantages that: compared with the prior art, the invention has the advantages that: the enameled wire insulation impregnating varnish provided by the invention has excellent insulativity, heat resistance, freezing resistance, chemical corrosion resistance, and excellent adhesion and flexibility. The invention can finish the preparation of the enameled wire insulating impregnating varnish at normal temperature and normal pressure by adopting the existing general equipment, and has simple components and simple and easy operation of the preparation process. The enameled wire insulating impregnating varnish is applied to the magnetizing fixture coil, after the electric wire of the magnetizing fixture coil is repeatedly wound, folded and electrified and magnetized, the coating is complete and does not fall off, the electrification and magnetization are carried out for months, the insulating property of the copper wire is good, and the market scene is very large.
Detailed Description
The technical solution of the present invention is described in detail below, but the scope of the present invention is not limited to the embodiments.
Example 1: the invention provides enameled wire insulation impregnating varnish, which comprises: component A, component B and a diluent.
The component A comprises:
NPES-619A epoxy resin, the addition of which is 0.98kg, the manufacturer is south Asia (Kunshan) resin factory, the specification is industrial grade, 50% xylene solution;
BYK-054 defoamer, the addition amount is 0.01kg, and the manufacturer is German Bike;
BYK-306 leveling agent, the addition amount is 0.01kg, and the manufacturer is German Bike.
The component B is polyamide 650 with the addition of 0.33kg, and the manufacturer is Changzhou Ming Yao chemical new material company Limited.
The diluent is prepared from dimethylbenzene and isobutanol according to the weight ratio of 7: 3.
Mixing the component A and the component B according to the weight ratio of 1:0.33, adding a proper amount of diluent, and uniformly stirring; and measuring the viscosity by using a coating-4 cup, and if the viscosity is still higher, adding a proper amount of diluent until the viscosity reaches about 150 seconds/coating-4 cup/25 ℃, thus obtaining the enameled wire insulating impregnating varnish.
Applying the prepared enameled wire insulating impregnating varnish to a magnetizing clamp coil: and (3) soaking the copper wire of the magnetizing clamp coil in enameled wire insulating impregnating varnish, vertically hanging the soaked copper wire, air-drying for 24 hours, and then sending the copper wire into an oven at 150 ℃ for 30min for drying.
The enameled wire insulated impregnating varnish coated copper wire prepared by the method is practically used in a magnetizing workshop, and after the wire is repeatedly wound, folded and electrified and magnetized, the coating is complete and does not fall off, and the copper wire is electrified and magnetized for months and has good insulation property.
As noted above, while the present invention has been shown and described with reference to certain preferred embodiments, it is not to be construed as limited thereto. Various changes in form and detail may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (9)

1. The utility model provides an enameled wire insulation impregnating varnish which characterized in that: the adhesive comprises a component A and a component B, wherein the weight ratio of the component A to the component B is 1: 0.32-1: 0.35; the component A is prepared from the following raw materials in parts by weight: 98 parts of epoxy resin, 1 part of defoaming agent and 1 part of flatting agent; the component B is a curing agent.
2. The wire enamel according to claim 1, wherein: the curing agent is polyamide.
3. The wire enamel according to claim 1, wherein: the weight ratio of the component A to the component B is 1: 0.33.
4. The wire enamel according to claim 1, wherein: also includes a diluent.
5. The wire enamel according to claim 4, wherein: after the diluent is added, the enameled wire insulation impregnating varnish is subjected to viscosity test by adopting a coating-4 cup for 150 seconds at 25 ℃.
6. The wire enamel according to claim 4, wherein: the diluent is prepared from dimethylbenzene and isobutanol according to the weight ratio of 7: 3.
7. A preparation method of enameled wire insulation impregnating varnish is characterized by comprising the following steps:
(1) mixing the component A and the component B according to the weight ratio of 1:0.33, and the component A is prepared from the following raw materials in parts by weight: 98 parts of epoxy resin, 1 part of defoaming agent and 1 part of flatting agent, wherein the component B is a curing agent;
(2) adding a diluent, and uniformly stirring to obtain the enameled wire insulating impregnating varnish;
(3) and (3) adopting a coating-4 cup to carry out viscosity on the enameled wire insulation impregnating varnish obtained in the step (2) until the viscosity reaches 150 seconds at 25 ℃, otherwise, repeating the step (2).
8. The use of the wire enamel for insulation and impregnation according to any of claims 1 to 6 in magnetizing jig coils.
9. The use of the wire enamel for the insulation and impregnation of enamel wires according to claim 8, wherein: the method comprises the following steps: and (3) soaking the copper wire of the magnetizing clamp coil in enameled wire insulating impregnating varnish, vertically hanging the soaked copper wire, air-drying for 24 hours, and then sending the copper wire into an oven for drying at 150 ℃ for 30min for use.
CN202011013224.8A 2020-09-23 2020-09-23 Enameled wire insulation impregnating varnish and preparation method and application thereof Pending CN112063270A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202011013224.8A CN112063270A (en) 2020-09-23 2020-09-23 Enameled wire insulation impregnating varnish and preparation method and application thereof

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CN202011013224.8A CN112063270A (en) 2020-09-23 2020-09-23 Enameled wire insulation impregnating varnish and preparation method and application thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7046280B1 (en) * 2021-05-13 2022-04-01 三菱電機株式会社 Insulation varnish composition, insulation varnish cured product, coil and method for manufacturing the coil

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1539899A (en) * 2003-04-21 2004-10-27 索玛株式会社 mfg. method of soaking adaptable liquid epoxy resin compound, and generator thereof
JP2007213908A (en) * 2006-02-08 2007-08-23 Hitachi Cable Ltd Self-lubricating enamel wire and coating material
CN105925137A (en) * 2016-06-18 2016-09-07 合肥浦尔菲电线科技有限公司 Environment-friendly insulating paint and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1539899A (en) * 2003-04-21 2004-10-27 索玛株式会社 mfg. method of soaking adaptable liquid epoxy resin compound, and generator thereof
JP2007213908A (en) * 2006-02-08 2007-08-23 Hitachi Cable Ltd Self-lubricating enamel wire and coating material
CN105925137A (en) * 2016-06-18 2016-09-07 合肥浦尔菲电线科技有限公司 Environment-friendly insulating paint and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
《电气工程师手册》第二版编辑委员会: "《电气工程师手册》", 30 June 2000, 北京:机械工业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7046280B1 (en) * 2021-05-13 2022-04-01 三菱電機株式会社 Insulation varnish composition, insulation varnish cured product, coil and method for manufacturing the coil

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Application publication date: 20201211

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