CN111945190A - Additive atomization and dispersion device and working mode thereof - Google Patents

Additive atomization and dispersion device and working mode thereof Download PDF

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Publication number
CN111945190A
CN111945190A CN202010596671.4A CN202010596671A CN111945190A CN 111945190 A CN111945190 A CN 111945190A CN 202010596671 A CN202010596671 A CN 202010596671A CN 111945190 A CN111945190 A CN 111945190A
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China
Prior art keywords
atomizing
additive
tank
liquid
atomization
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CN202010596671.4A
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CN111945190B (en
Inventor
文孟平
万大勇
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Hubei Zhongyi Technology Co ltd
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Hubei Zhongyi Technology Co ltd
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Priority to CN202010596671.4A priority Critical patent/CN111945190B/en
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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25DPROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
    • C25D1/00Electroforming
    • C25D1/04Wires; Strips; Foils
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40Mixing liquids with liquids; Emulsifying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/71Feed mechanisms
    • B01F35/717Feed mechanisms characterised by the means for feeding the components to the mixer
    • B01F35/7179Feed mechanisms characterised by the means for feeding the components to the mixer using sprayers, nozzles or jets

Abstract

The invention discloses an additive atomization and dispersion device which comprises an atomization assembly and a liquid purification tank, wherein the atomization assembly is coaxially arranged at the top of the liquid purification tank and is movably connected with the liquid purification tank; atomizing subassembly includes atomizing casing, spray set, connecting rod and swiveling wheel, atomizing casing bottom central authorities are equipped with the relative open structure's in biconical groove top through-hole, spray set inlays to be located through-hole department, spray set top side is passed through the connecting rod with the axle center of swiveling wheel is connected, the swiveling wheel slide set up in atomizing casing bottom is kept away from on the annular spout of clean fluid reservoir one side. According to the invention, by arranging the atomization assembly and utilizing the spraying assembly double-cone rotary structure, the diluent containing the additive can be uniformly sprayed and completely covers the liquid level of the clean liquid tank, so that the additive is uniformly added, and the uniformity of the subsequently prepared electrolyte is improved.

Description

Additive atomization and dispersion device and working mode thereof
Technical Field
The invention relates to a copper foil preparation process device, in particular to an additive atomization and dispersion device and a working mode thereof.
Background
At present, the method for electrolyzing copper foil is the most common method for preparing wide-width copper foil, and the process method mainly comprises the steps of dissolving a copper raw material by acid to form a copper-containing electrolyte, filtering the copper electrolyte to remove impurities, electrolyzing in an electrolytic bath, and finally depositing on a cathode roller to obtain the copper foil. Before the above-mentioned electrolytic copper foil's technological process, need dissolve the required copper material of electrolysis in dissolving the copper jar, then obtain comparatively pure electrolyte and leading-in the net fluid reservoir after filtration treatment many times, at this moment need add some complementary medicines to the ration in the net fluid reservoir, nevertheless because the net fluid reservoir often is bulky, and the addition volume of additive is less relatively, make the additive of adding difficult to even dispersion in the solution of net fluid reservoir, thereby can produce great influence to the homogeneity of electrolyte of follow-up preparation, and then can influence the quality of electrolytic copper foil. It is therefore desirable to provide a device capable of uniformly dispersing the additive in order to solve the above problems.
Disclosure of Invention
The invention aims to provide an additive atomization and dispersion device and a working mode thereof, which are used for solving the problem that in the prior art, an additive is difficult to be uniformly dispersed in a solution of a clean liquid tank.
In order to solve the technical problem, the invention provides an additive atomization and dispersion device which comprises an atomization assembly and a clean liquid tank, wherein the atomization assembly is coaxially arranged at the top of the clean liquid tank and is movably connected with the clean liquid tank; the atomizing component comprises an atomizing shell, a spraying component, a connecting rod and a rotating wheel, a through hole of a double-cone groove top relative communication structure is formed in the center of the bottom of the atomizing shell, the spraying component is embedded in the through hole, the top side of the spraying component is connected with the axis of the rotating wheel through the connecting rod, and the rotating wheel is arranged on an annular sliding groove, far away from one side of the liquid purifying tank, in the bottom of the atomizing shell in a sliding mode.
Wherein, the spray assembly comprises an atomization tank and an atomization nozzle; the atomizing jar is the toper structure container, and toper top downward sloping setting and atomizer intercommunication, and the toper bottom slope side of atomizing jar is connected with the axle center of runner through the connecting rod, and the vertical top in toper bottom of atomizing jar is equipped with air inlet and inlet.
The double-conical groove communication structure of the through hole comprises an upper conical groove and a lower conical groove, and an O-shaped ring is arranged between the upper conical groove and the lower conical groove; an inclined bus of the atomizing tank conical structure is in parallel butt joint with a bus of the upper conical groove, and a vertical bus of the atomizing tank conical structure is superposed with the axis of the purified liquid tank; the atomizing cone angle of the atomizing nozzle is less than or equal to half of the cone angle of the lower conical groove.
Wherein, the additive atomization dispersing device also comprises a diluting tank, a liquid outlet valve, a delivery pump and a booster pump; the diluting tank is communicated with the liquid inlet of the atomizing tank through a pipeline after passing through the delivery pump, the liquid outlet valve is arranged at the position of the pipeline between the diluting tank and the delivery pump, and the booster pump is communicated with the air inlet of the atomizing tank through the pipeline.
Wherein, the lateral wall of clean fluid reservoir top is provided with the feed liquor pipe, and clean fluid reservoir bottom lateral wall is provided with the drain pipe, and feed liquor pipe and drain pipe all communicate with the inner chamber of clean fluid reservoir.
In order to solve the technical problem, the invention also provides a working mode of the additive atomization and dispersion device, which comprises the following steps: introducing the initial electrolyte into a clean liquid tank, adding an additive and a solvent into a dilution tank, and mixing uniformly to prepare an additive diluent; the additive diluent is guided into the atomization tank through the delivery pump, and the rotating wheel is driven to rotate along the annular sliding groove, so that the additive is uniformly added, and the electrolyte mixed with the additive is formed.
Preferably, the ratio of the additive to the solvent is 1 (40-60). The invention has the beneficial effects that: the additive atomization dispersing device and the working mode thereof are different from the prior art, and the atomization assembly is arranged, and the spraying assembly double-cone rotary structure is utilized, so that diluent containing additives can be uniformly sprayed and completely covers the liquid level of a clean liquid tank, the additives are uniformly added, and the uniformity of subsequently prepared electrolyte is improved.
Drawings
FIG. 1 is a schematic structural view of an embodiment of an additive atomizing and dispersing apparatus according to the present invention;
FIG. 2 is a schematic view of the structure of the through hole of the atomizing housing in one embodiment of the additive atomizing and dispersing device of the present invention;
in the figure: 1: an atomization assembly: 11: an atomizing housing; 111: a through hole; 111 a: an upper conical groove; 111 b: a lower conical groove; 112: a chute; 113: an O-shaped ring; 12: a spray assembly; 121: an atomizing tank; 122: an atomizing spray head; 13: a connecting rod; 14: a rotating wheel; 2: a liquid purifying tank; 21: a liquid inlet pipe; 22: a liquid outlet pipe; 3: a dilution tank; 4: a liquid outlet valve; 5: a delivery pump; 6: a booster pump; 7: an additive diluent; 8: a copper-containing solution.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
Referring to fig. 1 and 2, fig. 1 is a schematic structural view of an embodiment of an additive atomizing and dispersing device according to the present invention, and fig. 2 is a schematic structural view of a through hole of an atomizing housing according to an embodiment of an additive atomizing and dispersing device according to the present invention. The additive atomization and dispersion device comprises an atomization component 1, a clean liquid tank 2, a dilution tank 3, a liquid outlet valve 4, a delivery pump 5 and a booster pump 6, wherein the atomization component 1 is coaxially arranged at the top of the clean liquid tank 2 and is movably connected with the clean liquid tank 2, the dilution tank 3 is communicated with a liquid inlet of the atomization component 1 through a pipeline after passing through the delivery pump 5, the liquid outlet valve 4 is arranged at the position of the pipeline between the dilution tank 3 and the delivery pump 5, and the booster pump 6 is communicated with an air inlet of the atomization component 1 through a pipeline. The respective constituent parts of the additive atomizing and dispersing device will be described in detail below.
Specifically, atomizing subassembly 1 includes atomizing casing 11, spray assembly 12, connecting rod 13 and swiveling wheel 14, and atomizing casing 11 bottom center is equipped with the through-hole 111 of the relative connectivity in biconical groove top, and spray assembly 12 inlays and locates through-hole 111 department, and spray assembly 12 top side is connected with the axle center of swiveling wheel 14 through connecting rod 13, and swiveling wheel 14 slides and sets up in atomizing casing 11 bottom and keeps away from on the annular spout 112 of clean liquid jar 2 one side.
Specifically, the spray assembly 12 includes an atomization tank 121 and an atomization nozzle 122; atomizing jar 121 is the toper structure container, and toper top downward sloping setting and atomizer 122 intercommunication, and the toper bottom slope side of atomizing jar 121 is connected with the axle center of runner 14 through connecting rod 13, and the vertical top in toper bottom of atomizing jar 121 is equipped with air inlet and inlet, and air inlet and inlet pass through the pipeline intercommunication with booster pump 6 and delivery pump 5 respectively.
In this embodiment, the double-tapered groove communication structure of the through hole 111 includes an upper tapered groove 111a and a lower tapered groove 111b, an O-ring 113 is disposed between the upper tapered groove 111a and the lower tapered groove 111b, and the O-ring 113 is provided to alleviate friction at the joint between the atomization tank 121 and the atomization nozzle 122 during rotation; an inclined bus of the conical structure of the atomizing tank 121 is in parallel butt joint with a bus of the upper conical groove 111a, and a vertical bus of the conical structure of the atomizing tank 121 is overlapped with the axis of the purified liquid tank 2, so that the conical atomizing tank 121 can rotate by taking the vertical bus as a rotating shaft to be attached to the inner wall of the upper conical groove 111a and drive the atomizing nozzle 122 communicated below to rotate synchronously, namely, the cone angle of the atomizing tank 121 is half of the cone angle of the upper conical groove 111 a; meanwhile, the atomizing cone angle of the atomizing nozzle 122 is less than or equal to half of the cone angle of the lower conical groove 111b, so that the atomized liquid sprayed by the atomizing nozzle 122 can reach the surface of the copper-containing solution 8, and preferably, the elliptical major axis of the projection area of the liquid droplet sprayed by the atomizing nozzle 122 is equal to the radius of the liquid surface of the copper-containing solution 8, so that the area sprayed after the atomizing nozzle 122 rotates for one circle can uniformly cover the surface of the copper-containing solution 8, and the additive diluent 7 can be uniformly dispersed in the copper-containing solution 8.
Specifically, a liquid inlet pipe 21 is arranged on the side wall of the top of the liquid purifying tank 2, a liquid outlet pipe 22 is arranged on the side wall of the bottom of the liquid purifying tank 2, and the liquid inlet pipe 21 and the liquid outlet pipe 22 are both communicated with the inner cavity of the liquid purifying tank 2 and are respectively provided with a corresponding valve; the filtered initial electrolyte is guided into the liquid purification tank 2 through the liquid inlet pipe 21, and is guided out to be sent to a subsequent electrolytic tank through the liquid outlet pipe 22 after additives are added and uniformly mixed.
Further, based on the structural description of the additive atomization and dispersion device, the working mode is explained in detail: 1) introducing the filtered initial electrolyte into a clean liquid tank 2 through a liquid inlet pipe 21, adding an additive and a solvent into a dilution tank 3, uniformly mixing to prepare an additive diluent 7, wherein in the embodiment, the preferable ratio of the additive to the solvent is 1 (40-60), and the additive is properly diluted to be beneficial to subsequent spraying dispersion; 2) after the additive diluent 7 is prepared, the liquid outlet valve 4 is opened, the delivery pump 5 is started, the additive diluent 7 is guided into the atomizing tank 121, the rotating wheel 14 is driven to rotate along the annular sliding groove 112, the inclined atomizing tank 121 is driven to be attached to the upper conical groove 111a through the connecting rod 13 to rotate, so that the atomizing nozzle 122 also rotates, the whole copper-containing solution 8 liquid level can be uniformly sprayed after the atomizing nozzle 122 rotates for a circle, the additive is uniformly added, and the electrolyte mixed with the additive is formed; 3) when the pressure in the atomizing tank 121 is insufficient, the booster pump 6 can be started to adjust the pressure of the additive diluent 7 in the atomizing tank 121, so that the spraying rate of the additive diluent 7 is adjusted, after the additive is sprayed and uniformly mixed, the inclined atomizing tank 121 stops rotating, a valve at the liquid outlet pipe 22 is opened, and the electrolyte mixed with the additive is led out from the liquid outlet pipe 22 and is sent to a subsequent electrolytic tank.
The additive atomization dispersing device and the working mode thereof are different from the prior art, and the atomization assembly is arranged, and the spraying assembly double-cone rotary structure is utilized, so that diluent containing additives can be uniformly sprayed and completely covers the liquid level of a clean liquid tank, the additives are uniformly added, and the uniformity of subsequently prepared electrolyte is improved.
The above-mentioned embodiments only express the embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.

Claims (7)

1. The additive atomization and dispersion device is characterized by comprising an atomization assembly and a liquid purification tank, wherein the atomization assembly is coaxially arranged at the top of the liquid purification tank and is movably connected with the liquid purification tank;
atomizing subassembly includes atomizing casing, spray set, connecting rod and swiveling wheel, atomizing casing bottom central authorities are equipped with the relative open structure's in biconical groove top through-hole, spray set inlays to be located through-hole department, spray set top side is passed through the connecting rod with the axle center of swiveling wheel is connected, the swiveling wheel slide set up in atomizing casing bottom is kept away from on the annular spout of clean fluid reservoir one side.
2. The additive atomizing and dispersing device of claim 1, wherein the spray assembly comprises an atomizing tank and an atomizing spray head;
the atomizing jar is the toper structure container, and toper top downward sloping set up with the atomizer intercommunication, the toper bottom slope side of atomizing jar is passed through the connecting rod with the axle center of swiveling wheel is connected, the vertical top in toper bottom of atomizing jar is equipped with air inlet and inlet.
3. The additive atomizing and dispersing device according to claim 2, wherein the double-conical groove communicating structure of the through hole comprises an upper conical groove and a lower conical groove, and an O-ring is arranged between the upper conical groove and the lower conical groove;
an inclined bus of the atomization tank conical structure is in parallel butt joint with a bus of the upper conical groove, and a vertical bus of the atomization tank conical structure is superposed with an axis of the purified liquid tank;
the atomization cone angle of the atomization nozzle is less than or equal to half of the cone angle of the lower conical groove.
4. The additive atomizing and dispersing apparatus as set forth in claim 3, further comprising a dilution tank, a liquid outlet valve, a delivery pump and a booster pump;
the diluting tank warp behind the delivery pump with the inlet of atomizing jar passes through the pipeline intercommunication, go out the liquid valve set up in pipeline department between diluting tank and the delivery pump, the booster pump pass through the pipeline with the air inlet intercommunication of atomizing jar.
5. The device for atomizing and dispersing the additive according to claim 1, wherein a liquid inlet pipe is disposed on a side wall of the top of the liquid purifying tank, a liquid outlet pipe is disposed on a side wall of the bottom of the liquid purifying tank, and the liquid inlet pipe and the liquid outlet pipe are both communicated with an inner cavity of the liquid purifying tank.
6. An operating method of the additive atomizing and dispersing device as set forth in any one of claims 1 to 5, characterized in that it comprises the steps of:
introducing the initial electrolyte into a clean liquid tank, adding an additive and a solvent into a dilution tank, and mixing uniformly to prepare an additive diluent;
the additive diluent is guided into the atomization tank through the delivery pump, and the rotating wheel is driven to rotate along the annular sliding groove, so that the additive is uniformly added, and the electrolyte mixed with the additive is formed.
7. The working mode of the additive atomizing and dispersing device according to claim 6 is characterized in that the ratio of the additive to the solvent is 1 (40-60).
CN202010596671.4A 2020-06-28 2020-06-28 Additive atomization and dispersion device and working mode thereof Active CN111945190B (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0190688A2 (en) * 1985-02-07 1986-08-13 L. & C. Steinmüller GmbH Process and apparatus for cleaning smoke by a fluid absorbent by the air current atomization principle
CN1484724A (en) * 2001-01-05 2004-03-24 ���ջ�����ʽ���� Water spraying device
CN101039756A (en) * 2004-08-13 2007-09-19 约瑟夫·H·克莱尔曼 Spray apparatus and dispensing tubes therefore
CN203540756U (en) * 2013-10-25 2014-04-16 中国石油化工股份有限公司 Liquid material atomization adding device
CN103774179A (en) * 2014-01-28 2014-05-07 白银有色集团股份有限公司 Device and method for automatic control of additive in copper electrolysis production
CN204125500U (en) * 2014-09-17 2015-01-28 河南工信华鑫环保科技有限公司 A kind of molten copper groove of eddy flow feed liquor

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0190688A2 (en) * 1985-02-07 1986-08-13 L. & C. Steinmüller GmbH Process and apparatus for cleaning smoke by a fluid absorbent by the air current atomization principle
CN1484724A (en) * 2001-01-05 2004-03-24 ���ջ�����ʽ���� Water spraying device
CN101039756A (en) * 2004-08-13 2007-09-19 约瑟夫·H·克莱尔曼 Spray apparatus and dispensing tubes therefore
CN203540756U (en) * 2013-10-25 2014-04-16 中国石油化工股份有限公司 Liquid material atomization adding device
CN103774179A (en) * 2014-01-28 2014-05-07 白银有色集团股份有限公司 Device and method for automatic control of additive in copper electrolysis production
CN204125500U (en) * 2014-09-17 2015-01-28 河南工信华鑫环保科技有限公司 A kind of molten copper groove of eddy flow feed liquor

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