CN112048399A - Preparation method of high-quality hexadecyl industrial detergent - Google Patents
Preparation method of high-quality hexadecyl industrial detergent Download PDFInfo
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- CN112048399A CN112048399A CN202010742761.XA CN202010742761A CN112048399A CN 112048399 A CN112048399 A CN 112048399A CN 202010742761 A CN202010742761 A CN 202010742761A CN 112048399 A CN112048399 A CN 112048399A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/30—Amines; Substituted amines ; Quaternized amines
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/06—Phosphates, including polyphosphates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2072—Aldehydes-ketones
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/24—Organic compounds containing halogen
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/3418—Toluene -, xylene -, cumene -, benzene - or naphthalene sulfonates or sulfates
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3703—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3726—Polyurethanes
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
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Abstract
The invention discloses a method for preparing a high-quality hexadecyl industrial detergent, which has the technical scheme that: the detergent comprises, by weight, 5-8 parts of hexadecyltrimethylammonium chloride, 4-7 parts of industrial acetone, 8-11 parts of a builder, 30-60 parts of water, 2-5 parts of a diluent, 9-12 parts of 1, 3-butanediol diacetate, 13-16 parts of amyl alcohol, 9-12 parts of a plant extract, 3-6 parts of a surfactant, 4-12 parts of cocoyl amine propyl betaine and 2-8 parts of alkylphenol polyoxyethylene ether, wherein the detergent has good fragrance and irritation taste, and the added surfactant has good capability of removing greasy dirt and is hydrophilic and lipophilic.
Description
Technical Field
The invention relates to the technical field of industrial detergents, in particular to a preparation method of a high-quality hexadecyl industrial detergent.
Background
Detergents are products specifically formulated for cleaning by a washing process. The main components are usually composed of surfactants, builders, additives and the like. Detergents are widely classified into heavy-duty detergents and light-duty detergents according to the type of dirt removed; the product can be divided into various forms such as powder, block, paste, slurry, liquid and the like according to the appearance of the product, the industrial development is faster and faster, mechanical equipment in the industry is more and more used, the sanitary condition of work is higher, the cleaning is required by using a detergent, and a chemical preparation for cleaning industrial dirt is required to be high in dirt cleaning speed and complete in dirt dissolving. The cleaning agent has strong reaction, dispersion or dissolution cleaning capability to dirt, and can remove the dirt more thoroughly in a limited construction period.
The Chinese patent with the publication number of CN109554235A discloses an industrial detergent and a preparation method thereof, and the industrial detergent comprises the following components in parts by weight: 20-30 parts of sodium phosphate, 6-15 parts of carotene, 12-18 parts of fatty acid amide, 8-16 parts of amyl alcohol, 10-18 parts of maleic acid, 2-8 parts of reinforcing agent, 6-12 parts of sodium carbonate, 7-15 parts of sodium chloride, 4-10 parts of antirust agent, 0.2-0.8 part of essence and the balance of deionized water.
The industrial detergent is mixed with ionized water; however, the industrial detergents of the above type still have some disadvantages, such as: plant extract and surfactant are lacking as raw materials.
Disclosure of Invention
The present invention aims at providing a method for preparing a high-quality hexadecyl industrial detergent to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
the preparation method of the high-quality hexadecyl industrial detergent comprises the following components, by weight, 5-8 parts of hexadecyl trimethyl ammonium chloride, 4-7 parts of industrial acetone, 8-11 parts of a builder, 30-60 parts of water, 2-5 parts of a diluent, 9-12 parts of 1, 3-butanediol diacetate, 13-16 parts of amyl alcohol, 9-12 parts of a plant extracting solution, 3-6 parts of a surfactant, 4-12 parts of cocoyl amido propyl betaine and 2-8 parts of alkylphenol polyoxyethylene ether.
Preferably, the diluent is one or a mixture of more of a silicone heat-resistant diluent, a polyurethane diluent, an epoxy diluent and a perchloroethylene diluent.
Preferably, the builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fiber, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate and the carboxymethyl fiber is 8: 2: 5: 6: 4.
preferably, the plant extract is extracted from chamomile, honeysuckle and mint.
Preferably, the plant extract is prepared by the following steps:
s1: weighing the materials with the specific gravity of 2: 1: 1: 2, putting the chamomile, the honeysuckle and the mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 60-70-mesh sieve for sieving;
s3: after being screened, water with the weight of 8-12 times is added for soaking for 28-32 minutes, heating is carried out until the water is boiled, and filtering is carried out when the temperature reaches 50-60 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain the plant extract.
Preferably, the surfactant is one of an amino acid surfactant and a betaine surfactant.
Preferably, the water is deionized water
Preferably, the preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing the hexadecyl trimethyl ammonium chloride, the industrial acetone, the ionic water, the 1, 3-butanediol diacetate, the amyl alcohol, the cocoyl aminopropyl betaine and the alkylphenol ethoxylate into a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 60-90 ℃, and stirring the mixture for 30-60 minutes to fully mix the mixture;
step three: and cooling to 30-40 ℃, adding the builder, the diluent, the surfactant and the plant extracting solution according to the mass proportion, stirring for 30-40 minutes, and cooling to normal temperature to obtain the detergent.
Preferably, the detergent is used for cleaning greasy dirt, stain, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
Compared with the prior art, the invention has the beneficial effects that:
the high-quality hexadecyl industrial detergent consists of hexadecyl trimethyl ammonium chloride, industrial acetone, a builder, water, a diluent, 1, 3-butanediol diacetate, amyl alcohol, a plant extracting solution, a surfactant, cocoyl amido propyl betaine, alkylphenol polyoxyethylene ether and the like.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
A method for preparing a high-quality hexadecyl industrial detergent comprises the following components in parts by weight: 5 parts of hexadecyl trimethyl ammonium chloride, 4 parts of industrial acetone, 8 parts of a builder, 30 parts of water, 2 parts of a diluent, 9 parts of 1, 3-butanediol diacetate, 13 parts of amyl alcohol, 9 parts of a plant extracting solution, 3 parts of a surfactant, 4 parts of cocoyl amido propyl betaine and 2 parts of alkylphenol polyoxyethylene ether.
Wherein, the diluent is organic silicon heat-resistant diluent.
The builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fibers, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate to the carboxymethyl fibers is 8: 2: 5: 6: 4, when the builder is prepared according to the proportion, the detergent is beneficial to improving the dirt-removing capacity of the industrial detergent.
Wherein the plant extract is extracted from flos Matricariae Chamomillae, flos Lonicerae, and herba Menthae.
Wherein, the plant extract adopts the following steps:
s1: weighing the materials with the specific gravity of 2: 1: 1: 2, putting the chamomile, the honeysuckle and the mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 60-mesh sieve for sieving;
s3: after being screened, 8 times of water is added for soaking for 28 minutes, the mixture is heated until the mixture is boiled, and the mixture is filtered when the temperature reaches 50 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain the plant extract.
Wherein the surfactant is an amino acid surfactant.
Wherein the water is deionized water.
The preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing hexadecyl trimethyl ammonium chloride, industrial acetone, ionized water, 1, 3-butanediol diacetate, amyl alcohol, cocoyl amido propyl betaine and alkylphenol polyoxyethylene ether in a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 60 ℃, and stirring the mixture for 30 minutes;
step three: cooling to 30 deg.C, adding builder, diluent, surfactant and plant extractive solution, stirring for 30 min, and cooling to room temperature to obtain the final product.
The detergent is used for cleaning greasy dirt, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
Example 2
A method for preparing a high-quality hexadecyl industrial detergent comprises the following components in parts by weight: 6 parts of hexadecyl trimethyl ammonium chloride, 5 parts of industrial acetone, 9 parts of a builder, 40 parts of water, 3 parts of a diluent, 10 parts of 1, 3-butanediol diacetate, 14 parts of amyl alcohol, 10 parts of a plant extracting solution, 4 parts of a surfactant, 7 parts of cocoyl amido propyl betaine and 4 parts of alkylphenol polyoxyethylene ether.
Wherein the diluent is a polyurethane diluent.
The builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fibers, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate to the carboxymethyl fibers is 10: 1: 4: 8: 2, when the builder is prepared according to the proportion, the detergent is beneficial to improving the dirt-removing capacity of the industrial detergent.
Wherein the plant extract is extracted from flos Matricariae Chamomillae, flos Lonicerae, and herba Menthae.
Wherein, the plant extract adopts the following steps:
s1: weighing the materials with the specific gravity of 1: 2: 2: 1, putting chamomile, honeysuckle and mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 70-mesh sieve for sieving;
s3: after being screened, 9 times of water is added for soaking for 29 minutes, the mixture is heated until the mixture is boiled, and the mixture is filtered when the temperature reaches 54 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain plant extract
Wherein the surfactant is betaine surfactant.
Wherein the water is deionized water.
The preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing hexadecyl trimethyl ammonium chloride, industrial acetone, ionized water, 1, 3-butanediol diacetate, amyl alcohol, cocoyl amido propyl betaine and alkylphenol polyoxyethylene ether in a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 70 ℃, and stirring the mixture for 40 minutes;
step three: cooling to 33 deg.C, adding builder, diluent, surfactant and plant extractive solution, stirring for 34 min, and cooling to room temperature to obtain the final product.
The detergent is used for cleaning greasy dirt, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
Example 3
A method for preparing a high-quality hexadecyl industrial detergent comprises the following components in parts by weight: 7 parts of hexadecyl trimethyl ammonium chloride, 6 parts of industrial acetone, 10 parts of a builder, 50 parts of water, 4 parts of a diluent, 11 parts of 1, 3-butanediol diacetate, 15 parts of amyl alcohol, 11 parts of a plant extracting solution, 5 parts of a surfactant, 9 parts of cocoyl amido propyl betaine and 6 parts of alkylphenol polyoxyethylene ether.
Wherein the diluent is an epoxy diluent.
The builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fibers, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate to the carboxymethyl fibers is 8: 3: 2: 6: 4, when the builder is prepared according to the proportion, the detergent is beneficial to improving the dirt-removing capacity of the industrial detergent.
Wherein the plant extract is extracted from flos Matricariae Chamomillae, flos Lonicerae, and herba Menthae.
Wherein, the plant extract adopts the following steps:
s1: weighing the materials with the specific gravity of 3: 2: 1: 1, putting chamomile, honeysuckle and mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 60-mesh sieve for sieving;
s3: after being screened, water with the weight being 10 times that of the raw materials is added for soaking for 31 minutes, the raw materials are heated until the raw materials are boiled, and filtering is carried out when the temperature reaches 57 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain the plant extract.
Wherein the surfactant is an amino acid surfactant.
Wherein the water is deionized water.
The preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing hexadecyl trimethyl ammonium chloride, industrial acetone, ionized water, 1, 3-butanediol diacetate, amyl alcohol, cocoyl amido propyl betaine and alkylphenol polyoxyethylene ether in a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 80 ℃, and stirring the mixture for 50 minutes;
step three: cooling to 37 deg.C, adding builder, diluent, surfactant and plant extractive solution according to mass ratio, stirring for 37 min, and cooling to room temperature to obtain the final product.
The detergent is used for cleaning greasy dirt, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
Example 3
A method for preparing a high-quality hexadecyl industrial detergent comprises the following components in parts by weight: 8 parts of hexadecyl trimethyl ammonium chloride, 7 parts of industrial acetone, 11 parts of a builder, 60 parts of water, 5 parts of a diluent, 12 parts of 1, 3-butanediol diacetate, 16 parts of amyl alcohol, 12 parts of a plant extracting solution, 6 parts of a surfactant, 12 parts of cocoyl amido propyl betaine and 8 parts of alkylphenol polyoxyethylene ether.
Wherein the diluent is perchloroethylene diluent.
The builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fibers, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate to the carboxymethyl fibers is 11: 2: 1: 7: 3, when the builder is prepared by the above proportion, the detergent is beneficial to improving the dirt-removing capacity of the industrial detergent.
Wherein the plant extract is extracted from flos Matricariae Chamomillae, flos Lonicerae, and herba Menthae.
Wherein, the plant extract adopts the following steps:
s1: weighing the materials with the specific gravity of 4: 1: 1: 2, putting the chamomile, the honeysuckle and the mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 70-mesh sieve for sieving;
s3: after being screened, water with the weight being 12 times that of the raw materials is added for soaking for 32 minutes, the raw materials are heated until the raw materials are boiled, and filtering is carried out when the temperature reaches 60 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain the plant extract.
Wherein the surfactant is betaine surfactant.
Wherein the water is deionized water.
The preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing hexadecyl trimethyl ammonium chloride, industrial acetone, ionized water, 1, 3-butanediol diacetate, amyl alcohol, cocoyl amido propyl betaine and alkylphenol polyoxyethylene ether in a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 90 ℃, and stirring the mixture for 50 minutes;
step three: cooling to 40 deg.C, adding builder, diluent, surfactant and plant extractive solution according to mass ratio, stirring for 40 min, and cooling to room temperature to obtain the final product.
The detergent is used for cleaning greasy dirt, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. A high-quality hexadecyl industrial detergent comprises the following components in parts by weight: 5-8 parts of hexadecyl trimethyl ammonium chloride, 4-7 parts of industrial acetone, 8-11 parts of a builder, 30-60 parts of water, 2-5 parts of a diluent, 9-12 parts of 1, 3-butanediol diacetate, 13-16 parts of amyl alcohol, 9-12 parts of a plant extract, 3-6 parts of a surfactant, 4-12 parts of cocoyl amido propyl betaine and 2-8 parts of alkylphenol polyoxyethylene ether.
2. A high quality cetyl industrial detergent as set forth in claim 1, wherein: the diluent is one or a mixture of more of organic silicon heat-resistant diluent, polyurethane diluent, epoxy diluent and perchloroethylene diluent.
3. A high quality cetyl industrial detergent as claimed in claim 2, wherein: the builder comprises sodium alkyl benzene sulfonate, sodium sulfate, sodium toluene iodate, sodium tripolyphosphate and carboxymethyl fibers, wherein the mass ratio of the sodium alkyl benzene sulfonate, the sodium sulfate, the sodium toluene iodate, the sodium tripolyphosphate to the carboxymethyl fibers is 8: 2: 5: 6: 4.
4. a high quality cetyl industrial detergent as set forth in claim 1, wherein: the plant extract is extracted from chamomile, honeysuckle and mint.
5. A method for manufacturing a high quality cetyl industrial detergent as claimed in any of claims 1-4, characterized in that: the plant extract is prepared by the following steps:
s1: weighing the materials with the specific gravity of 2: 1: 1: 2, putting the chamomile, the honeysuckle and the mint in a container, and grinding into powder;
s2: putting the ground and crushed chamomile, honeysuckle and mint into a 60-70-mesh sieve for sieving;
s3: after being screened, water with the weight of 8-12 times is added for soaking for 28-32 minutes, heating is carried out until the water is boiled, and filtering is carried out when the temperature reaches 50-60 ℃;
s4: evaporating and concentrating the filtered solution until the original volume is 1/4 to obtain the plant extract.
6. The method for manufacturing a high-quality cetyl industrial detergent as claimed in claim 5, wherein: the surfactant is one of an amino acid surfactant and a betaine surfactant.
7. The method for manufacturing a high-quality cetyl industrial detergent as claimed in claim 5, wherein: the water is deionized water.
8. The method for manufacturing a high-quality cetyl industrial detergent as claimed in claim 5, wherein: the preparation method of the detergent comprises the following steps:
the method comprises the following steps: placing the hexadecyl trimethyl ammonium chloride, the industrial acetone, the ionic water, the 1, 3-butanediol diacetate, the amyl alcohol, the cocoyl aminopropyl betaine and the alkylphenol ethoxylate into a reaction kettle according to the mass proportion for mixing;
step two: heating the mixture in a reaction kettle after mixing, heating the mixture to 60-90 ℃, and stirring the mixture for 30-60 minutes to fully mix the mixture;
step three: and cooling to 30-40 ℃, adding the builder, the diluent, the surfactant and the plant extracting solution according to the mass proportion, stirring for 30-40 minutes, and cooling to normal temperature to obtain the detergent.
9. The method for manufacturing a high-quality cetyl industrial detergent as claimed in claim 5, wherein: the detergent is used for cleaning greasy dirt, grease and the like on the ground and the surface of mechanical equipment in an industrial place.
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| CN114085715A (en) * | 2021-11-29 | 2022-02-25 | 厦门普诺尔新材料科技有限公司 | Water-based grinding fluid cleaning agent and preparation method thereof |
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