CN112055546B - Roll paper for non-combustion heating type smoking article, and electric heating type smoking system - Google Patents
Roll paper for non-combustion heating type smoking article, and electric heating type smoking system Download PDFInfo
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- CN112055546B CN112055546B CN201880093033.1A CN201880093033A CN112055546B CN 112055546 B CN112055546 B CN 112055546B CN 201880093033 A CN201880093033 A CN 201880093033A CN 112055546 B CN112055546 B CN 112055546B
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- 229940117916 cinnamic aldehyde Drugs 0.000 description 1
- 229940017545 cinnamon bark Drugs 0.000 description 1
- 239000010632 citronella oil Substances 0.000 description 1
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 1
- 239000001524 citrus aurantium oil Substances 0.000 description 1
- 239000000701 coagulant Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000010636 coriander oil Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- ANJTVLIZGCUXLD-DTWKUNHWSA-N cytisine Chemical compound C1NC[C@H]2CN3C(=O)C=CC=C3[C@@H]1C2 ANJTVLIZGCUXLD-DTWKUNHWSA-N 0.000 description 1
- 229940027564 cytisine Drugs 0.000 description 1
- 229930017327 cytisine Natural products 0.000 description 1
- FYTRVXSHONWYNE-UHFFFAOYSA-N delta-octanolide Chemical compound CCCC1CCCC(=O)O1 FYTRVXSHONWYNE-UHFFFAOYSA-N 0.000 description 1
- 230000002542 deteriorative effect Effects 0.000 description 1
- 239000010621 dill oil Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- ANJTVLIZGCUXLD-UHFFFAOYSA-N ent-cytisine Natural products C1NCC2CN3C(=O)C=CC=C3C1C2 ANJTVLIZGCUXLD-UHFFFAOYSA-N 0.000 description 1
- 239000001813 ethyl (2R)-2-methylbutanoate Substances 0.000 description 1
- 229940090910 ethyl 2-methylbutyrate Drugs 0.000 description 1
- 229940116333 ethyl lactate Drugs 0.000 description 1
- 229940093503 ethyl maltol Drugs 0.000 description 1
- LVGKNOAMLMIIKO-QXMHVHEDSA-N ethyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC LVGKNOAMLMIIKO-QXMHVHEDSA-N 0.000 description 1
- 229940093471 ethyl oleate Drugs 0.000 description 1
- 229940067592 ethyl palmitate Drugs 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- IFYYFLINQYPWGJ-VIFPVBQESA-N gamma-Decalactone Natural products CCCCCC[C@H]1CCC(=O)O1 IFYYFLINQYPWGJ-VIFPVBQESA-N 0.000 description 1
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 239000001087 glyceryl triacetate Substances 0.000 description 1
- 235000013773 glyceryl triacetate Nutrition 0.000 description 1
- 235000019674 grape juice Nutrition 0.000 description 1
- 238000007646 gravure printing Methods 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- UFLHIIWVXFIJGU-UHFFFAOYSA-N hex-3-en-1-ol Natural products CCC=CCCO UFLHIIWVXFIJGU-UHFFFAOYSA-N 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- GJRQTCIYDGXPES-UHFFFAOYSA-N iso-butyl acetate Natural products CC(C)COC(C)=O GJRQTCIYDGXPES-UHFFFAOYSA-N 0.000 description 1
- 229940117955 isoamyl acetate Drugs 0.000 description 1
- 229940094941 isoamyl butyrate Drugs 0.000 description 1
- FGKJLKRYENPLQH-UHFFFAOYSA-M isocaproate Chemical compound CC(C)CCC([O-])=O FGKJLKRYENPLQH-UHFFFAOYSA-M 0.000 description 1
- OQAGVSWESNCJJT-UHFFFAOYSA-N isovaleric acid methyl ester Natural products COC(=O)CC(C)C OQAGVSWESNCJJT-UHFFFAOYSA-N 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 239000002655 kraft paper Substances 0.000 description 1
- 239000010501 lemon oil Substances 0.000 description 1
- 239000001475 levisticum officinale koch root oil Substances 0.000 description 1
- 229940069445 licorice extract Drugs 0.000 description 1
- 229930007744 linalool Natural products 0.000 description 1
- 229940043353 maltol Drugs 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000001525 mentha piperita l. herb oil Substances 0.000 description 1
- 239000001683 mentha spicata herb oil Substances 0.000 description 1
- 229940041616 menthol Drugs 0.000 description 1
- 229930007503 menthone Natural products 0.000 description 1
- 229940102398 methyl anthranilate Drugs 0.000 description 1
- WBYWAXJHAXSJNI-UHFFFAOYSA-N methyl p-hydroxycinnamate Natural products OC(=O)C=CC1=CC=CC=C1 WBYWAXJHAXSJNI-UHFFFAOYSA-N 0.000 description 1
- 229960001047 methyl salicylate Drugs 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 239000001627 myristica fragrans houtt. fruit oil Substances 0.000 description 1
- 239000001186 myroxylon pereirae klotzsch oil Substances 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 description 1
- 239000005445 natural material Substances 0.000 description 1
- WASNIKZYIWZQIP-AWEZNQCLSA-N nerolidol Natural products CC(=CCCC(=CCC[C@@H](O)C=C)C)C WASNIKZYIWZQIP-AWEZNQCLSA-N 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- YYZUSRORWSJGET-UHFFFAOYSA-N octanoic acid ethyl ester Natural products CCCCCCCC(=O)OCC YYZUSRORWSJGET-UHFFFAOYSA-N 0.000 description 1
- 238000007645 offset printing Methods 0.000 description 1
- 239000010502 orange oil Substances 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- VWMVAQHMFFZQGD-UHFFFAOYSA-N p-Hydroxybenzyl acetone Natural products CC(=O)CC1=CC=C(O)C=C1 VWMVAQHMFFZQGD-UHFFFAOYSA-N 0.000 description 1
- ZRSNZINYAWTAHE-UHFFFAOYSA-N p-methoxybenzaldehyde Chemical compound COC1=CC=C(C=O)C=C1 ZRSNZINYAWTAHE-UHFFFAOYSA-N 0.000 description 1
- QNGNSVIICDLXHT-UHFFFAOYSA-N para-ethylbenzaldehyde Natural products CCC1=CC=C(C=O)C=C1 QNGNSVIICDLXHT-UHFFFAOYSA-N 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 235000019477 peppermint oil Nutrition 0.000 description 1
- WVDDGKGOMKODPV-ZQBYOMGUSA-N phenyl(114C)methanol Chemical compound O[14CH2]C1=CC=CC=C1 WVDDGKGOMKODPV-ZQBYOMGUSA-N 0.000 description 1
- 229940081310 piperonal Drugs 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 229940090181 propyl acetate Drugs 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 229940107700 pyruvic acid Drugs 0.000 description 1
- NJGBTKGETPDVIK-UHFFFAOYSA-N raspberry ketone Chemical compound CC(=O)CCC1=CC=C(O)C=C1 NJGBTKGETPDVIK-UHFFFAOYSA-N 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000010666 rose oil Substances 0.000 description 1
- 235000019719 rose oil Nutrition 0.000 description 1
- 235000013533 rum Nutrition 0.000 description 1
- 239000010670 sage oil Substances 0.000 description 1
- 239000010671 sandalwood oil Substances 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- VQTLGLGPQXZERV-UHFFFAOYSA-M sodium;4-hydroxyundecanoate Chemical compound [Na+].CCCCCCCC(O)CCC([O-])=O VQTLGLGPQXZERV-UHFFFAOYSA-M 0.000 description 1
- 239000011122 softwood Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- UNYNVICDCJHOPO-UHFFFAOYSA-N sotolone Chemical compound CC1OC(=O)C(O)=C1C UNYNVICDCJHOPO-UHFFFAOYSA-N 0.000 description 1
- 235000019721 spearmint oil Nutrition 0.000 description 1
- 239000010676 star anise oil Substances 0.000 description 1
- 239000006188 syrup Substances 0.000 description 1
- 235000020357 syrup Nutrition 0.000 description 1
- 239000010660 tarragon oil Substances 0.000 description 1
- PINIEAOMWQJGBW-FYZOBXCZSA-N tenofovir hydrate Chemical compound O.N1=CN=C2N(C[C@@H](C)OCP(O)(O)=O)C=NC2=C1N PINIEAOMWQJGBW-FYZOBXCZSA-N 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 239000010678 thyme oil Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 description 1
- BJIOGJUNALELMI-ONEGZZNKSA-N trans-isoeugenol Chemical compound COC1=CC(\C=C\C)=CC=C1O BJIOGJUNALELMI-ONEGZZNKSA-N 0.000 description 1
- 229960002622 triacetin Drugs 0.000 description 1
- 239000001069 triethyl citrate Substances 0.000 description 1
- VMYFZRTXGLUXMZ-UHFFFAOYSA-N triethyl citrate Natural products CCOC(=O)C(O)(C(=O)OCC)C(=O)OCC VMYFZRTXGLUXMZ-UHFFFAOYSA-N 0.000 description 1
- 235000013769 triethyl citrate Nutrition 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- OENHQHLEOONYIE-JLTXGRSLSA-N β-Carotene Chemical compound CC=1CCCC(C)(C)C=1\C=C\C(\C)=C\C=C\C(\C)=C\C=C\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C OENHQHLEOONYIE-JLTXGRSLSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/40—Constructional details, e.g. connection of cartridges and battery parts
- A24F40/46—Shape or structure of electric heating means
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/12—Chemical features of tobacco products or tobacco substitutes of reconstituted tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/02—Cigars; Cigarettes with special covers
- A24D1/025—Cigars; Cigarettes with special covers the covers having material applied to defined areas, e.g. bands for reducing the ignition propensity
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/042—Cigars; Cigarettes with mouthpieces or filter-tips with mouthpieces
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/04—Cigars; Cigarettes with mouthpieces or filter-tips
- A24D1/045—Cigars; Cigarettes with mouthpieces or filter-tips with smoke filter means
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/18—Selection of materials, other than tobacco, suitable for smoking
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/20—Cigarettes specially adapted for simulated smoking devices
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/50—Control or monitoring
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/03—Non-macromolecular organic compounds
- D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
- D21H17/14—Carboxylic acids; Derivatives thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/22—Proteins
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H5/00—Special paper or cardboard not otherwise provided for
- D21H5/12—Special paper or cardboard not otherwise provided for characterised by the use of special fibrous materials
- D21H5/14—Special paper or cardboard not otherwise provided for characterised by the use of special fibrous materials of cellulose fibres only
- D21H5/16—Tobacco or cigarette paper
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/20—Devices using solid inhalable precursors
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Paper (AREA)
Abstract
The present invention provides a roll paper for a non-combustion heating type smoking article, which has a portion to which a thermosensitive material is added on one surface of the outer peripheral surface of the non-combustion heating type smoking article, and a color difference delta E between the portion to which the thermosensitive material is added in the roll paper before heating and the portion to which the thermosensitive material is added after heating the roll paper at 200 ℃ for 5 minutes is 15 or more.
Description
Technical Field
The present invention relates to a roll paper for a non-combustion heating type smoking article, and an electric heating type smoking system.
Background
Non-combustion heated smoking articles of the type which deliver volatile components to a user by heating from the surroundings of a tobacco rod (tobacco rod) containing cut tobacco are known. In the case of a non-combustion heating type smoking article, although the tobacco rod wrapped with the roll paper is heated, unlike the conventional cigarette, the tobacco rod does not burn and remains after use (after heating).
In the conventional cigarettes, white (colorless) paper is generally used as a wrapping paper for wrapping cut tobacco, although a logo or the like is sometimes provided.
Disclosure of Invention
Problems to be solved by the invention
It is known that when a roll paper used for a conventional cigarette is used as a roll paper of a wrapped tobacco in a non-combustion heating type smoking article, a color change may occur which is uncomfortable for the user due to heating during use.
Accordingly, an object of the present invention is to provide a roll paper for non-combustion heating type smoking articles which does not cause discomfort relating to appearance due to heating.
Means for solving the problems
In order to solve the above problems, the present inventors focused on using roll paper having a portion having a color difference Δe that is equal to or greater than a predetermined value after heating, so that the discolouration that is uncomfortable was not noticeable.
When paper made of pulp as a main material is heated at a temperature equal to or higher than a predetermined temperature, the paper is burned and turns brown, and the physical change of the constituent components of the pulp and paper due to thermal decomposition is caused, so that such discoloration cannot be prevented simply. However, it was found that, in order not to recognize discoloration due to scorching as an uncomfortable color even if the discoloration occurs, a specific heat-sensitive material was previously added to roll paper so that a color difference of a certain or more occurs before and after heating, whereby the uncomfortable discoloration may become inconspicuous.
The present invention addresses the problem specific to non-combustion heating type smoking articles that are heated by an electric heating type device, and is not a problem that occurs in conventional smoking articles (cigarettes, etc.).
Namely, the present invention is as follows.
[1] A roll paper for a non-combustion heating type smoking article, which has a portion to which a thermosensitive material is added on one surface of the non-combustion heating type smoking article as an outer peripheral surface,
color difference deltae between a portion of the roll paper before heating to which the heat-sensitive material is added and a portion of the roll paper after heating at 200 ℃ for 5 minutes * 15 or more.
[2] The roll paper for non-combustion heating type smoking articles according to [1], wherein the thermosensitive material is 1 or more selected from the group consisting of organic acids or salts thereof, monosaccharides, disaccharides, polysaccharides and amino acids.
[3] The roll paper for non-combustion heating type smoking articles according to [2], wherein the organic acid or a salt thereof is at least 1 selected from acetic acid, potassium acetate, sodium acetate, citric acid, potassium citrate, sodium citrate, tartaric acid, potassium tartrate, sodium tartrate, phosphoric acid, sodium phosphate, potassium phosphate, malic acid, sodium malate, magnesium malate, lactic acid, and calcium lactate.
[4] The roll paper for non-combustion heating type smoking articles according to [2], wherein the monosaccharide is 1 or more selected from fructose, galactose and glucose, the disaccharide is 1 or more selected from maltose, lactose and sucrose, the polysaccharide is 1 or more selected from carboxymethyl cellulose, carrageenan, pectin and starch, and the amino acid is 1 or more selected from valine, leucine, isoleucine, glutamine, alanine, asparagine and arginine.
[5] The roll paper for non-combustion heating type smoking articles according to any one of [1] to [4], wherein the heat sensitive material is colorless.
[6]According to [1]]～[5]A roll paper for non-combustion heating type smoking articles according to any one of the preceding claims, wherein the content of the heat sensitive material in the portion to which the heat sensitive material is added in the roll paper is 0.007mg/cm 2 The above.
[7] The roll paper for non-combustion heating type smoking articles according to any one of [1] to [6], wherein the portion to which the thermosensitive material is added includes a portion heated to 150 to 250 ℃.
[8] The roll paper for non-combustion heating type smoking articles according to any one of [1] to [7], wherein the proportion of the area of the portion to which the heat sensitive material is added to the total area of the roll paper is 1 to 50%.
[9] A non-combustion heated smoking article, comprising: a tobacco rod portion formed by wrapping a filler containing tobacco shreds and an aerosol-generating substrate with a first roll paper around which the filler is wrapped; and a mouthpiece portion constituting an end portion on an opposite side of the tobacco rod portion, wherein the tobacco rod portion and the mouthpiece portion are connected together using a second roll paper which is the same as or different from the roll paper on which the filler is wound, and at least one of the first roll paper and the second roll paper is the roll paper described in any one of [1] to [8 ].
[10] An electrically heated smoking system comprising an electrically heated device and the non-combustion heated smoking article of [9], wherein the electrically heated device comprises a heater member, a heat transfer member for transferring heat from the heater member, a battery unit as a power source for the heater member, and a control unit for controlling the heater member, and the non-combustion heated smoking article of [9] is fitted in contact with the heat transfer member.
ADVANTAGEOUS EFFECTS OF INVENTION
According to the present invention, it is possible to provide a roll paper for non-combustion heating type smoking articles which does not cause discomfort relating to appearance which occurs due to heating.
Drawings
Fig. 1 is a schematic diagram showing one embodiment of a non-combustion heating type smoking article.
Fig. 2 is a schematic diagram illustrating one embodiment of an electrically heated smoking system.
Symbol description
10. Non-combustion heated smoking article
11. Filling material
12. First roll paper
13. Second roll paper (tipping paper)
14. Paper tube part
15. Filter part
16. Smoke mouth
20. Electric heating device
21. Battery cell
22. Control unit
23. Main body
24. Heater
25. Heat transfer member
30. Electrical heating type smoking system
Detailed Description
The present invention will be described in detail with reference to the following embodiments and examples, but the present invention is not limited to the following embodiments and examples, and may be implemented with any modification within the scope of the present invention.
< paper roll for non-combustion heating type smoking article >
In the present specification, the term "paper for non-combustion heating type smoking article" refers to paper for non-combustion heating type smoking articles described later. Hereinafter, the roll paper according to the embodiment of the present invention will also be simply referred to as "roll paper". As for the use of the roll paper according to the embodiment of the present invention, "for a non-combustion heating type smoking article" may be mentioned: a roll paper for a tobacco rod, which is used for producing a tobacco rod by wrapping a filler containing tobacco shreds; in order to connect members adjacent to the tobacco rod (for example, members constituting the mouthpiece) are used as tipping paper (tip paper) for wrapping the outer peripheral surfaces of the members.
The roll paper according to the embodiment of the present invention is a roll paper for a non-combustion heating type smoking article having a portion to which a thermosensitive material is added on one surface of the outer peripheral surface of the non-combustion heating type smoking article,
color difference DeltaE of a portion of the roll paper before heating to which the thermosensitive material is added and a portion of the roll paper after heating at 200 ℃ for 5 minutes * 15 or more. By generating such a color difference before and after heating, the uncomfortable color change that is generated in the non-combustion heating type smoking article in normal use can be made less noticeable.
In the roll paper according to the embodiment of the present invention, the portion to which the thermosensitive material is added is one surface of the non-combustion heating type smoking article as the outer peripheral surface. In other words, for example, when the roll paper according to the embodiment of the present invention is used as a roll paper for a tobacco rod, a heat-sensitive material is added to a surface which is not in contact with a tobacco filler described later. In addition, in the case where the roll paper according to the embodiment of the present invention is used as the tipping paper, a heat-sensitive material is added to a surface that is not in contact with a member (for example, a member of the mouthpiece portion) adjacent to the tobacco rod.
The portion to which the thermosensitive material is added may be present on the entire surface of the roll paper according to the embodiment of the present invention, or may be present at least in a portion to be heated (heating by an electric heating type device described later).
The proportion of the area of the portion to which the thermosensitive material is added to the total area of the roll paper is 1 to 50%. The proportion of the area of the portion to which the heat-sensitive material is added to the total area of the roll paper may be about 1 to 10% or about 1 to 5% in the case where the portion to which the heat-sensitive material is added is a portion such as a logo or a letter. In addition, in the mode in which the thermosensitive material is added to most of the portions of the roll paper that are heated, the thermosensitive material may be added to 40 to 50% of the area of the roll paper.
Examples of the thermosensitive material to be added to the roll paper according to the embodiment of the present invention include 1 or more selected from the group consisting of organic acids or salts thereof, monosaccharides, disaccharides, polysaccharides, and amino acids. In the case of using a plurality of combinations, examples thereof include: combinations of an organic acid or a salt thereof and at least 1 sugar selected from the group consisting of monosaccharides, disaccharides and polysaccharides (including combinations of an organic acid or a salt thereof and monosaccharides, combinations of an organic acid or a salt thereof and disaccharides, combinations of an organic acid or a salt thereof and polysaccharides), combinations of monosaccharides and amino acids, combinations of monosaccharides and polysaccharides, and the like. The following modes can be mentioned: these heat-sensitive materials are suitably dissolved in, for example, water to prepare an aqueous solution of the heat-sensitive materials, which is added to roll paper.
The concentration of the thermosensitive material in the preparation of the aqueous solution is not particularly limited, and examples thereof include 0.1 to 50% by weight, preferably 0.2 to 40% by weight.
The organic acid or a salt thereof includes at least 1 selected from acetic acid, potassium acetate, sodium acetate, citric acid, potassium citrate, sodium citrate, tartaric acid, potassium tartrate, sodium tartrate, phosphoric acid, sodium phosphate, potassium phosphate, malic acid, sodium malate, magnesium malate, lactic acid, and calcium lactate. It is considered that by using these organic acids or salts thereof, the amount of heat required for the oxidation reaction of the pulp of the roll base paper is reduced, and color development occurs.
The monosaccharide is preferably 1 or more selected from fructose, galactose and glucose. The disaccharide is preferably 1 or more selected from maltose, lactose and sucrose.
The polysaccharide is preferably at least 1 selected from carboxymethyl cellulose, carrageenan, pectin, and starch.
It is considered that when the above monosaccharides, disaccharides, and polysaccharides are used, color development due to caramelization reaction occurs.
The amino acid is preferably at least 1 selected from valine, leucine, isoleucine, glutamine, alanine, asparagine and arginine. It is considered that these amino acids develop color due to maillard reaction with carbonyl groups contained in pulp of roll paper base paper.
The aqueous solution of the thermosensitive material was transparent in appearance. In addition, when these heat-sensitive materials are added to the roll paper base paper, the color of the roll paper does not change. That is, the heat sensitive material is transparent in appearance before heating. Thus, the color that does not appear on the base paper of the roll paper before the use of the non-combustion heating type smoking article can be developed on the roll paper by heating at the time of use, and the color change of the base paper of the roll paper that is not caused by the development of the color of the heat-sensitive material can be made inconspicuous.
The content of the thermosensitive material in the roll paper according to the embodiment of the present invention may be 0.007mg/cm, based on the content of the portion to which the thermosensitive material is added 2 The above is preferably 0.07mg/cm 2 The above. On the other hand, as the upper limit value of the content of the thermosensitive material, for example, 7mg/cm may be mentioned in terms of the content of the portion to which the thermosensitive material is added 2 In the following, another example is 6mg/cm 2 In the following, another example is 5mg/cm 2 The following is given. By being in such a content range, it is possible to contribute to ΔE of the portion to which the thermosensitive material is added before and after heating * The value is 15 or more.
In the roll paper according to the embodiment of the present invention, Δe before and after heating is applied to the portion to which the thermosensitive material is applied * As the value of (2), 5 points in which a thermosensitive material was added to paper as a sample were measured, and the arithmetic average value was used. As a measurementThe object of (2) is to add an arbitrary portion of the paper to which the heat sensitive material is added, but when characters or patterns such as logos are present on the paper, the portion where such characters or logos are not present is the object. ΔE * The value may be determined by using a spectrophotometer.
Specifically, a spectrophotometer (manufactured by X-Rite corporation, trade name SpectroEye) was used. The measurement was performed by placing 1 sample on a paper having 92% ISO brightness under the conditions of light source D65, no light source filter, and a view angle of 2 °, and pressing a spectrophotometer thereon.
The method of adding the aqueous solution in which the thermosensitive material is dissolved to the roll paper base paper is not particularly limited, and examples thereof include coating, printing, and the like. The method of coating is not particularly limited. In the case of adding a heat-sensitive material to a roll paper base paper by printing, the above-described characteristics can be easily added to the roll paper.
The printing method is not particularly limited, and examples thereof include gravure printing and offset printing.
Printing may be exemplified by: the printing method is a method of printing on the entire surface of paper as a base paper, or at least a portion of the surface of the base paper heated by an electric heating device described later.
On the surface of the roll paper, it is preferable that at least a heated portion (a portion subjected to heating by an electric heating type device) has a color difference Δe before and after heating * 15 or more. In the surface of the roll paper, by providing the portion heated by an electric heating type device described later with the above-described characteristics, it is possible to prevent the impression of the heated appearance from deteriorating.
The shape of the roll paper for non-combustible smoking articles may be square or rectangular. In the case of using the paper as a roll for wrapping tobacco (for making a tobacco rod), the length of one side is about 19 to 70mm, the length of the other side is 15 to 26.5mm, and the preferable length of the other side is 24mm.
When a cigarette rod is wound by connecting the rod to another member adjacent to the rod like tipping paper, the length of one side is 20 to 60mm, and the length of the other side is 15 to 26.5mm.
The basis weight of the roll base paper according to the embodiment of the present invention is, for example, generally 20g/m 2 The above is preferably 35g/m 2 The above is more preferably 40g/m 2 The above. On the other hand, the weight per unit area is usually 65g/m 2 Hereinafter, it is preferably 50g/m 2 The following is given.
The thickness of the roll paper according to the embodiment of the present invention is not particularly limited, but is usually 10 μm or more, preferably 20 μm or more, more preferably 30 μm or more, and is usually 100 μm or less, preferably 75 μm or less, more preferably 50 μm or less, from the viewpoints of rigidity, air permeability, and ease of adjustment in paper making.
As a roll paper base paper according to an embodiment of the present invention, a paper having pulp as a main component is exemplified. The pulp may be a paper produced by mixing non-wood pulp, which is usually used for roll paper for smoking articles, such as flax pulp, hemp pulp, sisal pulp, spanish grass (esparto), and the like, in addition to pulp such as softwood pulp and hardwood pulp.
As the kind of pulp, chemical pulp, groundwood pulp, chemical groundwood pulp, thermomechanical pulp, and the like obtained by a sulfate cooking method (kraft cooking), an acidic/neutral/alkaline sulfite cooking method, a soda cooking method, and the like can be used.
As the pulp, for example, pulp composed of a mixed pulp of bleached pulp and unbleached pulp can be used.
In the case of using the mixed pulp, spruce as a conifer and aspen as a broadleaf tree were prepared as bleached pulp, and pine was prepared as unbleached pulp. The bleached pulp and unbleached pulp in the desired proportions are fed into a pulper to disintegrate the pulp. The dissociated pulp is then transferred to a refiner where it is beaten. Separately, calcium carbonate as a filler and a coagulant as a production aid were prepared and mixed with pulped pulp. The bleached pulp and the unbleached pulp may be separately disintegrated by using a plurality of pulpers, and pulped by using a refiner, and the bleached pulp, the unbleached pulp, the filler, and the manufacturing auxiliary agent, which are pulped, may be mixed in a mixing box.
Next, the mixed pulp is used to manufacture roll paper by adjusting the quality and uniformity in a paper making process using a fourdrinier, cylinder machine, cylinder short wire composite machine, or the like. The wet reinforcing agent may be added to impart water resistance to the roll paper and the sizing agent may be added to adjust the printing state of the roll paper, if necessary. Further, additives for papermaking such as aluminum sulfate, various anionic, cationic, nonionic or amphoteric yield improvers, drainage improvers, paper strength improvers and the like for papermaking and additives for papermaking such as dyes, pH adjusters, antifoaming agents, pitch control agents and residue control agents may be added.
When the bleached pulp and the unbleached pulp are used in combination, the ratio of the unbleached pulp in the roll paper is, for example, preferably 1% by weight or more and 90% by weight or less, more preferably 5% by weight or more and less than 86% by weight, and still more preferably 5% by weight or more and 60% by weight or less.
In addition to the above pulp, a filler may be contained in the roll base paper of the embodiment of the present invention. The content of the filler may be 30% by weight or more and less than 60% by weight relative to the total weight of the roll paper according to the embodiment of the present invention.
As the filler, calcium carbonate, titanium dioxide, kaolin, etc. can be used, and from the viewpoint of smoke smell, etc., calcium carbonate is preferably used.
Papers containing such fillers typically exhibit a bright color of the white series. On the other hand, roll paper made of mixed pulp generally has a color imparted by unbleached pulp.
As the roll paper base paper of the embodiment of the present invention, reconstituted tobacco (sheet tobacco) composed of reconstituted tobacco may be used.
As the reconstituted tobacco, there can be mentioned a papermaking reconstituted tobacco obtained by a papermaking method, and a slurry reconstituted tobacco obtained by drying a slurry.
Typical manufacturing methods for papermaking reconstituted tobacco may include: extracting natural tobacco materials (tobacco leaf, tobacco shred, vein, stem, root, etc.) with an extraction solvent such as water; a step of separating the extract and the residue obtained by the extraction operation; a step of making paper from the residue to produce a regenerated tobacco web; and pouring the extract subjected to the classification treatment as needed back to the regeneration net. Such a production method is described in, for example, international publication No. 2004/006001 as a wet papermaking method.
The slurry reconstituted tobacco can be produced by the method described in Japanese patent application laid-open No. 11-266851, for example. The raw stock slurry comprises wood pulp, tobacco powder and a binder which are mixed and defibrated in water. The raw stock slurry is extruded from a slurry feeder between a conveyor belt and a roller, and stretched into a sheet shape on the conveyor belt. Then, the sheet-like raw material slurry on the conveyor belt is conveyed to a drying furnace, and dried while passing through the drying furnace, thereby forming reconstituted tobacco.
When reconstituted tobacco is used as the base roll paper according to the embodiment of the invention, the basis weight thereof is 30 to 80g/m 2 The air permeability may be in the range of 0 to 60CU (CORESTA unit, cigarette paper air permeability unit).
As another method for producing reconstituted tobacco, there is a dry papermaking method described in japanese unexamined patent publication No. 61-52269, for example, in which reconstituted tobacco obtained by the former dry papermaking method is composed of wood pulp fibers, a binder and a stem portion of tobacco.
The roll paper according to the embodiment of the present invention may or may not contain a combustion improver contained in conventional roll paper for tobacco rods. The roll paper according to the embodiment of the present invention may be used as a first roll paper for use in a non-combustion heating type smoking article described later, or may be used as a second roll paper.
< non-combustion heating type smoking article >
As a non-combustion heating type smoking article according to an embodiment of the present invention, for example, an article having the structure of fig. 1 is cited.
The non-combustion heating type smoking article 10 of fig. 1 includes a filler 11, a tobacco rod portion formed by winding a first roll paper 12 of the filler 11, and a mouthpiece portion 16 constituting an end portion on the opposite side of the tobacco rod portion, and the tobacco rod portion and the mouthpiece portion are connected together by using a second roll paper 13 (tipping paper in fig. 1) which is the same as or different from the roll paper of the filler.
At least one of the first roll paper and the second roll paper is the roll paper according to the embodiment of the present invention described above. Preferably, at least the first roll paper is the roll paper of the embodiment of the present invention. In addition, it is also preferable that both the first roll paper 12 and the second roll paper are roll papers according to the embodiment of the present invention described above.
In the embodiment shown in fig. 1, the mouthpiece section 16 includes a paper tube section 14 and a filter section 15. Further, as the second roll paper for connecting them, a tipping paper 13 is provided. In fig. 1, the mouthpiece 16 is formed of 2 segments, and the mouthpiece 16 may be formed of a single segment or 3 or more segments. The segment constituting the mouthpiece portion may be constituted to include both the paper tube portion and the filter portion, or may be constituted only by one of them.
The vapor containing the aerosol-generating substrate and the tobacco flavor component generated by heating the tobacco rod is cooled by contact with the air in the paper tube as it passes through the paper tube portion 14, and is liquefied to generate an aerosol.
The non-combustion heating type smoking article 10 may have micropores (not shown) for allowing air from the outside to enter in a part of the paper tube portion 14 and the second roll paper 13 (tipping paper) surrounding the paper tube portion 14. By the presence of such micropores, air flows into the paper tube portion 14 from the outside during use, and the vapor containing the aerosol-generating substrate and the tobacco flavor component generated by heating the tobacco rod contacts with the air from the outside, thereby reducing the temperature, and liquefying the vapor to generate aerosol more reliably.
The paper tube portion 14 is, for example, a paper tube portion formed by processing thick paper into a cylindrical shape.
The filter portion 15 may be, for example, a filter portion using acetate tow as a material. The single filament fineness and the total fineness of the acetate tow are not particularly limited.
In fig. 1, the filter portion 15 is constituted by a single segment, but may be constituted by a plurality of segments. In the case of a plurality of segments, for example, a hollow segment is arranged on the upstream side, and the cross section of the mouthpiece is filled with acetate tow as a segment on the downstream side (the mouthpiece end side of the user). According to this aspect, unnecessary loss of the generated aerosol can be prevented, and the appearance of the non-combustion heating type smoking article can be improved.
In the manufacture of the filter, the air permeation resistance can be adjusted and additives (known adsorbents, flavors, flavor-retaining materials, etc.) can be added.
The material of the second roll paper 13 (tipping paper) is not particularly limited, and a roll paper of an embodiment of the present invention may be used in part or all. Examples of the second roll paper 13 include: after the wrapping, the tobacco rod, paper tube portion 14 and filter portion 15 are fixed around them with a vinyl acetate based adhesive.
The tobacco rod includes cut tobacco as the filler 11, and the material of the cut tobacco is not particularly limited, and known materials such as lamina and vein can be used. In the case of a tobacco rod having a circumferential length of 22mm and a length of 20mm, the content range of filler in the tobacco rod is 200 to 400 mg/tobacco rod, preferably 250 to 320 mg/tobacco rod. The moisture content of the filler is 10 to 15% by weight, preferably 11 to 13% by weight. When the moisture content is such, the occurrence of package stains can be suppressed, and the rolling suitability in the manufacture of tobacco rods can be improved.
The size of the tobacco shred used as the filler and the preparation method thereof are not particularly limited. For example, cut tobacco having a width of 0.8 to 1.2mm may be used.
In addition, the following cut filler may be used: the dried tobacco leaves are crushed and homogenized to have an average particle diameter of about 20 to 200 mu m, and the tobacco leaves are subjected to sheet processing and cut into cut tobacco with a width of 0.8 to 1.2 mm.
Further, tobacco shreds obtained by performing a pleat (gather) process without cutting the processed product obtained by processing the sheet may be used as the filler.
The filler comprises an aerosol-generating substrate that generates an aerosol mist. The type of the aerosol-generating substrate is not particularly limited, and extracts derived from various natural substances and/or constituent components thereof may be selected according to the application. As the aerosol-generating substrate, there may be mentioned: glycerol, propylene glycol, triacetin, 1, 3-butanediol, and mixtures thereof.
The content of the aerosol-generating substrate in the filler is not particularly limited, but is usually 5% by weight or more, preferably 10% by weight or more, and is usually 50% by weight or less, preferably 20% by weight or less, from the viewpoint of sufficiently generating an aerosol and imparting a good smoke taste.
The filling may comprise a fragrance. The type of the flavor is not particularly limited, and from the viewpoint of imparting a good smoke flavor, examples thereof include: acetoanisole, acetophenone, acetylpyrazine, 2-acetylthiazole, alfalfa extract, amyl alcohol, amyl butyrate, trans-anethole, star anise oil, apple juice, peru balsam oil, beeswax absolute, benzaldehyde, benzoin extract, benzyl alcohol, benzyl benzoate, benzyl propionate, 2, 3-butanedione, 2-butanol, butyl butyrate, butyric acid, caramel, cardamom oil, carob absolute (Carob absolute), beta-carotene, carrot juice, L-carvone, beta-caryophyllene, cinnamon bark oil, cedar oil, celery seed oil, chamomile oil, cinnamaldehyde, cinnamic acid, cinnamyl alcohol, cinnamyl cinnamate, citronella oil, DL-citronellol, south European extract, cocoa coffee, kang Naike oil, coriander oil, cumyl aldehyde, tarragon oil, delta-decalactone, gamma-decalactone, capric acid, dill oil, 3, 4-dimethyl-1, 2-cyclopentanedione, 4, 5-dimethyl-3-hydroxy-2, 5-dihydrofuran-2-one, 3, 7-dimethyl-6-octenoic acid, 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, 2, 6-dimethylpyrazine, ethyl 2-methylbutyrate, ethyl acetate, ethyl butyrate, ethyl caproate, ethyl isovalerate, ethyl lactate, ethyl laurate, ethyl levulinate, ethyl maltol, ethyl caprylate, ethyl oleate, ethyl palmitate, ethyl phenylacetate, ethyl propionate, ethyl stearate, ethyl valerate, ethyl vanillin glucoside, 2-ethyl-3, (5 or 6) -dimethylpyrazine, 5-ethyl-3-hydroxy-4-methyl-2 (5H) -furanone, 2-ethyl-3-methyl pyrazine, eucalyptol, trigonella absolute, cytisine absolute (Genet extract), gentian infusion, geraniol, geranyl acetate, grape juice, guava extract, gamma-heptanolide, gamma-caprolactone, caproic acid, cis-3-hexen-1-ol, hexyl acetate, hexanol, hexyl phenylacetate, honey, 4-hydroxy-3-pentenoic acid lactone, 4-hydroxy-4- (3-hydroxy-1-butenyl) -3, 5-trimethyl-2-cyclohexen-1-one, 4- (p-hydroxyphenyl) -2-butanone, sodium 4-hydroxyundecanoate, cermetin absolute, beta-ionone isoamyl acetate, isoamyl butyrate, isoamyl phenylacetate, isobutyl acetate, isobutyl phenylacetate, jasmin absolute, ke Laguo extract, lablab oil, terpeneless lemon oil, licorice extract, linalool, linaloyl acetate, linaloe root oil (Lovage root oil), maltol, maple syrup, menthol, menthone, L-menthyl acetate, p-methoxybenzaldehyde, methyl-2-pyrrolidone, methyl anthranilate, methyl phenylacetate, methyl salicylate, 4' -methylacetophenone, methylcyclopentenolone, 3-methylpentanoic acid, mimosa absolute, molasses, myristic acid, nerol, nerolidol, gamma-nonenolactone, nutmeg oil, delta-octanolide, octanol, octanoic acid, neroli oil, orange oil, iris root oil, palmitic acid, omega-pentadecanolide, peppermint oil, yerba mate orange leaf essential oil, phenethyl alcohol, phenethyl phenylacetate, phenylacetic acid, piperonal, plum extract, propenyl guaiacol, propyl acetate, 3-propylindene phthalide, prune juice, pyruvic acid, raisin extract, rose oil, rum, sage oil, sandalwood oil, spearmint oil, storax absolute, calendula oil, tea distillate, alpha-terpineol, terpineol acetate, 5,6,7, 8-tetrahydroquinoxaline, 1,5,5,9-tetramethyl-13-oxacyclo (8.3.0.0 (4.9)) tridecane, 2,3,5, 6-tetramethylpyrazine, thyme oil, tomato extract, 2-tridecanone, triethyl citrate, 4- (2, 6-trimethyl-1-cyclohexenyl) 2-4-one, 2, 6-trimethyl-1-cyclohexenyl) 2-4-one, 6-dimethyl-1-cyclohexanolide, 3, 6-trimethyl-1-cyclohexanolide, 2-methyl-3, 6-cyclohexanolide, 3-methyl-menthone, and especially 2, 6-methyl-cyclohexanolide. In addition, 1 kind of these perfumes may be used alone, or 2 or more kinds may be used in combination.
The content of the perfume in the filler is not particularly limited, but is usually 10000ppm or more, preferably 20000ppm or more, more preferably 25000ppm or more, and is usually 50000ppm or less, preferably 40000ppm or less, more preferably 33000ppm or less, from the viewpoint of imparting a good smoke taste.
The filling density of the filler is not particularly limited, but is usually 250mg/cm from the viewpoint of securing the performance of the non-combustion heating type smoking article and imparting a good smoke flavor 3 The above is preferably 320mg/cm 3 The above, in addition, is usually 520mg/cm 3 Hereinafter, it is preferably 420mg/cm 3 The following is given.
In the production of the non-combustion heating type smoking article according to the embodiment of the present invention, the roll paper according to the embodiment of the present invention described above may be used. Specifically, a filler including cut tobacco and an aerosol-generating substrate is molded, and then the molded filler is wrapped with the roll paper according to the embodiment of the present invention, whereby a tobacco rod can be obtained. Further, by wrapping the tobacco rod and the member constituting the mouthpiece portion with tipping paper (or roll paper according to the embodiment of the present invention), a non-combustion heating type smoking article can be obtained. In the winding, a known winding device may be used.
By using the roll paper according to the embodiment of the present invention as the roll paper and/or tipping paper of the tobacco rod at the time of manufacturing the non-combustion heating type smoking article, it is possible to provide a non-combustion heating type smoking article which does not impair the appearance impression after use (after heating).
< electrically heated smoking System >
One embodiment of an electrically heated smoking system is shown in figure 2. The electrically heated smoking system 30 is used by being fitted so that the non-combustion heated smoking article 10 described above is in contact with the heat transfer member 25, and the heat transfer member 25 is disposed inside the electrically heated device 20 and in contact with the heater 24.
The electric heating device 20 includes a battery unit 21 and a control unit 22 in a resin main body 23, for example.
As described above, the non-combustion heating type smoking article includes the filler 11, the tobacco rod portion formed of the first roll paper 12 on which the filler 11 is wrapped, and the mouthpiece portion 16 forming the end portion on the opposite side to the tobacco rod portion, and the tobacco rod portion and the mouthpiece portion are connected together using the second roll paper that is the same as or different from the roll paper on which the filler is wrapped. When the non-combustion heating type smoking article is fitted into the electric heating type device, the outer peripheral surface of the rod and a part of the outer peripheral surface formed by the second roll paper (tipping paper 13) connecting the rod and the paper tube portion 14 are in contact with the heat transfer member 25 inside the electric heating type device 20.
The heater 24 inside the electric heating type device 20 generates heat by control by the control unit 22. This heat is transferred to the rod of the non-combustion heating type smoking article via the heat transfer member 25, whereby the aerosol-generating substrate and the flavor component contained in the filler 11 of the rod are volatilized together.
The tobacco rod is heated to about 150 to 250 c by heating with the heater 24.
The above ΔE will be measured * The heating temperature of the roll paper at this time was set to 200 ℃ and the time was set to 5 minutes, which was set on the premise of using the electrically heated smoking system according to the embodiment of the present invention.
The vapor containing the aerosol-generating substrate and the flavor component generated by the heating generates an aerosol in the paper tube portion 14 by the mechanism described above, and passes through the filter portion 15 of the non-combustion type smoking article 10 to reach the mouth of the user.
Examples
The present invention will be described more specifically with reference to examples, but the present invention is not limited to the following examples without departing from the spirit thereof.
< preparation of paper sample >
A commercially available roll paper for tobacco rods was cut into 5cm by 5cm pieces.
As the heat-sensitive material, the substances shown in table 1 below were selected, and aqueous solutions of the respective substances were prepared at the concentrations shown in table 1. Each aqueous solution was applied to the cut roll paper with a width of 3cm using a brush pen.
As a control, a roll paper was used, which was not coated with any substance on the cut roll paper. In the commercially available roll paper for tobacco rods, citric acid (shown in table 1 as a coating amount, but not coated) was contained as a combustion improver in an amount of about 1.2% by weight based on the total amount of the roll paper.
Further, a commercially available roll paper for self-extinguishing tobacco rods (a self-extinguishing agent is coated on a surface in contact with tobacco shreds) was prepared as comparative example 1.
For each sample, the sample was placed on a household aluminum foil (material: aluminum foil thickness: 11 μm), and heated at 200℃for 5 minutes in a muffle furnace (product name: model Muffle Furnace FO, manufactured by Yamato Scientific).
< measurement of color difference >
For each sample before and after heating, ΔE was measured using a spectrophotometer (manufactured by X-Rite corporation, trade name SpectroEye) * . The measurement was performed by placing 1 sample on a paper having 92% ISO brightness under the conditions of light source D65, no light source filter, and a view angle of 2 °, and pressing a spectrophotometer thereon.
For the portion coated with the thermosensitive material, measurement was repeated at 5 sites, and the average value was used for analysis.
The results of the color difference measurement are shown in table 1.
TABLE 1
From the results of Table 1, it was found that the sample obtained by applying the aqueous solution containing the substances shown in Table 1 as the heat-sensitive material to the roll paper had a color difference ΔE before and after heating at 200℃for 5 minutes * At least 15, in contrast to the color difference ΔE of control, comparative example 1 * Less than 15. In addition, for the color difference delta E * For samples of 15 or moreIn other words, the difference ΔE between before and after heating is used * The discoloration was observed to a degree of 15 or more, but the test piece was not perceived as an uncomfortable color even after heating by the panelist.
On the other hand, for the color difference ΔE * As a result of observation by the panelists of the control and comparative example 1, which was smaller than 15, the appearance after heating gave a slightly unpleasant impression as compared with that before heating.
Claims (9)
1. A roll paper for non-combustion heating type smoking articles, which is less likely to cause uncomfortable discoloration due to heating,
the roll paper has a portion to which a heat-sensitive material is added on one surface of a non-combustion heating type smoking article as an outer peripheral surface,
color difference deltae between a portion of the roll paper before heating to which the heat-sensitive material is added and a portion of the roll paper after heating at 200 ℃ for 5 minutes * Is more than or equal to 15 percent,
the ratio of the area of the portion to which the thermosensitive material is added to the total area of the roll paper is 40 to 50%,
the portion to which the thermosensitive material is added is present at least in a portion heated by an electric heating type device.
2. The roll paper for non-combustion heating type smoking articles according to claim 1, wherein the thermosensitive material is 1 or more selected from the group consisting of organic acids or salts thereof, monosaccharides, disaccharides, polysaccharides, and amino acids.
3. The roll paper for non-combustion heating type smoking articles according to claim 2, wherein the organic acid or a salt thereof is 1 or more selected from acetic acid, potassium acetate, sodium acetate, citric acid, potassium citrate, sodium citrate, tartaric acid, potassium tartrate, sodium tartrate, phosphoric acid, sodium phosphate, potassium phosphate, malic acid, sodium malate, magnesium malate, lactic acid, and calcium lactate.
4. The roll paper for non-combustion heating type smoking articles according to claim 2, wherein the monosaccharide is 1 or more selected from fructose, galactose and glucose, the disaccharide is 1 or more selected from maltose, lactose and sucrose, the polysaccharide is 1 or more selected from carboxymethyl cellulose, carrageenan, pectin and starch, and the amino acid is 1 or more selected from valine, leucine, isoleucine, glutamine, alanine, asparagine and arginine.
5. The roll paper for non-combustion heating type smoking articles according to any one of claims 1 to 4, wherein the heat sensitive material is colorless.
6. The roll paper for non-combustion heating type smoking articles according to any one of claims 1 to 4, wherein the content of the thermosensitive material in the portion to which the thermosensitive material is added in the roll paper is 0.007mg/cm 2 The above.
7. The roll paper for non-combustion heating type smoking articles according to any one of claims 1 to 4, wherein the portion to which the thermosensitive material is added includes a portion heated to 150 to 250 ℃.
8. A non-combustion heated smoking article, comprising:
a tobacco rod portion formed by wrapping a filler containing tobacco shreds and an aerosol-generating substrate with a first roll paper around which the filler is wrapped; and
a mouthpiece portion constituting an end portion on the opposite side of the tobacco rod portion,
the tobacco rod portion and the mouthpiece portion are connected together using a second roll paper that is the same as or different from the roll paper that is wrapped around the filler,
at least one of the first roll paper and the second roll paper is the roll paper according to any one of claims 1 to 7.
9. An electrically heated smoking system comprising an electrically heated device and the non-combustion heated smoking article of claim 8, the electrically heated device comprising a heater member, a heat transfer member for transferring heat from the heater member, a battery unit as a power source for the heater member, and a control unit for controlling the heater member, wherein the non-combustion heated smoking article of claim 8 is fitted in contact with the heat transfer member.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/JP2018/017407 WO2019211890A1 (en) | 2018-05-01 | 2018-05-01 | Rolling paper for non-combustion-heating-type smoking product, non-combustion-heating-type smoking product, and electric-heating-type smoking system |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN112055546A CN112055546A (en) | 2020-12-08 |
| CN112055546B true CN112055546B (en) | 2024-04-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201880093033.1A Active CN112055546B (en) | 2018-05-01 | 2018-05-01 | Roll paper for non-combustion heating type smoking article, and electric heating type smoking system |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20210045433A1 (en) |
| EP (1) | EP3777579A4 (en) |
| JP (2) | JP7053810B2 (en) |
| KR (1) | KR102562462B1 (en) |
| CN (1) | CN112055546B (en) |
| WO (1) | WO2019211890A1 (en) |
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| CN110680019B (en) * | 2019-11-26 | 2024-04-09 | 上海龙殷生物科技有限公司 | Cigarette bullet for heating non-burning cigarettes |
| KR102431771B1 (en) * | 2020-05-11 | 2022-08-11 | 주식회사 케이티앤지 | Wrapper for non-combustible cigarette and method for manufacturing same |
| EP4208050A1 (en) * | 2020-09-02 | 2023-07-12 | JT International S.A. | Heat-not-burn aerosol-generating article comprising non-combustible filler material |
| CN113152145B (en) * | 2021-04-14 | 2022-04-01 | 浙江大学 | Preparation method of heating non-combustion cigarette paper containing boron nitride heat-conducting filler |
| CN113796569A (en) * | 2021-09-24 | 2021-12-17 | 河南中烟工业有限责任公司 | Incompletely separated cigarette for paperless heating |
| JP7563671B2 (en) | 2021-11-18 | 2024-10-08 | ケーティー アンド ジー コーポレイション | WALLPAPER COMPOSITION AND WALLPAPER RELEASING FLAVORANT COMPONENT BY HEAT |
| CN114854493A (en) * | 2022-05-25 | 2022-08-05 | 深圳波顿香料有限公司 | Preparation method of Maillard reaction product by using raisin extract |
| CN115413811B (en) * | 2022-09-23 | 2023-11-14 | 南通烟滤嘴有限责任公司 | Preparation method and application of burnt sweet tea flavored heating cigarette |
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Also Published As
| Publication number | Publication date |
|---|---|
| CN112055546A (en) | 2020-12-08 |
| JP7053810B2 (en) | 2022-04-12 |
| KR20200139206A (en) | 2020-12-11 |
| US20210045433A1 (en) | 2021-02-18 |
| WO2019211890A1 (en) | 2019-11-07 |
| JP2022050552A (en) | 2022-03-30 |
| EP3777579A1 (en) | 2021-02-17 |
| EP3777579A4 (en) | 2021-11-24 |
| KR102562462B1 (en) | 2023-08-02 |
| JPWO2019211890A1 (en) | 2021-01-07 |
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