CN112051112A - Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower - Google Patents

Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower Download PDF

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Publication number
CN112051112A
CN112051112A CN202011057816.XA CN202011057816A CN112051112A CN 112051112 A CN112051112 A CN 112051112A CN 202011057816 A CN202011057816 A CN 202011057816A CN 112051112 A CN112051112 A CN 112051112A
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China
Prior art keywords
outlet
sampling
glass tube
flue gas
moisture
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Pending
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CN202011057816.XA
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Chinese (zh)
Inventor
井新经
王勇
刘圣冠
李杨
周元祥
林琳
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Xian Xire Energy Saving Technology Co Ltd
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Xian Xire Energy Saving Technology Co Ltd
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Priority to CN202011057816.XA priority Critical patent/CN112051112A/en
Publication of CN112051112A publication Critical patent/CN112051112A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/02Devices for withdrawing samples
    • G01N1/10Devices for withdrawing samples in the liquid or fluent state
    • G01N1/20Devices for withdrawing samples in the liquid or fluent state for flowing or falling materials

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention discloses a sampling device and a method for flue gas moisture at an outlet of a desulfurizing tower, which comprises a plastic hose, a plastic glass tube and a sampling container; one end of the plastic hose is communicated with the horizontal flue at the outlet of the desulfurizing tower, and the other end of the plastic hose is connected with the plastic glass tube; the plastic glass tube is arranged vertically to the axis of the horizontal flue, the upper end is a steam exhaust port, and the lower end is a condensed water outlet; the sampling container is communicated with a condensed water outlet at the lower end of the plastic glass tube and is used for collecting condensed water. The sampling device has the advantages of simple structure, safety and reliability, can meet the requirement of sampling the moisture in the flue gas, and can be used as a sampling device for continuously sampling the moisture in the flue gas at the outlet of the wet desulphurization tower of the coal-fired boiler. The sampling device is suitable for sampling the moisture of the flue gas at the outlet of the wet desulphurization tower of the coal-fired boiler, can meet the requirement of continuous sampling when the ambient air temperature is not more than 35 ℃, is convenient to operate, and has strong adaptability to field conditions.

Description

Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of boilers, and particularly relates to a sampling device and a sampling method for flue gas moisture at an outlet of a desulfurizing tower.
[ background of the invention ]
In order to relieve the current situation of water resource shortage, part of coal-fired units begin to recover water in flue gas, and mainly recover water in flue gas at the outlet of a desulfurizing tower. Most of the water in the flue gas at the outlet of the desulfurizing tower is the desulfurizing process water evaporated from the flue gas, and the rest is the moisture generated by coal combustion. The water condensed from the flue gas usually carries a certain amount of dissolved salts and pollutants, and the water can be used for desulfurization process water through simple treatment, but is limited by the water balance of a desulfurization system, and most of the water still needs to be treated more strictly to be utilized, so that the water in the flue gas needs to be sampled and tested before the cooling water taking project is implemented to better utilize the recovered water, and an accurate treatment scheme is formulated. However, no smoke moisture sampling device for the purpose is available in the market at present.
[ summary of the invention ]
The invention aims to solve the problems in the prior art and provides a sampling device and a sampling method for flue gas moisture at an outlet of a desulfurizing tower.
In order to achieve the purpose, the invention adopts the following technical scheme to realize the purpose:
a sampling device of desulfurizing tower export flue gas moisture includes:
one end of the plastic hose is communicated with the horizontal flue at the outlet of the desulfurizing tower, and the other end of the plastic hose is connected with the plastic glass tube;
the plastic glass tube is arranged perpendicular to the axis of the horizontal flue, the upper end of the plastic glass tube is provided with a steam exhaust port, and the lower end of the plastic glass tube is provided with a condensed water outlet;
and the sampling container is communicated with a condensed water outlet at the lower end of the plastic glass tube and is used for collecting condensed water.
The invention further improves the following steps:
the plastic hose, the plastic glass tube and the sampling container are connected through a tee joint.
The plastic glass tube is hollow and cylindrical, the height c of the plastic glass tube is 0.4-0.8 m, and the diameter b of the plastic glass tube is 10-20 mm.
The diameter a of the plastic hose is 20-40 mm, and a is larger than or equal to 2 b.
The tee joint is connected with the sampling container through threads.
The volume of the sampling container is 0.3-1L.
A sampling method of flue gas moisture at an outlet of a desulfurizing tower comprises the following steps:
when the unit normally operates and the environmental temperature is not higher than 35 ℃, smoke in a horizontal flue at the outlet of the desulfurizing tower enters a plastic glass tube above the tee joint through a plastic hose and the tee joint, the smoke with water vapor in a supersaturated state is in the tube, air with the temperature not higher than 35 ℃ is outside the tube, the water vapor in the smoke is condensed, the inner wall of the plastic glass tube of the smoke downwards enters a sampling container under the action of gravity, the sampling of moisture in the smoke is completed after the preset time, the quality of the moisture is determined through moisture assay, and support is provided for determining the early water treatment specific scheme of the water taking engineering from the smoke.
Compared with the prior art, the invention has the following beneficial effects:
the smoke is connected into a tee joint by a plastic hose, a thin-wall round glass tube is connected above the tee joint, and a glass or transparent plastic container is connected below the tee joint; flue gas at the outlet of the desulfurizing tower is in positive pressure, and enters the atmosphere through a glass tube by using static pressure difference between the flue gas at the outlet of the desulfurizing tower and the atmosphere as power; the temperature of the flue gas entering the glass tube is about 50 ℃, and the water vapor is in a supersaturated state, when the temperature of the ambient air is not higher than 35 ℃, the flue gas passing through the glass tube exchanges heat due to the temperature difference between the flue gas and the air, the water vapor begins to condense after the temperature of the flue gas is reduced, but because the length of the glass tube exceeds the height of a water column which can be overcome by static pressure difference, the condensed water drops fall into a container below the tee joint under the action of gravity. The sampling device has the advantages of simple structure, safety and reliability, can meet the requirement of sampling the moisture in the flue gas, and can be used as a sampling device for continuously sampling the moisture in the flue gas at the outlet of the wet desulphurization tower of the coal-fired boiler. The sampling device is suitable for sampling the moisture of the flue gas at the outlet of the wet desulphurization tower of the coal-fired boiler, can meet the requirement of continuous sampling when the ambient air temperature is not more than 35 ℃, is convenient to operate, and has strong adaptability to field conditions.
[ description of the drawings ]
In order to more clearly explain the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention, and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.
FIG. 1 is a schematic view of the apparatus of the present invention.
Wherein, 1 is the horizontal flue of desulfurizing tower export, 2 is the plastic hose, 3 is the tee bend, 4 is circular plastic glass pipe, 5 is the sample container.
[ detailed description ] embodiments
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. The components of embodiments of the present invention generally described and illustrated in the figures herein may be arranged and designed in a wide variety of different configurations.
Thus, the following detailed description of the embodiments of the present invention, presented in the figures, is not intended to limit the scope of the invention, as claimed, but is merely representative of selected embodiments of the invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
It should be noted that: like reference numbers and letters refer to like items in the following figures, and thus, once an item is defined in one figure, it need not be further defined and explained in subsequent figures.
In the description of the embodiments of the present invention, it should be noted that if the terms "upper", "lower", "horizontal", "inner", etc. are used for indicating the orientation or positional relationship based on the orientation or positional relationship shown in the drawings or the orientation or positional relationship which is usually arranged when the product of the present invention is used, the description is merely for convenience and simplicity, and the indication or suggestion that the referred device or element must have a specific orientation, be constructed and operated in a specific orientation, and thus, cannot be understood as limiting the present invention. Furthermore, the terms "first," "second," and the like are used merely to distinguish one description from another, and are not to be construed as indicating or implying relative importance.
Furthermore, the term "horizontal", if present, does not mean that the component is required to be absolutely horizontal, but may be slightly inclined. For example, "horizontal" merely means that the direction is more horizontal than "vertical" and does not mean that the structure must be perfectly horizontal, but may be slightly inclined.
In the description of the embodiments of the present invention, it should be further noted that unless otherwise explicitly stated or limited, the terms "disposed," "mounted," "connected," and "connected" should be interpreted broadly, and may be, for example, fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood by those skilled in the art according to specific situations.
The invention is described in further detail below with reference to the accompanying drawings:
referring to fig. 1, the flue gas of a horizontal flue 1 at the outlet of a desulfurization tower is introduced into a tee joint 3 through a plastic hose 2, a round glass tube 4 is connected above the tee joint 3, a sampling container 5 is connected below the tee joint 3, the flue gas enters the atmosphere through the plastic hose 2, the tee joint 3 and the round glass tube 4 due to static pressure difference of the flue gas in the flue at the outlet of the desulfurization tower and the atmosphere, the flue gas with water vapor in a supersaturated state is subjected to heat exchange with the air outside the flue gas when passing through the glass tube to reduce the temperature, the water vapor is condensed, the height of the round glass tube 4 exceeds the water column height which can be overcome by the static pressure difference, the flow of the flue gas is controlled within a certain range, and water drops condensed from the flue gas enter the sampling container 5 downwards along the inner wall of the round glass tube.
According to the invention, the circular glass tube 4 is vertical to the horizontal flue, the height c of the circular glass tube is 0.4-0.8 m, the larger the maximum static pressure value of flue gas in the horizontal flue at the outlet of the desulfurization tower is, the larger the height c value of the circular glass tube is, so that the flue gas with water vapor in a supersaturated state can be ensured to fully exchange heat with air and reduce the temperature when passing through the circular glass tube, and water drops condensed from the flue gas can flow downwards under the action of gravity. Other components and connections are the same as in the first embodiment.
The diameter a of the plastic hose 2 is 20-40 mm, the diameter b of the round glass tube 4 is 10-20 mm, and a is larger than or equal to 2 b. So design, the flue gas is better through the cooling water intaking effect of circular glass pipe 4. Other components and connection relationships are the same as those in the second embodiment.
The tee joint 3 is connected with a sampling container 5 through threads, and the volume of the sampling container 5 is between 0.3L and 1L. By the design, the single sampling amount can meet the requirement of water assay.
The working process of the invention is as follows:
when the unit normally operates and the environmental temperature is not higher than 35 ℃, smoke in a horizontal flue at the outlet of the desulfurizing tower enters a circular glass tube 4 above a tee joint 3 through a plastic hose 2 and the tee joint 3, smoke with water vapor in a supersaturated state (about 50 ℃) is arranged in the circular glass tube 4, and air with low temperature (not higher than 35 ℃) is arranged outside the circular glass tube, due to the temperature difference between the inside and the outside of the circular glass tube, the smoke with the water vapor in the supersaturated state is cooled to generate water drops, the water drops downwards enter a sampling container 5 through the inner wall of the circular glass tube under the action of gravity, the sampling of moisture in the smoke can be completed after a period of time, the quality of the moisture can be determined through moisture testing, and further support is provided for determining the specific scheme of the early-stage water treatment of the.
The above is only a preferred embodiment of the present invention, and is not intended to limit the present invention, and various modifications and changes will occur to those skilled in the art. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (7)

1. The utility model provides a sampling device of desulfurizing tower export flue gas moisture which characterized in that includes:
one end of the plastic hose (2) is communicated with the horizontal flue (1) at the outlet of the desulfurizing tower, and the other end of the plastic hose (2) is connected with a plastic glass tube (4);
the plastic glass tube (4) is perpendicular to the axis of the horizontal flue (1), the upper end of the plastic glass tube (4) is provided with a steam exhaust port, and the lower end of the plastic glass tube is provided with a condensed water outlet;
and the sampling container (5), the sampling container (5) is communicated with a condensed water outlet at the lower end of the plastic glass tube (4) and is used for collecting condensed water.
2. The sampling device of the flue gas moisture at the outlet of the desulfurizing tower of claim 1, wherein the plastic hose (2), the plastic glass tube (4) and the sampling container (5) are connected through a tee joint (3).
3. The sampling device of the flue gas moisture at the outlet of the desulfurizing tower as claimed in claim 1, wherein the plastic glass tube (4) is hollow cylindrical, the height c is 0.4-0.8 m, and the diameter b is 10-20 mm.
4. The sampling device of the flue gas moisture at the outlet of the desulfurizing tower is characterized in that the diameter a of the plastic hose (2) is 20-40 mm, and a is more than or equal to 2 b.
5. The desulfurization tower outlet flue gas moisture sampling device according to claim 2, characterized in that the tee joint (3) is connected with the sampling container (5) through screw threads.
6. The sampling device for the moisture in the flue gas at the outlet of the desulfurization tower is characterized in that the volume of the sampling container (5) is 0.3-1L.
7. A method for sampling the moisture in flue gas at the outlet of a desulfurizing tower by using the sampling device of any one of claims 1-6, which is characterized by comprising the following steps:
when the unit normally operates and the environmental temperature is not higher than 35 ℃, smoke in a horizontal flue (1) at the outlet of the desulfurizing tower enters a plastic glass tube (4) above the tee joint (3) through a plastic hose (2) and the tee joint (3), the smoke with water vapor in a supersaturated state is in the smoke, air with the temperature not higher than 35 ℃ is outside the smoke, water vapor in the smoke is condensed, the inner wall of the plastic glass tube (4) of the smoke downwards enters a sampling container (5) under the action of gravity, sampling of moisture in the smoke is completed after preset time, the moisture quality is determined through moisture assay, and support is provided for determination of a specific scheme of water treatment in the earlier stage of a smoke water taking project.
CN202011057816.XA 2020-09-29 2020-09-29 Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower Pending CN112051112A (en)

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CN202011057816.XA CN112051112A (en) 2020-09-29 2020-09-29 Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower

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CN202011057816.XA CN112051112A (en) 2020-09-29 2020-09-29 Sampling device and sampling method for flue gas moisture at outlet of desulfurizing tower

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1923952A (en) * 2005-08-30 2007-03-07 包立根 Collection method of bamboo vinegar stock solution
CN204214696U (en) * 2014-11-30 2015-03-18 深圳睿境环保科技有限公司 Condensable particle sampling device
CN205620407U (en) * 2016-05-19 2016-10-05 武汉钢铁股份有限公司 Coke oven tedge smoke and dust gas sampling analysis device
CN206057283U (en) * 2016-08-27 2017-03-29 华电电力科学研究院 A kind of many dot matrix type flue gas on-line continuous monitoring devices
CN208187625U (en) * 2018-06-04 2018-12-04 西安建筑科技大学 Anti-blocking device for pressure measurement suitable for wet flue gas pressure measurement
CN211328769U (en) * 2019-11-20 2020-08-25 烟台龙源电力技术股份有限公司 Flue gas treatment system of thermal power factory

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1923952A (en) * 2005-08-30 2007-03-07 包立根 Collection method of bamboo vinegar stock solution
CN204214696U (en) * 2014-11-30 2015-03-18 深圳睿境环保科技有限公司 Condensable particle sampling device
CN205620407U (en) * 2016-05-19 2016-10-05 武汉钢铁股份有限公司 Coke oven tedge smoke and dust gas sampling analysis device
CN206057283U (en) * 2016-08-27 2017-03-29 华电电力科学研究院 A kind of many dot matrix type flue gas on-line continuous monitoring devices
CN208187625U (en) * 2018-06-04 2018-12-04 西安建筑科技大学 Anti-blocking device for pressure measurement suitable for wet flue gas pressure measurement
CN211328769U (en) * 2019-11-20 2020-08-25 烟台龙源电力技术股份有限公司 Flue gas treatment system of thermal power factory

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Application publication date: 20201208